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Exp. 6: Analysis of Bleach and Copper (II) Unknown

This document describes an experiment analyzing an unknown bleach sample and copper (II) compound. It standardizes a sodium thiosulfate solution and uses it to titrate the bleach to determine its available chlorine content. Two bleach samples are tested and the average chlorine content is calculated. The copper compound is also tested by titrating with sodium thiosulfate to identify the unknown compound and calculate its copper percentage. Key results and identification of the copper compound are summarized.

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fiza
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23 views

Exp. 6: Analysis of Bleach and Copper (II) Unknown

This document describes an experiment analyzing an unknown bleach sample and copper (II) compound. It standardizes a sodium thiosulfate solution and uses it to titrate the bleach to determine its available chlorine content. Two bleach samples are tested and the average chlorine content is calculated. The copper compound is also tested by titrating with sodium thiosulfate to identify the unknown compound and calculate its copper percentage. Key results and identification of the copper compound are summarized.

Uploaded by

fiza
Copyright
© © All Rights Reserved
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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Exp.

6: Analysis of bleach and copper(II) unknown

Abstract:

Introduction:

Objective:

Methodology

Results
A. Standardisation of Sodium Thiosulphate Solution
1 2
Final reading of thiosulphate 34.50 31.10
solution (ml)
Initial reading of thiosulphate 4.60 1.40
solution (ml)
Volume of thiosulphate solution
(mL)

B. Analysis of Bleach
Brand of Bleach 1: Dobi
a. Molarity of Na2S2O3 solution: 0.0336 M
b. Mass of volumetric flask + l0 mL bleach: 68.8924 g
c. Mass of volumetric flask: 58.2794 g
d. Mass of l0 mL bleach: ________ g
e. Density of bleach = ________ g/ml

Sample 1 Sample 2
Final reading of thiosulphate solution (ml) 3.90 4.00
Initial reading of thiosulphate solution (ml) 0.00 0.00
Volume of thiosulphate solution (ml)
Moles of Na2S2O3
Moles of NaCIO in l0 mL aliquot
Moles of NaCIO in 10 mL aliquot
Moles of NaClO in 10 mL bleach sample
Average moles of NaClO in l0 mL bleach
sample
Gram/L of NaCIO in bleach
Mass percent of NaCIO in bleach
Mass percent of NaCIO from >5.25%
manufacturer's label
Percent deviation between experimental
and label values

C. Analysis of Copper(II) Unknown


Sample 1 Sample 2
Mass of copper(II) compound taken (g) 0.3001 0.3252
Final reading of Na2S2O3 solution (mL) 23.20 34.40
Initial reading of Na2S2O3 solution (mL) 10.60 21.70
Volume of Na2S2O3 solution used (mL
Moles of Na2S2O3
Moles of Cu2+
Gram of Cu2+
Weight percent of copper in sample taken
Average weight percent of copper in
sample
Theoretical mass percent of copper in
sample
Percent error
Name of unknown copper(II) unknown
Chemical formula of copper(II) unknown

Calculation
Discussion
Conclusion
References

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