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Indian Standard
CHOICE OF GROUTING ,MATERIALS FOR
ALLUVIAL GROUTING - GUIDELINES
ICS 91.100
0 BIS 1996
A,vril 1996
Foundation and Substructures Sectional Committee, RVD 8
FOREWORD
This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the
Foundation and Substructures Sectional Committee had been approved by the River Valley Division
Council.
Grouting in alluvial soils can be resorted to as a temporq measure in case of stabilising the foundation
soil of-any adjoining building during excavation for foundation; and as a permanent measure like stopping
seepage through foundation of a clam. Before commencing any grouting project, it is essential that full
consideration be given to all available grouting materials, in order to choose the most appropriate
materials for a particular application. From a practical point of view grouta are usually divided into two
broad groups namely particulate grouts (suspensions) and non-particulate srouts (solutions). This
division is important in grouting, since the presence of solid particles in a grout immediately places an
absolute limit on the type of ground which the grout can effectively permeate. In other words the pore
size in alluvium must be sufficiently large for the solid particles to pass through.
For the purpose of deciding whether a particular requirement of this standard is complied with, the final
value, observed or calculated, expressins the result of a test or analysis,shall be rounded off in accordance
with IS 2 : 1960 ‘Rules for rounding off numerical values (~eljised)‘. The number of significant -places
retained in the rounded off value should be the same as that of the specified value in this standard.
AMENDMENT NO.1 MARCH 2011
TO
IS 14343 : 1996 CHOICE OF GROUTING MATERIALS FOR ALLUVIAL
GROUTING - GUIDELINES
(Page I, clause 3, line 6) - Substitute 'non-particulate (see 6)' for 'chemical (see 6)'.
PERMEABILITY GROUTABILITY
K = less than 10.6 em/sec Ungroutable
Groutable with difficulty by grouts having viscosity lower than 5
K= 10-6 em/sec to less than 10.5 em/sec
cP and ungroutable at higher viscosities
Groutable with low viscosity grouts but with difficulty when
K= 10.5 em/sec to less than 10.3 em/sec
viscosity is greater than 10 cP
K = 10.3 em/sec to less than 10. 1 em/sec Groutable with all commonly used chemical grouts
Groutable with suspended solids grout or chemical grout with
K = 10. 1 em/sec or more
filler
(Page 4, Table 2, col heading 3) - Substitute 'Optimum Dosage (percentage by weight of cement)' for
'Optimum Dosage (pe~centage by weight)'
(Page 5, clause 6.3, para 5, line 5) - Substitute' A newly made silica gel will, upon standing, exude
water and shrink and this process is called synersis.' for' A newly made silica gel will, upon standing, exude
water and shrink. '
(Page 6, clause 6.4.2, Title) - Substitute 'Lignosulfonate Grouts' for 'Lingnosulfonate Grouts'.
(Page 8, clause 6.6.2.2, line 4) - Substitute 'Materials which are highly sensitive, cause difficulty in
handling. Prior knowledge of sensitivity of chemical grout to particular pH is useful. If not, trial experiments
should be conducted.' for 'Materials which are highly sensitive cause difficulty in handling.'
(WRD 8)
Indian Standard
CHOICE OF GROUTING MATERIALS FOR
ALLUVIAL GROUTING - GUIDELINES
1 SCOPE IS No. Title
12584 : 1989 Specification for bentonite for
1.1 This standard lays down guidelines to cover
grouting in civil engineering
primarily both suspension and solution grouts with works
particular reference to alluvial grouting. Under
suspension grouts, grout materials like cement, 3 GENERAL
clays, bentonite, flyash, etc, are covered, whereas
under solution grouts, chemical grout materials are Grout materials can be broadly classified into two
covered. groups:
1.2 This standard does not cover compaction a) Particulate grouts, and
grouting or grouting for reducing compressibility b) Non-particulate grouts.
of soil which is excluded from the scope of this
The functional difference between particulate
standard.
(see 5) and chemical (see 6) grouts is that the
2 REFERENCES penetrability of the former is a function of particle
size, while in the latter, it is a function of solution
The Indian Standards listed below are necessary viscosities.
adjuncts to this standard: Suspension grouts actually require a small quantity
IS No. Title of water for gellificatiomhydration. However, in
269 : 1989 Specification for 33 grade or- order to increase their flowability, a high propor-
dinary portland cement (fourr!r tion of water is added initially. Most of this excess
revision) water is separated during passage of grout through
383 : 1970 Specification for coarse and fine voids. In solution grouts, on the other hand, the
aggregates from natural sources final water solid ratio is same as the initial.
for concrete
4 CI-IOICE OF A GROUT MATERIAL
1344 : 1981 Specification for calcined clay
pozzolana 4.1 Selection of grout materials involves a balance
1489 Specification for portland between various desirable characteristics of grout
(Part 1) : 1991 pozzolana cement: Part 1 Fly ash materials ai well as requirement of groul slurries
based (third revision) such as particle size, viscosity, gellification lime, gel
1489 Specification for portland poz- strength, stability and permanence coupled with
(Part 2) : 1991 zolana cement: Part 2 Calcined economy. Grout solutions should be non-toxic,
clay based (z/md revision) non-corrosive and non-exploding.
1892 : 1979 Code of practice for sub surface 4.2 Choice of grouting materials and mixtures for
investigations for foundations appropriate field conditions are given in IS 4999 :
(first revision) 1991. Permeability is the soil property most closely
3812 : 1981 Specification for fly ash for use as related to groutability. The general relationship
pozzolana and admixtures (first between these two factors is shown in Table 1.
revision)
4999 : 1991 Recommendations for grouting 5 PARTICULATE GROUTS
of pervious soils (first revision)
5.0 Particulate grouts are suspensions or multi-
5529 Code of practice for in-situ per- phase systems capable of forming subsystems after
(Part 1) : 1985 meability test: Part 1 Test in over- being subjected to natural sieving processes, with
burden chemical properties which must be carefully
11293 Guidelines for the design of grout scrutinized so as to ensure that they do not militate
(Part 1) : 1985 curtains: Part 1 Earth and Rock- against controlled properties of setting or strength.
fill dams
1
IS 14343 : 1996
2
IS 14343 : 1996
EL.BOW PI
id-+ 20 PIPE
3
IS 14343: 1996
5.2 Characteristics of Grout Slurries viscosity to be easily pumped, but not so low as to
travel undesirably long distances without appreci-
Grout slurry should have good penetrability (which
able pressure drop. Viscosity of a grout can be
is based on particle size of grout materials), high
measured in laboratory by a rotational~viscometer.
fluidity, stability, controllable gellification time and
However, this type of instrument is not commonly
high set strength.
used. Therefore some form of funnel viscosity is
5.2.1 Penetrability is the property of the grout usually preferred for giving information about
which mostly controls the selection of a particular fluidity of the grout slurry. A description of meab-
grout for treatment of soil. Penetrabilityofa grout urement of lluidity by Marsh Funnel Test is given
depends mainly on the average particle size of the in Annex A. The Marsh Funnel Test is a good
grout material and the average size of openings in indicator of true viscosity of the grout slurry, it is
the soil. While average particle size of a grout also an important index property for quality control
material can easily be ascertained and controlled, it of field mixes.
is difficult to ascertain the size of average openings
52.3 Stnbiliry
in the alluvium to be treated. Some estimation of
the average opening in the soil can be had from A stable mix will generally maintain its charac-
ilkhi permeability test and grain size curve of soil. teristics during pumping, penetration and final gel-
From these Dis of the soil can be _judged. - As an lification.
Drs (soil)
initial guide should be kept more than Stability of a grout suspension is commonly deter-
Dss (grout) mined by a bleeding (or sedimentation) test. A
25. This will ensure ‘reasonable penetration of stable mix is taken as one having less than 5 percent
grout into the soil to be treated. Table 1 should be bleeding.
referred to for selection of grout on the basis of
permeability. The stability criteria is not applicable to cement
and other cement grouts which would have a
52.2 Viscosity
water/solid ratio considerably smaller than the
Once the grout materials are selected for a par- initial value after deposition and setting.
ticular grouting project based on particle size re-
quirement, the next stage is to decide the
proportion of these materials in the grout mix, such A fundamentvl requirement of a grout is that it
that the resulting grout slurry has sufficiently low shall develop adequate gel strength after a control-
4
IS 14343 : 1996
6.4.1 Aclylamide Grouts dehyde and an alkaline base. All three components
A acrylamide grouts consist of a mixture of two are health hazardi and potential environmental
organic monomers, acrylamide (or methanol pollutants. Gels formed are generally inert (non-
acrylamide, methacrylcyanide) and meththylene toxic and non-caustic).
bis-acrylamide, a cross linking agent. The other 6.4.4 Polyurethane Grouts
activators used are TEA (Triethanolamine) and
Polyurethanes are plastics that are used in a wide
DMAPN (Dimethyl amino propionate). The
range of fields as hard or elastic, and unfoamed or
acrylamide grouts are considered to be an ideal
foamed materials. Polyurethanes are formed by the
grout. They can penetrate more readily, mdintain
reaction of two components namely
constant viscosity during the induction period and
polyisocyanates and polyalcohols or with other
have better gel time control and adequate strength
chemicals such as polyethers, polyesters and
for most applications. Acrylamide grouts are more
glycols, which have hydroxyl groups.
costly than silicate grouts and are neurotoxic. The
stiffness of the grouts can be changed by changing The catalysts used are tertiaryamines and tin salts
the acrylamide to methylene ratio. The values of may be used to control the reaction rate. Surface
unconfined compression (UC) and Young’s active agents are used to control bubble size. The
Modulus increase with the increase in percentage foam structure itself is produced by a blowing agent
of methylene bis-acrylamide from 3 to 10. Grout reacting chemically to produce carbon dioxide.
solution with up to 20 percent solids have vis- 6.4.5 Antinoplasts or Urea Resins
cosities well under 2 cP. The gels are considered
The major ingredients of this type of grout are urea
permanent. The minimum concentration of grout
and formaldehyde. In addition to urea, melamine,
from which a gel will form is temperature dependent.
ethjllene and propylene urea, aniline and other
6.4.2 Lingnosulfonate Grouts chemically related materials can be used. These
Lignosulfonates are thewaste liquor by-products of grouts will set only in acidic conditions, therefore,
the wood processing industries. Lignosulfonate they should be used only when it is known that
-grouts consists of lignosulfonate and a hexavalent ground and groundwater pH is below 7. Urea for-
chromium compound. Generally calcium lignosul- maldehyde grouts have viscosities between 10 and
fonate is used with sodium dichromate. Initial vis- 20 cP. Soils stabilised by these grouts have
cosity varies from 3 to 8 cP. The strength of the soils strengths comparable to the phenoplasts. The
grouted with lignosulfonates is of the same order grout is toxic and corrosive. However the gel is
of magnitude, but somewhat less, than that of inert.
acrylamide grouts. Since lignosulfonales are by- 6.5 Other Chemical Grouts
products of other processes, they are relatively
It is possible, to a certain extent, to combine two
cheaper and can compete on cost basis with any
available grouts so as to simultaneously ob,tain the
other chemical grout. Lignosulphonates are con-
optimum properties of each. To do so the materials
sidered to be permanent materials. However, they
must be chemically compatible. The silicates and
are toxic and should be handled with care.
the actylamides can be used together. Polyesters
6.4.3 Phenopfasts and epoxies have been used to anchor rock rein-
Phenoplasts are polycondensates resulting from forcement in drilled holes
the reaction of a phenol or aldehyde. Mostly resor- 6.6 Grout properties
cinol and formaldehyde are used and sodium
Grout properties which are of importance may be
hydroxide is used as a catalyst. The only control of
broadly classified as given in 6.6.1 to 6.6.3.
setting time is the dilution of grout components.
Setting time varies greatly with solutionpH, being 6.6.1 Mechanical Properties
shortest for any given grout concentration at apH 6.6.1.1 Permanence
slightly above 9. Initial viscosities of resorcinol- All grouts which contain water not chemically
formaldehyde grouts range from 1.5 to 3 CP for bound to the grout particles, are prone to mechani-
concentrations normally used for field work. The cal deterioration if subjected to alternate freeze-
viscosity remains constant at those low~levels until thaw and/or wet-dry cycles. The rate of such
gellation starts. Thestrength ofsoil grouted by this deterioration varies with the amount of free water
grout is comparable to high concentration silicates. available in the grout as well as with the dcgrcc of
The strength of soils stabilised by resorcinol for- drying or freezing. Chemical deterioration of
maldehyde grout is directly proportional to the grouts can occur if the grouts react with the soil or
resin content. Resistance to wet-dry cycles is poor groundwatcr, or if the grout itself is soluble in
and can lead to complete disintegration. groundwater or if the reaction products, which
Phenoplasts always contain a phenol, formal- form the grout, are inherently unstable.
6
IS 14343 : 1996
AMINOPLAS1S
I kOMP$;SSE
FIG. ZA PENETRABILITY
OF VARIOUSGROUTS
FIG. 2B EFFECTIVE
RANGEOF GROUNI?WATER CONTROLMEASURES
GROUTS
SANDCEMENTS __
I
PFNCEMENIS c~--.m---- --c---c
CEMENTS
CEMENTSCLAYS
CEUENTISENTCUITES
SENTONITUCEMENTS
_SENTONlTEX.HEMlCAL C----.--w
HIGH CYNCENTRATIQN SblCATES
LOW CCiNCEIJTRATIONSILICATES
CLAR,FIEDSILlCATES ,--- c) -..*
PHENOX RESINS
LlGN!NS
CLARIFIEDUGNINS
ACRYLAMIDES C---c)---)
AMINOPLASTS
PCLYURETWNE
FIG. 2C INDICATIVE
RANGEOF GROUNDWATERTREATMENT
7
1s 14343 : 1996
AND F!OLYACRYLAMIDE
1
NTS
TES
ACRYLAMIDE
t,
1 0.1 0.01 0.1
GRAIN IN SIZE mm
FIG.~D GROUTPENETRABILITY
B
z
II
5 50
20
10
ANNEX A
(Chse 5.2.2)
DESCRIPTION OF MARSH FUNNEL AND METHOD FOR DETERMINATION OF FLUIDITY OF
GROUT SLURRY
A-l DESCRIPTION OF MARSII FUNNEL Record the time taken for 1000 cc of the slurry to
pass through the funnel into the measuring
A Marsh Funnel as shown in Fig. 3 has a diameter cylinder. The result to the nearest second is the
of 150 mm at the top and a height of 300 mm, the Marsh funnel viscosity. For clear water at 21°C the
bottom orifice’outlet has an inside diameter of Marsh funnel viscosity is 27 seconds. For grout
about 5 mm. The top of the cone has a screen with slurries, the Marsh funnel viscosity has a good
1.5 mm openings, for screening out lumps of poorly relationship with viscosity in centipoise deter-
mixed slurry. mined by a rotational viscometer. The relationship
A-2 METHOD is nearly straight line~in the range of 30-40 seconds.
This can be developed for each individual grout
Pour 2 000 cc of slurry into the funnel. mix.
I 4I \ -f -- -1 - - CONE
Y
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This Indian Standard has been developed from Dot : No. RVD 8 ( 14 ).
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