TYPE TEST ACCORDING TO ISO 15848 - 1 REV Page 1 of 4

TYPE TEST ACCORDING TO ISO 15848 - 1 FIRST EDITION 2006-01-15

PROCEDURE NO.: ATIPL-FET-01, Rev. 04 DATE: 25/05/2007 PAGE

REPORT NO.: ATIPL/FET/GLV/02 DATE: 13/06/2007 01 OF 06

1. VALVE SPECIFICATION

MANUFACTURER M/s Associated Toolings (INDIA) Pvt.. Ltd.

LOCATION/ ADDRESS Balitikuri, Kalitala, Howrah – 13
CLIENT M/s LARSEN & TOUBRO LTD.
PROJECT Naptha Cracker
TEST DURATION 11/06/2007 to 13/06/2007.
VALVE TYPE & MODEL Isolation, Globe Valve, 8409-8609
VALVE SIZE (Nominal Bore) 20 mm
VALVE CLASS (ANSI) # 800
TIGHTNESS CLASS C
ENDURANCE CLASS C01
VALVE SR. NO. 02
STEM DIAMETER MM 11.2 – 11.3 mm
MANUFACTURER G. A. DRAWING NO. A4.20.8409 SW3K
VALVE MATERIAL SPECIFICATION ASTM – A 105

2. TEST CONDITION

TEST PRESSURE 2000 psi @ RT and 1400 psi @ TT

TEST TEMPRATURE RT and 400 C
TEST MEDIUM Helium Gas 99.938%
OPERATING EQUIPMENT Manual
GLAND BOLT TIGHTNING TORQUE 35 Nm
VALVE MOUNTING Stem Horizontal
VALVE OPERATING TORQUE 16 Nm
B184161 MODEL: EVT 600A,MAKE: BRITOOL,
TORQUE WRINTCH No.
ENGLAND

3. REFERENCE DOCUMENTS

01 ISO 15848 – 1 First edition 2006 – 01 – 15

02 CLIENT SPECIFICATION: 12605-H-225
03 ANSI B16.34

4. TEST EQUIPMENT DETAIL

FOR MEASURING IN STD CC/SEC.

EQUIPMENT MAKE: H. Fillunger, Pune MODEL: HLD – C – 01D SR. NO.: 302

STANDARD LEAK MAKE: Laco Technology, USA MODEL:CM11X – 71113 SR. NO.: 1920

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FOR MEASURING IN PPM

EQUIPMENT MAKE: Varian MODEL: PHD - 4 SR. NO.:203320

SR. NO.:MSC-5649(.5
CALIBRATION GAS CONCETRATION: 25 PPM CERT. DATE: 25/05/07
Ltrs)
MAKE: Pricol MODEL: Bordon SR. NO.:PG - 018
PRESSURE GAUGE
CALIBRATED ON:27/12/06 CAL. VALID: 27/06/07 RANGE: 0 -160KG/CM2
5. CALIBRATION DETAIL

STANDARD LEAK VALUE CALIBRATED ON

2.8X 10 -7STD CC/SEC 26.09.2006

INITIAL CALIBRATION LEAK VALUE FINAL CALIBRATION LEAK VALUE

2.8X 10 -7 STD CC/SEC 2.8X 10 -7 STD CC/SEC

INITIAL BACK GROUND FINAL BACK GROUND

Less Than 10 -8 STD CC/SEC Less Than 10 -8 STD CC/SEC

RESPONSE TIME CLEAN UP TIME HELIUM CONCENTRATION

10 Seconds 15 Seconds ≈ 99%

6. TESTING PERSONNEL

NAME NDT CERTIFICATION CERTIFICATE NO. VALIDITY

S. Ansari NDT L – II GE/NDT/LT/222B 31.08.2008
A.P. Mishra NDT L – III 126592 2008

7. LEAK DETECTION METHOD

SNIFFING AS PER ISO 15848 – I ANNEX B

VACUUM AS PER ISO 15848 – I ANNEX A, A.1

8. PACKING DETAIL

BODY-BONNET GASKET MATERIAL SS.316 SPWND. WITH GRAFOIL FLR.

BODY-BONNET GASKET CONFIGURATION 0D – 45 mm, ID – 34 mm, THK. – 3.2 mm
GLAND PACKING MATERIAL Braided Graphite die moulded rings.
OD – 17.95 mm, ID – 11.30 mm, THK. – 4.5 mm, No. of Rings – 05
GLAND PACKING CONFIGURATION nos.

9. ACCEPTANCE CRITERION

As per ISO 15848 – I 3.14X10-4 mg/s/meter

As per ABB Specification H - 225 500 PPMv

10. PROCEDURE BRIEF

1 EQUIPMENT CALIBRATION /MEASUREMENT 2 MEASUREMENT OF BACKGROUND IF ANY

3 READING FOR RT BEFORE CYCLING @ 2000 PSI. 4 READING FOR RT AFTER CYCLING @ 2000 PSI

READING AT 4000 C AFTER CYCLING @ 1400

5 READING AT 4000 C BEFORE CYCLING @ 1400 PSI 6
PSI

7 READING FOR RT BEFORE CYCLING @ 2000 PSI 8 READING FOR RT AFTER CYCLING @ 2000 PSI

9 READING AT 4000 C BEFORE CYCLING @ 1400 PSI 10

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READING AT 4000 C AFTER CYCLING @ 1400

PSI

11 READING M3 FOR RT @ 2000 PSI. -- ---

11. QUALIFIED RANGE OF VALVES:

This test shall qualify the valves as per following:

1. The stem (shaft) seals and body seals are of the same material, design, shape and construction as
the
tested valve. The Dimension of sealing component (Body-Bonnet Gasket & Gland Packing) shall as
per
the standard design of different size & type of valve.
2. Valve Operation shall be manual.
3. The type of motion of the stem (shaft) is identical to tested valve.
4. Tolerances classes and surface finish specification of all valve components which affect sealing
performance are identical to tested valve.
5. Stem diameters are within the range of 5.5 mm to 22.5 mm with shank diameter surface finish
0.4 – 0.8 micron.
6. This type test qualifies Horizontal, Vertical & Inclined mounting valves.
7. The valve class designation is equal to # 800 and lower.
8. The required temperature class falls between the room temperature and the test temperature
(400 C) of the qualified valve.
9. This type test qualifies the TIGHTNESS CALSS ‘C’.
10. This type test qualifies the valves with endurance class C01.

12. TEST RESULTS

ü Body Seal And Gland Leakage Detection In Sniffing Mode In ppmv

ü Gland Seal In Vacuum Mode In Mg/S/Meter
ü Reading Are After Calculation If Any.

TEST TEMP. IN C LEAKAGE (GLAND) BODY

PR.
SR. TEST SEAL
CYCLE IN Vacuum Sniffing
NO. STAGE T1 T2 T3 LEAK
psi mg/s/m (ppm)
(ppm)
01 RT 0 35 33 32 2000 5.16X10-7 11 10
02 RTC 125 36 33 33 2000 < 10-7 9 -
03 TT 0 391 404 403 1400 2.8X10-8 6 -
1400 -7 6.2
04 TTC 125 400 401 395 1.4X10 -
05 RT 0 49 42 38 2000 5.6X10-7 29 -
06 RTC 125 39 35 34 2000 6.53X10-6 47 -
07 TT 0 402 394 387 1400 2.52X10-7 43 -
08 TTC 125 389 403 394 1400 3.36X10-7 14 -
09 RT 0 49 44 38 2000 5.6X10-7 31 42

RT: Room Temp., RTC: Testing at Room Temp. After Cycle.

TT: Test Temp., TTC: Testing at Test Temp. After Cycle.
T1 : Test temperature (Flow path).,T2 : Body Temperature.T3 : Gland Temperature.

13. MARKING:

ISO FE BH – CO1 – SSA 0 – T (RT, 400 C) – CL#800 – ISO 15848 – I.

The Production valves qualified by type testing will be marked with ‘ISO FE’.

14. POST TEST EXAMINATION:

• After testing valve is dismantled and all sealing component & stem are visually examined,
• no wear and any other significant defect observed.

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• The valve is identified asstamped on body and bonnet flange for identification.

15. TEST RESULT: ACCEPTED.

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