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Astm D790-10

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Designation: D790 − 10

StandardTest Methods for


Flexural Properties of Unreinforced and Reinforced Plastics
and Electrical Insulating Materials1
This standard is issued under the fixed designation D790; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.

1. Scope* priate safety and health practices and determine the applica-
1.1 These test methods cover the determination of flexural bility of regulatory limitations prior to use.
properties of unreinforced and reinforced plastics, including NOTE 1—These test methods are not technically equivalent to ISO 178.
high-modulus composites and electrical insulating materials in
the form of rectangular bars molded directly or cut from sheets, 2. Referenced Documents
plates, or molded shapes. These test methods are generally 2.1 ASTM Standards:2
applicable to both rigid and semirigid materials. However, D618 Practice for Conditioning Plastics for Testing
flexural strength cannot be determined for those materials that D638 Test Method for Tensile Properties of Plastics
do not break or that do not fail in the outer surface of the test D883 Terminology Relating to Plastics
specimen within the 5.0 % strain limit of these test methods. D4000 Classification System for Specifying Plastic Materi-
These test methods utilize a three-point loading system applied als
to a simply supported beam. A four-point loading system D4101 Specification for Polypropylene Injection and Extru-
method can be found in Test Method D6272. sion Materials
1.1.1 Procedure A, designed principally for materials that D5947 Test Methods for Physical Dimensions of Solid
break at comparatively small deflections. Plastics Specimens
1.1.2 Procedure B, designed particularly for those materials D6272 Test Method for Flexural Properties of Unreinforced
that undergo large deflections during testing. and Reinforced Plastics and Electrical Insulating Materi-
1.1.3 Procedure A shall be used for measurement of flexural als by Four-Point Bending
properties, particularly flexural modulus, unless the material E4 Practices for Force Verification of Testing Machines
specification states otherwise. Procedure B may be used for E691 Practice for Conducting an Interlaboratory Study to
measurement of flexural strength only. Tangent modulus data Determine the Precision of a Test Method
obtained by Procedure A tends to exhibit lower standard 2.2 ISO Standard:3
deviations than comparable data obtained by means of Proce- ISO 178 Plastics—Determination of Flexural Properties
dure B.
1.2 Comparative tests may be run in accordance with either 3. Terminology
procedure, provided that the procedure is found satisfactory for 3.1 Definitions—Definitions of terms applying to these test
the material being tested. methods appear in Terminology D883 and Annex A1 of Test
1.3 The values stated in SI units are to be regarded as the Method D638.
standard. The values provided in parentheses are for informa-
tion only. 4. Summary of Test Method
1.4 This standard does not purport to address all of the 4.1 A bar of rectangular cross section rests on two supports
safety concerns, if any, associated with its use. It is the and is loaded by means of a loading nose midway between the
responsibility of the user of this standard to establish appro- supports. A support span-to-depth ratio of 16:1 shall be used
unless there is reason to suspect that a larger span-to-depth

1 2
These test methods are under the jurisdiction of ASTM Committee D20 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Plastics and are the direct responsibility of Subcommittee D20.10 on Mechanical contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Properties. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved April 1, 2010. Published April 2010. Originally the ASTM website.
approved in 1970. Last previous edition approved in 2007 as D790 – 07 ϵ1. DOI: 3
Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
10.1520/D0790-10. 4th Floor, New York, NY 10036, http://www.ansi.org.

*A Summary of Changes section appears at the end of this standard


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D790 − 10
ratio may be required, as may be the case for certain laminated measuring system shall not exceed 61 % of the maximum load
materials (see Section 7 and Note 7 for guidance). expected to be measured. It shall be equipped with a deflection
4.2 The specimen is deflected until rupture occurs in the measuring device. The stiffness of the testing machine shall be
outer surface of the test specimen or until a maximum strain such that the total elastic deformation of the system does not
(see 12.7) of 5.0 % is reached, whichever occurs first. exceed 1 % of the total deflection of the test specimen during
testing, or appropriate corrections shall be made. The load
4.3 Procedure A employs a strain rate of 0.01 mm/mm/min indicating mechanism shall be essentially free from inertial lag
(0.01 in./in./min) and is the preferred procedure for this test at the crosshead rate used. The accuracy of the testing machine
method, while Procedure B employs a strain rate of 0.10 shall be verified in accordance with Practices E4.
mm/mm/min (0.10 in./in./min).
6.2 Loading Noses and Supports—The loading nose and
5. Significance and Use supports shall have cylindrical surfaces. The default radii of the
5.1 Flexural properties as determined by these test methods loading nose and supports shall be 5.0 6 0.1 mm (0.197 6
are especially useful for quality control and specification 0.004 in.) unless otherwise specified in an ASTM material
purposes. specification or as agreed upon between the interested parties.
When the use of an ASTM material specification, or an agreed
5.2 Materials that do not fail by the maximum strain upon modification, results in a change to the radii of the
allowed under these test methods (3-point bend) may be more loading nose and supports, the results shall be clearly identified
suited to a 4-point bend test. The basic difference between the as being obtained from a modified version of this test method
two test methods is in the location of the maximum bending and shall include the specification (when available) from which
moment and maximum axial fiber stresses. The maximum axial the modification was specified, for example, Test Method D790
fiber stresses occur on a line under the loading nose in 3-point in accordance with Specification D4101.
bending and over the area between the loading noses in 4-point 6.2.1 Other Radii for Loading Noses and Supports—When
bending. other than default loading noses and supports are used, in order
5.3 Flexural properties may vary with specimen depth, to avoid excessive indentation, or failure due to stress concen-
temperature, atmospheric conditions, and the difference in rate tration directly under the loading nose, they must comply with
of straining as specified in Procedures A and B (see also Note the following requirements: they shall have a minimum radius
7). of 3.2 mm (1⁄8 in.) for all specimens. For specimens 3.2 mm or
5.4 Before proceeding with these test methods, reference greater in depth, the radius of the supports may be up to 1.6
should be made to the ASTM specification of the material times the specimen depth. They shall be this large if significant
being tested. Any test specimen preparation, conditioning, indentation or compressive failure occurs. The arc of the
dimensions, or testing parameters, or combination thereof, loading nose in contact with the specimen shall be sufficiently
covered in the ASTM material specification shall take prece- large to prevent contact of the specimen with the sides of the
dence over those mentioned in these test methods. Table 1 in nose. The maximum radius of the loading nose shall be no
Classification System D4000 lists the ASTM material specifi- more than four times the specimen depth.
cations that currently exist for plastics. 6.3 Micrometers— Suitable micrometers for measuring the
width and thickness of the test specimen to an incremental
6. Apparatus discrimination of at least 0.025 mm (0.001 in.) should be used.
6.1 Testing Machine— A properly calibrated testing ma- All width and thickness measurements of rigid and semirigid
chine that can be operated at constant rates of crosshead motion plastics may be measured with a hand micrometer with ratchet.
over the range indicated, and in which the error in the load A suitable instrument for measuring the thickness of nonrigid
test specimens shall have: a contact measuring pressure of
25 6 2.5 kPa (3.6 6 0.36 psi), a movable circular contact foot
TABLE 1 Flexural Strength
6.35 6 0.025 mm (0.250 6 0.001 in.) in diameter and a lower
Values Expressed in Units of %
of 103 psi
fixed anvil large enough to extend beyond the contact foot in
Material Mean, 103 psi
VrA VRB rC RD
all directions and being parallel to the contact foot within 0.005
ABS 9.99 1.59 6.05 4.44 17.2
mm (0.002 in.) over the entire foot area. Flatness of foot and
DAP thermoset 14.3 6.58 6.58 18.6 18.6 anvil shall conform to the portion of the Calibration section of
Cast acrylic 16.3 1.67 11.3 4.73 32.0 Test Methods D5947.
GR polyester 19.5 1.43 2.14 4.05 6.08
GR polycarbonate 21.0 5.16 6.05 14.6 17.1
SMC 26.0 4.76 7.19 13.5 20.4 7. Test Specimens
A
Vr = within-laboratory coefficient of variation for the indicated material. It is 7.1 The specimens may be cut from sheets, plates, or
obtained by first pooling the within-laboratory standard deviations of the test
results from all of the participating laboratories: Sr = [[(s1 )2 + ( s2)2 . . . + ( sn)2]/n] molded shapes, or may be molded to the desired finished
1/2
B
then Vr = (S r divided by the overall average for the material) × 100. dimensions. The actual dimensions used in Section 4.2, Cal-
Vr = between-laboratory reproducibility, expressed as the coefficient of variation:
SR = {Sr2 + SL2} 1/2 where SL is the standard deviation of laboratory means. Then:
culation, shall be measured in accordance with Test Methods
VR = (S R divided by the overall average for the material) × 100. D5947.
C
r = within-laboratory critical interval between two test results = 2.8 × Vr.
D
R = between-laboratory critical interval between two test results = 2.8 × VR. NOTE 2—Any necessary polishing of specimens shall be done only in
the lengthwise direction of the specimen.

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D790 − 10
7.2 Sheet Materials (Except Laminated Thermosetting Ma- 12.7 by 3.2 mm (5 by 1⁄2 by 1⁄8 in.) tested flatwise on a support
terials and Certain Materials Used for Electrical Insulation, span, resulting in a support span-to-depth ratio of 16 (tolerance
Including Vulcanized Fiber and Glass Bonded Mica): 61). Thicker specimens should be avoided if they exhibit
7.2.1 Materials 1.6 mm (1⁄16 in.) or Greater in Thickness— significant shrink marks or bubbles when molded.
For flatwise tests, the depth of the specimen shall be the 7.5 High-Strength Reinforced Composites, Including Highly
thickness of the material. For edgewise tests, the width of the Orthotropic Laminates—The span-to-depth ratio shall be cho-
specimen shall be the thickness of the sheet, and the depth shall sen such that failure occurs in the outer fibers of the specimens
not exceed the width (see Notes 3 and 4). For all tests, the and is due only to the bending moment (see Note 7). A
support span shall be 16 (tolerance 61) times the depth of the span-to-depth ratio larger than 16:1 may be necessary (32:1 or
beam. Specimen width shall not exceed one fourth of the 40:1 are recommended). For some highly anisotropic compos-
support span for specimens greater than 3.2 mm (1⁄8 in.) in ites, shear deformation can significantly influence modulus
depth. Specimens 3.2 mm or less in depth shall be 12.7 mm (1⁄2 measurements, even at span-to-depth ratios as high as 40:1.
in.) in width. The specimen shall be long enough to allow for Hence, for these materials, an increase in the span-to-depth
overhanging on each end of at least 10 % of the support span, ratio to 60:1 is recommended to eliminate shear effects when
but in no case less than 6.4 mm (1⁄4 in.) on each end. Overhang modulus data are required, it should also be noted that the
shall be sufficient to prevent the specimen from slipping flexural modulus of highly anisotropic laminates is a strong
through the supports. function of ply-stacking sequence and will not necessarily
NOTE 3—Whenever possible, the original surface of the sheet shall be correlate with tensile modulus, which is not stacking-sequence
unaltered. However, where testing machine limitations make it impossible dependent.
to follow the above criterion on the unaltered sheet, one or both surfaces
shall be machined to provide the desired dimensions, and the location of NOTE 7—As a general rule, support span-to-depth ratios of 16:1 are
the specimens with reference to the total depth shall be noted. The value satisfactory when the ratio of the tensile strength to shear strength is less
obtained on specimens with machined surfaces may differ from those than 8 to 1, but the support span-to-depth ratio must be increased for
obtained on specimens with original surfaces. Consequently, any specifi- composite laminates having relatively low shear strength in the plane of
cations for flexural properties on thicker sheets must state whether the the laminate and relatively high tensile strength parallel to the support
original surfaces are to be retained or not. When only one surface was span.
machined, it must be stated whether the machined surface was on the
tension or compression side of the beam. 8. Number of Test Specimens
NOTE 4—Edgewise tests are not applicable for sheets that are so thin 8.1 Test at least five specimens for each sample in the case
that specimens meeting these requirements cannot be cut. If specimen
of isotropic materials or molded specimens.
depth exceeds the width, buckling may occur.
7.2.2 Materials Less than 1.6 mm (1⁄16 in.) in Thickness— 8.2 For each sample of anisotropic material in sheet form,
The specimen shall be 50.8 mm (2 in.) long by 12.7 mm (1⁄2 in.) test at least five specimens for each of the following conditions.
wide, tested flatwise on a 25.4-mm (1-in.) support span. Recommended conditions are flatwise and edgewise tests on
specimens cut in lengthwise and crosswise directions of the
NOTE 5—Use of the formulas for simple beams cited in these test sheet. For the purposes of this test, “lengthwise” designates the
methods for calculating results presumes that beam width is small in principal axis of anisotropy and shall be interpreted to mean the
comparison with the support span. Therefore, the formulas do not apply
rigorously to these dimensions.
direction of the sheet known to be stronger in flexure. “Cross-
NOTE 6—Where machine sensitivity is such that specimens of these wise” indicates the sheet direction known to be the weaker in
dimensions cannot be measured, wider specimens or shorter support flexure and shall be at 90° to the lengthwise direction.
spans, or both, may be used, provided the support span-to-depth ratio is at
least 14 to 1. All dimensions must be stated in the report (see also Note 5). 9. Conditioning
7.3 Laminated Thermosetting Materials and Sheet and 9.1 Conditioning—Condition the test specimens in accor-
Plate Materials Used for Electrical Insulation, Including dance with Procedure A of Practice D618 unless otherwise
Vulcanized Fiber and Glass-Bonded Mica—For paper-base and specified by contract or the relevant ASTM material specifica-
fabric-base grades over 25.4 mm (1 in.) in nominal thickness, tion. Conditioning time is specified as a minimum. Tempera-
the specimens shall be machined on both surfaces to a depth of ture and humidity tolerances shall be in accordance with
25.4 mm. For glass-base and nylon-base grades, specimens Section 7 of Practice D618 unless specified differently by
over 12.7 mm (1⁄2 in.) in nominal depth shall be machined on contract or material specification.
both surfaces to a depth of 12.7 mm. The support span-to-depth 9.2 Test Conditions—Conduct the tests at the same tempera-
ratio shall be chosen such that failures occur in the outer fibers ture and humidity used for conditioning with tolerances in
of the specimens, due only to the bending moment (see Note accordance with Section 7 of Practice D618 unless otherwise
7). Therefore, a ratio larger than 16:1 may be necessary (32:1 specified by contract or the relevant ASTM material specifica-
or 40:1 are recommended). When laminated materials exhibit tion.
low compressive strength perpendicular to the laminations,
they shall be loaded with a large radius loading nose (up to four 10. Procedure
times the specimen depth to prevent premature damage to the 10.1 Procedure A:
outer fibers. 10.1.1 Use an untested specimen for each measurement.
7.4 Molding Materials (Thermoplastics and Thermosets)— Measure the width and depth of the specimen to the nearest
The recommended specimen for molding materials is 127 by 0.03 mm (0.001 in.) at the center of the support span. For

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D790 − 10
specimens less than 2.54 mm (0.100 in.) in depth, measure the D = midspan deflection, mm (in.),
depth to the nearest 0.003 mm (0.0005 in.). These measure- r = strain, mm/mm (in./in.),
ments shall be made in accordance with Test Methods D5947. L = support span, mm (in.), and
10.1.2 Determine the support span to be used as described in d = depth of beam, mm (in.).
Section 7 and set the support span to within 1 % of the NOTE 8—For some materials that do not yield or break within the 5 %
determined value. strain limit when tested by Procedure A, the increased strain rate allowed
by Procedure B (see 10.2) may induce the specimen to yield or break, or
10.1.3 For flexural fixtures that have continuously adjust-
both, within the required 5 % strain limit.
able spans, measure the span accurately to the nearest 0.1 mm NOTE 9—Beyond 5 % strain, this test method is not applicable. Some
(0.004 in.) for spans less than 63 mm (2.5 in.) and to the nearest other mechanical property might be more relevant to characterize mate-
0.3 mm (0.012 in.) for spans greater than or equal to 63 mm rials that neither yield nor break by either Procedure A or Procedure B
(2.5 in.). Use the actual measured span for all calculations. For within the 5 % strain limit (for example, Test Method D638 may be
flexural fixtures that have fixed machined span positions, verify considered).
the span distance the same as for adjustable spans at each 10.2 Procedure B:
machined position. This distance becomes the span for that 10.2.1 Use an untested specimen for each measurement.
position and is used for calculations applicable to all subse- 10.2.2 Test conditions shall be identical to those described
quent tests conducted at that position. See Annex A2 for in 10.1, except that the rate of straining of the outer surface of
information on the determination of and setting of the span. the test specimen shall be 0.10 mm/mm (in./in.)/min.
10.1.4 Calculate the rate of crosshead motion as follows and 10.2.3 If no break has occurred in the specimen by the time
set the machine for the rate of crosshead motion as calculated the maximum strain in the outer surface of the test specimen
by Eq 1: has reached 0.05 mm/mm (in./in.), discontinue the test (see
R 5 ZL 2 /6d (1) Note 9).
where: 11. Retests
R = rate of crosshead motion, mm (in.)/min,
L = support span, mm (in.), 11.1 Values for properties at rupture shall not be calculated
d = depth of beam, mm (in.), and for any specimen that breaks at some obvious, fortuitous flaw,
Z = rate of straining of the outer fiber, mm/mm/min (in./in./ unless such flaws constitute a variable being studied. Retests
min). Z shall be equal to 0.01. shall be made for any specimen on which values are not
calculated.
In no case shall the actual crosshead rate differ from that
calculated using Eq 1, by more than 610 %.
10.1.5 Align the loading nose and supports so that the axes 12. Calculation
of the cylindrical surfaces are parallel and the loading nose is 12.1 Toe compensation shall be made in accordance with
midway between the supports. The parallelism of the apparatus Annex A1 unless it can be shown that the toe region of the
may be checked by means of a plate with parallel grooves into curve is not due to the take-up of slack, seating of the
which the loading nose and supports will fit when properly specimen, or other artifact, but rather is an authentic material
aligned (see A2.3). Center the specimen on the supports, with response.
the long axis of the specimen perpendicular to the loading nose 12.2 Flexural Stress (σf)—When a homogeneous elastic
and supports. material is tested in flexure as a simple beam supported at two
10.1.6 Apply the load to the specimen at the specified points and loaded at the midpoint, the maximum stress in the
crosshead rate, and take simultaneous load-deflection data. outer surface of the test specimen occurs at the midpoint. This
Measure deflection either by a gage under the specimen in stress may be calculated for any point on the load-deflection
contact with it at the center of the support span, the gage being curve by means of the following equation (see Notes 10-12):
mounted stationary relative to the specimen supports, or by
measurement of the motion of the loading nose relative to the σ f 5 3PL/2bd2 (3)
supports. Load-deflection curves may be plotted to determine
the flexural strength, chord or secant modulus or the tangent where:
modulus of elasticity, and the total work as measured by the σ = stress in the outer fibers at midpoint, MPa (psi),
area under the load-deflection curve. Perform the necessary toe P = load at a given point on the load-deflection curve, N
compensation (see Annex A1) to correct for seating and (lbf),
indentation of the specimen and deflections in the machine. L = support span, mm (in.),
10.1.7 Terminate the test when the maximum strain in the b = width of beam tested, mm (in.), and
outer surface of the test specimen has reached 0.05 mm/mm d = depth of beam tested, mm (in.).
(in./in.) or at break if break occurs prior to reaching the NOTE 10—Eq 3 applies strictly to materials for which stress is linearly
maximum strain (Notes 8 and 9). The deflection at which this proportional to strain up to the point of rupture and for which the strains
strain will occur may be calculated by letting r equal 0.05 are small. Since this is not always the case, a slight error will be
introduced if Eq 3 is used to calculate stress for materials that are not true
mm/mm (in./in.) in Eq 2: Hookean materials. The equation is valid for obtaining comparison data
D 5 rL2 /6d (2) and for specification purposes, but only up to a maximum fiber strain of
5 % in the outer surface of the test specimen for specimens tested by the
where: procedures described herein.

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D790 − 10
NOTE 11—When testing highly orthotropic laminates, the maximum
stress may not always occur in the outer surface of the test specimen.4
Laminated beam theory must be applied to determine the maximum
tensile stress at failure. If Eq 3 is used to calculate stress, it will yield an
apparent strength based on homogeneous beam theory. This apparent
strength is highly dependent on the ply-stacking sequence of highly
orthotropic laminates.
NOTE 12—The preceding calculation is not valid if the specimen slips
excessively between the supports.
12.3 Flexural Stress for Beams Tested at Large Support
Spans (σ f)—If support span-to-depth ratios greater than 16 to
1 are used such that deflections in excess of 10 % of the
support span occur, the stress in the outer surface of the
specimen for a simple beam can be reasonably approximated
with the following equation (see Note 13):
σ f 5 ~ 3PL/2bd2 ! @ 116 ~ D/L ! 2 2 4 ~ d/L !~ D/L ! # (4)
where:
σf, P, L, b, and d are the same as for Eq 3, and
D = deflection of the centerline of the specimen at the
middle of the support span, mm (in.).
NOTE 13—When large support span-to-depth ratios are used, significant
end forces are developed at the support noses which will affect the
NOTE 1—Curve a: Specimen that breaks before yielding.
moment in a simple supported beam. Eq 4 includes additional terms that
Curve b: Specimen that yields and then breaks before the 5 % strain
are an approximate correction factor for the influence of these end forces
limit.
in large support span-to-depth ratio beams where relatively large deflec-
Curve c: Specimen that neither yields nor breaks before the 5 % strain
tions exist.
limit.
12.4 Flexural Strength (σfM)—Maximum flexural stress sus- FIG. 1 Typical Curves of Flexural Stress (ςf) Versus Flexural
tained by the test specimen (see Note 11) during a bending test. Strain (´f)
It is calculated according to Eq 3 or Eq 4. Some materials that
do not break at strains of up to 5 % may give a load deflection
curve that shows a point at which the load does not increase in accordance with Eq 3 or Eq 4 by letting P equal the load read
with an increase in strain, that is, a yield point (Fig. 1, Curve from the load-deflection curve at the deflection corresponding
B), Y. The flexural strength may be calculated for these to the desired strain (for highly orthotropic laminates, see Note
materials by letting P (in Eq 3 or Eq 4) equal this point, Y. 11).
12.5 Flexural Offset Yield Strength—Offset yield strength is 12.8 Flexural Strain, ´f—Nominal fractional change in the
the stress at which the stress-strain curve deviates by a given length of an element of the outer surface of the test specimen
strain (offset) from the tangent to the initial straight line portion at midspan, where the maximum strain occurs. It may be
of the stress-strain curve. The value of the offset must be given calculated for any deflection using Eq 5:
whenever this property is calculated. ϵ f 5 6Dd/L 2 (5)
NOTE 14—This value may differ from flexural strength defined in 12.4.
Both methods of calculation are described in the annex to Test Method where:
D638.
´f = strain in the outer surface, mm/mm (in./in.),
12.6 Flexural Stress at Break (σfB )—Flexural stress at D = maximum deflection of the center of the beam, mm
break of the test specimen during a bending test. It is calculated (in.),
according to Eq 3 or Eq 4. Some materials may give a load L = support span, mm (in.), and
deflection curve that shows a break point, B, without a yield d = depth, mm (in.).
point (Fig. 1, Curve a) in which case σ fB = σfM. Other
materials may give a yield deflection curve with both a yield 12.9 Modulus of Elasticity:
and a break point, B (Fig. 1, Curve b). The flexural stress at 12.9.1 Tangent Modulus of Elasticity—The tangent modulus
break may be calculated for these materials by letting P (in Eq of elasticity, often called the “modulus of elasticity,” is the
3 or Eq 4) equal this point, B. ratio, within the elastic limit, of stress to corresponding strain.
It is calculated by drawing a tangent to the steepest initial
12.7 Stress at a Given Strain—The stress in the outer straight-line portion of the load-deflection curve and using Eq
surface of a test specimen at a given strain may be calculated 6 (for highly anisotropic composites, see Note 15).
E B 5 L 3 m/4bd 3 (6)
4
For a discussion of these effects, see Zweben, C., Smith, W. S., and Wardle, M.
W., “Test Methods for Fiber Tensile Strength, Composite Flexural Modulus and where:
Properties of Fabric-Reinforced Laminates, “ Composite Materials: Testing and
EB = modulus of elasticity in bending, MPa (psi),
Design (Fifth Conference), ASTM STP 674, 1979, pp. 228–262.

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D790 − 10

L = support span, mm (in.), ´f1 are the flexural strain values, calculated from Eq 5 and
b = width of beam tested, mm (in.), measured at the predetermined points on the load deflection
d = depth of beam tested, mm (in.), and curve.
m = slope of the tangent to the initial straight-line portion of
12.10 Arithmetic Mean— For each series of tests, the
the load-deflection curve, N/mm (lbf/in.) of deflection.
arithmetic mean of all values obtained shall be calculated to
NOTE 15—Shear deflections can seriously reduce the apparent modulus
of highly anisotropic composites when they are tested at low span-to- three significant figures and reported as the “average value” for
depth ratios.4 For this reason, a span-to-depth ratio of 60 to 1 is the particular property in question.
recommended for flexural modulus determinations on these composites.
Flexural strength should be determined on a separate set of replicate 12.11 Standard Deviation—The standard deviation (esti-
specimens at a lower span-to-depth ratio that induces tensile failure in the mated) shall be calculated as follows and be reported to two
outer fibers of the beam along its lower face. Since the flexural modulus significant figures:
of highly anisotropic laminates is a critical function of ply-stacking
sequence, it will not necessarily correlate with tensile modulus, which is s5 =~ ( X 2
2 nX̄ 2
! /~n 2 1! (8)
not stacking-sequence dependent.
12.9.2 Secant Modulus— The secant modulus is the ratio of where:
stress to corresponding strain at any selected point on the
s = estimated standard deviation,
stress-strain curve, that is, the slope of the straight line that
X = value of single observation,
joins the origin and a selected point on the actual stress-strain n = number of observations, and
curve. It shall be expressed in megapascals (pounds per square X¯ = arithmetic mean of the set of observations.
inch). The selected point is chosen at a prespecified stress or
strain in accordance with the appropriate material specification 13. Report
or by customer contract. It is calculated in accordance with Eq
6 by letting m equal the slope of the secant to the load- 13.1 Report the following information:
deflection curve. The chosen stress or strain point used for the 13.1.1 Complete identification of the material tested, includ-
determination of the secant shall be reported. ing type, source, manufacturer’s code number, form, principal
12.9.3 Chord Modulus (Ef)—The chord modulus may be dimensions, and previous history (for laminated materials,
calculated from two discrete points on the load deflection ply-stacking sequence shall be reported),
curve. The selected points are to be chosen at two prespecified 13.1.2 Direction of cutting and loading specimens, when
stress or strain points in accordance with the appropriate appropriate,
material specification or by customer contract. The chosen 13.1.3 Conditioning procedure,
stress or strain points used for the determination of the chord 13.1.4 Depth and width of specimen,
modulus shall be reported. Calculate the chord modulus, Ef 13.1.5 Procedure used (A or B),
using the following equation:
13.1.6 Support span length,
E f 5 ~ σ f2 2 σ f1 ! / ~ ϵ f2 2 ϵ f1 ! (7) 13.1.7 Support span-to-depth ratio if different than 16:1,
where:
13.1.8 Radius of supports and loading noses, if different
σf2 and σf1 are the flexural stresses, calculated from Eq 3 or than 5 mm. When support and/or loading nose radii other than
Eq 4 and measured at the predefined points on the load 5 mm are used, the results shall be identified as being generated
deflection curve, and ´ f2 and by a modified version of this test method and the referring
specification referenced as to the geometry used.
13.1.9 Rate of crosshead motion,
13.1.10 Flexural strain at any given stress, average value
TABLE 2 Flexural Modulus and standard deviation,
Values Expressed in units of % 13.1.11 If a specimen is rejected, reason(s) for rejection,
Material Mean, 103 psi of 103 psi
VrA VRB rC RD
13.1.12 Tangent, secant, or chord modulus in bending,
ABS 338 4.79 7.69 13.6 21.8
average value, standard deviation, and the strain level(s) used
DAP thermoset 485 2.89 7.18 8.15 20.4 if secant or chord modulus,
Cast acrylic 810 13.7 16.1 38.8 45.4 13.1.13 Flexural strength (if desired), average value, and
GR polyester 816 3.49 4.20 9.91 11.9
GR 1790 5.52 5.52 15.6 15.6 standard deviation,
polycarbonate 13.1.14 Stress at any given strain up to and including 5 % (if
SMC 1950 10.9 13.8 30.8 39.1
desired), with strain used, average value, and standard devia-
A
Vr = within-laboratory coefficient of variation for the indicated material. It is tion,
obtained by first pooling the within-laboratory standard deviations of the test
results from all of the participating laboratories: Sr = [[(s1 )2 + ( s2)2 . . . + ( sn)2]/ n] 13.1.15 Flexural stress at break (if desired), average value,
1/2 then Vr = (S r divided by the overall average for the material) × 100. and standard deviation,
B
Vr = between-laboratory reproducibility, expressed as the coefficient of variation:
SR = {Sr2 + SL2 }1/2 where SL is the standard deviation of laboratory means. Then: 13.1.16 Type of behavior, whether yielding or rupture, or
VR = (SR divided by the overall average for the material) × 100.
C
both, or other observations, occurring within the 5 % strain
r = within-laboratory critical interval between two test results = 2.8 × Vr.
D
R = between-laboratory critical interval between two test results = 2.8 × VR.
limit, and
13.1.17 Date of specific version of test used.

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14. Precision and Bias 14.2.1 Repeatability— Two test results obtained within one
14.1 Tables 1 and 2 are based on a round-robin test laboratory shall be judged not equivalent if they differ by more
conducted in 1984, in accordance with Practice E691, involv- than the r value for that material. r is the interval representing
ing six materials tested by six laboratories using Procedure A. the critical difference between two test results for the same
For each material, all the specimens were prepared at one material, obtained by the same operator using the same
source. Each “test result” was the average of five individual equipment on the same day in the same laboratory.
determinations. Each laboratory obtained two test results for 14.2.2 Reproducibility— Two test results obtained by differ-
each material. ent laboratories shall be judged not equivalent if they differ by
more than the R value for that material. R is the interval
NOTE 16—Caution: The following explanations of r and R
(14.2-14.2.3) are intended only to present a meaningful way of consider- representing the critical difference between two test results for
ing the approximate precision of these test methods. The data given in the same material, obtained by different operators using differ-
Tables 2 and 3 should not be applied rigorously to the acceptance or ent equipment in different laboratories.
rejection of materials, as those data are specific to the round robin and may
not be representative of other lots, conditions, materials, or laboratories.
14.2.3 The judgments in 14.2.1 and 14.2.2 will have an
Users of these test methods should apply the principles outlined in approximately 95 % (0.95) probability of being correct.
Practice E691 to generate data specific to their laboratory and materials, or
between specific laboratories. The principles of 14.2-14.2.3 would then be 14.3 Bias—No statement may be made about the bias of
valid for such data. these test methods, as there is no standard reference material or
14.2 Concept of “r” and “R” in Tables 1 and 2—If Sr and reference test method that is applicable.
SR have been calculated from a large enough body of data, and
for test results that were averages from testing five specimens 15. Keywords
for each test result, then: 15.1 flexural properties; plastics; stiffness; strength

ANNEXES

(Mandatory Information)

A1. TOE COMPENSATION

A1.1 In a typical stress-strain curve (see Fig. A1.1) there is alignment or seating of the specimen. In order to obtain correct
a toe region, AC, that does not represent a property of the values of such parameters as modulus, strain, and offset yield
material. It is an artifact caused by a takeup of slack and point, this artifact must be compensated for to give the
corrected zero point on the strain or extension axis.
A1.2 In the case of a material exhibiting a region of
Hookean (linear) behavior (see Fig. A1.1), a continuation of
the linear (CD) region of the curve is constructed through the
zero-stress axis. This intersection (B) is the corrected zero-
strain point from which all extensions or strains must be
measured, including the yield offset (BE), if applicable. The
elastic modulus can be determined by dividing the stress at any
point along the Line CD (or its extension) by the strain at the
same point (measured from Point B, defined as zero-strain).
A1.3 In the case of a material that does not exhibit any
linear region (see Fig. A1.2), the same kind of toe correction of
the zero-strain point can be made by constructing a tangent to
the maximum slope at the inflection Point H'. This is extended
to intersect the strain axis at Point B', the corrected zero-strain
point. Using Point B' as zero strain, the stress at any point (G')
on the curve can be divided by the strain at that point to obtain
a secant modulus (slope of Line B' G'). For those materials with
no linear region, any attempt to use the tangent through the
NOTE 1—Some chart recorders plot the mirror image of this graph. inflection point as a basis for determination of an offset yield
FIG. A1.1 Material with Hookean Region point may result in unacceptable error.

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NOTE 1—Some chart recorders plot the mirror image of this graph.
FIG. A1.2 Material with No Hookean Region

A2. MEASURING AND SETTING SPAN

A2.1 For flexural fixtures that have adjustable spans, it is


important that the span between the supports is maintained
constant or the actual measured span is used in the calculation
of stress, modulus, and strain, and the loading nose or noses are
positioned and aligned properly with respect to the supports. FIG. A2.1 Markings on Fixed Specimen Supports
Some simple steps as follows can improve the repeatability of
your results when using these adjustable span fixtures.
A2.2 Measurement of Span:
A2.2.1 This technique is needed to ensure that the correct FIG. A2.2 Markings on Rotatable Specimen Supports
span, not an estimated span, is used in the calculation of
results.
A2.2.2 Scribe a permanent line or mark at the exact center
of the support where the specimen makes complete contact. A2.3 Setting the Span and Alignment of Loading
The type of mark depends on whether the supports are fixed or Nose(s)—To ensure a consistent day-to-day setup of the span
rotatable (see Figs. A2.1 and A2.2).
and ensure the alignment and proper positioning of the loading
A2.2.3 Using a vernier caliper with pointed tips that is nose, simple jigs should be manufactured for each of the
readable to at least 0.1 mm (0.004 in.), measure the distance standard setups used. An example of a jig found to be useful is
between the supports, and use this measurement of span in the shown in Fig. A2.3.
calculations.

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FIG. A2.3 Fixture Used to Set Loading Nose and Support Spacing and Alignment

APPENDIX

(Nonmandatory Information)

X1. DEVELOPMENT OF A FLEXURAL MACHINE COMPLIANCE CORRECTION

X1.1 Introduction X1.3.4 Computer Software to make corrections to the dis-


X1.1.1 Universal Testing instrument drive systems always placements
exhibit a certain level of compliance that is characterized by a X1.3.5 Steel bar, with smoothed surfaces and a calculated
variance between the reported crosshead displacement and the flexural stiffness of more than 100 times greater than the test
displacement actually imparted to the specimen. This variance material. The length should be at least 13 mm greater than the
is a function of load frame stiffness, drive system wind-up, load support span. The width shall match the width of the test
cell compliance and fixture compliance. To accurately measure specimen and the thickness shall be that required to achieve or
the flexural modulus of a material, this compliance should be exceed the target stiffness.
measured and empirically subtracted from test data. Flexural
modulus results without the corrections are lower than if the X1.4 Safety Precautions
correction is applied. The greater the stiffness of the material
the more influence the system compliance has on results. X1.4.1 The universal testing machine should stop the ma-
chine crosshead movement when the load reaches 90 % of load
X1.1.2 It is not necessary to make the machine compliance cell capacity, to prevent damage to the load cell.
correction when a deflectometer/extensometer is used to mea-
sure the actual deflection occurring in the specimen as it is X1.4.2 The compliance curve determination should be
deflected. made at a speed no higher than 2 mm/min. Because the load
builds up rapidly since the steel bar does not deflect, it is quite
X1.2 Terminology easy to exceed the load cell capacity.
X1.2.1 Compliance—The displacement difference between
test machine drive system displacement values and actual X1.5 Procedure
specimen displacement NOTE X1.1—A new compliance correction curve should be established
each time there is a change made to the setup of the test machine, such as,
X1.2.2 Compliance Correction—An analytical method of load cell changed or reinstallation of the flexure fixture on the machine. If
modifying test instrument displacement values to eliminate the the test machine is dedicated to flexural testing, and there are no changes
to the setup, it is not necessary to re-calculate the compliance curve.
amount of that measurement attributed to test instrument
NOTE X1.2—On those machines with computer software that automati-
compliance. cally make this compliance correction; refer to the software manual to
determine how this correction should be made.
X1.3 Apparatus
X1.5.1 The procedure to determine compliance follows:
X1.3.1 Universal Testing machine
X1.5.1.1 Configure the test system to match the actual test
X1.3.2 Load cell configuration.
X1.3.3 Flexure fixture including loading nose and specimen X1.5.1.2 Place the steel bar in the test fixture, duplicating
supports the position of a specimen during actual testing.

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X1.5.1.3 Set the crosshead speed to 2 mm/min. or less and
start the crosshead moving in the test direction recording
crosshead displacement and the corresponding load values.
X1.5.1.4 Increase load to a point exceeding the highest load
expected during specimen testing. Stop the crosshead and
return to the pre-test location.
X1.5.1.5 The recorded load-deflection curve, starting when
the loading nose contacts the steel bar to the time that the
highest load expected is defined as test system compliance.
X1.5.2 Procedure to apply compliance correction is as
follows:
X1.5.2.1 Run the flexural test method on the material at the
crosshead required for the measurement.
X1.5.2.2 It is preferable that computer software be used to
make the displacement corrections, but if it is not available
compliance corrections can be made manually in the following
manner. Determine the range of displacement (D) on the load FIG. X1.2 Compliance Curve for Steel Bar
versus displacement curve for the material, over which the
modulus is to be calculated. For Young’s Modulus that would
steepest region of the curve below the proportional limit. For X1.6 Calculations
Secant and Chord Modulii that would be at specified level of X1.6.1 Calculation of Chord Modulus
strain or specified levels of strain, respectively. Draw two X1.6.1.1 Calculate the stresses (σf1, σf2) for load points L1
vertical lines up from the displacement axis for the two chosen and L2 from Fig. X1.1 using the equation in 12.2, Eq 3.
displacements (D1, D2) to the load versus displacement curve X1.6.1.2 Calculate the strains (´f1, ϵf2) for displacements
for the material. In some cases one of these points maybe at D1-c1 and D2-c2 from Fig. X1.3 using the equation in 12.8, Eq
zero displacement after the toe compensation correction is 5.
made. Draw two horizontal lines from these points on the load X1.6.1.3 Calculate the flexural chord modulus in accor-
displacement curve to the Load (P) axis. Determine the loads dance with 12.9.3, Eq 7.
(L1, L2). X1.6.2 Calculation of Secant Modulus
X1.5.2.3 Using the Compliance Correction load displace- X1.6.2.1 Calculation of the Secant Modulus at any strain
ment curve for the steel bar, mark off L1 and L2 on the Load along the curve would be the same as conducting a chord
(P) axis. From these two points draw horizontal lines across till modulus measurement, except that σf1 = 0, L1= 0, and D1-c1
they contact the load versus displacement curve for the steel = 0.
bar. From these two points on the load deflection curve draw
two vertical lines downwards to the displacement axis. These X1.6.3 Calculation of Young’s Modulus
two points on the displacement axis determine the corrections X1.6.3.1 Determine the steepest slope “m” along the curve,
(c1, c2) that need to be made to the displacements measure- below the proportional limit, using the selected loads L1 and
ments for the test material. L2 from Fig. X1.1 and the displacements D1-c1 and D2-c2
X1.5.2.4 Subtract the corrections (c1, c2) from the mea- from Fig. X1.3.
sured displacements (D1, D2), so that a true measures of test
specimen deflection (D1-c1, D2-c2) are obtained.

FIG. X1.3 Example of the Material Curve Corrected for the Com-
FIG. X1.1 Example of Modulus Curve for a Material pliance Corrected Displacement or Strain

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X1.6.3.2 Calculate the Young’s modulus in accordance with
12.9.1, Eq 6.

SUMMARY OF CHANGES

Committee D20 has identified the location of selected changes to this standard since the last issue
(D790 - 07ϵ1) that may impact the use of this standard. (April 1, 2010)

(1) Revised Section 9.

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