Designation: G 123 – 00

Standard Test Method for

Evaluating Stress-Corrosion Cracking of Stainless Alloys
with Different Nickel Content in Boiling Acidified Sodium
Chloride Solution1
This standard is issued under the fixed designation G 123; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

1. Scope statements, see Section 7 .

1.1 This test method describes a procedure for conducting 2. Referenced Documents
stress-corrosion cracking tests in an acidified boiling sodium
chloride solution. This test method is performed in 25 % (by 2.1 ASTM Standards:
mass) sodium chloride acidified to pH 1.5 with phosphoric D 1193 Specification for Reagent Water3
acid. This test method is concerned primarily with the test E 8 Test Methods for Tension Testing of Metallic Materials4
solution and glassware, although a specific style of U-bend test E 691 Practice for Conducting an Interlaboratory Study to
specimen is suggested. Determine the Precision of a Test Method5
1.2 This test method is designed to provide better correla- G 15 Terminology Relating to Corrosion and Corrosion
tion with chemical process industry experience for stainless Testing6
steels than the more severe boiling magnesium chloride test of G 16 Guide for Applying Statistics to Analysis of Corrosion
Practice G 36. Some stainless steels which have provided Data6
satisfactory service in many environments readily crack in G 30 Practice for Making and Using U-Bend Stress Corro-
Practice G 36, but have not cracked during interlaboratory sion Test Specimens6
testing2 using this sodium chloride test method. G 36 Practice for Evaluating Stress-Corrosion-Cracking
1.3 This boiling sodium chloride test method was used in an Resistance of Metals and Alloys in a Boiling Magnesium
interlaboratory test program to evaluate wrought stainless Chloride Solution6
steels, including duplex (ferrite-austenite) stainless and an G 49 Practice for Preparation and Use of Direct Tension
alloy with up to about 33 % nickel. It may also be employed to Stress Corrosion Test Specimens 6
evaluate these types of materials in the cast or welded G 107 Guide for Formats for Collection and Compilation of
conditions. Corrosion Data for Metals for Computerized Database
1.4 This test method detects major effects of composition, Input6
heat treatment, microstructure, and stress on the susceptibility 3. Terminology
of materials to chloride stress-corrosion cracking. Small dif-
ferences between samples such as heat-to-heat variations of the 3.1 Definitions:
same grade are not likely to be detected. 3.1.1 For definitions of corrosion-related terms used in this
1.5 The values stated in SI units are to be regarded as the test method, see Terminology G 15.
standard. The values given in parentheses are for information 4. Summary of Test Method
only.
1.6 This standard does not purport to address all of the 4.1 A solution of 25 % sodium chloride (by mass) in reagent
safety concerns, if any, associated with its use. It is the water is mixed, and the pH is adjusted to 1.5 with phosphoric
responsibility of the user of this standard to establish appro- acid. The solution is boiled and U-bends (or other stressed
priate safety and health practices and determine the applica- specimens) are exposed in fresh solution for successive one-
bility of regulatory limitations prior to use. For specific hazard week periods.
4.2 The test may be continued for as many weeks as
necessary, but six weeks (about 1000 h) or less are expected to
1
This test method is under the jurisdiction of ASTM Committee G01 on
be sufficient to crack susceptible materials. Longer exposures
Corrosion of Metals and is the direct responsibility of Subcommittee G01.06 on
Stress Corrosion Cracking and Corrosion Fatigue.
3
Current edition approved Oct. 10, 2000. Published October 2000. Originally Annual Book of ASTM Standards, Vol 11.01.
4
published as G 123 – 94. Last previous edition G 123 – 96. Annual Book of ASTM Standards, Vol 03.01.
2 5
Interlaboratory test program including UNS S30400, S31600, S32550, and Annual Book of ASTM Standards, Vol 14.02.
6
N08020. These data are available at ASTM Headquarters. Request RR G01-1013. Annual Book of ASTM Standards, Vol 03.02.

Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.

1
 G 123
provide greater assurance of resistance for those materials
which do not crack.
4.3 It is recommended that samples of a susceptible mate-
rial, for example, UNS S30400 or S31600 (Type 304 or Type
316 stainless, respectively), be included as a control when
more resistant materials are evaluated.

5. Significance and Use

5.1 This test method is designed to compare alloys and may
be used as one method of screening materials prior to service.
In general, this test method is more useful for stainless steels
than the boiling magnesium chloride test of Practice G 36. The
boiling magnesium chloride test cracks materials with the
nickel levels found in relatively resistant austenitic and duplex
stainless steels, thus making comparisons and evaluations for
many service environments difficult.
5.2 This test method is intended to simulate cracking in
water, especially cooling waters that contain chloride. It is not
intended to simulate cracking that occurs at high temperatures
(greater than 200°C or 390°F) with chloride or hydroxide.
NOTE 1—The degree of cracking resistance found in full-immersion
tests may not be indicative of that for some service conditions comprising
exposure to the water-line or in the vapor phase where chlorides may
concentrate.
5.3 Correlation with service experience should be obtained
when possible. Different chloride environments may rank
materials in a different order.
5.4 In interlaboratory testing, this test method cracked
annealed UNS S30400 and S31600 but not more resistant
materials, such as annealed duplex stainless steels or higher
nickel alloys, for example, UNS N08020 (for example 20Cb-37
FIG. 1 Apparatus Used for Stress-Corrosion Cracking Test
stainless). These more resistant materials are expected to crack
when exposed to Practice G 36 as U-bends. Materials which
withstand this sodium chloride test for a longer period than S31600) and resistant (for example, UNS N08020) materials
UNS S30400 or S31600 may be candidates for more severe are included in the study.)
service applications. 6.1.3 Hot Plate, capable of maintaining the solution at its
5.5 The repeatability and reproducibility data from Section boiling point.
11 and Appendix X1 must be considered prior to use. Inter-
laboratory variation in results may be expected as occurs with 7. Reagents
many corrosion tests. Acceptance criteria are not part of this 7.1 Purity of Reagents—Reagent grade chemicals shall be
test method and if needed are to be negotiated by the user and used in all tests. Unless otherwise indicated, it is intended that
the producer. all reagents shall conform to the specifications of the Commit-
tee on Analytical Reagents of the American Chemical Society,
6. Apparatus where such specifications are available.8 Other grades may be
6.1 The glassware used for this test method is shown in Fig. used provided it is first ascertained that the reagent is of
1 and is as follows: sufficiently high purity to permit its use without affecting
6.1.1 Flask—1000-mL Erlenmeyer flask with a 45/50 results.
ground-glass joint. 7.2 Purity of Water—Solutions shall be made with water of
6.1.2 Condenser, a four-bulb Allihn condenser with a 45/50 purity conforming to at least Type IV reagent water as specified
ground glass joint (water-cooled joint suggested), a water in Specification D 1193 (except that for this method limits for
jacket at least 20 cm (8 in.) long and a 1 to 2.5 cm (0.4 to 0.95 chlorides and sodium may be ignored).
in.) long drip tip is used. (Modified Allihn condensers with no
drip tip and condensers with longer drip tips may produce
different results. These alternate Allihn condenser designs may 8
Reagent Chemicals, American Chemical Society Specifications, American
be used if control samples of susceptible (for example, UNS Chemical Society, Washington, DC. For suggestions on the testing of reagents not
listed by the American Chemical Society, see Analar Standards for Laboratory
Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,
7
20Cb-3 is a registered trademark of Carpenter Technology Corp., Reading, PA. MD.

2
 G 123
7.3 Sodium Chloride (NaCl)—A solution of 25 % NaCl (by 9.5.3 The metallic fastener must be electrically isolated
mass) acidified to pH 1.5 with phosphoric acid (H3PO4) is from the specimen by a rigid shoulder washer, (that is, zirconia
used. The solution may be prepared by adding 750 g H2O (750 or another material that will not be compressed during the test).
mL) to 250 g NaCl, and adjusting to pH 1.5 with H3PO4. 9.5.4 The extended end of the bolt may require cutting to fit
Varying quantities of solution may be prepared and larger into the test vessel.
amounts may be stored indefinitely in appropriate glassware. 10. Procedure
The pH must be determined prior to each use.
10.1 Stress the specimens, examine at 203, and replace any
8. Hazards specimens with cracks or other defects.
8.1 Normal precautions for handling boiling liquid should NOTE 2—The direction and intensity of the incident light may affect
be observed. crack detection during the 203 examination.
8.2 All heating or boiling of the NaCl solution should be 10.2 Degrease in a halogen-free solvent or laboratory deter-
done in an area where personnel are not likely to accidentally gent, rinse as necessary, and dry. It is best practice to stress the
bump the flask. A hooded area is preferred. specimens immediately before the beginning of the test. Any
8.3 Minimum personal protective equipment for handling storage of the specimens should be in a clean enclosure. A
boiling sodium chloride should include safety glasses or desiccant such as silica gel may be used. The specific level of
goggles, face shield, laboratory coat, and rubber gloves. relative humidity is not important for the alloys of interest.
(Warning—U-bends (and other highly stressed test speci- 10.3 Place duplicate specimens in each 1000-mL Erlenm-
mens) may be susceptible to high rates of crack propagation eyer flask. Duplicate flasks (four specimens) are necessary to
and a specimen containing more than one crack may splinter evaluate a given sample of the specific material, material
into two or more pieces. This may also occur due to a cracked condition, etc. (The specimens may be placed in the flasks after
restraining bolt. Due to the highly stressed condition in a the solution has been added, if convenient.)
U-bend specimen, these pieces may leave the specimen at high 10.4 The specimens in each flask must be kept separate and
velocity and can be dangerous.) completely submerged. Tight crevices between the stressed
9. Test Specimens (bend) area and any means of specimen support should be
avoided. The stressed area should be free from direct contact
9.1 U-bends are preferred but other stress corrosion crack-
with heated surfaces. Specimens may be supported on glass
ing specimens may be used with this test solution. The
rods or tubes or by glass fixtures.
specimen style chosen should provide sufficient stress to crack
10.5 Drop boiling chips9 into the flasks.
less resistant materials (for example, UNS S30400 or S31600)
10.6 Add 600 mL of 25 % NaCl solution, pH 1.5 to each
in 1000 h or less). (See Annex A1.) Regardless of the specimen
flask. When each flask contains two U-bends as described in
style, it is recommended that UNS S30400 or UNS S31600, or
Annex A1, the solution volume to sample surface area ratio is
both, be included as controls.
5:1 mL/cm 2 (33 mL/in2).
9.2 The test specimen must be thick enough so that the
10.7 Place the flasks on a hot plate and insert the condenser.
applied stress does not cause mechanical rupture of less
Begin recording the test duration when the solution begins
resistant materials if the cross section is reduced by pitting or
boiling. The boiling point during interlaboratory testing was
general corrosion.
106 to 110°C (223 to 230°F).
9.3 The size of alternate specimens (other than those in
10.8 After one week remove the flask from the hot plate,
Annex A1) must allow a solution volume to specimen surface
determine the final pH of the solution at room temperature, and
area ratio of at least 5:1 mL/cm2 (33 mL/in.2).
discard the remaining solution. A final pH over about 2.5
9.4 A minimum of four replicates (two per flask) is required
suggests that general corrosion or pitting of the specimen or
because of the variability typical in stress-corrosion testing.
fastening device has occurred. A pH at this level is expected to
9.5 Methods of fabricating U-bend specimens are provided
reduce the test severity and may delay or preclude failures of
in Annex A1. These procedures are based on Practice G 30, but
UNS S31600. More rapid cracking of UNS S31600 appears
in addition provide a specimen that fits through a 45/50
likely with a final pH of about 2 or less.
ground-glass joint. Assurance that the legs are stressed suffi-
10.9 Rinse and dry the specimens. Examine the bend area,
ciently by the bolt is also provided.
legs, and area adjacent to the crevice (at the fastener) at 203
9.5.1 Other methods of producing U-bends described in
for cracking. See Note 3. Record location of cracks. Additional
Practice G 30 may be used; however, during exposure the
exposures or metallographic evaluation may be used to deter-
U-bends must be (a) in the plastic range and (b) stressed to the
mine if questionable indications are, in fact, stress-corrosion
maximum applied tensile load experienced during fabrication.
cracks.
The same methodmust be used to fabricate all the U-bends in
a given study. NOTE 3—Any cracking at the fastener is very likely due to residual
9.5.2 The bolt, nut, and flat washer must be made of a stresses and more aggressive solution which may be formed in crevices. If
material resistant to general corrosion, pitting, and stress
9
corrosion cracking in the environment. UNS N10276 (Alloy The sole source of supply of amphoteric alundum granules known to the
committee at this time is Hengar Co., Philadelphia, PA. If you are aware of
C-276) is recommended because some other materials (for alternative suppliers, please provide this information to ASTM Headquarters. Your
example, titanium or UNS N06600 [Alloy 600]) may be comments will receive careful consideration at a meeting of the responsible
attacked resulting in an increase in solution pH. technical committee, which you may attend..

3
 G 123
crevices are expected in service (due to design of service equipment or and reproducibility for time-to-fail data developed using UNS
deposits), a U-bend specimen employing a crevice on the bend may be S30400 and S31600 in an interlaboratory test program (Ap-
evaluated. pendix X1). Such variability is typical in time-to-fail data for
10.10 Periodic removal of the specimens from the solution stress-corrosion cracking tests, and is expected to preclude
may be necessary during the first-week to determine the time detection of small differences between samples.
when cracks first appear. Removal of the specimens is expected 12.1.1 Histograms of the time-to-crack for UNS S30400
to disturb local corrosion cells and may influence test results. and S31600 tested in accordance with this test method appear
All specimens in a given test program should have the same in Appendix X1 along with data from each laboratory. The
removal/examination schedule. When the time-to-crack is time-to-crack values in Appendix X1 are not necessarily the
recorded, the test duration at the previous examination (no maximum or minimum values which could be obtained in other
cracks) should also be noted. testing.
10.11 Expose for additional one-week periods as necessary. 12.1.2 Every specimen of UNS S30400 and S31600 cracked
Fresh solution must be used for each exposure and the initial within the 1000-h interlaboratory test duration while no crack-
and final pH (at room temperature) must be recorded weekly. ing occurred for more resistant materials, UNS S32550 (Fer-
See 10.8 regarding the effect of the final pH. ralium11 Alloy 225) and N08020.
10.12 After the final 203 examination (following the last 12.1.3 It has been observed in stress-corrosion tests of
test period) remove the fastener and examine the crevice areas various metal-alloy systems that the precision is best for tests
at 203 for cracking. of specimens that have either a very low probability of
10.13 A final examination for cracks may be performed by stress-corrosion cracking (few, if any, failures in the prescribed
additionally bending the specimens until the ends of the legs test duration) or a high probability (short failure times). The
touch. This may expose tight cracks which were not previously precision is least for groups of test specimens with an inter-
detected. The additional bending may not be appropriate for mediate probability. This was observed in the interlaboratory
materials which are susceptible to hydrogen embrittlement in test program. There were no failures of the more resistant
this environment. Do not re-expose specimens after this materials, (UNS S32550 and UNS N08020), generally rapid
additional bending. failure of the least resistant material (UNS S30400, see Fig.
10.14 Ruptured specimens should also be examined for X1.3) and greater variation in failure times for the material
evidence of mechanical failure resulting from the action of expected to have intermediate resistance (UNS S31600, see
applied stress on specimens whose cross sections have been Fig. X1.4).
reduced by general or pitting corrosion, or both. Such failures 12.1.4 Reproducibility between laboratories frequently var-
usually show evidence of ductility. Repeat tests with thicker ied more widely than repeatability within each laboratory.
specimens should be made in case of doubt. Although this variation is substantial, it is within what may be
expected for a stress-corrosion cracking test. The effects of
11. Report
interlaboratory variation must be considered if data from
11.1 Report the type of specimen used, method of specimen multiple laboratories are used.
fabrication, times to cracking (including maximum time with- 12.1.5 Analysis of the interlaboratory test data using a log
out cracks), location of cracks, final pH of each exposure, and normal distribution appears in Appendix X1.
details regarding the Allihn condenser drip tip. Note whether or 12.2 Bias—The procedure in this test method for measuring
not metallographic techniques or additional bending of the time-to-cracking of specimens in acidified sodium chloride
specimen (see section 9.13) were employed. Electronic data solution has no bias because the time-to-cracking is defined
exchange can be facilitated by using the fields suggested in only in terms of this test method, and there is no absolute
Appendix X2. (excerpted from Guide G 107). standard for reference. Time-to-cracking is a function of
11.2 Data for resistant materials shall be accompanied by specimen type as well as stress and material composition.
data for at least four susceptible control specimens for ex-
ample, UNS S30400 or UNS S31600. 13. Keywords
13.1 boiling acidified sodium chloride (NaCl); glassware;
12. Precision and Bias 10 histograms; stress corrosion cracking; U-bend specimens; UNS
12.1 Precision—Variability occurred in both repeatability N08020

10 11
The data used to evaluate precision are filed at ASTM Headquarters. Request Ferralium is a registered trademark of Langley Alloys, Ltd. of Slough, United
RR G01-1013. Kingdom.

4
 G 123
ANNEX

(Mandatory Information)

A1. SUGGESTED TEST SPECIMEN

A1.1 Using the procedure described in this test method, the

U-bend specimen described in A1.2 has produced cracking of
UNS S30400 and S31600 in less than 1000 h, without cracking
more resistant duplex stainless and higher nickel (for example,
about 33 %) materials.

A1.2 Suggested specimen dimensions appear in Fig. A1.1.

The specimen differs slightly from those suggested in Practice
G 30 to allow the completed U-bend to pass through a 45/50
ground-glass joint while being large enough to accommodate
ceramic insulators of sufficient size to resist cracking during
use.

A1.3 If surface finish is not the subject of the evaluation,

prepare the specimens to produce a 120-grit finish or its
equivalent with machining techniques.

A1.4 Bend the specimens around a 9.5 mm (0.375-in.)

diameter mandrel using an adjustable die similar to that in Fig.
A1.2 as follows. (This figure is the same as Fig. 4a in Practice
G 30.)
A1.4.1 Mark the centerline on the specimen to aid aligning.
A1.4.2 Set the gap in the die at the mandrel diameter plus
two times the specimen thickness. NOTE 1—Mandrel has 9.5 mm (0.375-in.) diameter. Dimension Z is
A1.4.3 First, depress the mandrel (hydraulic) until the apex mandrel diameter plus two times the specimen thickness.
of the U-bend is approximately level with the bottom of the FIG. A1.2 Suggested Stressing Fixture
die. Continue stressing until the legs of the U-bend are nearly (fastener inserted while specimen in die)
parallel. Final stressing is preferably done with the fastener.
The specimen may be stressed in the die or it may be removed
and restressed outside the die. Partial stressing in the die
followed by final stressing outside the die may be optimum.
A1.4.4 Insert the stressing fastener. Use ceramic insulators
(zirconia or other non-compressible, corrosion resistant, non-
conductive material). Flat washers should be used between the
ceramic insulator and fastener to extend the life of the
insulator. The bolt, nut, and flat washer must resist corrosion in
the NaCl environment. UNS N10276 is recommended for all
three items.
NOTE 1— A1.4.5 Stress the U-bend so that the legs are parallel, that is,
L, mm (in) M, mm (in) W, mm (in) T, mm (in) D, mm (in) the U-bend is more severely bent than it was due to the die
101.6 (4) 82.6 (31⁄4) 19.0 (3⁄4) ; 3.2 (; 1⁄8) 9.5 (3⁄8) pressure. The inside dimension between the legs will be about
FIG. A1.1 Suggested U-Bend Specimen Dimensions 11.4 mm (about 0.450 in.).

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APPENDIXES

(Nonmandatory Information)

X1. SUMMARY OF INTERLABORATORY TEST DATA ANALYSIS

X1.1 Test Method

X1.1.1 Testing in accordance with this test method was
performed by seven laboratories and included UNS S30400,
S31600, S32550, and N08020. Each laboratory exposed a
series of duplicate flasks, each containing two U-bends of each
grade. UNS N10276 fasteners were used by most laboratories
and the solution was replaced weekly. Examinations were
scheduled after 6 h, daily for one week, and weekly for six
weeks. Concerns of Practice E 691 and Guide G 16 were
considered as possible and appropriate.
X1.1.2 The pH was recorded before and after each expo-
sure. The initial pH was specified as 1.5. The change in pH
during all the one-week periods for all laboratories ranged
from +0.6 to +2.8 for UNS S30400 and −0.1 to +2.72 for UNS NOTE 1—Four replicates tested per laboratory. Examinations scheduled
S31600. Only one of the laboratories experienced a pH after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.2 Time-To-Crack for UNS S31600 U-Bends in pH 1.5 NaCl
increase greater than 0.55 for UNS S31600 and this increase
Test
may have been related to attack of the fasteners.

X1.2 Interlaboratory Test Data Analysis Using

Histograms
X1.2.1 Fig. X1.1 and Fig. X1.2 present the time-to-crack
data for all U-bends of susceptible materials, UNS S30400 and
UNS S31600, respectively. The within-laboratory repeatability
was often better than the between-laboratory reproducibility.
This could occur if different operators had different ability to
detect cracks or tended to find cracks in all samples after cracks
in one sample were noticed.
X1.2.2 The nature of the data suggest that analysis by
histogram is superior to attempting to calculate mean and
standard deviation values.
X1.2.3 Fig. X1.3 and Fig. X1.4 present histograms of the NOTE 1—Seven laboratories, each tested four replicates. Examinations
time-to-crack data for UNS S30400 and UNS S31600, respec- scheduled after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.3 Histogram of Time-To-Crack Data for UNS S30400
tively. All but one of the failures occurred in 28 days orless.
Stainless U-Bends in pH 1.5 NaCl Test

Cracks in one sample of UNS S31600 were found after 42 days

(1000 h). An increase in pH due to attack of the UNS N06600
fasteners may have delayed this cracking for at least one week.
X1.2.4 Four U-bends of UNS S32550 and N08020 were
exposed by each laboratory. These materials have demon-
strated good resistance to stress-corrosion cracking in service
and none of the U-bends cracked in the 42-day test.
X1.2.5 Analysis of the interlaboratory test data indicates
that materials which withstand this 42-day test without cracks
are more resistant to stress-corrosion cracking than UNS
S30400 and UNS S31600. This statement is based upon use of
the sampling and testing procedures employed in this inter-
laboratory test program.
NOTE 1—Four replicates tested per laboratory. Examinations scheduled X1.3 Interlaboratory Test Data Analysis Using a Log
after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.1 Time-To-Crack for UNS S30400 U-Bends in pH 1.5 NaCl
Normal Distribution
Test X1.3.1 The average time to cracking for the four replicates

6
 G 123

NOTE 1—Seven laboratories, each tested four replicates. Examinations

scheduled after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.4 Histogram of Time-To-Crack Data for UNS S31600
Stainless U-Bends in pH 1.5 NaCl Test

FIG. X1.5 Distribution of Average Cracking Time

of each grade tested at each laboratory are plotted in Fig. X1.5.
The tendency to follow straight line relationships suggests UNS S31600. The interlaboratory variation (95 % confidence
these data approximate a log normal distribution. interval) is 0.029 to 35.6 times the average for UNS S30400
X1.3.2 The log average time to cracking is 1.0 day for UNS and 0.15 to 6.6 times this average for UNS S31600. All
S30400 and 6.4 days for UNS S31600. The intralaboratory calculations are based on the seven participating laboratories
variation (95 % confidence interval) is 0.685 to 1.46 times this and the assumption that the data follow a log normal distribu-
average for UNS S30400 and 0.36 to 2.79 times the average for tion.

X2. STANDARD DATA ENTRY FORMAT

X2.1 Table X2.1 defines the data categories and specific Table X2.1. Reference numbers not pertinent for this test
data elements (fields) considered necessary for searching and method have been omitted from the table.
comparing data using computerized databases. Pertinent items
from Guide G 107 have been included along with additional X2.3 Items in Table X2.1 which are not pertinent for a
items specific to evaluation of stress-corrosion cracking using specific test series (for example, details for wrought-annealed
this test method. specimens) may simply be omitted from the report.
X2.2 The Guide G 107 Reference Number is shown in

7
 G 123

TABLE X2.1 Standard Data Entry Format for Corrosion Database Development
Guide G 107
Field Field Name/Description Category Sets/Fields Type/UnitsA
Reference Number
1 5.1.1 Individual test number to identify grouping of specimens tested alphanumeric
concurrently. See subsequent entries for test method
Type of Test
2 5.1.2.1 Standard test specification alphanumeric
3 5.1.2.2 Laboratory test L = laboratory
4 5.1.2.3 Date test started YYYYMMDD
Test Emphasis
5 5.1.3.1 Type(s) of corrosion evaluatedB stress corrosion
Chemistry of EnvironmentC
6 5.1.4.1 Generic description of environment 25 % NaCl (by mass) acidified to pH
1.5 with H3PO4
7 5.1.4.2 Component, common name sodium chloride, phosphoric acid
8 5.1.4.3 Chemical abstracts registry number NaCl-7647-14-5
H3PO4-7664-38-2
9 5.1.4.4 Concentration (liquids) g/L
10 5.1.4.6 Component form (1) solid
(2) liquid
11 5.1.4.7 Ionic species Na+, Cl−, H+, PO4−3
Exposure Conditions
12 5.1.5.1 Exposure duration days
13 5.1.5.4 Temperature, average boiling
14 5.1.5.7 pH, min real number
15 5.1.5.8 pH, max real number
16 5.1.5.9 pH, average real number
17 5.1.5.16 Flow none
18 5.1.5.18 Sparging none-less than saturated (open to air)
19 5.1.5.20 Exposure zone continuous immersion
20 5.1.5.24 Ratio of specimen surface area to corrodent volume mm2/L, in.2/L
21 ... Allihn condenser drip tip (1) none
(2) length in mm
Material IdentificationD
22 5.1.6.1 Material class alphanumeric
23 5.1.6.2 Subdivision of class alphanumeric
24 5.1.6.3 Finer subdivision of class alphanumeric
25 5.1.6.4 Common name/trade name (include owner of trade name) alphanumeric
26 5.1.6.5 Material Designation—UNS No. alphanumeric
27 5.1.6.6 Specification/standard alphanumeric
28 5.1.6.7 Product shape (1) pipe/tube
(2) plate
(3) sheet/strip
(4) wire/rod/bar
(5) other—describe in 5.1.6.8
29 5.1.6.8 Description for (5) in 5.1.6.7 alphanumeric
30 5.1.6.9 Product production method (1) extrusion
(2) forging
(3) casting
(4) rolling
(5) powder compaction
(6) other—describe in 5.1.6.10
31 5.1.6.10 Description of (6) in 5.1.6.9 alphanumeric
32 5.1.6.11 Heat/lot identification alphanumeric
33 5.1.6.12 Heat/lot chemical analysis alphanumeric
Specimen Identification
34 5.1.7.1 Specimen thickness mm, in.
35 5.1.7.2 Specimen width/diameter mm, in.
36 5.1.7.3 Specimen length mm, in.

8
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TABLE X2-1 Continued

Guide G 107 Refer-
Field Field Name/Description Category Sets/Fields Type/UnitsA
ence Number
37 5.1.7.4 Specimen surface area mm2, in.2
38 5.1.7.5 Density kg/mm3, lb/in.3
39 5.1.7.6 Welded specimen (1) Y = yes
(2) N = no
40 5.1.7.7 Type of weld (see section 5.1.7.8 for additional detail) (1) autogenous
(2) matching filler
(3) dissimilar metal weld
41 5.1.7.8 Weld detailsE alphanumeric
42 5.1.7.9 Welds ground or machined (1) ground
(2) machined
(3) as deposited
(4) glass bead blasted
43 5.1.7.10 Thermomechanical condition (1) standard temper—describe in
5.1.7.11
(2) annealed
(3) normalized
(4) sensitized
(5) as-cold-worked
(6) as-hot-worked
(7) aged
(8) other H.T./processing—describe in
5.1.7.11
44 5.1.7.11 Description for (1) or (7) in 5.1.7.10 alphanumeric
45 5.1.7.12 Final reduction step (1) cold-worked—give percent reduction
in 5.1.7.13
(2) hot-worked (includes extrusion and
forging)
46 5.1.7.13 Percent cold reduction %
47 5.1.7.14 Ultimate tensile strength MPa, ksi
48 5.1.7.15 Yield strength MPa, ksi
49 5.1.7.16 Percent offset for yield strength %
50 5.1.7.17 Fracture ductility (strain) %
51 5.1.7.18 Hardness real number
52 5.1.7.19 Hardness scale alphanumeric
53 5.1.7.20 Surface condition (1) as produced
(2) scaled
(3) machined/ground
(4) chemically cleaned
(5) sand/grit blasted
(6) other
54 5.1.7.21 Surface treatment (1) none
(2) nitrided
(3) carburized
(4) plated
(5) clad
(6) other
55 5.1.7.22 If (4), (5), or (6) in 5.1.6.21, plating or cladding material or other alphanumeric
surface treatment
56 5.1.7.23 Condition of edges (1) as cut
(2) as sheared
(3) ground
(4) machined
(5) other—describe in 5.1.7.24
57 5.1.7.24 Description of other edge condition alphanumeric
58 5.1.7.25 Sample orientation relative to working direction (1) longitudinal
(2) transverse
(3) short transverse
59 5.1.7.26 Stress-corrosion cracking (SCC) specimen type (1) double cantilever beam (DCB)
(2) wedge open loaded (WOL)—see
5.1.7.27
(3) bent beam—2 loaded
(4) bent beam—3 loaded
(5) bent beam—4 loaded
(6) standard tension specimen (Test
Methods E 8)
(7) subsize tension specimen (Test
Methods E 8)
(8) C ring
(9) stressed ring
(10) U-bend
(11) other

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TABLE X2-1 Continued

Guide G 107 Refer-
Field Field Name/Description Category Sets/Fields Type/UnitsA
ence Number
60 5.1.7.27 Material used for wedge in WOL specimen alphanumeric
61 5.1.7.28 Was stressing device insulated from specimen? alphanumeric
62 5.1.7.29 Stress-corrosion cracking specimen test area (1) smooth
(2) notched
(3) precracked
63 5.1.7.30 Direct tension stress-corrosion cracking specimen-applied (1) constant load
stress (Practice G 49)
(2) slowly increasing strain rate
(3) constant deflection
64 5.1.7.31 Stress-corrosion cracking specimen—stress level (absolute) MPa, ksi
Specimen Identification
65 5.1.7.32 Stress-corrosion cracking specimen—stress level (percent of %
yield strength at test temperature)
66 .... If U-bend used, note stressing method (1) single stage as in Practice G 30,
Fig. 4a, b, or c
(2) Two stage as in Practice G 30, Fig.
5
67 .... Diameter of mandrel (if used for stressing U-bend) mm
68 .... Outside of diameter of U-bend mm
Specimen Performance
69 5.1.8.6 Reduction in elongation %
70 5.1.8.7 Reduction in fracture ductility (strain) %
71 5.1.8.8 Reduction in tensile strength %
72 5.1.8.9 Reduction in yield strength %
73 5.1.8.10 Nature of corrosion products alphanumeric
74 5.1.8.11 Visible corrosion? (1) corroded
(2) no visible corrosion
75 5.1.8.17 Weld related corrosion (1) fusion line
(2) base metal
(3) weld metal
(4) heat-affected zone
76 5.1.8.19 Stress-corrosion cracking (SCC) test—severity of attack (1) no cracking
(2) microcracks
(3) total fracture (complete separation)
77 5.1.8.20 SCC cracking mode (1) transgranular
(2) intergranular
(3) mixed mode
(4) ductile
78 5.1.8.31 Time to initial crack detection hours
79 5.1.8.32 Measured crack length at time of first detection mm, in.
80 5.1.8.33 Method used to detect initial cracking alphanumeric (naked eye, 53 to 403,
metallographic section
[mag.] or additional bending)
81 5.1.8.37 Threshold stress intensity range, K MPa =m , ksi =in.
82 ... Maximum time without stress-corrosion cracking hours
83 ... Stress-corrosion threshold stress intensity MPa =m , ksi =in.
84 ... Location of cracking alphanumeric
Documentation
85 5.1.9.1 Test number alphanumeric
86 5.1.9.2 Published reference alphanumeric
87 5.1.9.3 Unpublished data—location alphanumeric
88 5.1.9.4 Technical committee report/file alphanumeric
89 5.1.9.5 Other documentation alphanumeric
Supplementary Notes
90 5.2.0.1 Supplementary notes alphanumericABCDE
A
Data should be reported in the units in which the original measurements were made. Subsequent conversions are at the discretion of data base developers. Units listed
are nonmandatory examples.
B
For example, general corrosion, stress corrosion, pitting, crevice corrosion, hot or cold wall effects, fretting, stray current, weld corrosion, corrosion-fatigue, galvanic
corrosion, and microbiological corrosion.
C
Many environments contain multiple components. Reference numbers 5.1.4.1 through 5.1.4.7 should be repeated for each component and no restrictions should be
placed on the number of components to be described for any given environment.
D
Reference numbers 5.1.6.1 through 5.1.6.6 are basic fields for use in material identification in database. Refer to Committee E49 guidelines for material identification
in computerized material property databases.
E
For example, preheat, welding process, number of passes, heat input, joint shape, cover gas, etc.

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