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Oil (Uco Efb Pome Mef) Receiving - in Bulk

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NO VB-QC-SOP-015
REV. NO 0
REV. DATE 01 OCTOBER 2023
PAGE 1 OF 1 PAGE

STANDARD OPERATING
TITLE : OIL (UCO/EFB/POME/MEF) RECEIVING - IN BULK (DISCHARGE PORT) PROCEDURE

Responsibilities Process Flow Key Control Procedures

1.0 The discharge survey includes both Q & Q


Logistics Executive 1.0 Logistics appoint surveyor for discharge survey. determination.

1.1 Instruction for quality will be given by QC


Chemist on the sampling steps and analysis
parameters.
Logistics Executive 2.0 Logistics will arrange for collection from Terminal -- draw sample from shore tank:
Shore Tank to Vance. (Rock Bottom, Bottom, Upper Bottom, Middle,
Top) : 2x250ml each level.
- 1x250ml from each level (to be sent to Vance,
attn: Chemist) .
Unloading 3.0 Drain 1 pail (35kg) and draw sample in 1x250ml -1x250ml from each level to be composited and
tested by 3rd party laboratory based on the
operator plastic bottle from bottom tanker discharge point. following full parameters:
FFA , M&I, IV, Mineral Oil, Ester Content , ICP,
Insoluble Impurities and Soap.

1.2 QC will update the compilation tested results


4.0 Send sample to the lab by draw sample in for Loadport and Discharge port in QC Skype
Unloading operator 1x250ml plastic bottle from bottom tanker Chat.
discharge point. 2.1 Instruction to maintain heating and stirrer will
be given by Logistics to the terminal as per
advice from QC and production.

3.1 Operation personnel shall conduct spin test


for the sample drawn. -Spin Test by centrifuge:
5.0 Tests YES Place 15ml sample inside a tube & heat in water
and bath 80DegC for 2 minutes. Centrifuge at 4000
approval RPM for 2 minutes. Compare centrifuged tube
against the printed reference that is provided by
QC.
NO Approval:
Passed : Less than 0.3ml (2%)
Unloading Operator 7.0 Draw top sample for Failed : More than 0.3ml (2%)
centrifuge analysis
9.0 If top sample pass, unloading operator will
drain into IBC until spin test pass (up to 3 IBC).
Spin test wil be conducted after every IBC
draining.

NO 11.0 Production to decide on discharge strategy


Chemist YES
8.0 Tests and as per advice from QC.
Approval

9.0 Unloading operator


to drain into IBC and
centrifuge at bay (up to
3 IBC)

NO 10.0 Tests and YES


approval
11.0 QC to advice 6.0 QC give
production on quality and approval to
production to decide on discharge.
discharge strategy. PREPARED BY CHECKED BY APPROVED BY

END END
JUNIOR CHEMIST SENIOR CHEMIST HOD

Copyright © 2023 Vance Bioenergy

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