BE Chemical 2010 PDF
BE Chemical 2010 PDF
BE Chemical 2010 PDF
Accredited By NAAC
Revised Syllabus of
Semester –VII
9 Project Work -- -- 4 4 -- 50 -- -- 50
[Note: - Examination scheme and term work marks strictly as per above structure]
2
Semester –VIII
[Note: - Examination scheme and term work marks strictly as per above structure]
3
SHIVAJI UNIVERSITY, KOLHAPUR
B E –(Chemical)
(To be introduced from June, 2010 )
1. CHEMICAL REACTION ENGINEERING-II
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral
Practical : 2 hrs/batch Internal : 25
External : 25
Deactivating catalysts(4)
4
Types of Deactivation , Mechanism of deactivation, Rate equation for deactivation,
Regeneration of catalyst
Scale-Up in Reactor Design: (6)
Factors affecting choice of reactor. Reactor stability Development and Scale-Up of
Reactors Similarity Criteria , Scale-Up in Relation to Various Factors Heat Effect ,
Coefficients of Process Stability Dimensional Analysis and Scale-Up Equations
Mathematical Modeling Scale-Up of a Batch Reactor
Heat Transfer Model Jacket Zoning of a Batch Reactor The Outlet Temperature of a
Scaled-Up Batch System Aspect Ratio (R) in Jacket Zoning and Scale-Up of a Batch
Reactor
Practical :
1. Studies on homogeneous batch reactor.
2. RTD Studies on tubular flow reactor.
3. RTD Studies on mixed flow reactor.
4. RTD Studies on mixed flow reactor in series.
5. Residence time distribution studies in structures and coils.
6. RTD Studies on packed bed reactor.
7. Determination Surface area of catalysts
8. Determination Pore volume of catalysts
9. Determination of bulk density, apparent density, and true density of catalyst.
10. Studies on general liquid reactions
Text Books
1. Octave Levenspiel, “Chemical Reaction Engineering”, 3 rd Edition, John Wiley,
London.
2. S.H. Fogler,” Elements of Chemical Reaction Engineering”, PHI, 4 th Edition.
3. J.M. Smith, “Chemical Engineering Kinetics”, 3rd Edition, McGraw Hill, New
York 1981.
References:
1 T.T. Carbery, “Chemical and Catalytic reaction Engineering”, McGrawHill, New
York - 2001.
5
2. CHEMICAL PROCESSES AND SYNTHESIS
Examination
Lectures: - 3 hrs per week Theory : 100
4. Fuels and Fuel gases: Natural gas, Water gas, Producer gas, LPG.
5. Chloro – alkali and electrolytic industries: Soda ash, caustic soda, Chlorine,
Bleaching powder, Sodium bicarbonate, Aluminum, Sodium, Chlorates and perchlorates.
11. Fermentation Industry : Absolute Alcohol, Beer , wines & liquors , vinegar ,
citric acid and lactic acid .
Text Book:
References:
1. S.D. Shukla, G.N. Pandey, “A Text book of Chemical Technology”, 3rd Edition
2. C.E. Dryden, “Outlines of Chemical Technology”, Affiliated East-West Press,
1973.
3. D. Venkteshwaralu, “Chemical Technology”, I & III manuals of Chemical
Technology Chemical Engg. Ed. Dev. III Madras, 1977.
4. Faith, “Industrial Chemicals”. Rogers, “Industrial Chemistry”.
6
(New Revised)
Examination
Lectures : - 4 hrs per week Theory : 100
(4 hrs. Question Paper)
Practical /Oral
Practical : 2 hrs/batch Internal : 25
External : 25
________________________________________________________________________
2. Flow sheet preparation and drawing: Sketching techniques, Equipment lettering and
numbering, Equipment symbols, Instruments symbols, Stream designations for process
and utility,
4. Piping Design: Pipe codes, Layout, Pipe Support design, Thermowell design -- Types,
Material of construction, Installing methods and pipe thread sizes, Piping installation,
Pump size selection.
14. Design of Binary Distillation Column with packed and sieve trays.
7
Note: The necessary data / tables / charts / graphs are to be supplied during the theory
examination by the respective institutes.
Books/References:
1. Equipment symbols
2. Instrument symbols and stream designations
3. P and I diagrams
Any one type of the following
4. Exchanger
5. Condenser
6. Evaporator
7. Agitated Reactor
8. Distillation Column
9. Rotary Dryer.
10. Gas - Solid Cyclone Separator
Note: Maximum 10 sheets needed to be drawn, out of which 4 should be drawn with the
help of software AutoCAD.
8
4. MODELING AND SIMULATION IN CHEMICAL ENGINEERING
Examination
Lectures: - 4 hrs per week Theory: 100
Practical /Oral
Practical: - 2 hrs per week/batch Internal: 25
External: 25
L=Lecture
Section I
Section II
5. Dynamic modeling: Plug flow reactor, Plug flow reactor contactors, Liquid –
liquid extraction column dynamics.(6L)
9
List of Practicals:
Books:
5. ELECTIVE – I
10
1.PETROLEUM REFINERY ENGINEERING
Lectures: - 3 hrs per week Examination
Theory: 100
Practical /Oral
Practical: -- Internal : --
External: --
Section I
1. Introduction to petroleum refineries: (3 Hrs.)
Resources of petroleum, petroleum industries in India and world.
Section II
11
Books:
12
5. ELECTIVE – I
2. BIO-TECHNOLOGY
Examination
Lectures : - 3 hrs per week Theory : 100
Practical /Oral
Internal : -
External : -
________________________________________________________________________
1. Introduction.
The pre – Pasteur era, Pasteur era, The antibiotic era, New Biotechnology era, Impact of
New Biotechnology on production of food, Chemicals and energy, Biotechnology as
interdisciplinary science, Role of Chemical Engineering in Biotechnology. (3)
2. Fundamentals of Biotechnology.
Cell structure and function, Prokaryotes and Eukaryotes, arch bacteria, Extremophiles,
Structure and function of microbial (Bacteria, yeast, fungi, algae, virus), Plant and animal
cells and cell division mitosis, meiosis. (4)
6. Fermentation.
Microbial staining, Growth of virus/phages, Microbial growth kinetics, Fundamental of
fermentation, submerged fermentation, solid state fermentation (Ethanol, antibiotics,
enzyme dairy products), Fermentation kinetics. (3)
13
7. Media Preparation and Sterilization.
Synthetic and natural media, Media preparations, Industrial medium, Nitrogen source,
Product formation, sterilization and methods of sterilization (3)
References:
14
5. ELECTIVE – I
Books:
15
5. ELECTIVE – I
4. PHARMACEUTICAL TECHNOLOGY – I
Examination
Lectures : - 3 hrs per week Theory : 100
Discussion of monographs such as limit test, LOD, ash value, saponifiction value,
ester acid value, determination of volatile oils etc., Inorganic chemicals of
Pharmaceutical importance with respect to their manufactures and uses, assay methods,
Chemotherapeutic agents, Antiinfectives other than antibiotics, Antifungal,
antimycobacterials- Antiprotozoal
16
Books:
17
5. ELECTIVE – I
Section II
References:
18
6. SEMINAR
Examination
Lectures: - Theory: -
Practical /Oral
Practical: 2 hrs/ batch Internal: 25
External: -
Students will be required to prepare one review report (seminar) on selected topics in
Chemical Engineering and should deliver one seminar (30 minute) and submit in the
form of a standard typed format to the staff member/guide
Student should submit title of seminar with min 10 reference in the first week of the
semester
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7. COMPREHENSIVE TEST
Examination
Lectures: - - Theory: -
Practical /Oral
Practical: 2 hrs./ Week Internal: 50
External: -
The objectives of the comprehensive test are to assess the overall level of proficiency and
the scholastic attainment of the student in the various subject’s studies during the degree
course by conducting weekly tests. The Staff member/members shall guide the student in
preparing for the weekly tests, which consists mainly bit questions and small problems.
The term work assessment shall be based on the performance of the student in the test.
Minimum 10 tests should be conducted. Syllabus of various subjects for the test is:
1. Mathematics: -
Linear Algebra, Calculus, Differential equations, Complex variables, Probability and
Statistics, Numerical Methods
2. Mechanical Operation: -
Size reduction and size separation; free and hindered settling; centrifuge and cyclones;
thickening and classification, filtration, mixing and agitation; conveying of solids.
3. Fluid Mechanics: -
Fluid statics, Newtonian and non-Newtonian fluids, Bernoulli equation, Macroscopic
friction factors, energy balance, dimensional analysis, shell balances, flow through
pipeline systems, flow meters, pumps and compressors, packed and fluidized beds,
elementary boundary layer theory
4. Heat Transfer: -
Conduction, convection and radiation, heat transfer coefficients, steady and unsteady heat
conduction, boiling, condensation and evaporation; types of heat exchangers and
evaporators and their design.
5. Process Calculations: -
Laws of conservation of mass and energy; use of tie components; recycle, bypass and
purge calculations; degree of freedom analysis.
6. Mass Transfer: -
Fick’s laws, molecular diffusion in fluids, mass transfer coefficients, film, penetration
and surface renewal theories; momentum, heat and mass transfer analogies; stage wise
and continuous contacting and stage efficiencies; HTU & NTU concepts design and
operation of equipment for distillation, absorption, leaching, liquid-liquid extraction,
drying, humidification, dehumidification and adsorption.
20
7. Chemical Reaction Engineering: -
Theories of reaction rates; kinetics of homogeneous reactions, interpretation of kinetic
data, single and multiple reactions in ideal reactors, non-ideal reactors; residence time
distribution, single parameter model; non-isothermal reactors; kinetics of heterogeneous
catalytic reactions; diffusion effects in catalysis.
8. Instrumentation & Process Control: -
Measurement of process variables; sensors, transducers and their dynamics, transfer
functions and dynamic responses of simple systems, process reaction curve, controller
modes (P, PI, and PID); control valves; analysis of closed loop systems including
stability, frequency response and controller tuning, cascade, feed forward control.
9. Chemical Technology: -
Inorganic chemical industries; sulfuric acid, NaOH, fertilizers (Ammonia, Urea, SSP and
TSP); natural products industries (Pulp and Paper, Sugar, Oil, and Fats); petroleum
refining and petrochemicals; polymerization industries; polyethylene, polypropylene,
PVC and polyester synthetic fibers.
10. Plant Design & Economics: -
Process design and sizing of chemical engineering equipment such as compressors, heat
exchangers, multistage contactors; principles of process economics and cost estimation
including total annualized cost, cost indexes, rate of return, payback period, discounted
cash flow, optimization in design.
Question Pattern for the test (50 Marks, Time Duration: 2 hr): -
1. 15 objective questions of 1 mark each
2. 15 problems of 2 marks each
3. 5 objective (aptitude) questions of 1 mark each
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References: -
22
8.INDUSTRIAL TRAINING
Examination
Lectures: -- Theory: -
Practical /Oral
Practical: -- Internal: 25
External: -
In-Plant Training Evaluation:
The students are required to undergo at least four weeks of In-plant training during
summer vacation between T.E. Part -II and B.E. Part –I. They will be required to submit
a written report on their In-plant training.
The report should consist of
In case, due to illness or any other reasonable problems the student fails to undergo above
said training, he may be allowed to visit/ tour some industries and submit a report.
23
9. Project Work
Examination
Lectures: -- Theory: -
Practical /Oral
Practical: 4hrs./Week Internal: 50
External: --
Objectives:
To work in a team in a planned manner on a chosen engineering topic based on the
knowledge gained throughout the engineering programme.
Contents:
Three to four students will be allotted project in a group. The project is to be completed
in two parts: Project I in Semester VII and Project II in Semester VIII. Each project will
have one guide from the faculty. Students may be encouraged to choose a co guide from
the industry, wherever possible.
A proper planning of the project work or research institute is expected. The project group
should prepare activity chart and submit the same along with the reports for part I and
part II. The group should also submit and present the work completed in semester I in an
appropriate format. The actual contents of the project report may be decided in
consultation with the project guide.
Students are expected to carry out an in-depth literature survey based on
chemical/engineering abstracts, national/international journals using online/print media.
24
Proposed work synopsis / abstract approved by guide should be submitted within two
month of the course started and approved by the guide.
Students will be required to prepare a critical review of selected projects in Chemical
Engineering and allied subjects and submit in the form of a standard typed report.
Typically, the report should contain and will be evaluated based on the following points:
(i) Introduction: 2 pages maximum,
(ii) Exhaustive review of literature, Critical analysis of the literature and comments on the
analysis (including figures): 12 to 15 pages: 50% weightage
(iii) Kinetics & thermodynamics study, material balance, energy balance,
experimentation / detailed design of equipments - 12 to15 pages: 50% weightage.
The critical analysis of literature should include the following points: Is the project
technically correct? Are assumptions reasonable; is the reasoning logical? If you think it
is not, specify what you think is incorrect and suggest the correct approach. Are the
methods used in the literature appropriate? Are there any internal contradictions or
computational errors and are there any loopholes in the observations? If so, please
explain it. Critical analysis of papers should also contain quantitative comparison of
observations, results and conclusion amongst the various papers. Each student will also
be required to make an oral presentation of the review. Weightage would be 40% for
presentation and 60% for the report. Additional details are given in table 1.
Half part of project work should be complete within the first semester. Term work consist
a reports of 30 to 40 pages which has to be submitted at the end of VII semester along
with the presentation before faculty and students.
The report should be prepared using the Times Roman font (size 12) using 1.5 spacing
leaving 1 inch margin on all sides producing approximately 29 lines per page. The report
is to be typed on one side of the paper and need not be bound in a hard cover binding.
Figures and tables should be shown as a part of the running text. Each figure should be
drawn inside a rectangular box of 12 cm width and 10 cm height. The figures must be
sufficiently clear and hand drawn figures will be acceptable. Particular care must be taken
if a figure is photocopied from source.
25
Each figure must have a sequence number and caption below. Each table must have a
sequence number and title at the top. The report must be precise. All important topic
should be given due considerations.
The total number of pages, including tables, figures and references should not exceed 40.
Chapters or subsections need be started on new pages, while getting the report typed.
General Project
1 Synopsis / Abstract
4 Block Diagram
feasibility
methodology of Experimentation
26
SHIVAJI UNIVERSITY, KOLHAPUR
(INTRODUCED FROM JUNE, 2010)
Revised syllabus structure of Chemical Engineering
B.E. Chemical Part – II
1. CHEMICAL PROCESSES AND GREEN TECHNOLOGY
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral
Practical : 2 hrs /batch Internal : 25
External : 25
Section – I
Section - II
Text Book:
1. George T. Austin, “Shreve's Chemical Process Industries”,5th edn., McGraw Hill
Book Company, 1985.
2. Paul T. Anastaj; “Green Chemistry – Theory and Practice”
3. Albert S. Matlack ; “Introduction to Green Chemistry”
References:
1. S.D. Shukla, G.N. Pandey. “A Text book of Chemical Technology”, 3rd
Edition.
2. C.E. Dryden, “Outlines of Chemical Technology”, Affiliated East-West Press,
1973.
3. D. Venkteshwaralu, “Chemical Technology”, I & III manuals of Chemical
Technology Chemical Engg. Ed. Dev. III Madras, 1977.
4. Faith, “Industrial Chemicals”
5. Rogers, “Industrial Chemistry”.
6.Anastas, P.; Warner, J. Green Chemistry: Theory and Practice; Oxford University
Press: London, 1998.
7.Zimmerman, J.B.; Anastas, P.T. “The 12 Principles of Green Engineering as a
Foundation for Sustainability” in Sustainability Science and Engineering: Principles. Ed.
Martin Abraham, Elsevier Science. available 2005.
8.Anastas, P.; Zimmerman, J. “Design through the Twelve Principles of Green
Engineering,” Environmental Science and Technology, 37, 94A – 101A, 2003.
28
2. TRANSPORT PHENOMENA
Lectures: 3 hrs per week Examination:
Tutorial : 1 Theory: 100
Practical /Oral:
Internal: 25
Section I
1. Viscosity and the mechanism of momentum transport: (2 Hrs.)
Newton’s law of viscosity, non Newtonian fluids, pressure & temperature dependence of
viscosity, estimation of viscosity from critical properties.
29
Section II
8. Temperature distributions in solids and in laminar flow: (4 Hrs.)
Shell energy balance, boundary conditions, Heat conduction with an electrical heat
source, Heat conduction in cooling fins, heat conduction with exothermic reactions.
30
Term Work:-
Minimum of eight assignments should be given to students. 50 % of assignments should
be numerical problems.
Text Book:
1. R.B. Bird, W.E. Stewart and E.N. Lightfoot, “Transport Phenomena”, John
Wiley & Sons, Inc, New York.
References:
1. C.O. Bennett, J.E. Mayers, “Momentum, Heat & Mass transfer”, 3rd Edn.,McGraw
Hill, Chemical Engineering Series,1985.
2. Alan S. Foust, Leonard A. Wenzel, Curtisw Clump, Louis Maus,L Bryce Andersen
“Principles of Unit Operations”,2nd edn.,McGraw Hill, 1985.
3. C.J. Geankoplis " Transport Processes Momentum And Mass" Bacon Inc. 1983.
4. L.E. Sissom & D.R. Ritts ,"Elements of Transport Phenomena" McGraw Hill, J.R.
Welty, R.E. Wilson & C.E. Wicks, " Fundamentals of momentum, heat & mass transfer"
2nd edn. John Wiley, New York 1973.
5. Anderson Jr J. D., “Computational Fluid Dynamics: The Basics with Applications”,
McGraw Hill.1995
6. Muralidhar K. and Sundararajan T., “Computational Fluid Flow and Heat Transfer”,
Narosa Publishing House. 2003
7. Ranade V. V, “Computation Flow Modeling for Chemical Reactor Engineering”,
Academic Press. 2002
31
3. PROCESS ECONOMICS AND PROJECT ENGINEERING (PEPE)
(New Revised)
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral
Practical : - Internal : 25
External : -
________________________________________________________________________
Section – I
1. Introduction.
2. General design considerations.
3. Process Design Development
4. Flow sheet Synthesis and Development
5. Cost and asset accounting.
6. Analysis of Cost estimation.
7. Interest, Time value of Money, Taxes and Fixed Charges.
8. Profitability, alternative investments and replacements.
9. Optimum design and Design strategy.
10. Written and Oral Design Reports.
Section – II
32
16. Project Engineering : Management and Organization, Project Planning, Scheduling
and Controlling , Use of bar and milestone chart, PERT/ CPM - Introduction, Activity
sequencing, Network building, Time estimates, Critical path calculations.
Text Books:
1. M.S. Peters & K.D.Timmerhaus, “Plant Design and Economics for Chemical
Engineers”, 5th edition, McGraw Hill International Book Co.,2003.
2. Lundu, “The Chemical Plant”.
3. J.M. Coulson & J.F Richardson, “Chemical Engineering”, Vol.6, 5th edition Pergamon
& ELES, 2003.
4. Modes J. & Philips, “Project Engineering with C.P.M. & PERT”, Rein hold.
5. Srinath L.S. “PERT & C.P.M. Principles and Applications”3rd edition, East-West
Publication 2003.
6. GAEL D. ULRICH, “A Guide to Chemical Engineering Process Design and E” John
Wiley & Sons, 1984.
7. N. D. Vohra, “Quantitative Techniques in Management”, 2nd edition Tata McGraw Hill
Publishing company Ltd., New Delhi 2005.
References:
1. Rase, H.F. Barrow, M.H. “Project Engineering of Process Plants”, John Wiley.
2. Schewayer, H.E. “Process Engineering Economics”, McGraw Hill
3. Chilton, C.H., “Cost Engineering in Process Industries”, McGraw Hill
4. Happel J. Jordan, D.G. “Chemical Process Economics”.
5. Tacmin A,J. Blank L.T. “Engineering Economy”
6. V.W. Wni. & A.W. Hankins, “Technical Economics for Chemical Engineers”
(AICHE)1971.
33
4.ELECTIVE – II
1. BIO-CHEMICAL ENGINEERING
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical :-
Internal : --
External : --
1. Introduction.
Biochemical Engineering – the interaction of two disciplines, Comparison of
chemical and biochemical process, Role of biochemical engineers in development of
modern formation industry, Future development, Applications of engineering
advances.
35
4. ELECTIVE – II
2. PETROCHEMICAL TECHNOLOGY
Lectures: 4 hrs per week Examination
Theory: 100
Practical/Oral Internal: -
External: -
Section I
1. General Introduction: (5 Hrs.)
Definition of petrochemicals, history of petrochemical industry, development of petrochemical
industry in India, product profile of petrochemicals, economics of petrochemical industry, general
cost considerations, indigenous technology v/s foreign know-how, economics of R&D, sources of
petrochemicals, natural gas & petroleum, classification of petrochemicals.
2. Raw Materials: (4 Hrs.)
Organic chemicals, coal, biomass petroleum, etc.
3. Chemicals from Methanol & Synthesis gas: (4 Hrs.)
Steam reforming, Oxo-Products, Methanol, Formaldehyde, Carbon-di-sulphide, Hydrogen cyanide.
4. Chemicals from Ethane, Ethylene & Acetylene: (4 Hrs.)
Synthetic Ethanol, Acetaldehyde, Acetic acid, Vinyl acetate, Ethylene oxide, Ethylene glycols,
Acrylonitrile, Ethanol amines.
5. Chemicals from Propane & Propylene: (4 Hrs.)
Isopropanol, Acetone, Glycerol, Propylene oxide, Propylene Glycols, Isoprene, Cumene.
Section II
6. Chemicals from Butanes & Pentanes: (4 Hrs.)
Butadiene, Butone epoxides & Butanol amines, Butyl acetate, Methyl-Ethyl Ketone, MTBE, TAME.
7. Chemicals from aromatics: (5Hrs.)
BHC, Nitrobenzene, Do-decyl benzene, Benzoic acid, Nitrotolune, Pthalic anhydride, Isopthalic
acid, TPA & DMT, Maleic anhydride, Adipic acid, Hexamethylene diamine, Aniline, Caprolactum.
8. Polymers: (4 Hrs.)
Polymers, elastomers, synthetic fibers, PVC, Nylon & Polyesters.
36
NOTE: The journals such as Hydrocarbon Processing, Chemical engg. Progress must be used for the
latest technologies.
Text Books:
1. B.K. Bhasker Rao, “A Text on Petrochemicals”2nd Edition, Khanna publishers, 1996.
2. Sukumar Maiti, “Introduction to Petrochemicals” Oxford & IBH publishing Co. Pvt. Ltd., 1991.
3. Ram Prasad, “Petroleum Refinery Technology”, Khanna publications.
References:
1. A.V.G. Halm, “The Petrochemical Industry”, McGraw Hill 1970.
2. A.L. Waddams, “Chemicals from Petroleum”, Chemical publishing Co.
3. Astle M.J., “The Chemistry of Petrochemicals”, Reinhold.
4. C.E. Dryden, “Outlines of Chemical Technology”, Affiliated East-West Press, 1973.
5. Faith Keys, “Industrial Chemicals”.
37
4. ELECTIVE – II
3. Alpha numeric and graphic I/O : Batch and Interactive processing; Data
input devices; Data Output devices; Combination at I/O devices; I/O
control devices; Graphic computer terminal, Graphic display; Graphics
terminals; Graphic Display, Graphics terminals; Plotters; Printers.
38
References:
1. M.P. Groover, E.W. Timmers, “Computer Aided Design and Manufacturing”,
Prentice Hall of India Pvt. Ltd., New Delhi, 1985.
2. L. Nashelsky, “Introduction to Digital Technology”, John Wiley and Sons,
New York, 1983.
3. E.J. Henley, and F.M. Rusen, “Material and Energy Balance Computations”,
John Wiley, New York, 1969.
4. E.D. Oliver, “Diffusional Separation Process”, John Wiley and Sons, New
York, 1966.
5. B.D. Smith, “Design of Equilibrium Stage Processes”, McGraw Hill Book Co.
New York, 1963.
6. Crowe, C.M. et. al., “Chemical plant simulation-An Introduction to
Computer aided steady-state process analysis”, Prentice Hall, 1971.
7. Franks, R.G.E., “Modelling and simulation in Chemical Engineering”, Wiley
Inter Science, 1972.
8. Holland C.D. “Fundamentals and modelling of separation processes”,
absorption, Distillatkion, evaporation and extractikon, Prentice Hall, 1975.
9. Afgan, N.H. and Schlunder, C.V., “Heat Exchangers-design and theory
source book” Scripta Book, Washington, 1974.
10. Chussain, A. “Chemical Process simulation”, Wiley eastern, 1986.
11. Wester Berg, A.W. et.al. "Process Flow Sheeting", Cambridge UniversityPress,
1979.
12. Myers, A.L. and Seeden, W.D. “Introduction to Chemical Engineering and
Computer Calculations” Prentice Hall, 1976.
13. Prausnitz, S., “Computer calculaltions in Multi Component vapour
liquidequilibria” Prentice Hall, 1980.
14. Welison, C. and Hobson P.M., “Combination for Process Engineers”,
Leonard Hill, 1973.
39
4. Elective – II
4. DISTILLATION
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : - -
Internal : -
External : -
Books:
40
4. Elective – II
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : -
Internal : -
External : -
41
4. Elective – II
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : - -
Internal : -
External : -
Books:
42
4. Elective – II
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : - -
Internal : -
External : -
43
8. Polarization phenomena and fouling concentration polarization,
Characteristic flux behavior in pressure driven membrane operation,
Various models, Temperature polarization, Membrane fouling, Methods to
reduce fouling.
9. Modules and process design plate and frame, Spiral wound, Tubular,
Capillary, Hollow fiber modules and their comparison, System design.
10. Membrane reactors, Applications of membrane reactors in biotechnology
11. Economics and feasibility of membrane technology, Comparison of
membrane technology with separation techniques, Scope in future,
Current and existing industrial applications.
Books:
44
4. Elective – II
8. NUCLEAR ENGINEERING
Examination
Lectures : - 3 hrs per week Theory : 100
Practical /Oral Practical : - -
Internal : -
External : -
Section I
1. Nuclear Physics: Atomic number and mass numbers, Isotopes, Nuclear energy
and nuclear forces, Binding Energy, Nuclear Stability, Radioactivity, Nuclear
reactions, Radioactive isotopes, Law of radioactivity, Interaction of radiation (alpha,
beta, gamma) with matter, Interaction of neutrons with matter, Absorption radiative
capture, Transmutation Fission, Cross section for nuclear reactions.
Fission process, Mechanism of nuclear fission, fission cross section, fission
products, Basic radio chemistry.
2. Reactor Physics: Neutron balance, Neutron diffusion, Diffusion equation, and its
solution, Showing down of neutrons, Showing down power and moderating ratio.
Reactor theory: Multiplication factors, Four factor formula, One group critical
equation, Age, Diffusion method, Non-leakage probabilities and effective
multiplication factor, Multigroup diffusion theory, Homogeneous and heterogeneous
reactor systems, Time dependent reactor behavior.
Section II
46
4. Elective – III
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : -
Internal : -
External : -
1. Energy conservation: An Introduction: Industrial energy use and economy,
Need for planning energy, importance of energy in production and employment,
Importance of energy cost in production, Energy and employment, The mystery
of conservation, (3 L)
3. Energy available for industrial use and the role of conservation: Methodology for
forecasting, Industrial energy supply and demand, Review of alternative approaches and
major models and studies, Method for forecasting industrial energy price and availability,
New energy technologies and conservations.(3 L)
47
9 Energy conservation in utilities: Thermal and electrical utilities and case studies of
stoichiometric amount of air required for the burning of fuel. Theoretical air required for
Propane, equivalent evaporation evaluation, Boiler efficiency evaluation by direct and
indirect method. Theoretical air requirement evaluation on CO2 basis, Calculation of
blow down percentage, Installation of economizer for boiler, Steam Balancing,
Optimization of steam piping size to reduce pressure drop, Utilization of blow down
water to generate flash steam, Steam use for power generation in an extraction cum
condensing turbine, Excess air optimization, Waste heat recovery, Conversion of
electrical furnace in to oil fired furnace, Insulation upgrade project, Annual fuel saving
by proper insulation, Cost saving achieved by insulating uninsulated steam line,
Calculation illustrating the most suitable insulation thickness, Improvement in specific
energy generation,(6L)
Reference books:
48
5. ELECTIVE – III
49
Text Books:
50
5. ELECTIVE – III
3. PHARMACEUTICAL TECHNOLOGY-II
Examination
Lectures : - 4 hrs per week Theory : 100
Practical /Oral Practical : -
Internal : -
External : -
Medicinal chemistry, Pattern of disease and drug action, Mode of action Clinical
application Chemistry of hormones, Analgesics, and antipyretics
Synthesis of drug molecules with selected types of reaction and writing the
synthetics giving approximate condition and emphasis on Techno- commercially
potential routes. Synthesis of some complex drug molecules (selected from vitamins and
alkaloids), Synthesis of peptide drugs, Bio-organic chemistry of vitamins.
Raw materials and Manufacturing processes for steroid drugs, Manufacturing
processes for some excepients, eg. cellulose, and its derivatives, Lactose, Chirality and
chiral technology. One topic of current interest, Effluent treatment
Raw materials for Pharmaceutical Industry,.
Enzymes as catalyst (a) in Synthesis for Pharmaceuticals (b) Introduction to
Principle of enzymes catalyst, Lipases and esterase’s for hydrolytic conversion. Lipases
and esterase’s in organic solvents, other hydrolytic reactions, Enzyme-catalyzed
oxidation reactions, Enzyme-catalyzed C-X bond synthesis, Enzyme-catalyzed reduction,
Chiral Technology Preformulation, Formulation, Evolution, Large scale manufacture and
packingwith focus on equipment with reference to Oral sustained and controlled release
dosageforms and Aerosols.
Introduction to Novel drug Delivery Systems: Transdermal, Transmucosal,
Ophthalmic, Colloidal: Liposome’s, nanoparticles, emulsion systems etc
Introduction to Radio pharmaceuticals, Overview of cosmetic products
Novel Drug Delivery Systems, Oral sustained and controlled release dosage
forms, Aerosols, Blood products, Glandular products, Radiopharmaceuticals, Surgical
sutures, ligatures, dressings. Physiology of Central Nervous System and Drugs acting on
Central Nervous System.
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Books:
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5. ELECTIVE – III
4. Models for analysis gas – liquid and gas – liquid – solid reactions, Film and
penetration theories, Transport resistances and heat effects.
6. Models for gas – liquid – solid reactors (Only model formulations with
assumption and final design equations wherever available. Numerical
solutions of model equation excluded).
Books:
Section – I
Section – II
References:
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6. ADVANCED SEPARATION PROCESSES
Examination
Lectures : - 1 hrs per week Theory : --
Practical /Oral : 2 hrs. Practical :
Internal : 25
External : 25
Introduction to advanced separation techniques such as :
1) Reverse Osmosis
2) Ultra filtration
3) Micro filtration
4) Pressure swing Adsorption
5) Electrostatic Precipitator
6) Supported Liquid Membranes
7) Supercritical Fluid Extraction etc.
Study of basic principles & different working modules used in above
separation techniques.
List of practicals:
Books:
1. C.J.King "Separation Processes" 2nd Ed., Tata McGraw Hill Publishing Co. Ltd.,
New Delhi, 1986.
2. Sirkar K. & Winston H.O. "Membrane Hand Book" Van Nostrand Reinhold,
New York, 1992.
3. McCabe & Smith "Unit Operations of Chemical Engineering" 5th
Ed.,McGraw Hill International .
4. Richardson and Coulson,“Chemical Engineering Volume –II”,Pergamon
Press,1970.
5. Schweitzer P.A , “Handbook of Separation Techniques for Chemical
Engineering” 2nd edn.,McGraw Hill Book Co.,1986.
6. Souri Rajan S. "Reverse Osmosis" Logos Press Ltd.
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7. PROJECT WORK
Examination:
Lectures: -- Theory: --
Practical /Oral
Practical: 6 hrs/week Internal : 50
External: 100
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15) Control & Safety of Process.
16) Plant layout & Location.
17) Cost Estimation & Economic Analysis
18) Pollution Control, Safety, Marketing
19) Conclusion & Remarks.
20) References.
Books.
Journals.
21) Appendix.
List of Tables.
Sample Calculation.
Data Tables, etc.
The object of the project is to make use of the knowledge gained by the
student at various stages of the degree course. This helps to judge the level
of proficiency, originality and capacity for application of the knowledge
attained by the student at the end of the course.
Each group should consist of maximum 3 students. For term-work (Internal)
75 marks, the assessment should be by conducting frequent written tests,
seminars during the year & an oral exam. at the end of the year conducted
by all the staff members of the dept. The Head of the Dept. should see that
the assessment procedure should be the same for all the students of the class.
For external 75 marks, the project work shall be assessed by an oral exam.
to be held by at last two examiners, one internal and one external preferably from
industry at
the end of the year.
The object of the VIVA VOCE examination (Internal and External Orals) is to
determine whether the objectives of the project work have been met by the
student as well as to assess the originality and initiative of the student as
demonstrated in the project work.
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EQUIVALENCE FOR B.E.( Chemical Engg.)
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