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    1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

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    1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

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    1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    7 views7 pages

    Ex

    Uploaded by

    bayarali1993
    1. The document describes a pipette calibration experiment conducted by an analytical laboratory. 2. The procedure involved weighing an empty beaker, adding measured volumes of tap water using a 10 mL pipette, and weighing the beaker with water to calculate volumes and check for accuracy. 3. The results showed the measured volumes were close to the expected volumes, with less than 1% error, indicating the pipette was properly calibrated.

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    Analytical laboratory

    Name of experiment: Pipette Calibration

    Department: oil

    Group: D

    Chemicals and Supplies


    Chemicals Supplies
    Tap water in room temperature Beaker 10 ml
    Pipette 10 ml
    Scale

    Procedure:
    1. Rinse the given pipette and beaker with small amount of tap water.
    2. Weight the empty beaker and record the mass.
    3. Use the empty clean and dry beaker and then use the pipet to add a volume of
    water (ml), students can take the variables shown table below, and record the
    mass of the water in the scale.

    9.9700 mL 10.0360 mL 9.9650 mL 10.0150 mL 10.0200 mL

    4. Measure the temperature of the water at room conditions and record it.
    5. notes the density of water at room temperature from table (Density of Liquid
    Water From 0°C to 100°C).
    6. Repeat step-3 for all students group to fined mass and volume measurements.
    7. Complete all calculations.
    8. Complete all information at table below.
    9. sketch graphic data between densities and volumes that calibrated and
    calculated.
    Analytical laboratory

    (Calibration Table)

    Solution Volume Beaker Beaker mass Water Density Volume Temp.


    No. ml mass + water mass mass g/ml water °c
    g g g ml
    1 3 42.489 45.460 2.971 0.998 2.976 18
    2 4 50.899 54.889 3.991 0.998 3.997 18
    3 5 48.908 53.894 4.986 0.998 4.995 18
    4 2 48.896 50.817 1.104 0.998 1.106 18
    5

    Calculations:

    Volume = 3 ml
    beaker mass = 42.489 g
    beaker mass+water mass = 45.460 g
    water mass = 2.971 g
    density = 0.998 g/ml at temp 18 °c

    water volume = mass /density

    = 2.971/0.998
    = 2.976 ml
    Analytical laboratory

    Discussion:

    We cleaned and dried a beaker and


    a pipette
    Then an empty beaker weight
    Then we added 3 ml of distilled
    water, then weighed it again, and
    calculated the weight of the water
    and its density at room
    temperature.
    It showed us through this
    experiment that the percentage of
    error is small, it is 0.024
    It was a successful experiment .
    Analytical laboratory
    Analytical laboratory

    sketch graphic data between densities and volumes that calibrated and
    calculated.

    v
    6

    v
    3

    0
    0 1 2 3 4 5 6
    Analytical laboratory

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