Construction and Building Materials: Vahid Afroughsabet, Togay Ozbakkaloglu
Construction and Building Materials: Vahid Afroughsabet, Togay Ozbakkaloglu
h i g h l i g h t s
Steel and PP fibers were used individually and in combination at 1.0% fiber content.
Introducing silica fume improved mechanical and durability properties of concrete.
Steel fiber remarkably increased splitting tensile and flexural strengths of FRC.
Addition of steel and PP fibers reduced the water absorption of concrete.
Substitution of steel with PP fiber reduced mechanical properties of concrete.
a r t i c l e i n f o a b s t r a c t
Article history: This study investigates the effect of the addition of steel and polypropylene fibers on the mechanical and
Received 20 March 2015 some durability properties of high-strength concrete (HSC). Hooked-end steel fibers with a 60-mm length
Received in revised form 10 May 2015 were used at four different fiber volume fractions of 0.25%, 0.50%, 0.75%, and 1.0%. Polypropylene fibers
Accepted 27 June 2015
with a 12-mm length were used at the content of 0.15%, 0.30%, and 0.45%. Some mixtures were produced
Available online 4 July 2015
with the combination of steel and polypropylene fibers at a total fiber volume fraction of 1.0% by volume
of concrete, in order to study the effect of fiber hybridization. All the fiber-reinforced concretes contained
Keywords:
10% silica fume as a cement replacement. The compressive strength, splitting tensile strength, flexural
Steel fibers
Polypropylene fibers
strength, electrical resistivity, and water absorption of the concrete mixes were examined. Results of
Hybrid-fiber-reinforced concrete the experimental study indicate that addition of silica fume improves both mechanical and durability
High-strength concrete properties of plain concrete. The results also indicate that incorporation of steel and polypropylene fibers
Mechanical properties improved the mechanical properties of HSC at each volume fraction considered in this study.
Electrical resistivity Furthermore, it was observed that the addition of 1% steel fiber significantly enhanced the splitting ten-
Water absorption sile strength and flexural strength of concrete. Among different combinations of steel and polypropylene
fibers investigated, the best performance was attained by a mixture that contained 0.85% steel and 0.15%
polypropylene fiber. Finally, the results show that introducing fibers to concrete resulted in a decrease in
water absorption and, depending on the type of fibers, significant or slight reduction in the electrical
resistivity of concrete compared to those of the companion plain concrete.
Ó 2015 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.conbuildmat.2015.06.051
0950-0618/Ó 2015 Elsevier Ltd. All rights reserved.
74 V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82
utilization of HSC. Additionally, it is well understood that the use of to fiber-reinforced concretes. The freshly concrete was cast in
supplementary cementitious materials such as silica fume (SF), 100-mm cubic specimens in order to obtain compressive strength,
ground granulated blast-furnace slag (GGBS), and fly ash (FA) as electrical resistivity and water absorption. Splitting tensile
part of binders is required for production of high strength con- strength tests were done on cylindrical specimens with a 100
cretes [9,10]. Generally, replacement of ordinary Portland cement diameter and 200 mm height. Flexural tests were performed on
(OPC) by pozzolans in concrete can decrease porosity of concrete, prismatic beams with dimensions of 80 100 400 mm. The
especially in the long-term [1]. On the other hand, mineral admix- experiments were carried out at 7, 28, and 91 days of curing age,
tures such as silica fume also increase the brittleness of concrete and in all tests three specimens were tested for each curing age.
[11]. The cracks generally develop over time due to a number of
reasons such as plastic shrinkage in pre-hardening state as well 2.1. Materials and mixing procedure
as drying shrinkage in hardened concrete. Subsequently these
cracks weaken waterproofing capabilities of concrete, exposing Ordinary Portland cement (ASTM Type I) produced by the
the concrete microstructure to destructive substances such as Hekmatan factory was used in the present study. Silica fume that
moisture, chloride, sulfates, bromine etc. [12–15]. Therefore, was used in the present study was a commercially available
improvement of the properties of hardened concrete is an impor- by-product of the ferrosilicon factory in Semnan. The chemical
tant goal in concrete science [16]. and physical properties of the cement and silica fume are given
Fibers are incorporated into cementitious concretes to over- in Table 1. Coarse aggregate with a maximum size of 19 mm and
come this weakness, producing materials with increased tensile fine aggregate with a 3.4 fineness modulus were used. The volume
strength, ductility, toughness and improved durability properties fraction of the coarse aggregate and sand was equal to 50%. The
[17–21]. The efficiency of the fiber is dependent upon factors such specific gravity and water absorption of the coarse and fine aggre-
as the properties of the fiber matrix, volume of fiber inclusion, fiber gates were 2.69 and 0.56% and 2.61 and 1.92%, respectively. The
geometry, type of fiber, and orientation of fiber in the concrete grading curves of the aggregates are shown in Fig. 1, and the pass-
mixture [22,23]. There is a wide range of fibers available to ing percentage is presented in Table 2. A Carboxylic 110 M (BASF)
improve toughness and different properties of hardened concrete. was used as a superplasticizer to adjust the workability of the con-
The fibers are mainly made of steel, carbon or polymer [24–26]. crete mixtures. Hooked-end steel fibers with a 60-mm length and
Among the polymer fibers, polypropylene (PP) has attracted the an aspect ratio of 80, and polypropylene fiber with a 12-mm length
most attention among researchers because of its low cost, out- were employed in this study. The geometry and the properties of
standing toughness and enhanced shrinkage cracking resistance fibers are provided in Fig. 2 and Table 3, respectively.
in concrete reinforced with this type of fiber [27–29]. However, Concrete mix proportions are provided in Table 4. In the table,
concrete reinforcement with a single type of fiber improves the the content of superplasticizer is given as a percentage of the total
properties of concrete in a limited range. On the contrary, hybrid weight of the cementitious material. During the preparation of
fiber-reinforced concretes, which are reinforced with two or more concrete mixes, slump tests were conducted in accordance with
different types of carefully selected fibers to provide superior prop- the ASTM C143 [40] to determine the workability of fresh concrete.
erties. Since cracks occur at different stages and sizes in concrete,
the use of various fibers with different lengths is a good way to
2.2. Specimen molding and testing methods
address this problem. In a well-designed composite system, there
is a beneficial interaction between the fibers, which in turn results
The specimens were cast in steel molds and were compacted on
in a better performance of the hybrid system than that of the mono
a vibration table. They were demolded after approximately 24 h
fiber composite [30–34]. The main purpose of the combination of
and were then exposed to lime-saturated water at 23 °C and
different type of fibers is to control cracks at different zones of
100% relative humidity until their testing ages. Compression tests
the cementitious material, at different size levels and during differ-
were carried out on 100-mm cubic specimens using a 3000-KN
ent loading stages [35,36].
universal compression machine. Fig. 3 shows the setup used for
In this study, a total of 12 different mixtures were manufac-
the flexural tests. The specific electrical resistivity was measured
tured to investigate the effect of steel fiber, polypropylene fiber,
with the AC-Impedance spectroscopy, with a 1.0 kHz frequency
and hybridization of two fibers. Among these mixtures, three
and a 1.0 MO final capacity. The water absorption tests were
hybrid fiber-reinforced concretes were produced to study the
effect of fiber hybridization at a total fiber content of 1.0%. The
mechanical properties of concrete such as: compressive strength, Table 1
splitting tensile strength, and flexural strength were evaluated to Chemical composition and physical properties of cementitious materials.
establish the optimum percentage of steel and polypropylene Item Cementitious materials (%)
fibers. The present study was aimed at investigating the behavior
Cement Silica fume
of fiber-reinforced concretes with low fiber volume fractions, as
SiO2 21.2 93.0
this material is widely used in various applications, but the
Al2O3 5.4 1.7
research on the topic has been limited. Furthermore, research on Fe2O3 3.4 1.2
durability properties of fiber-reinforced concrete, such as electrical MgO 1.4 1.0
resistivity and water absorption, has been very limited and the Na2O – 0.6
results of the existing studies have been contradictory [37–39]. K2O – 1.1
CaO 63.9 0.3
The study reported in this paper was aimed at making a significant
contribution toward the understanding of these important proper- Compounds
Concrete mixes with water–cement ratio of 0.3 were produced. Specific gravity (kg/m3) 3150 2210
Specific surface (m2/kg) 300 14,000
Silica fume as a cement replacement was added by 10% of weight
V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82 75
100 agreement with the findings of the previous studies that the sub-
Coarse Agg. stitution of Ordinary Portland Cement (OPC) with pozzolans can
Sand Agg. reduce the porosity of concrete particularly at higher age [44–47].
80
Mixture The results of the fiber-reinforced specimens show that the use
of fibers in any form and volume fraction resulted in an increase in
Passing [%]
3.1. Compressive strength The variation of the splitting tensile and flexural strengths of
different fiber-reinforced concretes at the ages of 7, 28, and 91 days
The results of the compressive strength tests are shown in Fig. 4 are shown in Figs.5 and 6, respectively, and are presented in
and Table 5 for specimens manufactured using different fiber types Table 5. As can be observed from Table 5, addition of silica fume
and volume fractions. The results indicate that incorporation of sil- into concrete led to an increase up to 12% and 7% on the 28-day
ica fume in concrete resulted in an increase in the compressive splitting tensile and flexural strengths, respectively. The increase
strength. The addition of silica fume into the matrix improves in the strength caused by the addition of silica fume can be attrib-
the bond between the cement paste and the aggregate particles uted to the improvement in the bond between the hydrated
as well as increasing the density of the cement paste, which in turn cement matrix and the aggregate. This improved bond is due to
improves the compressive strength of the concretes [42,43]. This the alteration of calcium hydroxide, which tends to form on the
increase was equal to 6%, 8%, and 11% after 7, 28, and 91 days of surface of aggregate particles, into calcium silicate hydrate in the
curing, respectively, as can be seen from Table 5, which indicates presence of reactive silica.
that the increase in strength that results from the addition of silica The results of fiber-reinforced concretes show that incorpora-
fume becomes more significant at higher curing ages. This is in tion of fibers, especially steel fibers, had a significant influence
on the splitting tensile strength of the concrete. As expected, an
increase in the fiber volume fraction resulted in an increase in
Table 2 the splitting tensile strengths. For example, the splitting tensile
Aggregate grading.
strength of the mixtures containing 0.15%, 0.3%, and 0.45%
Sieve size Passing percentage (%) polypropylene fibers increased by 13%, 16%, and 20% at 28 days,
Coarse agg. Sand agg. Mixtures agg. respectively, compared to that of the reference concrete. The
results also indicate that an increase in the splitting tensile
3/4 in. (19 mm) 100.0 100.0 100.0
1/2 in. (12.5 mm) 72.4 100.0 86.2 strength ranging from 13% to 58% was attained, through the addi-
3/8 in. (9.5 mm) 22.9 100.0 61.4 tion of steel fibers to the mix, depending on the fiber content and
1/4 in. (6.35 mm) 8.0 100.0 54.0 test age. As can be seen from Table 5, the improvement in the con-
No. 4 (4.75 mm) 2.0 95.4 48.7 crete strength was higher at later ages of curing. This suggest that
No. 8 (2.36 mm) 0.2 75.5 37.9
No. 16 (1.18 mm) 0.1 51.5 25.8
the presence of silica fume, in addition to improving the character-
No. 30 (0.6 mm) – 27.1 13.6 istics of interfacial layer of aggregate-paste, increased the bond
No. 50 (0.3 mm) – 9.5 4.8 between fibers and cement matrix. Also, this may be attributed
No. 100 (0.15 mm) – 1.9 1.0 to the fact that adding silica fume improves dispersion of fibers
No. 200 (0.075 mm) – 0.6 0.4
into the concrete [48]. The results of hybrid fiber-reinforced
76 V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82
(a) (b)
Fig. 2. Shape and dimension of different types of fibers: (a) polypropylene fiber and (b) steel fiber.
Table 4
Mix proportions of concrete mixes.
Mix No. Mixture ID W/B Water Cement Silica Fume Fine Agg. Coarse Agg. Fiber volume SP (%)* Slump (mm)
fraction (%)
(kg/m3) ST PP
1 Plain 0.3 156 520 – 860 886 – – 1.0 170
2 SF10 0.3 156 468 52 851 877 – – 1.0 145
3 PP0.15 0.3 156 468 52 849 875 – 0.15 1.2 130
4 PP0.30 0.3 156 468 52 847 873 – 0.30 1.3 115
5 PP0.45 0.3 156 468 52 845 871 – 0.45 1.4 80
6 ST0.25 0.3 156 468 52 847 873 0.25 – 1.1 150
7 ST0.50 0.3 156 468 52 844 870 0.50 – 1.1 120
8 ST0.75 0.3 156 468 52 841 867 0.75 – 1.2 125
9 ST1.0 0.3 156 468 52 838 863 1.00 – 1.2 80
10 PP0.15ST0.85 0.3 156 468 52 838 863 0.85 0.15 1.2 85
11 PP0.30ST0.70 0.3 156 468 52 838 863 0.70 0.30 1.2 95
12 PP0.45ST0.55 0.3 156 468 52 838 863 0.55 0.45 1.2 50
*
Percentage of total weight of cementitious material.
V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82 77
120 120
7 Days 7 Days
Compressive Strength [MPa]
90 90
80 80
70 70
60 60
Plain SF10 PP0.15 PP0.30 PP0.45 Plain SF10 ST0.25 ST0.50 ST0.75 ST1.0
Mixture Mixture
(a) (b)
120
7 Days
Compressive Strength [MPa]
110 28 Days
91 Days
100
90
80
70
60
Mixture
(c)
Fig. 4. Compressive strengths of different fiber-reinforced concretes: (a) polypropylene fiber-reinforced specimens, (b) steel fiber-reinforced specimens, and (c) hybrid
fiber-reinforced specimens.
78 V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82
Table 5
Compressive strength, splitting tensile strength, and flexural strength test results.
Mix no. Mixture ID Compressive strength (MPa) Splitting tensile strength (MPa) Flexural strength (MPa)
7 days 28 days 91 days 7 days 28 days 91 days 7 days 28 days 91 days
1 Plain 71.2 (–) 82.6 (–) 88.3 (–) 4.63 (–) 5.27 (–) 5.81 (–) 6.94 (–) 7.81 (–) 8.45 (–)
2 SF10 75.2 (6%) 88.8 (8%) 98.0 (11%) 5.02 (8%) 5.88 (12%) 6.30 (8%) 7.18 (3%) 8.38 (7%) 8.73 (3%)
3 PP0.15 74.9 (5%) 91.2 (10%) 98.6 (12%) 5.13 (11%) 5.95 (13%) 6.47 (11%) 7.36 (6%) 8.50 (9%) 8.97 (6%)
4 PP0.30 75.7 (6%) 91.5 (11%) 101.4 (15%) 5.17 (12%) 6.10 (16%) 6.45 (11%) 7.52 (8%) 8.59 (10%) 8.91 (5%)
5 PP0.45 77.1 (8%) 92.8 (13%) 100.3 (14%) 5.34 (15%) 6.30 (20%) 6.72 (16%) 7.75 (12%) 8.84 (13%) 9.12 (8%)
6 ST0.25 76.1 (7%) 92.3 (12%) 98.5 (12%) 5.24 (13%) 6.05 (15%) 6.60 (14%) 7.58 (9%) 8.93 (14%) 9.41 (11%)
7 ST0.50 77.4 (9%) 93.8 (14%) 102.0 (16%) 5.46 (18%) 6.41 (22%) 7.40 (27%) 8.64 (24%) 9.97 (28%) 10.92 (29%)
8 ST0.75 78.3 (10%) 95.0 (15%) 102.6 (16%) 6.16 (33%) 7.29 (38%) 7.87 (35%) 9.56 (38%) 10.61 (36%) 11.18 (32%)
9 ST1.0 79.9 (12%) 98.7 (19%) 104.3 (18%) 7.32 (58%) 8.17 (55%) 8.80 (51%) 10.66 (54%) 12.58 (61%) 13.10 (55%)
10 PP0.15ST0.85 80.1 (13%) 97.5 (18%) 104.0 (18%) 7.04 (52%) 7.98 (51%) 8.47 (46%) 10.37 (49%) 12.02 (54%) 12.64 (50%)
11 PP0.30ST0.70 81.4 (14%) 96.6 (17%) 103.2 (17%) 6.11 (32%) 7.35 (39%) 8.20 (41%) 9.83 (42%) 10.75 (38%) 11.12 (32%)
12 PP0.45ST0.55 77.9 (9%) 95.3 (15%) 102.8 (16%) 5.73 (24%) 6.68 (27%) 7.17 (23%) 9.05 (30%) 10.40 (33%) 10.96 (30%)
Note: The number in the () shows the percentage of strength increase over that of the plain concrete.
10 10
Spling Tensile Strength [MPa]
7 Days 7 Days
7 7
6 6
5 5
4 4
Plain SF10 PP0.15 PP0.30 PP0.45 Plain SF10 ST0.25 ST0.50 ST0.75 ST1.0
Mixture Mixture
(a) (b)
10
Spling Tensile Strength [MPa]
7 Days
9 28 Days
91 Days
8
Mixture
(c)
Fig. 5. Splitting tensile strengths of different fiber-reinforced concretes: (a) polypropylene fiber-reinforced specimens, (b) steel fiber-reinforced specimens, and (c) hybrid
fiber-reinforced specimens.
seen in Table 6, addition of steel fibers reduced the electrical resis- fiber-reinforced concretes indicate that an increase in the steel
tance of concretes up to 82% at 28 days, compared to that of the fiber content at a constant total fiber volume fraction of 1.0%
plain concrete mix with 10% silica fume (i.e. mix No. 2). Despite resulted in a reduction in the electrical resistivity of the concrete.
the adverse effect of steel fibers on the electrical resistivity of con-
crete, addition of silica fume in these mixtures resulted in an over- 3.4. Water absorption
all improvement on the overall electrical resistivity of steel
fiber-reinforced concretes compared to that of the plain concrete Another major factor that affects concrete durability is the
without silica fume. Furthermore, it was observed that the electri- resistance of concrete to the ingress of aggressive ions. The absorp-
cal resistance of concretes that incorporated silica fume and steel tion characteristics of concrete indirectly represent its porosity,
fiber was up to 152% greater than that of the plain concrete, while also supplying useful information about the permeable pore
depending on the replacement level of steel fibers. Therefore, it volume inside the concrete and connectivity between these pores.
can be concluded that the inclusion of 10% silica fume was suffi- The water absorption of different fiber-reinforced concretes of the
cient to overcome the reduction in electrical resistivity that present study are depicted in Fig. 9 and summarized in Table 6. The
resulted from the addition of steel fibers of up to 1.0% fiber volume results indicate that introducing silica fume in concrete caused a
fraction. As expected, in Table 6 the results of hybrid the significant reduction in the water absorption of concrete. For
V. Afroughsabet, T. Ozbakkaloglu / Construction and Building Materials 94 (2015) 73–82 79
14 14
7 Days 7 Days
28 Days 28 Days
10 10
8 8
6 6
Plain SF10 PP0.15 PP0.30 PP0.45 Plain SF10 ST0.25 ST0.50 ST0.75 ST1.0
Mixture Mixture
(a) (b)
14
7 Days
Flexural Strength [MPa]
28 Days
12 91 Days
10
Mixture
(c)
Fig. 6. Flexural strengths of different fiber-reinforced concretes: (a) polypropylene fiber-reinforced specimens, (b) steel fiber-reinforced specimens, and (c) hybrid
fiber-reinforced specimens.
600 600
100 100
0 0
Plain SF10 PP0.15 PP0.30 PP0.45 Plain SF10 ST0.25 ST0.50 ST0.75 ST1.0
Mixture Mixture
(a) (b)
300
200
100
Mixture
(c)
Fig. 8. Specific electrical resistivity of different fiber-reinforced concretes: (a) polypropylene fiber-reinforced specimens, (b) steel fiber-reinforced specimens, and (c) hybrid
fiber-reinforced specimens.
2.0 2.0
Early Ulmate Early Ulmate
1.6 1.6
0.8 0.8
0.4 0.4
0.0 0.0
Plain SF10 PP0.15 PP0.30 PP0.45 Plain SF10 ST0.25ST0.50ST0.75 ST1.0
Mixture Mixture
(a) (b)
2.0
Early Ulmate
1.6
Water Absorpon [%]
1.2
0.8
0.4
0.0
Mixture
(c)
Fig. 9. Early and ultimate water absorption of different fiber-reinforced concretes: (a) polypropylene fiber-reinforced specimens, (b) steel fiber-reinforced specimens, and (c)
hybrid fiber-reinforced specimens.
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