43 Grade Ordinary Portland Cement - Specification: Indian Standard
43 Grade Ordinary Portland Cement - Specification: Indian Standard
43 Grade Ordinary Portland Cement - Specification: Indian Standard
(Reaffirmed 2005)
Edition 2.8
(2005-05)
Indian Standard
UDC
666.942.2
BIS 2008
BUREAU
OF INDIAN
STANDARDS
Price Group 4
FOREWORD
This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards on 30
October 1989, after the draft finalized by the Cement and Concrete Sectional Committee had been
approved by the Civil Engineering Division Council.
This standard was first published in 1976 under the title Specification for high strength ordinary
Portland cement. Since publication of this standard, large number of amendments have been
issued from time to time in order to modify various requirements based on experience gained with
the use of the standard and the requirements of the users and also keeping in view the raw
materials and fuel available in the country for manufacture of cement. The important
amendments include increasing the value of total loss on ignition from 4 to 5 percent, modifying
the requirement of total sulphur content calculated as sulphuric anhydride (SO3) reducing the
fineness by specific surface of cement from 350 m2/kg to 225 m2/kg, making autoclave soundness
test compulsory irrespective of magnesia content, incorporating a provision for retest in respect of
autoclave soundness test after aeration of the cement, incorporating a clause on false set of
cement, permitting packaging of cement in 25 kg bags and making compulsory provision for
issuing a certificate indicating the total chloride content in cement. Further, in view of the decision
to designate ordinary Portland cement by its 28-day compressive strength, the title of this
standard was modified as 43 grade ordinary Portland cement Specification. In view of these
large number of amendments, the Sectional Committee decided to bring out the first revision of
the standard incorporating all these amendments, so as to make it more convenient for the users.
Specific requirements of ordinary Portland cement for manufacture of railway sleepers to be
designated as 43-S grade are given in the standard in 5.2, 6.1, 6.2.2, 6.3, 6.4 and 9.1. To
differentiate it with normal grade, 43-S grade shall be marked on the bags/packages for such
cement in place of 43-S grade.
Mass of cement packed in bags and the tolerance requirements shall be in accordance with the
relevant provisions of the Standards of Weights and Measures ( Packaged Commodities ) Rules,
1977 and B-1.2 ( see Annex B for information ). Any modification in these rules in respect of
tolerance on mass of cement would apply automatically to this standard.
This standard contains 11.4.1 which permits the purchaser to use his option for testing and 6.1,
6.5, 9.2.1 and 9.3 which call for agreement between the purchaser and the manufacturer.
In the formulation of this standard considerable assistance has been rendered by National Council
for Cement and Building Materials, New Delhi as many of these modifications are based on
studies carried out by them.
The composition of the committee responsible for the formulation of this standard is given in
Annex C.
This edition 2.8 incorporates Amendment No. 1 (January 1991), Amendment
(November 1991), Amendment No. 3 (November 1993), Amendment No. 4 (October
Amendment No. 5 (October 1999), Amendment No. 6 (June 2000), Amendment
(December 2003) and Amendment No. 8 (May 2005). Side bar indicates modification of the
the result of incorporation of the amendments.
No. 2
1998),
No. 7
text as
For the purpose of deciding whether a particular requirement of this standard is complied with,
the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded
off in accordance with IS 2 : 1960 Rules for rounding off numerical values ( revised ). The number
of significant places retained in the rounded off value should be the same as that of the specified
value in this standard.
IS 8112 : 1989
Indian Standard
1 SCOPE
1.1 This standard covers the manufacture,
chemical and physical requirements of 43 grade
ordinary Portland cement.
2 REFERENCES
2.1 The Indian Standards listed in Annex A are
necessary adjuncts to this standard.
3 TERMINOLOGY
3.1 For the purpose of this standard, the definitions given in IS 4845 : 1968 shall apply.
4 MANUFACTURE
4.1 43 grade ordinary Portland cement shall be
Performance Improver
Fly ash
Granulated slag
Silica fume
Limestone
Percentage
Addition, Max
5
5
5
5
Metakaoline
Requirement
As per IS 3812 (Part 1)
As per IS 12089
As per IS 15388
CaCO3 content calculated from CaO content shall not be less than 75
percent when tested as per IS 1760 (Part 3)
a) Reactive silica shall not be less than 85 percent when tested as
per IS 3812 (Part 1)
b) Pozzolanic Activity Index shall not be less than 90 percent when
tested as per 10 of IS 1727
c) Loss on ignition shall not be more than 8 percent when tested as
per IS 1727
a) Silicon dioxide (SiO2) plus aluminium oxide (Al2O3) plus iron
oxide (Fe2O3) in percent by mass shall not be less than 95
percent when tested as per IS 1727
b) Loss on ignition shall not be more than 1 percent when tested as
per IS 1727
c) Total alkalis as sodium oxide (Na2O) in percent by mass shall
not be more than 0.6 percent when tested as per IS 4032
d) Particles retained on 45 micron IS sieve (wet sieving) shall not be
more than 1 percent when test as per IS 1727
5 CHEMICAL REQUIREMENTS
IS 8112 : 1989
6 PHYSICAL REQUIREMENTS
6.2 Soundness
6.1 Fineness
Table 1
Sl
Characteristic
No.
(1)
(2)
i) Ratio of percentage of
lime to percentages of
silica, alumina and iron
oxide, when calculated by
the formula:
CaO 0.7SO 3
-----------------------------------------------------------------2.8SiO 2 + 1.2Al 2 O 2 +
Requirement
(3)
Not greater than 1.02
and not less than 0.66
0.65 Fe2O3
ii) Ratio of percentage of
Not less than 0.66
alumina to that of iron
oxide
iii) Insoluble residue, percent a) In case no flyash, silica
by mass
fume, rice husk ash and
metakaoline is added
Not more than 3.0
b) In case of addition of fly
ash and/or silica fume
and/or rice husk ash
and/or metakaoline
Not more than 5.0
iv) Magnesia, percent by
Not more than 6.0
mass
Not more than 2.5 and
v) Total sulphur content
3.0 when tricalcium
calculated as sulphuric
aluminate ( see Note 1 ),
anhydride (SO3), percent by mass
percent by mass is 5 or
less and greater than 5
respectively
vi) Total loss on ignition
Not more than 5
percent
NOTES
1 The tricalcium aluminate content (C3A) is calculated
by the formula:
C3A = 2.65 (Al2O3) 1.69 (Fe2O3),
where each symbol in brackets refers to the percent (by
mass of total cement) of the oxide, excluding any
contained in insoluble residue referred to at Sl No. (iii).
The tricalcium silicate content (C3S) is calculated by the
formula:
C3S = 4.07CaO - 7.60 SiO2 - 6.72 Al2O3 - 1.43 Fe2O3 2.85 SO3
2 Alkali aggregate reactions have been noticed in
aggregates in some parts of the country. On large and
important jobs where the concrete is likely to be exposed
to humid atmosphere or wetting action it is advisable
that the aggregate be tested for alkali aggregate
reaction. In the case of reactive aggregates, the use of
cement with alkali content below 0.6 percent expressed
as sodium oxide (Na2O) is recommended.
23 MPa
33 MPa
43 MPa
IS 8112 : 1989
the tonne or the net mass of the cement shall be
legibly and indelibly marked on each bag. In
case performance improvers are added, the
bags shall also be marked Permitted
performance improvers are added. Bags shall
be in good condition at the time of inspection.
9. DELIVERY
9.1 The cement shall be packed in bags [jute
sacking bag conforming to IS 2580 : 1982,
double hessian bituminized (CRI type),
multiwall paper conforming to IS 11761 : 1986,
polyethylene lined (CRI type) jute, light weight
jute conforming to IS 12154 : 1987, woven
HDPE conforming to IS 11652 : 1986, woven
polypropylene conforming to IS 11653 : 1986,
jute synthetic union conforming to IS
12174 : 1987 or any other approved composite
bags] bearing the manufacturers name or his
registered trade-mark, if any, and the words 43
Grade Ordinary Portland Cement or 43-S
Grade Ordinary Portland Cement, whichever
is applicable. The number of bags (net mass) to
IS 8112 : 1989
determination of the water content of mortar
for the compressive strength tests and for the
determination of soundness and setting time,
shall be obtained by the method described in
IS 4031 (Part 4) : 1988.
10 SAMPLING
10.1 Samples for Testing and by Whom to
be Taken
A sample or samples for testing may be taken
by the purchaser or his representative, or by
any person appointed to superintend the work
for purpose of which the cement is required or
by latters representative.
11 TESTS
11.1 The sample or samples of cement for test
shall be taken as described in 10 and shall be
tested in the manner described in the relevant
clauses.
12 REJECTION
12.1 Cement may be rejected if it does not
comply with any of the requirements of this
specification.
IS 8112 : 1989
ANNEX A
( Clause 2.1 )
LIST OF REFERRED INDIAN STANDARDS
IS No.
Title
IS No.
650 : 1966
2003
Specification : Part 1 For use as
pozzolana in cement, cement
mortar and concrete ( second
revision )
4031
Methods of physical test for
(Parts 1 to 13) hydraulic cement ( first revision )
4032 : 1985
Method of chemical analysis of
hydraulic cement ( first revision )
Title
4845 : 1968
4905 : 1968
11652 : 1986
11653 : 1986
11761 : 1986
12089 : 1987
Granulated
slag
for
the
manufacture of Portland slag
cement Specification
12154 : 1987
12174 : 1987
12423 : 1988
Method
for
calorimetric
analysis of hydraulic cement
15388 : 2003
ANNEX B
( Clause 9.2 )
TOLERANCE REQUIREMENTS FOR THE MASS OF CEMENT
PACKED IN BAGS
the minus error in none of such bags in the
sample shall exceed 4 percent of the specified
net mass of cement in the bag.
IS 8112 : 1989
ANNEX C
COMPOSITION OF THE TECHNICAL COMMITTEE
CEMENT AND CONCRETE SECTIONAL COMMITTEE, CED 2
Chairman
DR H. C. VISVESVARAYA
Representing
National Council for Cement and Building Materials, New Delhi
Members
SHRI K. P. BANERJEE
SHRI H ARISH N. MALANI ( Alternate )
SHRI S. K. BANERJEE
CHIEF ENGINEER (BD)
SHRI J. C. BASUR ( Alternate )
CHIEF ENGINEER (DESIGNS)
SUPERINTENDING ENGINEER (S & S)
( Alternate )
CHIEF ENGINEER (RESEARCH-CUMDIRECTOR)
RESEARCH OFFICER (CONCRETE
TECHNOLOGY) ( Alternate )
DIRECTOR
JOINT DIRECTOR ( Alternate )
DIRECTOR
CHIEF RESEARCH OFFICER ( Alternate )
DIRECTOR (C & MDD-II)
DEPUTY DIRECTOR (C & MDD-II)
( Alternate )
SHRI V. K. GHANEKAR
SHRI S. GOPINATH
SHRI A. K. GUPTA
SHRI J. SEN GUPTA
SHRI P. J. JAGUS
DR A. K. CHATTERJEE ( Alternate )
JOINT DIRECTOR STANDARDS (B & S)/CB-I
JOINT DIRECTOR STANDARDS (B & S)/
CB-II ( Alternate )
SHRI N. G. JOSHI
SHRI R. L. KAPOOR
SHRI R. K. SAXENA ( Alternate )
DR A. K. MULLICK
SHRI G. K. MAJUMDAR
SHRI P. N. MEHTA
SHRI S. K. MATHUR ( Alternate )
SHRI NIRMAL SINGH
SHRI S. S. MIGLANI ( Alternate )
SHRI S. N. PAL
SHRI BIMAN DASGUPTA ( Alternate )
SHRI R. C. PARATE
LT-COL R. K. SINGH ( Alternate )
SHRI H. S. PASRICHA
SHRI Y. R. PHULL
SHRI S. S. SEEHRA ( Alternate )
DR MOHAN RAI
DR S. S. REHSI ( Alternate )
SHRI A. V. RAMANA
DR K. C. NARANG ( Alternate )
SHRI G. RAMDAS
SHRI T. N. SUBBA RAO
SHRI S. A. REDDI ( Alternate )
IS 8112 : 1989
Members
Representing
DR M. RAMAIAH
DR A. G. MADHAVA RAO ( Alternate )
SHRI A. U. RIJHSINGHANI
SHRI C. S. SHARMA ( Alternate )
SECRETARY
SHRI K. R. SAXENA ( Alternate )
SUPERINTENDING ENGINEER (DESIGNS)
EXECUTIVE ENGINEER (SMD DIVISION)
( Alternate )
SHRI L. SWAROOP
SHRI H. BHATTACHARYA
( Alternate )
SHRI S. K. GUHA THAKURTA
SHRI S. P. SANKARNARAYANAN
( Alternate )
DR H. C. VISVESVARAYA
SHRI D. C. CHATURVEDI ( Alternate )
SHRI G. RAMAN,
Director (Civ Engg)
Members
DR A. K. MULLICK
( Alternates to Dr H. C. Visvesvaraya )
DR (SHRIMATI) S. LAXMI
SHRI S. K. BANERJEE
National Test House, Calcutta
Directorate General of Technical Development, New Delhi
SHRI N. G. BASAK
SHRI T. MADNESHWAR ( Alternate )
Cement Manufacturers Association, Bombay
SHRI SOMNATH BANERJEE
Irrigation Department, Government of Punjab
CHIEF ENGINEER (RESEARCH-CUMDIRECTOR)
RESEARCH OFFICER (CT) ( Alternate )
Gujarat Engineering Research Institute, Vadodara
SHRI N. B. DESAI
SHRI J. K. PATEL ( Alternate )
DIRECTOR
Maharashtra Engineering Research Institute, Nasik
RESEARCH OFFICER ( Alternate )
Central Water Commission, New Delhi
DIRECTOR (C & MDD II)
DEPUTY DIRECTOR (C & MDD II)
( Alternate )
Shree Digvijay Cement Co Ltd, Bombay
SHRI R. K. GATTANI
SHRI R. K. VAISHNAVI ( Alternate )
SHRI J. SEN GUPTA
National Buildings Organization, New Delhi
The Associated Cement Companies Ltd, Bombay
SHRI P. J. JAGUS
DR A. K. CHATTERJEE ( Alternate )
JOINT DIRECTOR, STANDARDS
Research, Designs and Standards Organization, Lucknow
(B & S)/CB-I
JOINT DIRECTOR, STANDARDS
(B & S)/CB-II ( Alternate )
Roads Wing (Ministry of Transport) (Department of Surface Transport),
SHRI R. L. KAPOOR
New Delhi
SHRI R. K. DATTA ( Alternate )
The Hindustan Construction Co Ltd, Bombay
SHRI W. N. KARODE
Chettinad Cement Corporation Ltd, Poliyur, Tamil Nadu
SHRI R. KUNJITHAPATTAM
SHRI G. K. MAJUMDAR
Hospital Services Consultancy Corporation (India) Ltd, New Delhi
IS 8112 : 1989
Members
SHRI K. P. MOHIDEEN
SHRI NIRMAL SINGH
SHRI S. S. MIGLANI ( Alternate )
SHRI Y. R. PHULL
SHRI M. R. CHATTERJEE ( Alternate )
SHRI A. V. RAMANA
DR K. C. NARANG ( Alternate )
COL V. K. RAO
SHRI N. S. GALANDE ( Alternate )
SHRI S. A. REDDI
DR S. S. REHSI
DR IRSHAD MASOOD ( Alternate )
SHRI A. U. RIJHSINGHANI
SHRI M. P. SINGH
SUPERINTENDING ENGINEER (D)
SENIOR DEPUTY CHIEF ENGINEER
(GENERAL) ( Alternate )
SHRI L. SWAROOP
SHRI H. BHATTACHARYA ( Alternate )
SHRI V. M. WAD
Representing
Central Warehousing Corporation, New Delhi
Development Commissioner for Cement Industry (Ministry of Industry)
Central Road Research Institute (CSIR), New Delhi
Dalmia Cement (Bharat) Ltd, New Delhi
Engineer-in-Chiefs Branch, Army Headquarters
Gammon India Ltd, Bombay
Central Building Research Institute (CSIR), Roorkee
Cement Corporation of India Ltd, New Delhi
Federation of Mini Cement Plants, New Delhi
Public Works Department, Government of Tamil Nadu
Date of Issue
Amd. No. 1
January 1991
Amd. No. 2
November 1991
Amd. No. 3
November 1993
Amd. No. 4
October 1998
Amd. No. 5
October 1999
Amd. No. 6
June 2000
Amd. No. 7
December 2003
Amd. No. 8
May 2005
Telegrams: Manaksanstha
(Common to all offices)
Regional Offices:
Central
Eastern
Telephone
323 76 17
323 38 41
60
38 43
20 25
Branches : A H M E D A B A D . B A N G A L O R E . B H O P A L . B H U B A N E S H W A R . C O I M B A T O R E .
FARIDABAD. GHAZIABAD. GUWAHATI. HYDERABAD. JAIPUR. KANPUR.
LUCKNOW. NAGPUR. NALAGARH. PATNA. PUNE. RAJKOT. THIRUVANANTHAPURAM.
VISHAKHAPATNAM.