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Engineering Standard: IPS-E-PR-745
Engineering Standard: IPS-E-PR-745
ENGINEERING STANDARD
FOR
FIRST EDITION
OCTOBER 2014
This Standard is the property of Iranian Ministry of Petroleum. All rights are reserved to the owner.
Neither whole nor any part of this document may be disclosed to any third party, reproduced, stored in
any retrieval system or transmitted in any form or by any means without the prior written consent of the
Iranian Ministry of Petroleum.
Oct. 2014 IPS-E-PR-745(1)
FOREWORD
The Iranian Petroleum Standards (IPS) reflect the views of the Iranian Ministry of Petroleum and are
intended for use in the oil and gas production facilities, oil refineries, chemical and petrochemical
plants, gas handling and processing installations and other such facilities.
IPS is based on internationally acceptable standards and includes selections from the items
stipulated in the referenced standards. They are also supplemented by additional requirements
and/or modifications based on the experience acquired by the Iranian Petroleum Industry and the
local market availability. The options which are not specified in the text of the standards are
itemized in data sheet/s, so that, the user can select his appropriate preferences therein
The IPS standards are therefore expected to be sufficiently flexible so that the users can adapt
these standards to their requirements. However, they may not cover every requirement of each
project. For such cases, an addendum to IPS Standard shall be prepared by the user which
elaborates the particular requirements of the user. This addendum together with the relevant IPS
shall form the job specification for the specific project or work.
The IPS is reviewed and up-dated approximately every five years. Each standards are subject to
amendment or withdrawal, if required, thus the latest edition of IPS shall be applicable
The users of IPS are therefore requested to send their views and comments, including any
addendum prepared for particular cases to the following address. These comments and
recommendations will be reviewed by the relevant technical committee and in case of approval will
be incorporated in the next revision of the standard.
GENERAL DEFINITIONS:
Throughout this Standard the following definitions shall apply.
COMPANY:
Refers to one of the related and/or affiliated companies of the Iranian Ministry of Petroleum such as
National Iranian Oil Company, National Iranian Gas Company, National Petrochemical Company
and National Iranian Oil Refinery And Distribution Company.
PURCHASER:
Means the “Company” where this standard is a part of direct purchaser order by the “Company”,
and the “Contractor” where this Standard is a part of contract documents.
CONTRACTOR:
Refers to the persons, firm or company whose tender has been accepted by the company.
EXECUTOR:
Executor is the party which carries out all or part of construction and/or commissioning for the
project.
INSPECTOR:
The Inspector referred to in this Standard is a person/persons or a body appointed in writing by the
company for the inspection of fabrication and installation work.
SHALL:
Is used where a provision is mandatory.
SHOULD:
Is used where a provision is advisory only.
WILL:
Is normally used in connection with the action by the “Company” rather than by a contractor,
supplier or vendor.
MAY:
Is used where a provision is completely discretionary.
Oct. 2014 IPS-E-PR-745(1)
1. SCOPE ................................................................................................................................... 2
2. REFERENCES ................................................................................................................................ 2
3. SYMBOLS AND ABBREVIATIONS ............................................................................................... 2
4. UNITS ................................................................................................................................... 3
5. GENERAL ................................................................................................................................... 3
5.1 Definition of Vacuum Pumps and Related Terms ................................................................ 3
5.2 Definition of Steam Jet Ejector and Related Term ............................................................ 11
5.3 Vacuum Equipment Classification ...................................................................................... 16
5.4 Type Selection Considerations ........................................................................................... 16
6. DESIGN CRITERIA ....................................................................................................................... 20
6.1 Common Basic Calculation ................................................................................................. 20
6.2 Design Considerations for Ejectors .................................................................................... 23
7. VACUUM SAFETY........................................................................................................................ 28
APPENDICES:
APPENDIX A ................................................................................................................................. 29
APPENDIX B TYPICAL PIPING AND INSTRUMENT DIAGRAMS (P & IDS) AROUND VACUUM
SYSTEMS ................................................................................................................. 31
APPENDIX C ESTIMATION OF POWER CONSUMPTION FOR VACUUM PUMPS ................... 33
APPENDIX D STANDARD EJECTOR UNITS DESIGNATIONS CONFORMING TO HEAT
EXCHANGE INSTITUTE .......................................................................................... 34
APPENDIX E TYPICAL EJECTOR DATA SHEET ........................................................................ 36
Oct. 2014 IPS-E-PR-745(1)
0. INTRODUCTION
"Pressure Reducing/Increasing Machineries and/or Equipment" are broad and contain variable
subjects of paramount importance. Therefore, a group of process engineering standards are
prepared to cover the subject.
This group includes the following standards:
VACUUM EQUIPMENT
(VACUUM PUMPS AND STEAM JET EJECTORS)
This Standard covers the process aspects of engineering calculations for vacuum systems and the
relevant equipment.
Since the working mechanism of certain types of vacuum pumps such as positive displacement
types are the same as gas compressors, these types are not discussed in detail in this standard
and therefore the "Design Criteria" section mainly discusses about the "Ejectors", which are the
most frequently used vacuum devices in Oil, Gas and Petrochemical processes.
In this standard, some of the subjects are adapted from the following specifications and handbooks:
− “Applied Process Design”, vol.1, 3th Edition, by Ernest Ludwig.
− Design Practice by ExxonMobil Engineering, “section XI-J (Ejectors)”, 2001
− “Process Plants Division, by Foster Wheeler”, Process STD 704 (Steam Jets & Ejectors),
Rev.10, 2002.
− “Standard Practice, by JGC”, STD-09-040 (Section3, Ejectors) Rev.0, 2003.
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1. SCOPE
This standard is intended to cover requirements for process design, selection of proper type of
vacuum equipment and process calculation including estimation for number of stages, air leakage
and rough estimation of utility consumption.
Note 1:
This standard specification is reviewed and updated by the relevant technical committee on
Aug. 1998. The approved modifications by T.C. were sent to IPS users as amendment No. 1
by circular No. 30 on Aug. 1998. These modifications are included in the present issue of
IPS.
Note 2:
This is a revised version of this standard, which is issued as revision (1)-2014. Revision (0)-
1993 of the said standard specification is withdrawn.
2. REFERENCES
Throughout this Standard the following dated and undated standards/codes are referred to. These
referenced documents shall, to the extent specified herein, form a part of this standard. For dated
references, the edition cited applies. The applicability of changes in dated references that occur
after the cited date shall be mutually agreed upon by the Company and the Vendor. For undated
references, the latest edition of the referenced documents (including any supplements and
amendments) applies.
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4. UNITS
This standard is based on international system of units (SI), as per IPS-E-GN-100 except where
otherwise specified.
5. GENERAL
Vacuum equipment, as called by ISO (International Organization for Standardization),"Vacuum
Pumps", are defined as devices for creating, improving and/or maintaining a vacuum.
In OGP industries the name "Vacuum Pump" is conventionally used for rotating machine vacuum
devices. Vacuum equipment are divided into two main groups, Vacuum Pumps and Ejectors.
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5.1.1.4.5 Cryopump
An entrapment pump consisting of surfaces refrigerated to low temperature sufficient to condense
residual gases. The condensate is then maintained at a temperature such that the equilibrium
vapour pressure is equal to or less than the desired low pressure in the chamber.
Note: The temperature chosen shall be in the range below 120 K depending on the nature of
the gases to be pumped.
5.1.2.1.2 Inlet
The port by which gas to be pumped enters a pump.
5.1.2.1.3 Outlet
The outlet or discharge port of a pump.
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Note: The term pump oil is also commonly used to describe pump fluids used in oil vapour
pumps. This note does not apply to the German expression.
5.1.2.3.2 Nozzle
The part of an ejector or diffusion pump used to direct flow of the pump fluid order to produce the
pumping action.
5.1.2.3.3 Jet
The stream of pump fluid issuing from a nozzle, in an ejector or diffusion pump.
5.1.2.3.4 Diffuser
The converging section of the wall of an ejector pump.
5.1.2.3.7 Skirt
The lower part of the nozzle assembly, usually enlarged, separating the returning condensed pump
fluid and the vapour generated by the pump boiler.
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5.1.3 Accessories
5.1.3.1 Trap
A device in which the partial pressure of the constituents of a mixture of gases and vapours is
reduced by physical or chemical means.
5.1.3.2 Baffle
A system of screens, possibly cooled, placed near the inlet of a vapour jet or diffusion pump, to
reduce back-streaming and back-migration.
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Note: For some pumps the failure does not occur abruptly and the critical backing pressure
cannot then be precisely stated.
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1. Diffuser 7. Suction
2. Suction Chamber 8. Discharge
3. Steam Nozzle 9. Steam Inlet
4. Nozzle Extensions (if used) 10. Nozzle Throat
5. Steam Chest 11. Diffuser Throat
6. Nozzle Plate (if used)
a) Absolute Pressure
Is the pressure measured from absolute zero; i.e., from an absolute vacuum.
b) Static Pressure
Is the pressure measured in the gas in such manner that no effect on the measurement is
produced by the velocity.
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c) Suction Pressure
Is the absolute static pressure prevailing at the suction of the ejector expressed in millimeters or
micrometers (microns) of mercury.
d) Discharge Pressure
Is the absolute static pressure prevailing at the discharge of the ejector expressed in millimeters
of mercury.
e) Breaking Pressure
Is that pressure of either the motive steam or the discharge, which causes the ejector to become
unstable.
g) Absolute Temperature
Is the temperature above absolute zero. It is shown by the symbol (T) and Expressed in degrees
kelvin (K), which is equal to degrees Celsius (°C) plus 273.15.
h) Suction Temperature
Is the temperature of the gas at the suction of the ejector.
i) Stable Operation
Is the operation of the ejector without violent fluctuation of the suction pressure.
j) Capacity
Is the mass rate of flow of the gas to be handled by the ejector. Capacity is shown by the symbol
(W) and the unit is kilograms per hour (kg/h).
k) Dry Air
Atmospheric air at normal room temperature is considered dry air. The very small mass of water
in it is considered insignificant and is ignored. For example, the mass of water vapor in
atmospheric air at 50 percent relative humidity and 27°C is less than 0.011 kg per kg of air.
l) Equivalent Air
Is a calculated mass rate of air that is equivalent to the mass rate of gas handled by the ejector
at the suction conditions. The unit is kilograms per hour.
m) Equivalent Steam
Is a calculated mass rate of steam that is equivalent to the mass rate of gas handled by the
ejector at the suction conditions. The unit is kilograms per hour.
n) Molecular Mass
Is the sum of the atomic masses of all the atoms in a molecule.
o) Mol
Mol is a mass numerically equal to the molecular mass.
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p) Mol Fraction
Mol fraction of a component in a homogeneous mixture is defined as the number of mols of that
component divided by the sum of the number of mols of all components.
s) Critical Flow
Is the flow through a nozzle when the downstream absolute pressure is below critical pressure,
i.e., the downstream absolute pressure must be less than 50 percent of the upstream absolute
pressure.
t) Subcritical Flow
Is the flow through a nozzle when the downstream absolute pressure is above critical pressure,
i.e., there is a relatively low pressure drop across the nozzle.
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Notes:
1) Ejectors have no moving parts.
2) A large amount of pressurized air needed. Cost and space saving, but large relieving
noise.
3) Atmospheric air used.
4) Rotary pump works in wide pressure range.
5) Atmospheric leg (10 m) and waste water treatment needed.
6) Motive water is used. Water consumption rte is high.
7) Not good for the case when a lot of inert gas exists.
SELECTION STEPS OF VACUUM EQUIPMENT
Fig. 4
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6. DESIGN CRITERIA
The basic design stage of vacuum pumps and ejectors, can be divided into two distinct parts, first is
the calculation of parameters or factors which are common for all vacuum devices, such as those
concerning the suction conditions. On the other hand, there are some calculations which regards
specifically on; and differs for; each equipment type. In the following sections, each part is
individually discussed, except that since vacuum pumps are considered principally as compressors,
no special basic calculation method for this type is presented here and methods presented in IPS-
E-PR-750, "Process Design of Compressors", shall be used for this purpose.
Typical P&I diagrams for vacuum pump and ejector vacuum systems are shown in Appendix B.
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- dissolved
- injected or carried in the process
- formed by reaction
- air leakage
6.1.3.1 Few vacuum systems are completely airtight, although some may have extremely low
leakage rates. Considering the air and non-condensable:
(kg/h air + non-condensable)= air-in leakage + process released air + process released non-
condensable
See Fig.6, recommended by "ExxonMobil Research and Engineering Company", which has been
used conventionally for estimation of air leakage.
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3
SYSTEM VOLUMES (m )
AIR LEAKAGE VALUES
Fig. 6
3
AIR RELEASED FROM WATER kg air /1000 m /h WATER
DISSOLVED AIR RELEASED FROM WATER ON DIRECT CONTACT IN VACUUM SYSTEMS
Fig. 7
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6.2.1 General
6.2.1.1 For construction design considerations and factors such as design pressure, etc., refer to
"HEI, General Construction Standards for Ejector Components other than Ejector Condensers",
(see. 2.) and IPS-M-ME-256 (see 2.).
6.2.1.2 The design and construction shall be proven in practice, robust and reliable. Unless
otherwise specified, the ejectors shall be designed in accordance with IPS-M-ME-256, "Ejectors".
6.2.1.3 Safety, ease of operation, inspection, maintenance, repair and cleaning are of major
concern. Nozzles, nozzle inspection ports and pressure taps shall be readily accessible.
6.2.1.4 Where there is danger from freezing during operation affecting parts that can not be drained,
protection against such freezing shall be provided.
6.2.1.5 Provisions shall be made for cases where there is danger of plugging due to the carry over
of high viscosity or high melting point liquids.
6.2.1.6 Adequate personnel protection or insulation shall be provided for all surfaces hotter than
60°C.
6.2.1.7 Performance of the ejector shall be guaranteed by the contractor in accordance with IPS-E-
PR-250 "Performance Guarantee" (see 2.).
6.2.1.8 Spectacle blind shall be considered between process and vacuum sources (ejector, vacuum
pump) for leak test to confirm vacuum performance.
6.2.2.1 Capacity
The following capacity requirements shall be specified:
a) The absolute pressure to be maintained.
b) The total mass in kilograms per hour of the gas to be entrained.
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Note:
When actual performance curves for the temperature and vapor mixture in question is not
available, the capacity should be evaluated on an equivalent air basis, using HEI method
(see 2.), an example of such evaluation is presented in Appendix A.
6.2.2.2 Utilities
6.2.2.2.1 Steam
The following characteristics of the operating steam shall be specified:
a) Maximum steam line pressure and temperature.
b) Maximum steam pressure and temperature at the ejector steam inlet.
c) Minimum steam pressure at the ejector steam inlet.
d) Design steam pressure and temperature.
e) Quality of the steam, if it is not superheated, at the ejector steam inlet.
To prevent the nozzle throat of the ejector from becoming too small to be practical and to ensure of
having stable operation of the unit, the manufacturer may elect to use design steam pressure lower
than the available steam pressure at the ejector steam inlet.
It is recommended that the design steam pressure never be higher than 90 percent of the minimum
steam pressure at the ejector steam inlet.
This design basis allows for stable operation under minor pressure fluctuations.
The higher the actual motive steam design pressure of an ejector the lower the steam consumption.
When this pressure is above 2500 kPa (ga.), the decrease in steam requirements will be negligible.
For ejector discharging to the atmosphere, steam pressures below 415 kPa (ga.) at the ejector are
generally uneconomical.
To ensure stable operations the steam pressure must be above a minimum value. This minimum is
called the "Motive Steam Pickup Pressure", and is stated by the manufacturer.
Effect of steam pressures on ejector capacity is shown in Fig. 8.
An increase in steam pressure over design will not increase vapor handling capacity for the normal
“fixed capacity” type of ejector.
The steam should be dry, to avoid erosion and clogging the nozzle with water droplets, the latter
affecting performance and resulting in fluctuating vacuum. To ensure suitable steam quality in
supplies with little or no superheat, the use of a steam separator should be considered. The steam
supply should be stated as dry and saturated or if superheated the normal and maximum expected
pressures and temperatures given.
The motive steam design pressure should be the minimum expected line pressure minus 5 to 10
p.s.i. This design basis allows for stable operation under minor pressure fluctuations.
For ejectors discharging to atmosphere, steam pressures below 60 psig at the ejector are usually
uneconomic.
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1- Service.
2- Preferred Condenser Type.
3- Suction Pressure, mm Hg (abs.).
4- Suction Temperature, °C.
5- Maximum Discharge Pressure, mm Hg (abs.).
6- Steam: Min. Pressure, kPa(abs.).
Temperature, °C.
Quality, %.
7- Water: Source.
Max. Inlet pressure, kPa.
Max. Inlet Temperature, °C.
Max. Outlet Temperature, °C.
8- Volume of Evacuated System, m3.
9- Expected Air Leakage, kg/h.
10- Max. Evacuating Time, min.
11- Ejector Load:
a) Condensable: Water vapor and other vapors should be separately listed, and a heat
curve for the vapors included if the system is of the condensing type.
- Rate, kg/h.
- Molecular Mass.
- Cp, kJ/(kg.K).
- Latent Heat, kJ/kg.
b) Non-Condensable:
- Rate, kg/h.
- Molecular Mass.
- Cp. kJ/(kg.K).
12- Corrosive Substance (if any), mol% .
7. VACUUM SAFETY
Safety around mechanical vacuum pumps is possibly no different than that for other process
mechanical rotating machinery. However, there is a decided danger of an implosion (collapse) of a
tank, reactor, other process equipment operating below atmospheric pressure if:
1) It is not designed to satisfy the ASME codes for total or “full” vacuum, regardless of the
expected actual operating vacuum on the equipment, vessel, etc.
2) There are non or inadequate vacuum relief devices on the equipment or system being
evacuated.
3) Block valves are installed to allow the blocking off of equipment (vessels, tanks, etc.) thereby
pulling a higher vacuum than design, if not for “full” vacuum.
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APPENDICES
APPENDIX A
W n M v P n 7 × 53 × 3
=
WV = = 10.965 kg h
M nP n 29 × 2
=
Average molecular mass
(=
4 + 10.965)
43.4
0.3448
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APPENDIX B
TYPICAL PIPING AND INSTRUMENT DIAGRAMS (P & IDS) AROUND VACUUM SYSTEMS
Note that:
1 How the height of the condenser drain (seal) is specified. This height, in most cases is
conventionally limited to be 15 m (min.).This is better shown in Fig. B.3.
2 Pressure in a vacuum system using steam ejectors can be controlled:
a) By introducing air or inert gas from outside,
b) By spilling back the motive steam, or,
c) By recycling the non-condensable gases in the system.
Methods (b) and (c) should be employed in such cases where noncondensable gases are definitely
present in the system and the introduction of air into the system is not desirable or where the
quantity of off-gas must not be increased.
In the case of Method (b), if non-condensable gases are not present in the system, the flow of the
steam spilled back may be reversed to the equipment.
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APPENDIX C
ESTIMATION OF POWER CONSUMPTION FOR VACUUM PUMPS
Where:
2.2 × AiroVolume ( kg = h )
S.F.(Size Factors) = (Eq. C.1)
operating pressure ( m Hg )
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APPENDIX D
STANDARD EJECTOR UNITS DESIGNATIONS CONFORMING TO HEAT EXCHANGE
INSTITUTE
The different types of condensing equipment used with the various series are identified by the
following letters:
B- Barometric Counter- Flow Condenser, Intercondenser and Aftercondenser
C- Surface Coil Type Condenser and Aftercondenser.
S- Surface Type Condenser, Intercondenser and Aftercondenser
N-Signifies no condenser in the series
J-Atmospheric Jet Condenser, Intercondenser and Aftercondenser
The operating range of the condensing equipment determines the nomenclature. Here are the basic
divisions.
Condenser 1.5" Hg-4" Hg abs
Intercondenser 4" Hg-10" Hg abs
Aftercondenser 30" Hg-32" Hg abs
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APPENDIX E
TYPICAL EJECTOR DATA SHEET
BY:
PAGE: OF
DATA:
D.S. No.:
1 NUMBER
2 NAME
3 CASE
4 1ST STAGE INTER-CONDENSER SYMBOL
5 2ND STAGE INTER-CONDENSER SYMBOL
6 AFTER CONDENSER SYMBOL
7 NUMBER OF SETS REQUIRED
8 NUMBER OF SETS NORMALLY OPERATING
PROCESS REQUIREMENTS
9 SUCTION FLUID DESCRIPTION
10 • NON-CONDENSIBLE RATE kg/hr
11 • NON-CONDENSIBLE MOL. WT.
12 • STEAM RATE kg/hr
13 • VAPOR RATE kg/hr
14 • VAPOR MOL. WT.
15 • TOTAL RATE kg/hr
16 • AVERAGE MOL. WT.
17 • OPERATING PRESSURE mm Hg
18 • OPERATING TEMPERATURE °C
19 DISCHARGE
20 • PRESSURE bara
21 • LOCATION
DESIGN AND CONSTRUCTION
22 DATA ON SURFACE CONDENSERS
23 STEAM CONDITIONS FOR EJECTOR DESIGN
24 • MIN. MOTIVE STEAM PRESSURE bara
25 • DEGREES SUPERHEAT °C
26
27 EJECTOR MECH. DESIGN CONDITIONS
28 • DESIGN PRESSURE bara
29 • DESIGN TEMPRATURE °C
30
31
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