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Loctite EA 9464: Product Description

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Technical Data Sheet

LOCTITE® EA 9464
Known as Hysol 9464
April-2016

PRODUCT DESCRIPTION Viscosity, DIN 54453, mPa·s (cP):


LOCTITE® EA 9464 provides the following product Shear rate 10 s-1 55,000
characteristics: Shear rate 100 s-1 35,000
Technology Epoxy
Thixotropic Index 1.6
Chemical Type Epoxy
Flash Point - See SDS
Appearance (Resin) White opaque paste
Appearance (Hardener) Black opaque paste
Mixed Properties
Appearance (Mixture) Gray opaque paste
Pot Life @ 22 °C, minutes:
Viscosity Thixotropic 100 g mass 15 to 20
Components Two part - Resin & Hardener
Mix Ratio, by volume - 1 : 1
Resin : Hardener
Mix Ratio, by weight - 100 : 100
Resin : Hardener TYPICAL CURING PERFORMANCE
Cure Room temperature cure after mixing Fixture Time
Fixture time is defined as the time to develop a shear strength of 0.1
Application Bonding N/mm².
Specific Benefit ● Shortened pot life Fixture Time, mixed, @ 22 °C, minutes 180
● Fast handling strength
● Non-sag slump resistance Cure Speed vs. Time/Temperature
● Easy to mix and use LOCTITE® EA 9464 will achieve handling strength in 3 to 4
● Good tensile shear strength hours at room temperature (note: this can vary with different
● Good peel strength bond configurations and ambient temperatures). Elevated
● Heat accelerated cure temperatures may be used to accelerate the cure. The
Key Substrates Metals , Phenolic plastics, Polyester,
following graph indicates development of shear strength
Hard boards & forestry products,
Ceramics, Rubbers, Masonry on mild steel (grit blasted) lapshears as a function of time
materials and other construction and temperature tested according to ISO 4587.
materials
125
% of Full Strength on GBMS

LOCTITE® EA 9464 is a faster cure version of Loctite® EA 150 °C 80 °C


120 °C
9461™. The fixture time and pot life are reduced by 100
60 °C 22 °C
approximately 50% while maintaining most of the performance
of Loctite® EA 9461™. 75

TYPICAL PROPERTIES OF UNCURED MATERIAL 50


Resin Properties
Specific Gravity @ 25 °C 1.35 25
Viscosity, DIN 54453, mPa·s (cP):
Shear rate 10 s-1 138,000 0
Shear rate 100 s-1 40,000 1min 5min10min 30min 1h 3h 6h 24h 72h 168h
Thixotropic Index 3.5 Cure Time

Flash Point - See SDS


TYPICAL PROPERTIES OF CURED MATERIAL
Hardener Properties
Cured for 7 days @ 22 °C, 1.2 mm thick samples.
Specific Gravity @ 25 °C 1.3 Physical Properties :
TDS LOCTITE® EA 9464, April-2016

Coefficient of Thermal Conductivity, ISO 8302, 0.6 Hot Strength


W/(m-K) Tested at temperature
Shore Hardness, ISO 868, Durometer D 80 35

Shear Strength - N/mm²


Glass Transition Temperature, ASTM D 1640, °C 50
Compressive Strength, ISO 604 N/mm² 50 30
(psi) (7,300)
25
Tensile Modulus , ISO 527-2 N/mm² 700
(psi) (101,000) 20

15
Electrical Properties:
Dielectric Constant / Dissipation Factor, IEC 60250: 10
1-kHz 4.4 / 3.1×10-3 5
1-MHz 3.8 / 4.7×10-2
10-MHz 3.5 / 6.2×10-2 0
-50 -35 -15 5 25 45 65 85 105 125 140
Surface Resistivity, IEC 60093, Ω 1.7×1015 Temperature, °C
Volume Resistivity, IEC 60093, Ω·cm 5.8×1014

Heat Aging
Aged under conditions indicated and tested at 22 °C.
TYPICAL PERFORMANCE OF CURED MATERIAL
Temperature % Initial strength retained after
Adhesive Properties
500 h 1,000 h 3,000 h
Cured for 7 days @ 22 °C
50 °C 150 115 140
Lap Shear Strength , ISO 4587:
80 °C 130 125 145
Mild steel (grit blasted) N/mm² 22
100 °C 125 130 135
(psi) (3,200)
120 °C 130 135 135
Aluminum (abraded) N/mm² 18
(Silicon Carbide Paper, A166 grit, P400A grade) (psi) (2,600) 150 °C 150 140 140
Aluminum (etched in acidic ferric sulphate) N/mm² 22
(psi) (3,200)
Chemical/Solvent Resistance
Stainless steel N/mm² 18
Immersed in conditions indicated and tested at 22 °C.
(psi) (2,600)
Brass N/mm² 9 % of initial strength
(psi) (1,300) Environment °C 500 h 1000 h 3000 h
Zinc dichromate N/mm² 15 Motor oil 22 100 100 100
(psi) (2,200)
Unleaded gasoline 22 95 75 60
Galvanized Steel (Hot Dipped) N/mm² 20
(psi) (2,900) Water/glycol 50/50 87 60 60 50
Polycarbonate N/mm² 4 Sodium hydroxide, 4% 22 50 55 50
(psi) (550) 98% RH 40 65 50 45
ABS N/mm² 5
(psi) (700) Water 21 80 75 70
GRP (Polyester resin matrix) N/mm² 5 Acetone 22 85 35 15
(psi) (680) Acetic Acid, 10% 22 80 70 45
180° Peel Strength, ISO 8510-2: Salt water solution,
22 90 85 80
Mild steel (grit blasted) N/mm 10.5 7.5%
(lb/in) (60)
Aluminum (acid etched) N/mm 7
(lb/in) (40) GENERAL INFORMATION
This product is not recommended for use in pure oxygen
IZOD Impact Resistance , ISO 9653 J/m²: and/or oxygen rich systems and should not be selected as
Grit Blasted Mild Steel 9.5 a sealant for chlorine or other strong oxidizing materials.

TYPICAL ENVIRONMENTAL RESISTANCE For safe handling information on this product, consult the
Cured for 7 days @ 22 °C Safety Data Sheet, (SDS).
Lap Shear Strength , ISO 4587:
Where aqueous washing systems are used to clean the
Mild Steel (grit blasted)
surfaces before bonding, it is important to check for
compatibility of the washing solution with the adhesive. In
some cases these aqueous washes can affect the cure and
performance of the adhesive.

Directions for use


1. For best performance surfaces for bonding should be
clean, dry and free of grease. For high strength structural

Americas Europe Asia


+860.571.5100 +49.89.320800.1800 +86.21.2891.8863
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
TDS LOCTITE® EA 9464, April-2016

bonds, special surface treatments can increase the bond Conversions


strength and durability. (°C x 1.8) + 32 = °F
2. To use, resin and hardener must be blended. Product can kV/mm x 25.4 = V/mil
be applied directly from dual cartridges by dispensing mm / 25.4 = inches
through the mixer head supplied. Discard the first 3 to 5 N x 0.225 = lb
cm of bead dispensed. Using bulk containers, mix N/mm x 5.71 = lb/in
thoroughly by weight or volume in the proportions psi x 145 = N/mm²
specified in the Product Description Matrix. For hand MPa = N/mm²
mixing, weigh or measure out the desired amount of resin N·m x 8.851 = lb·in
and hardener and mix thoroughly. Mix approximately 15 N·m x 0.738 = lb·ft
seconds after uniform color is obtained. N·mm x 0.142 = oz·in
3. It is recommended that this product is not mixed and mPa·s = cP
cured in bulk quantities of greater than 1 kg as excessive
heat build-up can occur. Mixing smaller quantities will Disclaimer
minimize the heat build-up. Note:
4. Apply the adhesive as quickly as possible after mixing to The information provided in this Technical Data Sheet (TDS) including the
recommendations for use and application of the product are based on our
one surface to be joined. For maximum bond strength knowledge and experience of the product as at the date of this TDS. The product
apply adhesive evenly to both surfaces. Parts should be can have a variety of different applications as well as differing application and
assembled immediately after mixed adhesive has been working conditions in your environment that are beyond our control. Henkel is,
therefore, not liable for the suitability of our product for the production processes
applied. and conditions in respect of which you use them, as well as the intended
5. For working life please see section 'Typical Properties of applications and results. We strongly recommend that you carry out your own
Uncured Material'. Higher temperatures and larger prior trials to confirm such suitability of our product.
Any liability in respect of the information in the Technical Data Sheet or any other
quantities will shorten this working time. written or oral recommendation(s) regarding the concerned product is excluded,
6. Keep the assembled parts from moving during cure. The except if otherwise explicitly agreed and except in relation to death or personal
joint should be allowed to develop full strength before injury caused by our negligence and any liability under any applicable mandatory
product liability law.
subjecting to any service loads.
In case products are delivered by Henkel Belgium NV, Henkel Electronic
7. Excess uncured adhesive can be wiped away with organic Materials NV, Henkel Nederland BV, Henkel Technologies France SAS and
solvent (e.g. Acetone). Henkel France SA please additionally note the following:
In case Henkel would be nevertheless held liable, on whatever legal ground,
8. After use and before adhesive hardens, mixing and Henkel’s liability will in no event exceed the amount of the concerned delivery.
application equipment should be cleaned with hot soapy In case products are delivered by Henkel Colombiana, S.A.S. the following
water. disclaimer is applicable:
The information provided in this Technical Data Sheet (TDS) including the
recommendations for use and application of the product are based on our
Not for product specifications knowledge and experience of the product as at the date of this TDS. Henkel is,
The technical data contained herein are intended as reference therefore, not liable for the suitability of our product for the production processes
only. Please contact your local quality department for and conditions in respect of which you use them, as well as the intended
applications and results. We strongly recommend that you carry out your own
assistance and recommendations on specifications for this prior trials to confirm such suitability of our product.
product. Any liability in respect of the information in the Technical Data Sheet or any other
written or oral recommendation(s) regarding the concerned product is excluded,
except if otherwise explicitly agreed and except in relation to death or personal
injury caused by our negligence and any liability under any applicable mandatory
Storage product liability law.
Store product in the unopened container in a dry location. In case products are delivered by Henkel Corporation, Resin Technology
Storage information may be indicated on the product container Group, Inc., or Henkel Canada Corporation, the following disclaimer is
labeling. applicable:
The data contained herein are furnished for information only and are believed to
be reliable. We cannot assume responsibility for the results obtained by others
Optimal Storage: 8 °C to 21 °C. Storage below 8 °C or over whose methods we have no control. It is the user's responsibility to
greater than 28 °C can adversely affect product properties. determine suitability for the user's purpose of any production methods mentioned
herein and to adopt such precautions as may be advisable for the protection of
property and of persons against any hazards that may be involved in the handling
Material removed from containers may be contaminated during and use thereof. In light of the foregoing, Henkel Corporation specifically
use. Do not return product to the original container. Henkel disclaims all warranties expressed or implied, including warranties of
Corporation cannot assume responsibility for product which merchantability or fitness for a particular purpose, arising from sale or use
of Henkel Corporation’s products. Henkel Corporation specifically
has been contaminated or stored under conditions other than disclaims any liability for consequential or incidental damages of any kind,
those previously indicated. If additional information is required, including lost profits. The discussion herein of various processes or
please contact your local Technical Service Center or compositions is not to be interpreted as representation that they are free from
Customer Service Representative. domination of patents owned by others or as a license under any Henkel
Corporation patents that may cover such processes or compositions. We
recommend that each prospective user test his proposed application before
repetitive use, using this data as a guide. This product may be covered by one or
more United States or foreign patents or patent applications.
Trademark usage
Except as otherwise noted, all trademarks in this document are trademarks of
Henkel Corporation in the U.S. and elsewhere. ® denotes a trademark
registered in the U.S. Patent and Trademark Office.

Reference 1.3

Americas Europe Asia


+860.571.5100 +49.89.320800.1800 +86.21.2891.8863
For the most direct access to local sales and technical support visit: www.henkel.com/industrial

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