Refinery Process
Refinery Process
Refinery Process
Petroleum Corporation Limited
(A Group company of IndianOil)
Slide 1
PRESENTATION PLAN
REFINERY PROCESSES
REFINERY CONFIGURATION
Slide 2
REFINERY PROCESS - Overview
SEPARATION PROCESS
CONVERSION PROCESS
FINISHING
Slide 3
REFINERY PROCESSING STEPS
Slide 4
SEPARATION PROCESS
Slide 5
DISTILLATION COLUMN
Slide 6
DISTILLATION PRINCIPLE
Slide 7
DEW POINT , BUBBLE POINT AND RELATIVE VOLATILITY
Slide 8
MAIN COMPONENTS OF DISTILLATION
Column
Column internals
Trays
Packing
Reboiler
Condenser
Reflux Drum
Slide 9
OPERATING VARIABLES
• Temperature
• Pressure
• Pump around
Slide 10
CRUDE- FEED PREPARATION
Impurities in crude:
– Inorganic salts
– Acids
Slide 11
PREHEAT TRAINS & FURNACE
Pre-heat trains:
Furnace:
– Natural draft
– Forced Draft
– Balanced Draft
Slide 12
ATMOSPHERIC DISTILLATION
Slide 13
VACUUM DISTILLATION
Slide 14
VACUUM DISTILLATION
Slide 15
CRUDE DESALTER
Slide 16
CRUDE FURNACE
Slide 17
CRUDE ATMOSPHERIC COLUMN
Slide 18
Lube Oil Base Stocks
• SPINDLE
• LIGHT NEUTRAL
• INTERMEDIATE NEUTRAL
• 500 NEUTRAL
• HEAVY NEUTRAL
• BRIGHT STOCK
Slide 19
LUBE PROPERTIES
Slide 20
LUBE PROCESSING STAGES
Slide 21
LUBE PROCESSING BLOCK
Crude Furfural
Atm. Distl
Column Extraction
Unit
MEK Lube
Extract Raffinate DWO LOBS
Dewax HyFi
RCO
Unit Unit
NMP
Vac. Distl Extraction
Vacuum
Unit
Distillatn
Column
DAO
Extract Slack Wax
Vac.
PDA
Residue Unit Pitch
Slide 22
WAX PROCESSING
INERT GAS
NH3
REFRIGERATION
SOLVENT
RECOVERY HY.FI PRODUCT
FILTERS UNIT
FROM WAX STORAGE
FEED CHILLING
DEOILED WAX
STORAGE
SOLVENT
RECOVERY
FROM
FOOTS OIL FOOTS OIL
Slide 23
CONVERSION AND TREATING PROCESS
Slide 24
CONVERSION AND TREATING PROCESS
•Conversion Process:
Thermal processes
Catalytic processes
•Treating Process
Catalytic processes
Slide 25
THERMAL (VISBREAKER UNIT)
Mild thermal decomposition (vis‐breaking)
Reduction of viscosity & pour point of feed
Desirable Reaction – Cracking
Some polymerization condensation reaction also occurs–
Coke formation
Slide 26
THERMAL (VISBREAKER UNIT)
0.95 kg/cm2 GAS
160˚ c
GAS
96˚ c 9.8 kg/cm2
39
26 210˚ c STAB NAPHTHA
Stabiliser
GO
STEAM
130˚ c
426˚ c 25 mmhg GAS + SLOPS
7.7 kg/cm2
LVGO
VISBREAKER
STEAM
440˚ c
FEED VACUUM
300˚ c FLASHED
FRACTIONATOR CRACKED
HEATER SOAKER VACUUM RESIDUE
FLASHER Slide 27
(Thermal) Delayed coking
Slide 28
CATALYTIC (REACTORS)
Reactor Design
Better performance and operational flexibility can be
achieved:
–Choice of catalyst
–Choice of feed
–Operating conditions
–Reactor configuration
–Better internals
Slide 29
REACTOR INTERNALS
Inlet nozzle
Distributor nozzle
Debris basket
Alumina Catalyst
balls
Catalyst unloading
nozzle
Outlet nozzle Screen Slide 30
REACTOR INTERNALS
Inlet nozzle
Distributor nozzle
Debris basket
Alumina Catalyst
balls
Quench
Catalyst
Catalyst unloading
nozzle
Outlet nozzle Screen Slide 31
CATALYTIC REFORMING
CHEMISTRY:
• De‐hydrogenation
• Isomerisation
• De‐hydro‐ cyclization
• Hydro‐cracking
Slide 32
CATALYTIC REFORMING
DEHYDROGENATION:
C7H14 ‐‐‐> C7H8 + 3H2
Methylcyclo hexane Toluene
Slide 33
CATALYTIC REFORMING
ISOMERISATION:
Naphthene Naphthene Aromatic
C + 3H2
Slide 34
CATALYTIC REFORMING
DEHYDROCYCLISATION:
Aromatic
Paraffin
C
-C-C-C-C-C-C-C- + 3H2
n-Heptane Toluene
RON 0.0 119.7
•Reaction is Endothermic
Slide 35
Naphtha Hydrotreating & Cat. Reforming
Naphtha
Impurities: S,N,
Metals Naphtha
Hydrotreating
Hydro treated
Risk of poisoning
Naphtha
CCR catalyst
Impurities:
Nil or low
No Risk of
poisoning
CCR catalyst
Reformate
High Octane
Low octane
Number: 102
number
Continuous
Catalytic
Reforming
Hydrogen
Rich gas
Slide 36
NHT CCR
Slide 37
CCR REACTOR-REGENERATOR
Slide 38
NHT ISOM
Slide 39
NHT ISOM
R2
R1 F1
Recycled H2
Diene Reactor
C1 C2
HDS Reactor
K2 A/B To R1
Feed NHDT C4
Surge Drum
Feed Heater Separator
Naphtha
NHDT Stripper
H2 Dryer
C13
R4 R3
Second Isomerization
K1A/B C17
Isomerization
C16
Reactor
Reactor
First
Feed Dryer
Splitter
C19
Light Isomerate
Storage
Stabilizer
Isom
Deisohexanizer
LPG Product
C22 To FCC
C5/C7+ Cut
LPG Separator
LPG Stripper
C29 C30
Heavy Isomerate
To Isomerate Storage
Slide 40
HYDROCRACKER BLOCK
Reaction Chemistry
• Hydro-treating Reactions
a) Demetallization
b) Desulfurization
c) Denitrification
d) Olefins Saturation
e) Aromatics Saturation
• Hydrocracking Reactions
Catalyst (Ni3S2)
CnH2n+2 + (x-1) H2 x C n/xH2n/x +2 + Heat
Slide 41
HYDROCRACKER
Quench Make-up H2
H2 Gas compressor
Recycle gas
Off-gas to PSA
Feed (for
VGO preheating Reactors HP H2 recovery)
feed and Furnace
172.5 Kg/cm2
filtration gas separator
3780C
LP
Liquid hydrocarbon gas separator
Heavier
hydrocarbons Kerosene / ATF
3600C
Furnace Fractionator
Diesel..
Slide 43
Products to
Main Column
FLUID CATALYTIC CRACKING UNIT
Reactor
Flue 500°C
Gas
680°C Flue Gas
Slide Valve
Stripping
Steam
Regenerator
650°C
Spent Catalyst
Slide Valve
Air
43000 Regenerated Catalyst
Raw OiL
nm3/hr Slide Valve
120 m3/hr
Catalyst circulation
370°C
10 MT/min
Slide 44
FINISHING PROCESS
Slide 45
DHDT UNIT (Hydrodesulphurization)
Slide 46
DHDT REACTOR
Reactor Dimensions
Height, m 31.3
Width, m 4.4
Slide 47
SULFUR RECOVERY UNIT
Chemical Reactions
Step 1:
H2S + 1 ½ O2 → SO2 + H2O + Heat
Step 2:
2H2S + SO2 → 3/n Sn + 2 H2O + Heat
Slide 48
Sulphur Recovery Block
Acid Gas
Amine
rich amine from
Lean amine Regn.
process units
(ARU)
Thermal
Sulphur Recovery Unit
Catalytic
Converters 2-stage Sour water from
SWS process units
Unit
Sulphur
stripped
water
Slide 49
CPCL SRU
Slide 50
PRESENTATION PLAN
1. REFINERY PROCESSES
2. REFINERY CONFIGURATION
Slide 51
Refinery Configuration
Key Considerations & Available Options
Slide 52
A TYPICAL REFINERY CONFIGURATION
Ref. Fuel
GAS Gas System LPG
Amine
Treating
CRUDE Amine Sulphur PROPYLENE
OIL LPG Amine/ Merox Regeneration Recovery PBFS/ MEKFS
STORAGE
Treating
HEXANE
NHT/ ISOM Isomerate
LT. NAP Naphtha Naphtha (45‐90 C) H2
Hexane Plant MS
Atmospheric
Distillation
Splitter
Hydrogen (H2)
Hydrogen
Generation NAPHTHA
Naphtha (90 ‐130C)
HY. NAP Catalytic Reformate
Reforming
ATF
ATF ATF Treating
SK
Diesel SK
DHDS/ DHDT
Long
H2 DIESEL
Residue LUBE Distillates
Extraction Dewaxing Lube HDT
LUBE OIL
Wax Deoiling & Wax Hydro finishing BASE STOCKS
VGO PARAFFIN
Distillation
Hydrocracker WAX
Vacuum
VB VGO/ HCGO
LCGO / VB Gas Oil
Coker Naphtha
LCO/ HCO
VB Naphtha
LPG Propylene FO
Treating Recovery
UCO
FCCU ASPHALT
Cracked
Merox Treating Gasoline
LPG
Short SULPHUR
Residue Visbreaking
Biturox Unit
Delayed Coking COKE
Slide 54
Global Oil Outlook
Slide 55
India - Net Oil Import Dependence
Slide 56
Projects Classification
Slide 57
Drivers for New Projects Identification
• Supply – Demand Balance
Slide 59
Stringent Product Specifications
GASOLINE Euro-III Euro-IV Euro-V
Sulphur, ppm 500 150 50 10
RON, min 88 91 91 95
MON, min - 81 81 85
RVP (max), Kpa 60 60 60 60
Benzene (max), vol% 5/3 1 1 1
Aromatics (max), vol% - 42 35 35
Olefins (max), vol% 21 21 18
• Capacity Expansion
Slide 61
Crude Feed Selection
Heavy Crudes
Slide 62
Trend in Crude Processing
Heavy/Sour Crudes
• Marker Crude Dubai rose higher than Brent in Dec ‘08 due to
– Rise in demand for sour crude
– OPEC production cuts, etc.
Slide 65
Types of Refineries
• Topping Refinery
• Skimming Refinery
• Coking refinery
• Integrated Refinery
• Lube Refinery
Slide 66
Processing Units in Oil Refineries
Slide 67
BORL Configuration, Bina, M.P
Slide 68
Refinery Configurations
Cases Studied
S.No SECONDARY UNITS RESID UNITS
1 VGO HDT + Petro‐FCC DCU
2 OHCU + Conv‐FCC DCU
3 Full Conv. HCU + DHT (Integrated) DCU
4 VGO HDT + Petro‐FCC SDA + Slurry HCU
(50% DAO)
5 OHCU + Petro‐FCC SDA + Slurry HCU
(50% DAO)
6 Full Conversion HCU SDA + Slurry HCU
(50% DAO)
7 Conventional FCC DCU
8 Full conversion HCU DCU
9 VGO HDT + Petro‐FCC SDA + Slurry HCU
(60% DAO)
10 OHCU + Petro‐FCC SDA + Slurry HCU
(60% DAO)
11 Full conversion HCU SDA + Slurry HCU
(60% DAO)
Slide 69
Sample Block - VGO HT + PFCC + DCU
LPG
ALKYLATION
PPU
POLYPROPYL
ENE
NHT/CCR/ISOM
Euro IV
GASOLINE
CDU/
VDU
Euro V
GASOLINE
DHT
VGO
HDT
KERO
DCU Euro IV
GASOIL
Euro V
FCC‐PC GASOIL
FCC Nap.Splitter
BITUMEN
COKE
Slide 70
Sample Block - FC HCU + DHDT + Slurry HCU
LPG
ALKYLATION
NHT/CCR/ISOM
Euro IV
GASOLINE
CDU/
VDU
Euro V
GASOLINE
DHT
KERO
Euro IV
GASOIL
HCU Euro V
GASOIL
SDA Slurry
HCU BITUMEN
COKE
Slide 71
Refinery Power & Utilities
Slide 72
Slide 73
Refinery ‐ Integration Benefits
Processing
Supply Products Distribution
Treating
Environmental
Concerns
Asset
Utilization
Slide 74
Integration with Petrochemicals
Petrochemical Sector: 13% annual growth projected
Major Petrochemicals : Ethylene, Propylene, Butadiene, PVC, HDPE, BTX, etc.
Crude Oil
Slide 75
Integration with Petrochemicals
Cases Studied
Case-3: OHCU, DCU, AC and PC (in this case OHCU bottoms are
routed to Naphtha Cracker)
Slide 76
Integrated Refinery with Aromatics complex
HY.
CDU / FCCU / NAPHTHA HEAVY NAPHTHA
OHCU / DCU HDT REFORMER
CCR
SPLITTER
HY. REFORMATE
XYLENE FRACTIONATION UNIT
PARA XYLENE 800 TMT
XYLENE ISOMERISATION
PARA XYLENE SEPARATION
Slide 77
Integrated Refinery with Petrochemical Block
PART DIESEL
FROM DHDT
VGO ETHYLENE
Syn. Diesel/ HY. NAPHTHA
Vac. GASOILS /
DHDT CRACKER
Crk. GASOILS Naphtha
UNIT UNIT FCC OFF GAS
CPCL NAPHTHA
PROPYLENE
668 TMT
ETHYLENE
1200 TMTPA
SWING UNIT LLDPE / HDPE
362 TMT
MEG
MEG UNIT 700 TMT
DEG
135 TMT
Slide 78
FCC Unit with Petrochemical Block
FCCU PC
POLY
PROPYLENE PROPYLENE POLY PROPYLENE
RECOVERY UNIT PROPYLENE UNIT
432 TMT 1120 TMT
CRACKED LPG
PROPYLENE EX-
CRACKER
668 TMT
Slide 79 of 64
Slide 79
Refinery – Power Integration
Gasification: A commercially proven process that converts
hydrocarbons such as heavy oil / petroleum coke, and coal into
hydrogen and carbon monoxide (synthesis gas).
4 CH + 2 H2O + O2 4 H2 + 4 CO
(Fuel) (Water) (Oxygen) (Hydrogen) (Carbon Monoxide)
“Syngas”
Gasification Technology
Slide 80
Gasification – Multiple Segment
Options
Fuels by F-T
Synthesis
Power
PetCoke/ Syngas
Hydrogen /
Coal Power / Steam
Sulphur
Chemicals
SNG thru’
Slag
Methanation
Slide 81
Refinery – Power Integration
Coke from Coker Unit can be Gasified to produce Syngas & Power / Hydrogen
Slide 82
Project – Execution Methodology
Phase-I Phase-II
Conceptualization of Project Project Completion
Pre-Commissioning &
Licensor Selection Commissioning stage
P&ID REVIEW
ENGINEERING KICKOFF
FLUSHING/
HAZOP & 3D MODELING LEAK TEST
P&ID
ORDERING/FABRICATION CHECK/INERTING
1ST DRYOUT
ERECTION/CONSTRUCTION
CAT. LOADING
2ND DRYOUT
P&ID CHECK/INSPECTION
FINAL INERTING
PRE-COMMISSIONING
FEED CUT-IN
Slide 84
Parameters Studied during the Project Evaluation
• Economic Feasibility
• Capex & Opex of projects
• Yield of Distillates
• Refinery Margins
• Plot Plan Availability
• Financial Appraisal
• Net present value
• Internal Rate of Return
Slide 85
Financial Appraisal
• Financing Assumptions
• D/E ratio, interest rate, repayment tenor, moratorium period, etc.
• Macro-economic assumptions
Slide 86
PRESENTATION PLAN
1. REFINERY PROCESSES
2. REFINERY CONFIGURATION
Slide 87
PROJECT DESIGN ASPECTS
Slide 88
Design Aspects
• Vacuum Design
• Instrumentation Philosophy
Slide 89
Codes & Standards
BIS Bureau of Indian standards
• API Standards
• Designed to help users improve the efficiency and cost-effectiveness
of their operations
• (e.g.) API 610 : centrifugal pumps
• (e.g.) API 682 : mechanical seals
• (e.g.) API 6D : Pipeline Valves
• (e.g.) API 560 : Fired Heaters
• (e.g.) API 616 : Gas Turbines
• (e.g.) API 617, 618 : Compressors
Slide 91
Other Codes & Standards…contd.
• IS (Indian Standard) Codes
• For civil works and construction
• (e.g.) IS-456 for Plain & Reinforced Concrete
• TEMA Standards
• For Heat Exchangers
Slide 92
Meteorological Design Data
Sl# Parameter Minimum Normal / Maximum /
Average Design
(A) METEOROLOGICAL DATA
1 Elevation above mean sea level, m 3.5
2 Barometric pressure, mbar
3 Ambient temperature, °C tmin =18 tnor = 35 tmax =45
4 Relative humidity, % @ tmin @ tnor 80% @ tmax
5 Rainfall data (mm) (a) for 1-hour 100
period 450
6 Wind data (a) (b) wind
for 24-hour
velocityperiod 180 km/hr (as per
IS:875 Part-III).
(b) wind direction North East & South
West
(B) DATA FOR EQUIPMENT DESIGN
1 Design dry bulb temperature, °C 38
2 Design wet bulb temperature, °C 29
3 Low ambient temperature for MDMT, °C NA
4 Design air temperature for air cooled exchangers 40
where followed by water cooling, °C
5 Design air temperature for air cooled exchangers 42
where not followed by water cooling, °C
6 Coincident temperature and relative humidity for Air Blower / Air Compressor 80 % at 45 o C
design.
7 Min. Design temperature for equipment 65 o C
Slide 93
Plant Life
Slide 94
Utility Conditions @ Unit Battery Limits
Sl Parameter Minimum Normal Maximum Mech Design
1 VERY VERY HIGH PRESSURE (VVHP) STEAM
Pressure, kg/cm2g 90 95 95 104/FV
Temperature, oC 495 505 505 505
2 VERY HIGH PRESSURE (VHP) STEAM
Pressure, kg/cm2g 44.8 48 54.9 58.0/FV
oC
Temperature, 379 425 435 440
3 HIGH PRESSURE (HP) STEAM
Pressure, kg/cm2g 29.5 30.5 32.5 36.0/FV
Temperature, oC 270 280 290 300
4 MEDIUM PRESSURE (MP) STEAM
Pressure, kg/cm2g 9.5 10.5 12.5 15.0/FV
oC
Temperature, 200 220 240 280
5 LOW PRESSURE (LP) STEAM
Pressure, kg/cm2g 2.7 3.5 4.0 7.0/FV
Temperature, oC Saturated 170 190 240
6 CONDENSATE RETURN
Pressure, kg/cm2g 5.0 13
Temperature, oC 140-150 210
7 SERVICE WATER
2g
Pressure, kg/cm 6.0 10.5
Temperature, oC Amb. 65
8 COOLING WATER
2g
Supply Pressure, kg/cm 4.5 8.0
Return Pressure, kg/cm2g 2.5 8.0
oC
Supply Temperature, 33 65
Return Temperature, oC 45 65
9 DEMINERALISED WATER
Pressure, kg/cm2g 7.0 8.0 9.0 14..0
Temperature, oC Amb. Amb. Amb. 65
Slide 95
Utility Conditions @ Unit Battery Limits
Slide 96
WATER SYSTEMS
Backflush arrangement shall be provided for
All cooling water consumers
Only overhead condensers
Cooling water consumers with water line sizes greater than ” NB.
Back flush lines to be provided with same size as main cooling water line when main line size is ≤ 6”. One size lower to be provided for main
line size > 6” For much higher line sizes e.g 14” and above to be decided based on case to case basis
Slide 97
Water Quality
l Parameter Cooling Water Cooling Water DM BFW
make up ( from Water
TTP of ETP)
PH 7.2-7.5 7.2-7.7 6.8-7.2/8.3-8.5 8.5-9.5
Slide 100
Refinery Fuel Systems
Liquid fuel system for the project shall be one of the following.
No liquid fuel system applies to the project.
Existing liquid fuel system in Refinery III shall cater to the project,
After Augmentation, if required. Alternately, new liquid fuel system
shall be provided.
Fuel gas system for the project shall be one of the following.
No fuel gas system applies to the project.
Existing fuel gas system in Refinery III shall cater to the project,
After Augmentation, if required.
New fuel gas system for the total project:
(a) Integrated to existing facility
(b) Independent of existing facility
Slide 101
Fuel Systems
Burner turndown requirements have to be met at liquid fuel pressures at burner
not less than the normal anticipated return header pressure. The fuel oil system
shall be designed for a recirculation rate of 2:1.
Fuel gas liquid knockout drums and tracing for piping shall be separate for
each process unit.
In-line strainers in burner piping are recommended for each unit. These shall
be located not more than 20 meters upstream of the burner manifold and shall
be 1 on-line + 1 spare strainer with mesh sizes 100 for Fuel Oil, Fuel Gas and
atomising steam.
Hot liquid fuel temperature shall be assumed to drop by 5oC between unit
battery limits and burner manifold.
Slide 102
Fuel Oil Specifications
Sl Parameter Case-1 Case-2 Case-3 (Note-C)
1 Name PG VR BH UCO+VR
VR+VAC.DIESEL
2 Crude stock
3 Density @ 15oC, kg/m3 930 - 1030 978 852-857
4 Sulfur content, wt% 4 (Note-1) 0.84 0.27
5 Nitrogen content, wppm 3700 1000 (max.) 300
6 Nickel content, wppm 18 3
7 Vanadium content, wppm 200 5 11
8 Sodium content, wppm 80 12
9 Copper content, wppm <1
10 Iron content, wppm 1.9
11 Water content, wppm traces*
12 Flash Point, oC 66 (min)
13 Pour Point, oC 66
14 Viscosity @ 50 oC, cst 7500 5.0 @ 80 oC
15 Viscosity @ 100 oC, cst 700 900 @ 90 oC 3.36
16 Viscosity @ 200 oC , cst 50 @ 120 oC
17 Temperature, oC required for 20 cst
Slide 103
Fuel Gas Specifications
COMPONENT Case A Case B Case C Case D Case E Case F Case G
MOLE % Max FG
Normal Refinery Start
production
Operation up case
H2O 0.81 0.13 1.29 0.43 0.31 0.69
Slide 104
Refinery Flare system
Flare systems for the project shall be:
Existing Refinery flare system will be used, if found adequate.
Alternately, new flare header shall be provided for the project.
Single flare for all released streams
Normal flare for hydrocarbons and Acid gas flare for released acid gases
Separate high-pressure flare header for flared hot, hydrogen rich
gases
Hydrocarbon drain from the Flare K.O. drum will be routed by gravity flow
to the CBD. In addition, pump-out facility will be provided for
the Flare K.O. drum.
For adherence to OISD standard # 106, individual units shall be provided with a flare
knock-out drum whenever significant liquid relief is anticipated from the pressure
relieving devices, apart from the main knock-out drums at the flare stack. Unit
designer / contractor shall specify a horizontal unit flare KOD, sized to separate out
liquid droplets down to a size of 400 μ.
Slide 105
Refinery Flare system
Maximum flare backpressure shall be considered for sizing of pressure
relief devices
# Flare system Built- up back Superimposed back Built-up back pressure
pressure, pressure at unit at PSV outlet,
kg/cm2g battery limits, kg/cm2g
kg/cm2g
1 Normal flare 0.2 default = 1.5 default = 1.7
2 Acid Gas flare 0.2 default = 0.5 default = 0.7
3 High Pressure flare
Slide 106
Liquid Pumpout & Drain Systems
Non-congealing hydrocarbon drains:
Buried Closed Blowdown drum shall be:
Standard size of ± 10m3 to cater to only residual drains.
Individually sized for each unit for single largest equipment inventory.
Provided with cooling coil
Connect equipment to closed blow down (CBD) network leading to a CBD drum.
CBD drum will be located in a pit
and the same will be sand filled. Design CBD system for 200oC.
Congealing hydrocarbon drains:
Combined with non-congealing hydrocarbon drains.
Provided with combined cooling and heating coil
Slide 107
Liquid Pumpout & Drain Systems
Acidic drains:
(a) Amine systems
Bulk amine drains shall be only lean amine, displaced to amine storage tank. All
rich amine streams shall be routed to amine regeneration section under own pressure
or under inert gas pressure or displaced with water.
Residual amine drains shall be connected to a buried amine closed blowdown
system located in the Amine Regeneration section. Amine-bearing drains from Amine
Wash sections shall be routed to this buried vessel or collected through temporary
facilities.
Individual units handling amine will be provided with separate buried amine
closed blowdown system from where amine stream will be pumped to regeneration
unit.
Slide 108
FLUSHING OIL SYSTEMS
P, T, oC P, kg/cm2g T, oC
kg/cm2g
1. Flushing Oil (Gas Oil) 6.0-16.0 40-103 27.0 141
2. Heavy Flushing Oil (VGO) 4.0-6.0 70-80 27.0 100
Slide 109
Energy integration
Improvement in overall energy efficiency shall call for unit-level and total plant-level
optimization of energy. Designer of a particular unit shall indicate the following at
the outset of design activities:
(a)The total energy consumption expressed as equivalent fuel oil (Btu/bbl or FOE
(b)The preferred temperatures for hot feeds and products from an energy
(c)integration standpoint, if these are significantly different from that stipulated in
unit BEDB.
(c)Energy shall be preferentially recovered into process streams. Steam generation
shall be considered thereafter to recover excess available energy. Steam
generation levels shall be chosen to preferably match the corresponding steam
level demand within unit.
(d) Low-level energy recoverable for external consumption, say, for Boiler Feed
Water preheat serving other units.
Slide 110
Vacuum Design
Vacuum design conditions are not to be specified for the eventuality of blocking
in after equipment steam-out or operator maloperation.
Slide 111
EQUIPMENT DESIGN PHILOSOPHY
%turnup %turndown
Process Towers (atmospheric or above) 10%
Process Towers (vacuum) 10%
Fired Heaters (potentially coking services) 15%*
Equipment and piping systems shall be designed for the most stringent
coincident temperature and pressure conditions, accommodating the maximum
expected working pressure and temperature without causing a relieving
condition
Vessels operating under vacuum shall be, in general, designed for an external
pressure of 1.033 kg/cm2abs and full internal vacuum, unless otherwise
specified
Slide 113
Selection Of Mechanical Design Conditions
Slide 114
Selection Of Mechanical Design Conditions
For shell-and-tube heat exchangers, the low pressure (LP) side shall be
preferably specified with a design pressure at least equal to 10/13 of high
pressure (HP) side design pressure, in order to avoid having to install a
pressure relief device on the LP side
For systems operating below 0°C, the mechanical design temperature shall
be equal to the lowest anticipated operating temperature.
Slide 115
Furnace - Design Aspects
Slide 116
FURNACE
TYPES OF FURNACE
• Cylindrical furnace
– Low plot space
– Low cost
– Higher heat flux
– For clean services
• Box furnace
– High plot space
– High cost
– Even heat flux
– For fouling services
Slide 117
FURNACE
TYPES OF FURNACE
• Natural Draft
– Air for combustion enters due to pressure difference
• Forced Draft
– FD fan is used to supply air and ID fan is used to suck the flue
gas and heat is exchanged between air and flue gas through an
external heat exchanger (APH)
Slide 118
FURNACE
TYPES OF FURNACE
• Single fired heater
– Common pattern in heaters
– For low fouling / sensitive fluid
– Peak flux >80% of average flux
• Double fired heater
– For high fouling service
– Low residence time
– Fire on both side of coil
– Uniform heat flux & peak flux < 20% of average flux
Slide 119
Fired Heaters
Selection of fuel
Fired heaters shall be designed for continuous operation with:
100% firing on either fuel oil or fuel gas or any combination of both,
unless constrained to reject use of fuel oil from reasons of process or acid
gas dew point.
100% firing on fuel gas for heaters less than 1.5 MMKcal/hr.
Target efficiencies
Achievable fired heater efficiencies depend on service, furnace heat duty,
process temperatures and quality of fuel. Highest target efficiencies shall be
pursued by a unit designer, as found economically justified. Options such as
cast tube and glass tube air preheaters, steam generation and superheat, etc.,
shall be evaluated.
Target efficiency shall be:
92% on fuel gas fired heaters only
90% on combination firing heaters (with either fuel oil or fuel gas or dual fuel
mode)
Excess Air Fuel Oil Fuel Gas
Natural Draft 25 % 20 %
Forced Draft 20 % 15 %
Slide 120
Fired Heaters
Heater stack
Stacks shall be individually mounted on each heater unless there are
considerations such as grade-mounted APH or combined APH system for a
group of heaters.
Minimum fired heater stack heights shall be the higher of indicated heights in
respective unit BEDB Part-A documents or as calculated from the formula
below:
H = 14 (Q)0.3
(Minimum stack height as per TNPCB / MoE&F to be provided, SOx
/ NOx nozzles to be provided)
where, H: stack height, metres
Q: total SO2 emission, kg/hr
Slide 121
HEX - Design Aspects
Furnace Burner
Slide 122
FURNACE
OPERATION
• Draft inside the furnace
• Air ingression
• Arch pressure slightly positive – Stack damper
• Combustion air control thro’ Air registrars
• Excess air : 5-10% for gas and 10-15% for fuel oil
• Monitored & controlled by Arch zone O2 analyser
• Skin temperature
• Stack temperature
Slide 123
FURNACE
Slide 124
Standard fired heater piping & instrumentation
(a) Low-low fuel oil supply pressure shuts down fuel oil supply and return
(b) Low-low fuel gas pressure shuts down fuel gas supply but keeps pilots running.
(c) Low-low heater pass flow shuts down fuel oil and fuel gas but keeps pilots running.
(d) Low Low pilot gas pressure shuts down the pilot gas supply
(e) Low-low differential pressure between atomising steam and fuel oil shuts down fuel oil
supply and return.
(f) Emergency shutdown shuts down fuel oil and fuel gas as well as pilots.
(g) Emergency coil steam, manual or automated, depending on criticality.
(h) Draft gage connections at:
• Burners • Below convection • Above stack damper • Below stack damper
(i) Flue gas sampling connections at:
• Below convection section • Below stack damper
(j) On-line analysis with location as per (g), connections mounted at the same plane:
• O2 analyser • NOx analyser • SOx analyser • SPM analyser • CO analyzer • HC
analyser
(k) Temperature measurement connections below convection section, below stack
damper, at hearth level.
(l) Skin thermocouples shall be considered for measuring temperature of furnace tubes. Slide 125
HEX - Design Criteria
Material selection
Thickness Calculations
Shell, Channel, Covers, Tube sheets
No of shell passes
Velocity of the fluid
Pressure Drop
Tube Pattern
Consideration of Fluids through Tubes
Easy maintenance
Tube size, U- Tube, Cover header, Fluid choice
Slide 126
HEX – Material of Selection
Tube MOC
Tube with Stainless
Metallurgy Steel
with Carbon
steel
Slide 127
HEX - Codes & Standards
Slide 128
Codes & Standards
Which type of TEMA Heat Exchanger?
Slide 129
HEX - Design Aspects
Criteria for selection of TEMA Type
Shell side Tube side Fouling TEMA type
Fouling Resistance Resistance (Hr-m2-°C/kcal)
> 0.0002 > 0.0002 Floating head
≤ 0.0002 > 0.0002 Floating Head
> 0.0002 ≤ 0.0002 U tube bundle
≤ 0.0002 ≤ 0.0002 Fixed tube
sheet/ U-tube
bundle
Preferred Sizes for Shell && Tube HEX
Slide 130
HEX - Design Aspects
Tube Pitch Selection
Rotated
60° Clean Rarely used
Triangular
Rotated
45° Fouling Laminar
Square
Slide 131
HEX – Sample Datasheet (Pg 1/2)
Slide 132
HEX – Sample Datasheet (Pg 2/2)
Slide 133
PUMPS
DESIGN
• Selection of type of pumps
• Sparing of pumps
# Operating pumps Rated capacity per pump Spare pumps
• Specification of pump seals
• Specification of drives
• Minimum flow bypass (MFB) provisions & controls
Slide 134
Steam Turbine drives
Slide 135
PUMPS – Sample Datasheet
Slide 136
IBR Requirements
Scope of IBR
Steam generators / steam users shall meet IBR regulations. Major IBR
requirements are summarized below:
a) Vessels: Any closed vessel exceeding 22.75 litres (five gallons) in
capacity which is used exclusively for generating steam under pressure and
include any mounting or other fittings attached to such vessels, which is
wholly or partly under pressure when steam is shut-off.
b) Piping: Any pipe through which steam passes and if:
i) Steam system mechanical design pressure exceeds 3.5 Kg/cm2 g OR
ii) Pipe size exceeds 254 mm internal diameter
c) The following are not in IBR scope:
i) Steam Tracing
ii) Heating coils
iii) Tubes of tanks
iv) Steam Jackets
d) All steam users (heat exchangers, vessels, condensate pots etc.) where
condensate is flashed to atmospheric pressure i.e. downstream is not
connected to IBR system are not under IBR and IBR specification break is done
at last isolation valve upstream of equipment.
e) All steam users where downstream piping is connected to IBR i.e.
condensate is flashed to generate IBR steam are covered under IBR
f) Deaerator, BFW pumps are not under IBR and IBR starts from BFW
pump discharge.
Slide 137
INSTRUMENTATION
• Instrumentation Philosophy for all equipments & pipelines
• E.g.) Packed Towers
For column differential pressure indication two separate PT shall be provided
and differential pressure shall be derived in DCS.
– Local differential pressure indication for each bed: yes no
– Local differential pressure indication for total section: yes no
– Control Room differential pressure indication for each bed: yes no
– Control Room differential pressure indication for critical beds: yes no
– Control Room differential pressure indication for total section: yes no
– 1+1 Basket strainers in lines going to packed beds: yes no
– Single basket strainers in lines going to packed beds: yes no
Slide 138
Utility Line Instrumentation
UTILITY local DCS PAL/ local DCS TAL/ DCS FAL/ DCS
PI PI PAH TI TI TAH FI FAH FQ
MP STEAM
LP STEAM
Condensate
CW supply
CW return
Plant Air
Inert Gas
Fuel Gas
Fuel Oil
DM Water
Service Water
Flare
Slide 139
Block & Bypass Valve Size for Control Valve Manifold
Line Block & By paas Control Valve Size
Size Valve
0.5 0.75 1 1.5 2 3 4 6 8 10 12 14 16
0.5 Block 0.5
Bypass 0.5
0.75 Block 0,75 0.75
Bypass 0.75 0.75
1 Block 1 1 1
Bypass 1 1 1 Notes:
1.5 Block 1.5 1.5 1.5 1.5 1.All sizes are nominal sizes in
Bypass 1.5 1.5 1.5 1.5 inches.
2 Block 2 2 2 2 2.Bypass pipe diameter shall
Bypass 2 2 2 2 be same as bypass valve.
3 Block 2 2 3 3 3.Bypass valve will be globe
Bypass 2 2 3 3 valve upto 8" size and gate
4 Block 3 3 4 4 valve above 8".
Bypass 3 3 3 4
6 Block 4 6 6
Bypass 4 4 6
8 Block 6 6 8 8
Bypass 6 6 6 8
10 Block 8 8 10 10
Bypass 8 8 8 10
12 Block 10 10 12 12
Bypass 10 10 10 12
14 Block 12 14 14
Bypass 10 12 14
16 Block 14 16 16
Bypass 12 14 16
Slide 140
Control Valve –
Sample Datasheet
Slide 141
PIPING & INSULATION
• Insulation thickness for heat conservation, personnel protection, electrically
traced lines & cold insulation
• Material Usage
– Cellular Glass for process temperatures upto 350ºC.
– Rock Wool for process temperature upto 550ºC
– Calcium Silicate for process temperatures from 551 – 760ºC.
• Adherence to stipulations of OISD standard # 118 for min. inter‐equipment
spacing and inter‐distance between process unit and offsites
• Steam tracing for piping handling congealing services shall be:
– Steam tracing within unit battery limits, electric tracing for offsites upto
150°C
– Steam tracing within unit battery limits, electric tracing for offsites upto
250°C
– Steam tracing for both battery limits and for offsites
– LP Steam upto vacuum gas oils, MP Steam for heavy residues
– MP Steam for all congealing services
Slide 142
Environmental Parameters
Slide 143
Environ Impact
Assessment Study
144
Slide 144
Isopleths Showing Measured SPM Concentrations
Scale
0 1000 2000 m
-15000 -10000 -5000 0 5000 10000 15000
15000 15000
Pollutant: SPM
Unit: ug/m3
10000 10000
Y Direction (North) Distance, m
300
5000 5000
250
34
29
28
30
32
3135
36
39
41
40
33
27
0 38
37
13
15
16
17
18
147
12
5
2021
22
23
1
2
3
4
9
8
10
11
6
19 26
25
24 0 200
150
-5000 -5000
100
-10000 -10000
50
0
-15000 -15000
-15000 -10000 -5000 0 5000 10000 15000
X Direction (East) Distance, m
145
Slide 145
Ambient Air Quality Data
6 NH3 5 57 6 – 34
7 HC and VOC 10 14 -
Fugitive Emissions from the Work Zone Area of MRC – Benzene < 1 ppm
(OSHA)
146
Slide 146
Environment – Noise & Water
Parameter Residential Commercial Industrial Inside the
Plant Area
Noise levels 46 - 82 72 - 79 66 - 79 77 - 84
(dBA)
Standard 55 65 75 85
(dBA)
Water Environment
Surface Water
Ground Water
Bacteriological Quality
147
Slide 147
Risk Analysis Study
37.5kW/m2
(315m)
12.5kW/m2
(591m)
4.0kW/m2
(1032m)
Heat Radiation Effects due to BLEVE (CDU‐VDU)
148
Slide 148
Risk Analysis Study
Individual & Societal Risk Factors due to that project are studied &
analysed
Slide 149
Slide 150