Indian Standard: Specification For Density Hydrometers
Indian Standard: Specification For Density Hydrometers
Indian Standard: Specification For Density Hydrometers
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(Reaffirmed 2014)
(Reaffirmed 2010)
UDC 531.756.3
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(Reaffirmed 2008)
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(Reaffirmed 2006)
© Copyright 1982
BUREAU OF INDIAN STANDARDS
(Reaffirmed 2005)
MANAK BHAVAN. 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
Gr 5 April 1982
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IS : 3104 ( Part I ) - 1982
Indian Standard
SPECIFICATION FOR
DENSITY HYDROMETERS
PART I REQUIREMENTS
( First Revision )
Members
S H R I S . V. GULAVANE ( Alternate to
Dr M. Sankar Das )
SHRI K. K. S. AGARWAL Development Commissioner, Small Scale
Industries, New Delhi
D R C . S . BAJWA Defence Science Laboratory Ministry of Defence,
Delhi
D R N . K . BANERJEE Indian Agricultural Research Institute, New
Delhi
DR K. S. R A M ( Alternate )
S H R I N . G . BASAK Directorate General of Techanical Development
S H R I I. K. K A P O O R ( Alternate )
S H R I P. K. BHATTACHARYYA National Council of Educational Research &
Training, New Delhi
COL M . CHAKRABORTY Director-General Armed Forces Medical Services,
Ministry of Defence, New Delhi
S H R I VEDA PRAKASH GUPTA Hicks Thermometers ( India ) Ltd, Aligarh
S H R I S . C . K A P I L A ( Alternate )
SHRI J. C. MAKANI Ministry of Defence ( DGI )
S H R I G . S . S H U K L A ( Alternate )
DR J. R. MERCHANT Institute of Science, Bombay
SHRI MOHINDER NATH National Physical Laboratory (CSIR), New
Delhi
SHRI B. G. M A T H U R ( Alternate )
( Continued on page 2 )
© Copyright 1982
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indian Copyright Act ( X I V of 1957 ) and
reproduction in whole or in part by any means except with written permission of the
publisher shall be deemed to be an infringement, of copyright under the said Act.
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IS : 3104 ( Part I ) - 1982
( Continued from page 1 )
Members Representing
DR S. K. MUKHERJEE Indian Council of Agricultural Research, New
Delhi
DR N. N. GOSWAMI ( Alternate )
SHRI P. R. R A O Borosil Glass Works Ltd, Bombay
S H R I A. K . B A N S A L ( Alternate )
SHRI H . N . RAVI Modern Instruments, Bangalore
S H R I H A R I N . MURTHY ( Alternate )
D R F . L . SALDHANA Haffkine Institute for Training, Research and
Testing, Bombay
S H R I A. B. C H U N O D K A R ( Alternate )
S H R I BHANU K . SAMPAT The Scientific Indian Glass Co Ltd, Calcutta
S H R I D . R . S E N ( Alternate )
S H R I S . K . SEHGAL Tarsons Products Ltd, Calcutta
SHRI J. C. SHANDILYA Top Syringe Manufacturing C o , Bombay
S H R I J. K. W A D ( Alternate )
DR B. C. SINHA Central Glass & Ceramic Research Institute
( C S I R ) , Calcutta
S H R I R. S E N ( Alternate )
S H R I G . P . SHIVASTAVA India Meteorological Department, New Delhi
S H R I S . G O P I N A T H ( Alternate )
DR H A R I B H A G W A N , Director General, ISI ( Ex-officio-Member )
Director ( Chem )
Secretary
SHRI ANJAN KAR
Deputy Director ( Chem ), ISI
Members
SHRI S. GHOSH National Test House, Calcutta
SHRI D. R. GUPTA Central Revenue Control Laboratory, New Delhi
S H R I K E S H A V P R A S A D ( Alternate )
DR U. K. MISHRA Alcohol Technologist to Government of U. P . ,
Kanpur
SHRI SAMIUL HAQUE Directorate of Weights & Measures, New Delhi
S H R I R . SRINIVASAM ( Alternate )
S H R I K . K . SHARMA Daurala Sugar Works Ltd, D a u r a l a
S H R I N . N . M E H T A ( Alternate )
SHRI Y. D. SHARMA All India Instruments Manufacturers and Dealers
Association, Bombay
SHRI P R I T H I R A J ( Alternate )
2
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IS : 3104 ( P a r t I ) - 1982
Indian Standard
SPECIFICATION FOR
DENSITY HYDROMETERS
PART I REQUIREMENTS
( First Revision )
0. FOREWORD
0.1 This Indian Standard ( Part I) ( First Revision ) was adopted by the
Indian Standards Institution on 28 January 1982, after the draft finalized
by the Laboratoryware and Related Apparatus Sectional Committee had
been approved by the Chemical Division Council.
0.2 This standard was first published in 1965. However, with the revision
of ISO 649-1968 'Laboratory glassware-Density hydrometers for general
Purposes' issued by the International Organization for Standardization
(ISO), the Committee responsible for the preparation of the standard
decided to revise it with a view to aligning it with the international
standard.
0.3 In this revision, the standard has been prepared in two parts. Part I
covers requirements of hydrometers and Part II covers methods of test
and use of these hydrometers.
0.4 Part I covers eight series of hydrometers comprising five main series
and three special sub-series. Each of the five main series comprises
hydrometers which cover the density interval 600 to 2 000 kg m3 or 0.6 to
2.0 g/ml ( see 11.1 ). These hydrometers are graduated to indicate density
at 20° C and are appropriate for use in liquids of low, medium and high
surface tension. The hydrometers of the three special sub-series are
graduated to indicate density at either 20 or 15°C, have smaller
tolerances, are limited to the range 600 to I 100 kg m3 or 0.6 to 1.1 g/ml
and are meant for use in liquids of low surface tension.
0.5 While preparing this standard, need was felt to have reference
temperature of 27°C. However, this has not been possible at present, as
calibration tables are not available for 27°C. Therefore, this standard
would be reviewed to change the reference temperature from 20 to 27°C
at an opportune time.
3
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IS : 3104 ( P a r t I ) - 1982
1. SCOPE
1.1 This standard ( Part I ) specifies requirements for glass hydrometers
having constant mass and graduated to indicate density ( kg/m 3 or g/ml )
at 20°C.
NOTE — Hydrometers of Special sub-series ( see 0.4 and 4.2 ) shall be graduated
to indicate density at either 20 or 15°C.
2. TERMINOLOGY
2.0 For the purpose of this standard, the following definitions in
addition to those given in IS : 1382-1981*, shall apply.
2.1 Density — The mass in kilograms per cubic metre ( kg/m 3 ) or in
grams per millilitre ( or cubic centimetre ) ( g/ml or g/cm 3 ) of a liquid at
a specified temperature.
2.2 S t e m — The thin tubing containing the scale.
2.3 Bulb — The wider portion of the hydrometer containing the loading
material.
3. BASIS OF SCALE
3.1 The basis of the scale shall be density ( mass per unit volume ) in
kilograms per cubic metre ( kg/m 3 ). The use of grams per cubic centi-
metre ( g/cm 3 ), for which the symbol g/ml may be used, is accepted.
NOTE — T h e term millilitre (ml) is commonly used as special n a m e for cubic
centimetre (cm 2 ), in accordance with a decision of the twelfth Conference General
des Poids et Mesures. T h e term millilitre is acceptable, in general, for reference
to capacities of volumetric glassware and is used in the present text.
4
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IS : 3104 ( Part I ) - 1982
4.2 Ranges — Each of the five main series of hydrometers shall cover a
total range of 600 to 2 000 kg/m 3 or 0.600 to 2.000 g/ml, each hydrometer
having a range of 20 kg/m3, 50 kg/m 3 or 100 kg/m 3 or 0.020 g/ml, 0.050
g/ml or 0.100 g/ml. The lower nominal limits of the scales of the L20
series hydrometers shall be 600, 620, 640, etc, or 0.600, 0.620, 0.640, etc.
Those of the L50, M50 and S50 series hydrometers shall be 600, 650, 700,
etc, or 0.600, 0.700, 0.800, etc, according to whether the scales are based
on kilograms per cubic metre or grams per millilitre.
5. REFERENCE TEMPERATURE
5.1 The reference temperature for density hydrometers, excluding the
special sub-series L50SP, M50SP and S50SP, shall be 20°C. When used
in a liquid at this temperature, the hydrometer shall indicate the density
of the liquid at 20°C.
6. SURFACE TENSION
6.0 General — The adjustment shall be related to the following specific
capillary conditions.
6.1 When the hydrometer is slightly displaced from its equilibrium
position in a liquid, the stem passes through the liquid surface without
causing any apparent alteration in the shape of the meniscus.
6.2 The hydrometer scale shall be adjusted either for a given liquid
having a given surface tension or for one of the standard categories of
surface tension given in Appendix A. Except where the highest precision
is required, one of the standard categories of surface tension given in
Appendix A shall be used.
6.2.1 For hydrometers of the highest precision, intended for use in
particular liquids, for example, alcohol solutions, the surface tension
5
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IS : 3104 ( Part I ) - 1982
7.2 The middle of the thickness of a scale line shall be taken as its
definitive position.
8. IMMERSION
8.1 Hydrometers shall be graduated for use with the emergent stem dry,
except in the immediate vicinity of the meniscus.
9. MATERIALS
9.1 Bulb a n d S t e m — The bulb and the stem shall be made of a suitable
transparent glass, selected and processed to be as free as possible from
stress and visible defects, and having a coefficient of cubical thermal
expansion of (25 ± 2) × 10-6 (°C)-1.
9.2 Loading Material — The loading material shall be fixed in the
bottom of the hydrometer. After the finished hydrometer has been kept
in a horizontal position for 1 h at 80°C and subsequently cooled in that
position, the instrument shall meet the requirements of 10.3.
9.3 Scale Strip — The strip on which the scale and inscriptions are
marked shall have a smooth matt surface. The strip shall show no
evidence of charring, and shall not become discoloured or distorted when
the stem is exposed for 1 h to a temperature of 80°C.
N O T E — If a hydrometer is intended to be used at a temperature above 80°C,
the loading material and the strip bearing the scale shall meet the requirements
of 9.2 and 9.3 at a temperature slightly above the temperature of use.
6
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IS : 3104 ( Part I ) - 1982
10.2 There shall be no abrupt changes in their cross section ( see Fig, 1 ).
NOTE — The tapered design shown in Fig. 1 is preferred, but any design which
does not permit air bubbles to be trapped is acceptable.
10.3 The cross-section of the stem shall remain unchanged for at least
5 mm below the lowest graduation line on ??? scale.
10.4 The stem shall extend unchanged in diameter at least 15 mm above
the uppermost graduation line on the scale.
10.5 T h e hydrometer shall float with its axis vertical to within 1.5° of
arc.
10.6 There shall be no loose material in the instrument.
7
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IS : 3104 ( Part I ) - 1982
10.7 The strip on which the scale and inscriptions are marked shall
remain securely fastened in place at the temperature of use ( see 9.3 ).
12. SCALE
12.0 General — No hydrometer shall have more than one type of scale.
If a hydrometer has duplicate scales, the values indicated by them shall
not significantly differ, and both scales shall comply with the requirements
of 13.
12.1 Recommended scales for the hydrometers are illustrated in Fig. 2.
8
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(1) (2) (3) (4) (5) (6) (7) (8) (9) (10) (12) (12)
Lines
L20 335 20 0.020 100 × 0.2 100 × 0.000 2 105 36 40 108 132 5 to 10
L50 335 50 0.050 100 × 0.5 100 × 0.000 5 125 23 27 50 65 2 to 5
M50 270 50 0.050 50 × 1 50 × 0.001 70 20 24 30 45 2 to 5
*For the diameter of the stem to exceed 4 mm (as required by 11 2) these volumes, for hydrometers covering the
range 1 700 to 2 000 kg/m 3 or 1.7 to 2.0 g/ml, will be nearer the maximum value than the minimum value.
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IS : 3104 ( Part I ) - 1982
12.2.6 The short, medium and long lines shall each be vertically
disposed so that either the mid-points, or the right hand ends or the left
hand ends of all graduation lines He on an imaginary line parallel to the
axis of the instrument. In the latter two cases, the vertical line may,
alternatively, be marked.
10
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IS : 3104 ( Part I ) - 1982
12.3.2 On hydrometer scales whose smallest interval is 2 kg/m 3 , or
2 g/ml:
a) every fifth graduation line shall be a long line, and
b) there shall be four short lines between two consecutive long
lines.
12.3.3 On hydrometer scales whose smallest interval is 5 kg/m 3
or 5 g/ml:
a) every tenth graduation line shall be a long line,
b) there shall be four medium lines between two consecutive long
line, and
c) there shall be one short line between two consecutive medium
lines and between consecutive medium and long lines.
11
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IS : 3104 ( Part I ) - 1982
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IS : 3104 ( Part I ) - 1982
12.4.3 The highest and lowest graduation lines of the nominal limits
shall be figured in full.
12.4.4 At least every tenth line shall be figured.
12.4.5 For density values expressed in grams per cubic centimetres, the
decimal sign shall be included for numbers expressed in full, but may be
omitted from abbreviated numbers.
13. ACCURACY
13.1 For the hydrometers the maximum instrument errors at any point on
the scale when determined in accordance with the method given in
Part II of this standard shall not exceed the values given in Table 3. It is
recommended that the hydrometers in the special sub-series be supplied
with certificates of correction, when required for reference purposes.
13
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IS : 3104 ( Part I ) - 1982
14.1.1 The hydrometers may also be marked with the Standard Mark.
14.1.2 The use of the Standard Mark is governed by the provisions of Bureau of
Indian Standards Act, 1986 and the Rules and Regulations made thereunder.
The details of conditions under which the licence for the use of Standard Mark
may be granted to manufacturers or producers may be obtained from the Bureau
of Indian Standards.
14
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IS : 3104 ( Part I ) - 1982
A P P E N D IX A
( Clause 6.2 )
STANDARD CATEGORIES OF SURFACE TENSION
FOR HYDROMETERS
A-0. GENERAL
A-0.1 The standard categories of surface tension given in Table 4 are
adopted for hydrometers for technical use, so as to provide a precise basis
for adjustment and verification and to permit the attainment of the
appropriate accuracy in measurements in the liquids indicated. The
adoption of these surface tension categories does not preclude the use of
other surface tensions as the basis of or for the adjustment of hydrometers,
provided such surface tensions are marked, in millinewtons per metre,
within the hydrometers or reference is made to the type of the liquid
(see 14.1.0).
APPENDIX B
( Clause 15.1 )
SAMPLING OF DENSITY HYDROMETERS
B-1. SCALE OF SAMPLING
B.1.1 Lot — All the hydrometers of same size, same series/sub-series and
same range, shall be grouped together to constitute a lot.
B-1.3 The number of samples to be taken from a lot shall depend on the
size of the lot and shall be according to Table 5.
B-1.3.1 The hydrometers in the sample shall be selected at random
from the lot. In order to ensure the randomness of selection, procedures
given in IS : 4905-1968* may be followed.
15
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cleaned
* A c e t i c a c i d s o l u t i o n s s h o w e x t r e m e v a r i a b i l i t y o f turface t e n s i o n .
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IS : 3104 ( P a r t I ) - 1982
(1) (2)
Up to 25 10
26 „ 50 16
51 „ 100 26
101 and above 41
Up to 25 5 0 First 5 5 0 2
Second 5 10 1 2
26 to 50 8 0 First 8 8 0 2
Second 8 16 1 2
51 to 100 13 0 First 13 13 0 2
Second 13 26 1 2
101 and above 20 1 First 20 20 0 3
Second 20 40 3 4
17
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IS : 3104 ( P a r t I ) - 1982
B-2.2 T h e lot having met the requirements for accuracy shall be tested
for other requirements of the specification. For this purpose, the
hydrometers tested for accuracy and found satisfactory according
to B-2.1 and the hydrometers remaining in the sample drawn according
to Table 5 shall be used. A hydrometer failing to satisfy any of these
requirements shall be considered as defective.
B-2.2.2 The lot shall be rejected without further testing if the number
of defectives found in the first sample is greater than or equal to the
corresponding rejection number given in col 8 of Table 6.
18
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BUREAU OF INDIAN STANDARDS
Headquarters:
Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002
Telephones : 331 01 31 Telegrams : Manaksanstha
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