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Jq/'iu1: B.E./B.Tech. Degree Examination, May/June 2007 '

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Jq\'iu1 A^L244

B.E./B.Tech.DEGREEEXAMINATION, MAY/JUNE2007'

Sixth Semester

Electronics and Instrumentation Engineering

EI 338 - ANALYTICAL INSTRUMENTS

(Common to Instrumentation and Control Engineering)

Time : Three hours Maximum: 100 marks

Answer ALL questions.

PARTA-(10 x2=20 marks)

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1. Defrne pH value of a solution?

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2. Name two moisture measuring sensors?

3. What is meant by thermal conductivity?


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4. Mention four types of industrial analysers?

What is meant by Gas chromatography?


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5.

6. Name four detectors that are used in liquid chromatoglaphy?


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7. State Beer-Lambert law.


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8., What are the advantagesof double beam spectrophotometerover single beam
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spectrophotometers?
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9. List any four Applications of NMR.

10. Mention any four sourcesof X-rays that are used in X-ray spectroscopy'

PARTB-(5x16=80marks)

11. (a) (i) With neat sketch, explain the principle and construction and
working of glasselectrode' (8)

(ii) With neat diagram, Describe the principle, construction and


working of dissolvedoxygen analyser' (8)

Or
(b) (i) Explain, with neat diagram, how measurement of conductance is
done by Null method. (8)

(ii) With neat sketch, Explain any one method of moisture


measurement. (8)

12. (a) With neat sketch, Describe the principle, construction and working of
' paramagnetic oxygen analyser. (16)

Or

(b) (i) With neat diagram, Explain the principle and working of
smokemeter. (8)
(ii) With neat sketch, Explain, the principle and working of dustmeter.
(8)

13. (a) Neatly draw the instrumentation diagram of Gas chromatogtaphy, and
Explain, how the separation of mixtures is done. (16)

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Or

(b) Explain the following detectorsused in liquid chromatography.


N.
(i) FID (Flame ionisation detector) (8)
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(ii) ECD (Electron capture detector) (8)
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14. (a) With neat line diagram, Explain the working of singie beam visible
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spectrophotometer. (16)
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Or
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(b) With a neat Block diagrarn, Explain the construction and working of
flame photometer. (16)
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15. (a) With neat Diagram, Explain the principle and working of NMR
Spectrometer. (16)

Or

(b) (i) Explain the principle of GM counter (Geiger Muller), (8)

(ii) Explain the principle of Proportional counter. (8)

AIzM

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