Asme Section II A-2 Sa-453 Sa-453m
Asme Section II A-2 Sa-453 Sa-453m
Asme Section II A-2 Sa-453 Sa-453m
SA-453 /SA-453M
1.
Scope
1.1 This specification covers four grades of bolting
materials with nine classes of yield strength ranging from
50 to 120 ksi [345 to 827 MPa] for use in high-temperature
service such as fasteners for pressure vessel and valve
flanges. The material requires special processing and is
not intended for general purpose applications. The term
bolting material, as used in this specification, covers
rolled, forged, or hot-extruded bars; bolts, nuts, screws,
washers, studs, and stud bolts. Headed bolts and rolled
threads may be supplied.
A 370 Test Methods and Definitions for Mechanical Testing of Steel Products
A 437 /A 437M Specification for Alloy-Steel TurbineType Bolting Material Specially Heat Treated for HighTemperature Service
E 30 Test Methods for Chemical Analysis of Steel, Cast
Iron, Open-Hearth Iron, and Wrought Iron
E 59 Practice for Sampling Steel and Iron for Determination of Chemical Composition
E 139 Practice for Conducting Creep, Creep-Rupture, and
Stress-Rupture Tests of Metallic Materials
2.2 ANSI Standards:
ANSI B1.1 Unified Screw Threads
ANSI B18.2.1 Square and Hex Bolts and Screws Including
Hex Cap Screws and Lag Screws
ANSI B18.2.2 Square and Hex Nuts
ANSI B18.3 Hexagon Socket and Spline Socket Screws
3.
Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 bolting material this covers rolled, forged,
or hot-extruded bars; bolts, nuts, screws, washers, studs,
and stud bolts; and also includes those manufactured by
upset heading or roll threading techniques.
3.1.2 heat-treatment charge one heat of material
heat treated in one batch. If a continuous operation is used,
the weight processed as a heat-treatment charge shall not
exceed the weights in Table 1.
3.1.3 lot a lot shall consist of the quantities shown
in Table 2.
2.
Referenced Documents
2.1 ASTM Standards:
A 193 /A 193M Specification for Alloy-Steel and Stainless
Steel Bolting Materials for High-Temperature Service
831
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SA-453 /SA-453M
4.
6.2.2 Samples for chemical analysis, except for spectro-chemical analysis, shall be taken in accordance with
Practice E 59. The chemical composition thus determined
shall conform to the requirements for product analysis
variation as specified in Table 4.
6.2.3 A product analysis shall be made by the manufacturer of bar stock made from vacuum-arc remelted steel.
Ordering Information
4.1 The inquiry and order shall indicate the following:
4.1.1 Quantity (weight or number of pieces),
4.1.2 Type of material (bars, bolts, nuts, etc.),
4.1.3 Grade and class,
4.1.4 Method of finishing (see 5.2),
4.1.5 Type of thread desired (see 5.2.2),
7.
Mechanical Properties
7.1 Tension Test:
7.1.1 Requirements The material shall conform to
the room-temperature tensile in each heat-treatment charge
(see 3.1.2).
7.1.2 Number of Specimens:
Chemical Composition
6.1 Heat Analysis An analysis of each heat of steel
shall be made by the manufacturer to determine the percentages of the elements specified in Table 4. This analysis
shall be made from a test sample taken during the pouring
of the heat. The chemical composition thus determined
shall be reported to the purchaser or his representative and
shall conform to the requirements specified in Table 4.
7.2.4.3 As an alternative procedure and, when specifically approved by the purchaser, separate smooth and
notched test specimens, machined from adjacent sections
of the same piece, with gage sections conforming to the
respective dimensions of Table 6, may be tested under the
above conditions. The notched specimen need not be tested
to rupture but shall not rupture in less time than the companion smooth specimen.
9.
7.2.4.4 When the minimum specified time to rupture in Table 5 has been achieved, incremental loading
may be used to accelerate the time to rupture. At intervals
of 8 to 16 h, preferably 8 to 10 h, the stress shall be
increased in increments of 5000 psi [34.5 MPa]. Rupture
location and elongation requirements shall be as prescribed
in Table 5, 7.2.4.2, and 7.2.4.3.
11. Inspection
11.1 The manufacturer shall afford the purchasers
inspector all reasonable facilities necessary to satisfy him
that the material is being furnished in accordance with the
specification. Mill inspection by the purchaser shall not
interfere unnecessarily with the manufacturers operations.
All tests and inspections shall be made at the place of
manufacture, unless otherwise agreed to.
SA-453 /SA-453M
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SA-453 /SA-453M
13. Certification
13.1 The producers certification shall include the bolting Grade, Class, and Type and shall state that the material
was manufactured and tested in accordance with this specification.
14.3 For purposes of identification marking, the manufacturer is considered the organization that certifies the
fastener was manufactured, sampled, tested, and inspected
in accordance with the specification and the results have
been determined to meet the requirements of this specification.
15. Keywords
15.1 boltssteel; fastenerssteel; marking; nutssteel;
precipitation hardening steels; pressure vessel service; revision letter; steel barsalloy; steel bolting material; steel
flanges; steel values; temperature service applications
high; year date
C
8
1/ in. rad
8
Detail sketch
A
60 deg
8
1/ deg
2
Rod
Detail
834
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SA-453 /SA-453M
TABLE 2
LOT SIZES
TABLE 1
CONTINUOUS HEAT-TREATMENT CHARGE SIZES
Diameter, in. [mm]
Weight, lb [kg]
To 134 [44]
Over 134 [44] to 212 [63]
Over 212 [63]
3000 [1400]
6000 [2700]
12000 [5400]
and under
[38] to 134 [44], incl
[44] to 212 [63], incl
[63]
TABLE 3
HEAT TREATMENT REQUIREMENTSA
Grade Class
660
A
B
C
651
662
A
B
665
A
B
Solution Treatment
Hardening Treatment
1650 25F [900 14C], hold 2 h, min, and liquid quench 1325 25F [720 14C], hold 16 h, air cool
1800 25F [980 14C], hold 1 h, min, and liquid quench 1325 25F [720 14C], hold 16 h, air cool
1800 25F [980 14C], hold 1 h, min, and oil quench
1425 25F [775 14C], hold 16 h, air cool
1200 25F [650 14C], hold 16 h, air cool
hot-cold worked at 1200F [650C] min with 15% min reduction
in cross-sectional area, stress-relief anneal at 1200F [650C]
min for 4 h, min
hot-cold worked at 1200F [650C] min with 15% min reduction
of cross-sectional area, stress-relief anneal at 1350F [730C]
min for 4 h, min
1800 25F [980 14C], hold 2 h, liquid quench
1350 to 1400F [730 to 760C], hold 20 h, furnace cool to
1200 25F [650 14C], hold 20 h, air cool
1950 25F [1065 14C], hold 2 h, liquid quench
1350 to 1400F [730 to 760C], hold 20 h, furnace cool to
1200 25F [650 14C], hold 20 h, air cool
1800 25F [980 14C], hold 3 h, liquid quench
1350 to 1400F [730 to 760C], hold 20 h, furnace cool to
1200 25F [650 14C], hold 20 h, air cool
2000 25F [1095 14C], hold 3 h, liquid quench
1350 to 1400F [730 to 760C], hold 20 h, furnace cool to
1200 25F [650 14C], hold 20 h, air cool
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SA-453 /SA-453M
TABLE 4
CHEMICAL REQUIREMENTS
Grade 660
Product Analysis Variation,
Over or Under, %
Content, %
Carbon
Manganese
Phosphorus
Sulfur
Silicon
Nickel
Chromium
Molybdenum
Tungsten
Titanium
ColumbiumA
Aluminum
Vanadium
Boron
0.08 max
2.00 max
0.040 max
0.030 max
1.00 max
24.027.0
13.516.0
1.001.50
...
1.902.35
...
0.35 max
0.100.50
0.0010.010
Copper
...
Grade 651
Content, %
0.01 over
0.04
0.005 over
0.005 over
0.05
0.20
0.20
0.05
...
0.05
...
0.05 over
0.03
0.0004 under to
0.001 over
...
0.280.35
0.751.50
0.040 max
0.030 max
0.300.80
8.011.0
18.021.0
1.001.75
1.001.75
0.100.35
0.250.60
...
...
...
0.02
0.04
0.005 over
0.005 over
0.05
0.15
0.25
0.05
0.05
0.05 over
0.05
...
...
...
0.50 max
0.03 over
Grade 662
Carbon
Manganese
Phosphorus
Sulfur
Silicon
Nickel
Chromium
Molybdenum
Titanium
Aluminum
Copper
Boron
A
Grade 665
Content, %
0.08 max
0.401.00
0.040 max
0.030 max
0.401.00
24.028.0
12.015.0
2.03.5
1.802.10
0.35 max
0.50 max
0.0010.010
Content, %
0.01 over
0.03
0.005 over
0.005 over
0.05
0.20
0.15
0.10
0.05
0.05 over
0.03 over
0.0004 under to
0.001 over
0.08 max
1.252.00
0.040 max
0.030 max
0.100.80
24.028.0
12.015.0
1.252.25
2.703.3
0.25 max
0.25 max
0.010.07
TABLE 5
STRESS RUPTURE REQUIREMENTS
Grade
Class
660
651
662
665
A, B, and C
A and B
A and B
A
B
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Stress,
ElongaTest
min
Time to
tion,
Temperature,
Rupture, min.,
F [C]
ksi MPa min., hA
%
1200
1200
1200
1200
1200
[650]
[650]
[650]
[650]
[650]
56
40
55
75
70
385
275
380
515
485
100
100
100
100
100
5
5
5
3
5
836
Licensee=Occidental Chemical Corp New sub account/5910419101
Not for Resale, 08/13/2007 15:25:08 MDT
SA-453 /SA-453M
TABLE 6
TEST SPECIMEN DIMENSIONS
Specimen
Type
Mid-length
Gage Dia D
and NotchRoot Dia F
Gage
Length,
G
Shoulder
Diameter,
H
NotchRoot
Radius
Inches
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1
2
3
4
5
6
Tolerance
0.125
0.160
0.178
0.252
0.357
0.505
0.001
0.5
0.65
0.75
1.0
1.5
2.0
0.05
0.177
0.226
0.250
0.375
0.500
0.750
0.003
0.005
0.005
0.005
0.007
0.010
0.015
0.0005
Millimeters
7
8
9
10
11
12
Tolerance
3.17
4.06
4.52
6.40
9.07
12.8
0.025
12.0
17.0
20.0
25.0
40.0
50.0
1.3
4.5
5.5
6.5
9.5
12.0
19.0
0.1
0.13
0.13
0.13
0.18
0.25
0.38
0.01
837
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SA-453 /SA-453M
TABLE 7
MECHANICAL PROPERTY REQUIREMENTS
Tensile
Strength,
min
Yield
Strength
(0.2%
Offset), min
Grade
Class
ksi
MPa
ksi
MPa
660
651
A, B, and C
A
130
100
895
690
95
655
A
B
A
B
130
125
170
155
895
860
1170
1070
85
70B
60C
60B
50C
85
80
120
120
585
485
415
415
345
585
550
830
830
662
665
Approximate Rockwell
Hardness,
B and C
Elongation in 4
DiamA,
min, %
Reduction of
Area, min,
%
Brinell
Hardness
Number
15
18
18
35
248341
217277
99 HRBD
95 HRB
37 HRC
29 HRC
18
35
212269
93 HRB
28 HRCE
15
15
12
12
18
18
15
15
255321
248321
311388
311388
100 HRBD
99 HRB
32 HRC
32 HRC
35
35
41
41
min
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max
HRCE
HRC
HRC
HRC
SA-453 /SA-453M
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TABLE 8
PERMISSIBLE VARIATIONS IN SIZE OF
HOT-ROLLED BARS
Permissible
Variations from
Specified Size
Specified Size
Over
Under
Out of
Round
TABLE 9
PERMISSIBLE VARIATIONS IN SIZE OF
COLD-FINISHED BARS
Inches
5
16 and under
Over 516 to 716, incl
Over 716 to 58, incl
Over 58 to 78, incl
Over 78 to 1, incl
1
Over
Over
Over
Over
Over
1 to 1
118 to
114 to
138 to
112 to
Over
Over
Over
Over
Over
Over
2 to 212, incl
212 to 312, incl
312 to 412, incl
412 to 512, incl
512 to 612, incl
612 to 712, incl
8, incl
114, incl
138, incl
112, incl
2, incl
0.005
0.006
0.007
0.008
0.009
0.005
0.006
0.007
0.008
0.009
0.008
0.009
0.010
0.012
0.013
0.010
0.011
0.012
0.014
1
64
0.010
0.011
0.012
0.014
1
64
0.015
0.016
0.018
0.021
0.023
0
0
0
0
0
0
0.023
0.035
0.046
0.058
0.070
0.085
32
64
1
16
5
64
1
8
5
32
3
Under
0.002 [0.05]
0.0025 [0.06]
0.003 [0.08]
0.002 [0.05]
0.0025 [0.06]
0.003 [0.08]
A
When it is necessary to heat treat or heat treat and pickle after
cold finishing, because of special hardness or mechanical property
requirements, the permissible variations are generally double those
shown in the table.
B
For size tolerances of sizes over 4 in. [100 mm], the manufacturer should be consulted.
TABLE 10
THREAD TYPES
Millimeters
8.0 and under
Over 8.0 to 11.0, incl
Over 11.0 to 16.0, incl
Over 16.0 to 22.0, incl
Over 22.0 to 25.0, incl
0.13
0.15
0.18
0.20
0.23
0.13
0.15
0.18
0.20
0.23
0.20
0.23
0.25
0.30
0.33
Over
Over
Over
Over
Over
25.0
29.0
32.0
35.0
38.0
29.0 incl
32.0, incl
35.0, incl
38.0, incl
51.0, incl
0.25
0.28
0.30
0.35
0.40
0.25
0.28
0.30
0.35
0.40
0.38
0.41
0.46
0.53
0.58
Over
Over
Over
Over
Over
Over
0.80
1.2
1.6
2.0
3.2
4.0
0
0
0
0
0
0
0.58
0.89
1.2
1.5
1.8
2.2
to
to
to
to
to
Over
Type
Operation
M1
M2
Machine cut
Machine cut
R1
R2
Rolled
Rolled
Post-precipitation hardening
Post-solution anneal and
pre-precipitation hardening
Post-precipitation hardening
Post-solution anneal and
pre-precipitation hardening
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SA-453 /SA-453M
SUPPLEMENTARY REQUIREMENT
The following supplementary requirement shall apply only when specified by the purchaser
in the inquiry, contract, and order.
S1. Marking
S1.1 Grade and manufacturers identification symbols
shall be applied to one end of studs and to the heads of
bolts of all sizes. (If the available area is inadequate, the
grade symbol may be marked on one end and the manufacturers identification symbol marked on the other end.) For
bolts and studs smaller than 14 in. [6 mm] in diameter and
for 14 in. [6 mm] studs requiring more than a total of
three symbols, the marking shall be a matter of agreement
between the purchaser and the manufacturer.
840
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