Manual Derteminator Ash Fusibility LecoAF700 - V1-1!7!09
Manual Derteminator Ash Fusibility LecoAF700 - V1-1!7!09
Manual Derteminator Ash Fusibility LecoAF700 - V1-1!7!09
Ash Fusibility
Determinator
INSTRUCTION MANUAL
Version 1.1x
Part Number 200-714
July 2009
Patents are Pending in U.S.A. and other countries
© 2007
© 2009LECO
LECO Corporation
Corporation
Minor revisions may not be reflected in this manual.
LECO Corporation
3000 Lakeview Avenue • St. Joseph, MI 49085-2396
Phone: 269-983-5531 • Fax: 269-983-3850
info@leco.com • www.leco.com • ISO-9001 • No. FM 24045
LECO is a registered trademark of LECO Corporation.
Quality at LECO Corporation means understanding our customer's
requirements and establishing specifications that clearly define those
requirements. The essence of our quality philosophy is the commitment to
quality objectives, aimed at never-ending improvement and complete
customer satisfaction.
Safety Symbols
These symbols may be found on LECO
equipment or their components. These
This symbol indicates a risk of
symbols indicate the use of specific safety
electrical shock.
guidelines. Important safety information is
highlighted in this manual by one of the
following symbols as well as WARNING and
CAUTION statements. Operator and service This symbol indicates a high
personnel must follow these instructions for temperature surface.
personal safety and to prevent damage to
the equipment.
This symbol indicates a
The instrument should be operated only by
caution.
technically qualified individuals who have
fully read and understand these instructions.
The instrument should be operated only in
accordance with these instructions. This symbol indicates a risk of
explosion.
The operator should follow all of the
warnings and cautions set forth in the
manual and the operator should follow and
employ all applicable standard laboratory This symbol indicates possible
safety procedures. auto loader motor damage.
Operating Precautions
The instrument should be operated only by technically qualified individuals who have fully read and
understand these instructions. The instrument should be operated only in accordance with these
instructions. The operator should follow all of the warnings and cautions set forth in the manual and the
operator should follow and employ all applicable standard laboratory safety procedures.
1 Introduction
Illustrations .................................................................................1–6
Software License ..........................................................................1–8
Warranty .................................................................................. 1–12
Transferring Ownership of a Dell Product ....................................... 1–14
Warning and Caution Symbols...................................................... 1–16
Warning Information................................................................... 1–17
Interference to Other Devices ...................................................... 1–18
Declaration of Conformity ............................................................ 1–19
Equipment Packages................................................................... 1–20
Options..................................................................................... 1–22
Components and Accessories List ................................................. 1–23
Specifications ............................................................................ 1–25
2 Installation
Illustrations .................................................................................2–2
Instrument Installation .................................................................2–3
Copy Protection Key ................................................................... 2–32
Software Installation................................................................... 2–34
Software Upgrade ...................................................................... 2–35
Software Registration ................................................................. 2–36
International Installation ............................................................. 2–37
3 Option Installation
Printer Installation........................................................................3–3
4 System Setup
5 Operation
Calibration ..................................................................................5–3
Loading Samples ..........................................................................5–6
Login Samples .............................................................................5–7
Analyze Samples ..........................................................................5–9
Print Analysis Results.................................................................. 5–11
Sample Editing Functions ............................................................ 5–16
Sample Signature....................................................................... 5–19
Export Data............................................................................... 5–21
Text Import Data ....................................................................... 5–28
Transmit Data............................................................................ 5–30
Transmit Selected Samples.......................................................... 5–40
Data Backup.............................................................................. 5–41
6 Maintenance
7 Theory of Operation
8 Diagnostics
Ambient Monitor ..........................................................................8–3
System Check..............................................................................8–6
Furnace Diagnostics......................................................................8–7
Network Diagnostics .....................................................................8–9
Solenoids and Switches ............................................................... 8–11
9 Service
Illustrations .................................................................................9–2
Replace the Furnace Heating Element..............................................9–3
Combustion Tube Replacement ......................................................9–4
10 Illustrations
11 Schematics
12 Index
I. Definitions
"Licensed Software" shall mean the software supplied with this
Software License, which is software developed and distributed by
LECO.
"Instruction Manual" shall mean a guide describing the use and
operation of the Licensed Software, together with any related
supporting documentation.
"Licensee" shall mean and include any of the Licensee's divisions and
departments within Licensee's organization, but shall not include
wholly or partially owned subsidiaries, affiliates, successors or assigns,
or independent third parties.
VII. Confidentiality
All information and materials regarding the software, provided to
Licensee by LECO which are not generally known in the trade are
confidential, are proprietary, and such information and materials are
furnished solely for the use of Licensee under this Software License.
Licensee agrees not to use or disclose any such information or material
otherwise without prior written consent from LECO and Licensee
further agrees to take all reasonable steps requested by LECO, or
otherwise necessary to protect the confidentiality of all such
information and materials. The foregoing obligations will survive
termination of this Software License, and Licensee agrees to return all
such information and materials to LECO upon request or any non-
renewal or termination of this Software License.
The following section explains the steps to transfer the warranty and
ownership of a Dell computer. This transfer is necessary to complete
when an equipment package that includes a Dell computer has been
purchased from LECO.
An internet connection is required to complete the transfer. If an
internet connection is not available, the transfer can be completed
by calling Dell at 800-624-9897.
To complete the transfer online through Dell's website, complete
either the Domestic Customer procedure or the International
Customer procedure as explained in the following steps.
This equipment has been tested and found to comply with the limits
for a Class B digital device, pursuant to Part 15 of the FCC Rules and
Regulations. These limits are designed to provide reasonable
protection against harmful interference in a residential installation.
This equipment generates, uses and can radiate radio frequency
energy and, if not installed and used in accordance with the
instructions, may cause interference to radio communications.
However, there is no guarantee that interference will not occur in a
particular installation. If this equipment does cause harmful
interference to radio or television reception, which can be determined
by turning the equipment off and on, the user is encouraged to try to
correct the interference by one or more of the following methods:
Reorient or relocate the radio or television receiving antenna.
Increase the separation between the equipment and the radio or
television receiver.
Connect the equipment to an outlet on a circuit different from that
which the radio or television receiver is currently connected.
Consult the radio or television dealer or an experienced radio/TV
technician for help.
Items listed below are repeated throughout this manual and are
subject to revision. Please consult the packing slip received with the
instrument.
NOTE For a complete listing of kits and packages, refer to Components and
Accessories List, page 1–23.
V~ denotes VAC.
Illustrations .................................................................................2–2
Instrument Installation .................................................................2–3
Carbon Monoxide Detectors ......................................................2–4
Heating Element Installation .....................................................2–6
Camera Installation ............................................................... 2–22
Apply Power ......................................................................... 2–25
Camera Configuration ............................................................ 2–26
Screen Definitions ............................................................ 2–28
Camera Adjustment ............................................................... 2–30
Copy Protection Key ................................................................... 2–32
Copy Protection Key Not Installed ............................................ 2–32
Copy Protection Key Not Registered ......................................... 2–33
Software Installation................................................................... 2–34
Software Upgrade ...................................................................... 2–35
Upgrade Camera Software ...................................................... 2–35
Software Registration ................................................................. 2–36
International Installation ............................................................. 2–37
5. Connect the Reducing gas supply to the Reducing gas inlet on the
back of the instrument (Figure 2-1, page 2–5).
6. Connect the Oxygen gas supply to the Oxygen gas inlet on the
back of the instrument (Figure 2-1, page 2–5).
7. Connect the Purge gas supply to the Purge gas inlet (Figure 2-1,
page 2–5).
! The furnace vent must be a 160 CFM active vent with no back
Warning pressure.
NOTE The carbon monoxide detector may require a longer warm up time
(approximately 10 minutes) after the instrument has been off for
extended periods of time. If the alarm sounds, wait 10 minutes for
any accumulated gas to dispel and then turn it off and back on.
1. Turn off the determinator and unplug it from the facility power
source. Allow sufficient time, if necessary, for it to cool to room
temperature.
2. Remove the following parts before proceeding with electrode and
furnace tube installation.
Both side panels
Top panel, refer to Figure 2-2, page 2–7
Furnace hood (flange), refer to Figure 2-2, page 2–7
Rear access cover
Front access cover (Use the key to unlock the door if locked),
refer to Figure 2-3, page 2–8.
Figure 2-4
Heating Elements
B. From the front of the furnace, install the metal washers,
ceramic washers and springs over the ends of the heating
elements. Refer to Figure 2-5 on page 2–10.
C. Curl one end of a braided cable around the element, as close
to the end of the element as possible. Refer to Figure 2-4
above.
D. Using the Expansion Tool, install a clamp onto the element
over the braided cable.
E. Curl the other end of the cable around the lower left
element, as close to the end of the element as possible, and
clamp it in place. The braided cable must not be taut.
F. Repeat steps B, C, and D for the four remaining elements.
G. From the back of the furnace, curl the free end of the left
braided cable around the lower left element, as close to the
end of the element as possible, and clamp it in place. Refer
to Figure 2-7, page 2–11.
H. Curl the free end of the right braided cable around the lower
right element, as close to the end of the element as possible,
and clamp it in place.
The braided cables must have sufficient slack to allow the
elements to expand during use, and the cables must be
routed to assure sufficient clearance of all nearby
components.
HEATING
ELEMENT
CERAMIC FIBER
WASHER
CABLE
STEEL
SPRING WASHER
CLAMP
Figure 2-5
Electrode, Clamp, Spring, and Washer Orientation
Figure 2-6
Electrodes Front View
633-101-362
BRAIDED
CABLE
(2 REQUIRED)
633-101-361
BRAIDED CABLE
773-066
STANDOFF
(2 REQ'D)
Figure 2-7
Electrode Rear View
Figure 2-8
Furnace Tube End Block Assembly
Figure 2-9
Furnace Tube Installation Back View
Figure 2-11
Furnace End Block Assembly
Figure 2-12
D-tube, Light Baffle, and Furnace Tube
Figure 2-13
D-tube Support Bracket
710-496, insulation
is inserted between
the furnace tube
and D-tube.
625-501-469,
insulation end tube D, 625-501-248,
is inserted into the D-tube
front of the D-tube support/cover
(behind cover). tabs cradle the
D-tube.
Figure 2-14
D-tube and Light Baffle Installation
Figure 2-15
Gas Inlet Tube
Figure 2-16
Thermocouple Installation
Figure 2-17
Thermocouple Installation
Figure 2-18
D-tube and Insulating Pad
1. Before installing the camera, install the neutral light filter (located
in the component pack, page 1–23) by placing it into the neutral
light filter arm assembly and tightening the screw as shown in
Figure 2-19, below.
Figure 2-19
Neutral Light Filter Installation
Figure 2-20
Camera Installation
Figure 2-21
Camera Assembly, USB Cable, Thermocouple Wire
NOTE The furnace is designed with a carbon monoxide detector that will
sound a warning alert if a carbon monoxide leak is detected inside the
furnace. This detector is not intended to replace Facility
Detectors. LECO recommends that all installations have an industrial
carbon monoxide detector installed near the instrument.
NOTE The carbon monoxide detector may require a longer warm up time
(approximately 10 minutes) after the instrument has been off for
extended periods of time. If the alarm sounds, wait 10 minutes for
any accumulated gas to dispel and then turn it off and back on.
NOTE This procedure is used for a single unit or dual unit installation. For a
single unit installation stop at step 9.
1. Plug the 621-710 Ethernet Hub into the Ethernet port on the rear
panel of the computer. Use the supplied 619-610 CAT-5 cable.
2. For each instrument do the following:
Plug the 619-950 USB cable into the computer USB port.
Follow the instructions in the Hardware Wizard. When it asks
to search for software select No, not this time.
The dialog box, shown above, will display twice for each
instrument when the USB 1.1 and USB 2.0 camera drivers are
installed.
When this process is complete for each instrument, unplug the
USB cable from the computer. They will be reconnected at a
later step in this procedure.
Repeat these steps for the second AF700 instrument.
3. Turn the AC power on both instruments
4. If dual instruments are being installed, connect one of the AF700
instruments into the Ethernet hub. DO NOT connect the other
AF700 instrument at this time. Skip this step if only one
instrument is being installed.
7. With only one instrument connected, and turned on, you should
see a dialog box similar to the one below. However, depending on
which instrument you have connected, it may indicate Unit #2.
The displayed Serial Number should match that of the unit you
have connected. Check the serial number on the back of the
instrument. In addition, the Network Address may be different
then that displayed below.
8. In the Camera S/N field the pull down list should show only one
camera serial number. This is the serial number of the camera
currently connected. Choose this serial number and then select
Continue.
9. Click Save to save the instrument configuration and then close
the application.
10. Connect the second instrument and run the AF700 Configuration
Management program.
11. With the second instrument connected, the displayed information
should look similar to the information in the dialog box below.
13. The AF700 software will come up again. This time the program
should be able to communicate with both instruments.
Screen Definitions
Show All—Display all instruments that are connected to the computer.
Refresh—Displays all instruments that are currently connected to the
computer.
Save—Saves current configuration.
1. Remove the lens cap and focus the camera using the supplied
target. Refer to Figures 2-22 and 2-23. The focus should be
performed with the camera aperture at the fully open position
(clockwise). Once the camera is focused, close the aperture by
turning it completely counter-clockwise, and then turn it
clockwise two click positions (refer to the note below). Lock the
set screw in this position. For additional information about the
Camera Setup, refer to page 4–12.
NOTE For low temperature applications, less than 700oC, turn the
camera aperture adjustment three click positions instead of two.
Figure 2-22
Camera Adjustments
A copy protection key is required to use the AF700 software. The key
should remain installed in one of the USB ports while using the
software.
A Software License Key Not Found or License Not Valid dialog box
might appear if the key is not installed or if the key is initialized for
use but not registered.
Refer to Copy Protection Key Not Installed, page 2–32, or Copy
Protection Key Not Registered, page 2–33.
1. Click Add.
2. Insert the copy protection key into the USB port on the computer.
3. Click Cancel. The Licenses dialog box appears.
4. Click Close. The Login screen appears.
If the copy protection key is installed when the Software License Key
Not Found or License Not Valid error message first appears on the
screen, the following dialog box appears.
For international installation, a HAR approved line cord for use in the
end country must be obtained. This product requires a disconnect
device that may either be the plug of the power cord or a disconnect
device installed at the installation site if the equipment is permanently
wired.
When the plug on the power supply cord is intended to serve as the
disconnect device, the socket/outlet must be installed near the
equipment and shall be easily accessible. When the wiring is
permanently connected, a disconnect device (such as a circuit breaker
or switch) must be lockable, installed near the equipment, and be
easily accessible.
Printer Installation........................................................................3–3
Use the following procedures along with the manual supplied with the
Printer to install the optional printer.
1. Shut down and turn off the Computer system if necessary.
2. Unpack the Printer and locate the printer interface cable.
3. Refer to the installation instructions supplied with the printer.
Install the printer on the work surface and connect all necessary
cables and components.
4. Turn on the Computer and Printer. It is not necessary to turn on
the instrument at this time.
5. Refer to the installation instructions supplied with the printer and
install the printer software.
6. After the printer is installed and tested, turn the computer and
printer OFF.
When the cones are dry attach them to the sample tray provided as
follows:
1. Place a drop of cone adhesive on the bottom of the cone.
2. Place the cone into the cone location. This must be done before
the adhesive sets up.
3. Repeat steps 1 and 2 until all the cones are attached to the
sample tray.
4. Use the spatula to remove any cones that are not properly
attached and the adhesive. The cone can then be remounted.
(This side can be used for single gold wire by removing cone #2)
P/N 625-501-615
(Use this side for calibration wires by removing Cone #2 and/or #4)
The numbers are not marked on the tray but the numbering scheme shown above
is suggested (cone flats to the front).
Image Cropping
Cone Position
Image Cropping
3. Click the About Camera to display a dialog box with details about
the camera. Verify that the camera ID is 92. If not contact LECO.
4. Click Reset to set the camera parameters back to the factory
default settings.
5. Click Focus to display a full size camera image on the screen to
focus the camera.
6. Click Snap Shot to take a picture of the image.
7. Click Save Image to save the image. The Save As dialog box is
displayed. Select the location, enter a filename and click OK to
save the image.
The default Calibration Target Height (0.75 inches) and Target Width
(1.98 inches) are for calibration with the Camera Focus Tray Assembly
provided in the component pack. The Height is measured from the top
of the "sample" pins to the bottom of the metal target. The Width is
measured from the left edge to the right edge of the base of the metal
target.
Figure 4-1
Camera Focus Tray
9. With the point of the cursor aligned with the left side of the
camera focus tray, select and hold the left mouse button, drag
the mouse down and align the point of the cursor with the right
side of the target, release the left mouse button. The number of
pixels will be displayed as the mouse is moved towards the right
of the target.
10. Click the Calibrate Width check box to uncheck it. When the left
mouse button is released the calibrated width of 1.98 inches will
be displayed.
11. Click OK to save the new Width Calibration.
The layout of the AF700 main screen can be arranged to improve the
ability to operate the instrument and manage or view data.
To move the panes, place the mouse pointer over the dashboard tab,
hold down the left mouse button and drag the pane to the desired
position. The cursor will change with an arrow indicating where the
pane will be relocated. If the cursor changes to four arrows, in the
form of a star, the dashboard being moved will be placed over the one
under the cursor. To display a dashboard pane that has been overlaid,
click the tab.
DASHBOARD
TABS
The four windows at the bottom display the sample image at the
following temperatures.
IT / Initial Temperature
ST / Sphere Softening Temperature
HT / Hemisphere Temperature
FT / Flow Fluid Temperature
Menu Buttons
F1 through F7 are used to access the on-board manual, Login sample
information, start an analysis, abort an analysis and pause an analysis.
The software can control two furnaces from one PC. Click to
select the furnace, any changes to the software will be applied to the
furnace selected.
Plot Buttons
Goto—click to goto a sample at the deformation temperature.
Set—click to set a sample at a specific deformation temperature.
Find—click to locate a sample at temperature where the height to
width becomes 1 or just below 1.
Temperature Slider—slide the bar to see the sample at different
temperatures.
<< Play button Forwardswitches play button to play forward.
||> or <|| Play button Foward or Reverse—click to start, click a second
time to stop.
>> Play button Reverse—switches play button to play in reverse.
The following buttons are located at the top of each plot pane:
…Click to measure the width of the camera focus tray for width
calibration.
Zoom Out and Zoom Out One Level are only available after you have
zoomed in on the sample image.
To zoom in on an area, click and drag the rectangle around the sample
image you wish to zoom in on.
Print—click Print to print the plot pane and plot parameters on the
system printer.
Print Preview—click Print Preview to preview the printout of the plot
pane and plot parameters.
Properties—click properties to configure the metrics plot.
Database Menu
Edit Menu
Diagnostics Menu
Maintenance Menu
Configure Fields
1. From the Configuration menu, click Display. The Sample Display
screen will appear.
Configure Font
1. Click Font to change the font name, style, size, and color. The
Font configuration screen will appear.
2. From the Font configuration screen select the Font Name, Style
and Size. A sample of the selected Font will appear in the Sample
Text preview box.
Log Bar
The log bar, located at the bottom of the screen, displays information
saved in the log file. It only appears when it displays information. This
information may be communication failures, severe errors or
operational procedures.
If Log Bar is not checked it will only display communications failures
and severe errors.
If Log Bar is checked it will display any information saved in the log
file. This includes communications failures, severe errors and
operational procedures.
Examples of operational procedures are sample data changes,
calibration changes, change to the sample mass and more.
Auto Widths
1. Select the Configuration menu.
2. Click Auto Widths to adjust the size of each cell in the sample
display to fit the text inside the cell.
Create a Method
1. From the Configuration menu, click Method. The Method screen
will appear.
4. Click the Add or Insert button to add a step and enter the Start
Temperature, End Temperature, Ramp Rate, Ramp Time and
Atmosphere.
The Melting Point equation is only used for the melting point of
Note wires.
General Definitions
Method Name—the name of the defined method used for identification.
Description—this can be any text the operator inserts. Description can
be information about the methods intended use or purpose.
Acquisition Temperature—the starting temperature at which image
data is acquired and saved for the analysis.
Acquisition Rate (deg)—the rate per degree that image data is saved
for the analysis result. Example: if set to one second, data is taken
every one second after the Acquisition Temperature is reached.
Acquisition Rate (sec)—the rate per second that image data is saved
prior to saving image data for analysis.
Image Metrics Acquisition—the start temperature for automated height
and width measurements.
Predefined ash fusibility temperatures (IT, ST, HT, and FT) may
Note be automatically determined, using Image Recognition Functions,
(IRF) when the furnace temperature is set to 700oC or above.
Ash fusibility temperatures below 700oC must be determined
manually.
Temperature Rounding—the temperature amount in degrees that the
displayed temperature, in the spreadsheet and main screen, is
rounded off to. Example: If temperature rounding is set to 10 and the
temperature result is 1002 then the temperature displayed will be
rounded to 1000.
The Melting Point equation is only used for the melting point of
Note wires.
2. Click the arrow, in the sample name selection box, and select a
defined Standard from the list.
3. Enter the information required in the Login Screen. Refer to
Standard Login Definitions, page 4–55, for additional information.
4. Click OK to login the standard.
The filters All Samples and Today’s Samples will always appear.
Note In addition, a filter will appear for each defined method.
2. Select a sample filter and click OK. The dialog box will disappear
and the sample grid will reappear with the filter applied.
3. Click Cancel to exit without applying the filter.
2. Click Add to define and add a sample filter to the list. A new filter
with the filter name New Filter will be added to the list.
3. To define the new filter, select New Filter and click Properties. The
Properties Dialog Box will appear.
Backup/Restore
Backup and Restore allows user to backup an existing calibration to a
file, or restore an old calibration from an existing file.
Format Examples
*Format
Number Format for Result Result
Type
A 4.50360 A 4.50360000
0.123456 F4.5 0.1235
0.000789 F3.5 0.00079
Fn.m
0.000789 F3.2 0.00
321.8765 F3.5 322
0.123456 S4.5 1.235E-1
0.000789 S3.5 7.9E-4
Sn.m
0.000789 S3.2 0.0E-1
321.8765 S3.5 3.22E+2
0.123456 E4.5 123.5E-3
0.000789 E3.5 790E-6
En.m
0.000789 E3.2 000E-3
321.8765 E3.5 322E+0
I 321.8765 I 322
* A = Default format
F = Fixed point format: A format in which the decimal point is located at a single
unchanging position in a predetermined number of digits.
S = Scientific notation: An exponential format (y.yyy x 10e) in which any number is
expressed as a number between 1 and 10 multiplied by a power of 10 that indicates
the correct position of the decimal in the original number.
E = Engineering format: An exponential format that displays the exponent in powers
of 3.
I = Integer
n = Total number of significant digits to be represented
m = Maximum number of digits after the decimal to define readability
Function Definition
+ Plus
- Minus
* Multiply
/ Divide
^ Raise to the power
= Equal
> Greater than
>= Greater than or equal to
< Less than
<= Less than or equal to
Presentation Time
This feature is only available if logging was enabled when the database
was created. It is used to view the database as it existed at some
previous point in time. For example, it could be used to view results
before a change in calibration was performed. When the presentation
time is set, changes are not allowed to the database, so samples
cannot be added and changes cannot be made to methods, etc.
NOTE After the Presentation Time and date are selected, the results from
that date will appear in the sample grid.
View History
This feature is only available if logging was enabled when the database
was created. View History displays a log of database changes that
could be used to identify the time/date when some particular change
took place. Since there is no description of what each change
represents, it can only be used to identify who made a change.
1. Click the Database menu and select View History. The View Log
screen will appear.
2. The following log items are shown:
Date/Time-The date and time that the database change occurred.
Entry ID-A unique identifying number for the database object that
was changed. For example, each sample would have a unique
number.
Action-The type of action that occurred; created, modified, or
deleted.
User-The logged in user who performed the action.
Time-The Local and UT checkboxes are used to display the
appropriate time zones.
NOTE The database size, speed of computer, and hard drive determine how
quickly the database is compressed or repaired.
Calibration ..................................................................................5–3
Standard Calibration ................................................................5–3
Create New Standard Calibration ..........................................5–3
Add Standards ...................................................................5–4
View Calibration .................................................................5–5
Edit Calibration ..................................................................5–5
Loading Samples ..........................................................................5–6
Login Samples .............................................................................5–7
Sample Login Definitions ..........................................................5–8
Analyze Samples ..........................................................................5–9
Abort an Analysis ....................................................................5–9
Pause/Delay Analysis ............................................................. 5–10
Remove a Programmed Pause or Delay .................................... 5–10
Print Analysis Results.................................................................. 5–11
Define Report Settings ........................................................... 5–11
Report Configuration ......................................................... 5–11
Fields Configuration .......................................................... 5–12
Font Configuration ............................................................ 5–13
Element Configuration....................................................... 5–13
Print Preview ........................................................................ 5–14
Recalculate Results................................................................ 5–15
Sample Editing Functions ............................................................ 5–16
Insert a Sample .................................................................... 5–16
Insert a Sample from the Login Screen..................................... 5–16
Fill Cells with the Same Data................................................... 5–17
Cut...................................................................................... 5–18
Copy ................................................................................... 5–18
Paste ................................................................................... 5–18
Standard Calibration
Standard Calibration is a process that adjusts the measured
temperature to that of known temperature standards (e.g. gold or
nickel wire). The application software permits two different types of
calibration: Single Standard or multipoint calibration. A single point
calibration can be performed using the curve type (single standard
sample); however, LECO recommends multipoint calibrations.
Calibrations are instrument specific not method calibrations.
Add Standards
Add standards permits the operator to add analyzed standards to the
list of standards used for calibration.
For the AF700, the typical standard is gold with a temperature of
1063C (1945F) and nickel wire 1452C (2645F)
1. Select the analyzed standard samples from the spreadsheet to be
added to the list of standards used for calibration. The FT
transition temperatures are used for this calibration.
2. Click Configuration and select Calibrations.
3. From the menu, click Add Standards.
4. The highlighted Analyzed Standards will be added to the list of
samples used for calibration.
Edit Calibration
Permits the operator to view and edit the current calibration.
Use the insolated tongs and sample tray, provided in the component
pack, to load the samples into the furnace.
1. Prepare the samples as described in Sample preparation,
page 4–5.
2. When the furnace has reached its start temperature, open the
furnace door and load the samples into the center of the furnace
using the insolated tongs.
3. Close the furnace door.
1. From the Samples menu, click Login. The Login dialog box is
displayed.
2. Login all samples entering the cone positions for each. Samples
cannot be logged in once the analysis starts. Refer to Sample
Login Definitions on the next page for more information.
1. After the samples are loaded, page 5–6 and logged in, page 5–7.
Click the F5 Analyze button or press F5 to start the analysis. As
the cones are analyzed, the window at the bottom of the screen
updates to show the different cone positions.
2. At any time, you can click the Stop button to abort the analysis.
Do NOT open the furnace door while the analysis is running.
3. After analysis, results will be shown in the spreadsheet and plot
window.
4. From the plot window, use:
Goto to locate and view the cone at the deformation
temperature.
Set to manually set deformation temperature of the cone
and override Auto Find.
Find searches until the ratio of height to width of the cone
becomes 1 (or slightly below) and displays it at that
temperature.
Temp Slider to review what the cones looked like at each
temperature.
Play Button to go through the entire melting process. The
play button flips to a reverse button to go through the
melting process in reverse.
5. In the spreadsheet or plot, you can right-click to display the
Short-cut menu for quick access to some of the most commonly
used commands.
Abort an Analysis
An analysis in progress can be aborted. If the analysis is aborted,
"Aborted" will appear under analysis date.
1. From the Samples menu, click Abort, press F6 or click the F6
Abort button. The analysis in progress will be aborted.
3. In the highlighted field, enter the date and time to start the
delayed analysis. The format for entering the date and time is
[4/7/2006 (MM/DD/YY) 4:30:00 PM]. To select the time from the
list, click the arrow. If pausing for operator intervention, select
Manually from the list.
4. Click OK to start the delayed analysis. A clock symbol will appear
in the spreadsheet next to the sample that will be analyzed at the
programmed delayed start time. If Manually was selected, a red
octagon will appear in the spreadsheet and the analysis will begin
only when the operator clicks analyze.
Report Configuration
1. From the Samples menu, click Print. The Report Settings dialog
box will appear.
2. Click the Report Format arrow and select the type of report.
Selections are: Tabular, Report with Plots or Group Report.
3. Click the Statistics arrow to select which report to print statistics
with. Selections are: None, Reports with Plots, or Tabular Report.
4. If desired, enter a Heading Text to title the report.
Fields Configuration
1. In the Report Setting dialog box, click the Fields tab to select the
fields to display in the report. The Report Fields screen will
appear.
Element Configuration
1. In the Report Setting dialog box, click the Display tab to select
the plot to display in the report. The Report Display screen will
appear.
Print Preview
Before analysis results are printed, the printed format should be
configured. Refer to Define Report Settings, page 5–11.
1. From the Samples menu, click Print Preview. The Report Settings
screen will appear.
Recalculate Results
1. Select the samples in the spreadsheet to recalculate.
2. From the Samples menu, click Recalculate. The selected samples
will be recalculated using the new calibration or blank.
A. If Results is chosen, the selected samples will be
recalculated using the existing deformation temperature
results for the new calibration.
B. If Deformation is chosen, the deformation temperatures for
the selected samples will be recalculated from the cone
metrics and the new calibration.
C. If metrics is chosen, the cone metrics and deformation
temperatures for the selected samples will be recalculated
using the raw image data and the new calibration.
Insert a Sample
If a sample is going to be added to the last row of the spreadsheet,
sample login should be used. If a sample should be inserted out of
sequence, between unanalyzed samples, Insert a Sample can be used.
NOTE An analysis method should be developed before a sample is logged
in. Refer to Create a Method, page 4–42.
1. Click and select a row in the spreadsheet after the last analyzed
sample. Insert will insert a row before the selected row.
2. From the Edit menu, click Insert. A row will be inserted into the
spreadsheet before the selected row.
Copy
Copy is used to copy a sample from the spreadsheet and copy it to the
Windows® Clipboard. From there it can be Pasted into another location
in the spreadsheet.
1. Select a sample by clicking on a row in the spreadsheet. The row
should be highlighted.
2. Select the Edit menu and click Copy. The sample will be copied to
the clipboard.
Paste
Paste is used to copy a sample that was cut or copied to the Windows®
Clipboard and insert it into the spreadsheet.
1. Select a sample location in the spreadsheet by clicking on a row.
The row should be highlighted.
2. Select the Edit menu and click Paste. The sample will be copied to
the spreadsheet.
Delete a Sample
Use Delete a Sample to remove a sample row from the spreadsheet.
1. Select a row in the spreadsheet to delete. If more than one row
should be deleted, click and drag the mouse pointer down the
desired number of rows to delete. More than one row will be
selected.
2. From the Samples menu, click Delete.
3. Click Yes to delete the row or rows of sample information. The
selected sample information will be deleted from the spreadsheet.
It is not possible to restore this data once it’s deleted.
NOTE If a database is created with log activity enabled, a deleted sample
can be viewed by setting the Presentation Time to a time prior to the
deletion.
Export Configuration
Filename
1. Select the Configuration menu and click Text Export Formats. The
Export Formats dialog box will appear.
2. Enter a name for the text export format in the Name field.
3. Click Properties to configure the text export format. The Filename
dialog box will appear.
2. Position the cursor in the Export Format and click the mouse to
place the cursor at the point in the format to edit a field. If
additional fields are desired, refer to User Defined Fields for
information on creating them, page 4–63.
3. Select a Field from the Fields box and click Add Field to Export
Format to add a field.
4. Highlight a Field in the Export Format and then press Delete on
the keyboard to delete it.
Text Import Data permits the operator to import sample data from
another application such as an Excel® spreadsheet.
The text import data, must be a text file. Each line can have the
following fields (must be in order): Sample Name,Sample Mass,Sample
Description,Sample Comment,Sample Operator. The fields must be
delimited by tabs or commas and each sample's data must be on a
separate line.
The line may have just the Sample Name (example: Sample5) or just
the Sample Name and Sample Mass (example: Sample6,0.95) and
skip the remainder of the line. To skip over fields (for instance, Sample
Name, Sample Mass, and Sample Operator and skip the Sample
Description and Sample Comment), you will need to put all the
delimiters in as placeholders to indicate which fields should be filled in
(example: Sample7,0.52,,,Joe Smith). The commas indicate that Joe
Smith goes in the Operator field.
A sample import text file could be:
Example 1
Sample5
Sample6,0.50
Sample7,0.52,,,Joe Smith
Sample 8,0.49,description,comment,Joe Smith
Example 2
Sample19,0.45
Sample20,0.46
Sample21,0.43
2. Position the cursor in the Export Format and click the mouse to
place the cursor at the point in the format to edit a field. If
additional fields are desired, refer to User Defined Fields for
information on creating them, page 4–63.
3. Select a Field from the Fields box and click Add Field to Export
Format to add a field.
4. Highlight a Field in the Export Format and then press Delete on
the keyboard to delete it.
Transmit Data permits the operator to select sample data and transmit
the data to a peripheral device. Sample data can be transmitted from
a serial port or over a network.
NOTE Before data is transmitted a transmission data format must be
defined. Refer to Transmit Data Format Configuration, page 5–30.
1. Click and drag the mouse pointer to select the rows with sample
data to transmit.
NOTE If no sample is selected only the last sample in the spreadsheet will
be transmitted.
2. Click the Sample menu and select Transmit. The Transmission
Format selection screen will appear.
NOTE The transmission format selection screen will not appear unless there
is more than one format available.
Transfer Export
1. Click and drag the mouse pointer to select the rows with sample
data to export to a file.
2. Click the Sample menu and select Transfer Export. The export file
selection screen will appear.
The log file is a history of past events. When any one of the following
events occurs, it is recorded in the log file.
Ambient monitor parameter values out of range
Date of last calibration, drift or blank
Date scheduled maintenance is performed
Network errors and network sign-on Errors
Sample aborted
Sample deleted
Standard check out of range
1. From the Maintenance menu, click View Log Files. The Log File
will appear.
2. Click Print to send a printout of the log file to the system printer.
3. Click OK when finished.
NOTE Default counters will only appear for one unit. If you’re using two
units you’ll need to enter all counters for the second unit.
Figure 6-1
Furnace Flow Filter Assembly
! Loosely pack the filter tube with 5 grams of glass wool. If the
CAUTION filter tube is pack to tightly it will restrict the flow of gas.
5. Remove the glass wool from the filter tube, clean the tube and
loosely repack it with 5 grams of glass wool.
6. To remove the micron filter slide it to the right and swing it out.
7. Replace the micron filter. It will be necessary to remove the
fittings on the ends of the filter and install them on the
replacement filter.
8. Install the left side panel.
9. Connect the instrument to facility power and then turn the AC
power on.
10. Start the applications software.
The outer surface of the instrument may be cleaned with a damp cloth.
Do not use organic solvents or abrasive materials.
Do not allow any water to get inside the interior of the
instrument.
Illustrations .................................................................................7–2
Theory of Operation......................................................................7–3
General Theory, Equations, and Definitions .................................7–5
Predictive Alogrithm for IT and FT .........................................7–6
NOTE The furnace is designed with a carbon monoxide detector that will
sound a warning alert if a carbon monoxide leak is detected inside the
furnace. This detector is not intended to replace Facility
Detectors. LECO recommends that all installations have an industrial
carbon monoxide detector installed near the instrument.
NOTE The carbon monoxide detector may require a longer warm up time
(approximately 10 minutes) after the instrument has been off for
extended periods of time. If the alarm sounds, wait 10 minutes for
any accumulated gas to dispel and then turn it off and back on.
Deformation Equation
IT {[Rounding]>9}And{[Height]<[Initial
Height]*0.9}
ST {[Height]<=[Width]}
HT {[Height]<=[Width]*0.5}
FT {[Height]<=[HT Height]*0.3}
MP {[Height]<[Initial Height]*0.1}
Rounding: The number of pixels in the largest circle that will fit in the
tip of a cone
Height: Height of the sample
Width: Width of the sample
0 1 2 3 4
IT ST HT FT
Figure 1
Ambient Chart
1. Click Diagnostics and select Chart to display the Ambient Monitor
Chart screen.
2. Click Start to system check and test the systems listed on the
screen.
3. The results of system check will be displayed to the right of the
system being checked under the results column. Also, the circle
will be filled with green to indicate the system checked passed or
with an X to indicate the system checked failed.
4. Click Print to print the results of the system check on the system
printer.
2. The meter will display the current temperature for the selection.
Poll Devices
Click Poll Devices to send a signal over the network to determine what
is connected to the network. Network hardware should appear under
devices indicating they are functioning and signing on to the network.
Upgrade a Device
1. To upgrade a device with a new version of application firmware,
click the Device to upgrade. Then click Download to download the
new firmware.
2. Click Reset Board to restart firmware application program on the
circuit board.
Network Definitions
Device—The name of the electronic assembly connected to the
network.
MAC-id—The network ID number assigned to the electronic assembly
connected to the network. This number is assigned at power up and
can vary.
Class—The type number of the electronic assembly signed on to the
network.
Instance—A unique number assigned to an electronic assembly. If two
or more of the same type electronic assemblies are installed in the
instrument this number will be different for each assembly and is used
by the controller to differentiate one from the other.
Serial—The hardware ID number assigned to the electronic assembly.
This number is assigned during manufacturing and is unique to each
electronic assembly. The serial number is stored on the circuit board in
a PROM.
Version—The version number of the application software located on
the electronic assembly. This software can be upgraded from the
network procedure.
Checksum—A number unique to the application software to verify if
the software was properly installed. There will be a checksum number
supplied with any software upgrades. Make sure that the number
appearing in the checksum cell is the same as the number supplied
with the software upgrade.
NI Version—The version number of the network control software
installed in the electronic assembly. This software is located in a PROM
and cannot be upgraded from the network procedure.
Hardware ID—The identification number of the hardware.
FPGA Version—The version number of the firmware.
NOTE The carbon monoxide detector may require a longer warm up time
(approximately 10 minutes) after the instrument has been off for
extended periods of time. If the alarm sounds, wait 10 minutes for
any accumulated gas to dispel and then turn it off and back on.
NOTE The furnace is designed with a carbon monoxide detector that will
sound a warning alert if a carbon monoxide leak is detected inside the
furnace. This detector is not intended to replace Facility
Detectors. LECO recommends that all installations have an industrial
carbon monoxide detector installed near the instrument.
POSSIBLE INJURY
WARNING After AC power is turned off and disconnected, permit
the combustion tube to cool to ambient temperature
before performing this procedure.
Figure 9-1
Furnace Assembly
Figure 9-2
Furnace End Disassembly
Figure 9-3
Combustion Tube with D-Tube
14. Remove the four Screws and remove the combustion flange.
Figure 9-4
Furnace Access Cover
Figure 9-5
Thermocouple and End Plate
Figure 9-6
Combustion Tube and Thermocouple
21. Install and tighten the two top combustion tube end assembly
mounting screws. Refer to Figure 9-2 on page 9–5.
22. Install the two Top Insulation Plates.
23. Install the Front Access Plate.
24. Install the front O-ring over the combustion tube. A new o-ring
should be used.
25. Install the Front Combustion Flange Assembly.
Figure 9-7
Furnace End Assembly
Figure 9-8
Furnace D-Tube Installation
31. Hold the D-Tube from the front and push the Thermocouple into
the combustion tube. Be careful not to hit the supports inside the
combustion tube.
32. Install the Furnace Top Cover.
33. Install the Top Panel and Side Panels.
34. Install the Rear Cover making sure the CO2 safety switch is
closed. A click will be heard when the switch is closed.
35. Connect the instrument to facility AC power.
625-501-625
MANIFOLD
193-055
WASHER
611-790 3 REQ'D
O-RING 206
4 REQ'D 625-501-627 190-867
PLATE SCREW
4 REQ'D
625-501-624
BLOCK
801-906
PIN DOWEL
625-501-646
190-877 BLOCK
SET SCREW 619-316
2 REQ'D TUBE
765-976
O-RING 208
772-520
O-RING 108
3 REQ'D
625-501-626
625-501-655 BLOCK
ASSY FILTER
619-126
INSERT
2-REQ'D
760-841
O-RING 011
2 REQ'D
ILS-00608-A
Figure 10-8
Gas Filter Panel Assembly
A
Abort an Analysis .................................................................... 5–9
Accessories List..................................................................... 1–23
Add Standards ........................................................................ 5–4
Ambient Chart ........................................................................ 8–3
Ambient Monitor...................................................................... 8–3
Analysis Method .................................................................... 4–42
Analysis, Delay ..................................................................... 5–10
Analyze Row in the Spreadsheet, Go to .................................... 4–39
Analyze Samples ..................................................................... 5–9
Apply Power ......................................................................... 2–25
Ash Cone Sample Preparation ................................................... 4–5
Auto Widths.......................................................................... 4–39
B
Backup, Data ........................................................................ 5–41
Backup/Restore..................................................................... 4–62
C
Calibration ............................................................................. 5–3
Calibration, View ..................................................................... 5–5
Caution, Symbols .................................................................. 1–16
Cleaning the Instrument........................................................... 6–9
Clone a Method ..................................................................... 4–47
Combustion Tube Replacement.................................................. 9–4
Components List ................................................................... 1–23
Configuration Menu ............................................................... 4–30
Configuration, Method............................................................ 4–42
Configuration, Sample Display................................................. 4–36
Configuration, System............................................................ 4–40