Is 17048
Is 17048
Is 17048
com)
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ICS 29.060.20
© BIS 2018
FOREWORD
This Indian Standard was adopted by the Bureau of Indian Standards after the draft finalized by the Power Cable
Sectional Committee had been approved by the Electro technical Division Council.
This standard covers the requirements for halogen free flame retardant cables/cords.
In the formulation of this standard, assistance has been derived from the following standards:
IS 694 : 2010 PVC insulated unsheathed and sheathed cables/cords with rigid and flexible
conductor for working voltage upto and including 1100 V with amendments
IS 1070 : 1992 Reagent grade water — Specification (third revision)
IS 8130 : 2013 Conductors of insulated electric cables and flexible cords — Specification
BS 7655-6.1 : 1997 Specification for insulating and sheathing materials for cables. Thermoplastic
sheathing compounds having low emission of corrosive gases, and suitable for use
in cables having low emission of smoke when affected by fire
BS 7655-8.1 : 2000 Specification for insulating and sheathing materials for cables. Crosslinked sheathing
compounds having low emission of corrosive gases, and suitable for use in cables
having low emission of smoke when affected by fire
BS EN 50267-2-2 : 1999 Common test methods for cables under fire conditions. Tests on gases evolved during
combustion of materials from cables. Procedures. Determination of degree of acidity
of gases for materials by Measuring pH and conductivity
BS EN 50363-7 : 2005 Insulating, sheathing and covering materials for low voltage energy cables. Halogen
Free, thermoplastic, insulating compounds
BS EN 50363-8 : 2005 Insulating, sheathing and covering materials for low voltage energy cables. Halogen
free, thermoplastic sheathing compounds
BS EN 50525-1 : 2011 Electric cables. Low voltage energy cables of rated voltages up to and including
450/750V (Uo/U). General requirements
IEC 60092-360 : 2014 Electric installation in ships — Part 360: Insulating materials for shipboard and off
shore units, power, control, instrumentation, telecommunication and data cables
IEC 60227 (all parts) PVC insulated cables of rated voltages up to and including 450/750V
IEC 60684-2 : 2011 Flexible insulation sleeving — Part 2: Methods of test
For the purpose of deciding whether a particular requirement of this standard is complied with the final value,
observed value, or calculated value expressing the result of a test or analysis shall be rounded off in accordance
with IS 2 : 1960‘Rules for rounding off numerical values ( revised ).’ The number of significant places retained in
the rounded off value should be the same as that of the specified value in this standard.
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IS 17048 : 2018
Indian Standard
HALOGEN FREE FLAME RETARDANT (HFFR)
CABLES FOR WORKING VOLTAGES UPTO
AND INCLUDING 1 100 VOLTS
1 SCOPE 2 Cables covered in this standard are suitable for indoor use
only.
1.1 This specification covers general requirements 3 The following types of cables are not covered in this standard:
of single and multicore cables/cords with rigid as a) Telephone cables,
well as flexible annealed bare/tinned copper and b) Data transmission cables,
aluminium conductor insulated and sheathed (if any) c) Instrumentation cables, and
with Thermoplastic or Crosslinked Halogen Free d) Screened communication cables.
Flame Retardant (HFFR) material for voltages up
to and including 1 100 V a.c., 50 Hz, used in power 2 REFERENCES
and lighting installations including cables for low
The standards listed below contain provisions which
temperature applications. These cables may be used
through reference in this text, constitute provisions of
on d.c. systems for rated voltages up to and including
this standard. At the time of publication, the editions
1 500 V to earth. These cables are suitable to use
indicated were valid. All standards are subject to
for conductor temperature not exceeding 70oC for
revision and parties to agreements based on this
thermoplastic or 90oC for crosslinked material.
standard are encouraged to investigate the possibility
1.2 This standard covers the following categories of of applying the most recent editions of the standards
cables: listed below:
1
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The smallest of the measured values of thickness of However, the thickness of sheath determined by taking
insulation (ti) shall not fall below the nominal value (ti) average of number of measurements shall be not less
specified in the relevant table by more than (0.1 mm + than nominal value (ts) specified in relevant tables and
0.1 ti). smallest of the measured value shall not fall below the
nominal value (ts) specified by more than (0.1 mm +
4.2.4 Mechanical Properties before and after 0.15 ts) for single core cables and (0.2 mm + 0.2 ts). for
Ageing multicore cables.
The insulation shall have adequate mechanical strength Compliance shall be checked by testing the dimensional
and elasticity within the temperature limits to which it requirements specified in Section 2 and Section 3 and
may be exposed in normal use. as per test method given in IS 10810 (Part 6).
The compliance shall be checked by carrying out
tensile strength and elongation test, for respective type 4.5.4 Mechanical Properties before and after Ageing
of compound, as per method given in IS 10810 (Part 7). The sheath shall have adequate mechanical strength
The applicable test values shall be obtained from Annex and elasticity within the temperature limits to which it
A, for appropriate type of compound. may be exposed in normal use.
4.3 Fillers The compliance shall be checked by carrying out
tensile strength and elongation test, shall meet the
4.3.1 The fillers, if provided, shall be of halogen free requirements given in Annex B.
flame retardant material.
4.5.5 Overall Dimensions
4.3.2 The filler materials shall be suitable for operating The maximum overall dimensions of the cables
temperature of the cable and compatible with other shall be within the limits specified in the Table 3
components of the cable. This shall not be harder than to Table 8 given in Section 2 and Section 3 of this
the HFFR material used for insulation and sheath. specification.
4.4 Binder Tape 4.5.5.1 Ovality
Binder tape if required, shall also be of suitable material The difference between maximum and minimum
of halogen free in nature. measured values of overall diameter of sheathed
4.5 Sheath circular cables shall not exceed 15 percent of the
maximum measured value at the same cross section.
4.5.1 The sheath shall consist of halogen free flame
retardant compound conforming to the requirements 4.5.6 Colour of Sheath
of HFS-TP 70 or HFS-TP 90or HFS – XL 70 or HFS- The preferred colour of the sheath is black. Any
XL90 given in Annex B. other colour agreed to between the purchaser and
NOTES manufacturer is also permissible
1 Insulation and sheath material shall be compatible with each
other as per the temperature rating of the cable. 5 TESTS
2 A combination of cross linked insulation and thermoplastic The testing on the cables will be conducted as given
sheath is also permissible. Table 2. For each category of cables listed under scope
4.5.2 Application of this standard.
The sheath shall be applied in a single layer: Unless otherwise stated, the tests shall be carried out in
accordance with appropriate part of IS 10810, taking
a) On the core, in the case of single-core cables; and into account the additional information given in this
b) On the assembly of cores and fillers or inner standard.
covering, if any, in the case of other cables.
The sheath shall not adhere to the cores. A 5.1 High Voltage Test (at Room Temperature)
separator, consisting of a film or tape, or talcum (Acceptance and Routine Test)
powder may be placed under the sheath. This In case of multicore cables and cords test voltage shall
separator shall be compatible with the insulation be applied for a period of 5 min between the cores.
and sheath materials. Single-core cables shall be immersed in water at
4.5.3 Thickness ambient temperature one hour before the testing and
the test voltage shall be applied between conductor and
The mean value of the thickness of sheath shall not water for the specified period.
be less than the specified nominal value for each type
and size of cable shown in the tables of the particular Cables/cords tested as above shall withstand without
specifications (see Section 3). breakdown an a.c. voltage of 3 kV (r.m.s) or a d.c.
voltage of 7.5 kV for 5 min.
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10.2.1 BIS Certification Marking rules and Regulations Made thereunder. The details of
The standard may also be marked with the standard the conditions under which the licence for use of the
mark. Standard Mark may be granted to manufacturer and
producers may be obtained from the Bureau of Indian
10.2.1.1 The use of Standard Mark is governed by Standards.
the Bureau of Indian Standards Act, 2016 and the
NOTES
1 In case of single-core cables used for control wiring of switchgear, any colour other than the above shall be permissible as agreed to
between the Purchaser and the Supplier.
2 The colour of insulation for parallel twin flexible cords may be any two of red, black, yellow, blue, white and grey. The cores may be
identified by a longitudinal rib on one core in case of same colour of the cores.
3 For cables and cords with more than five cores, as an alternative, it is permissible to have all cores of the same colour. In such case, the
cores shall be numbered sequentially (Hindu-Arabic numerals printed on the surface of the cores), starting with “1” for the innermost
layer. The gap between two successive printings shall not exceed 50 mm.
6
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Table 2 Tests
( Clause 11.4, 12.4, 13.7 14.7 and 15.7 )
Tests Requirements, Ref. to Method of Category
IS No./Clause of this Test, Ref. to
Standard Part of
IS 10810
(1) (2) (3) ( 4)
I Routine Tests
a) HV test or 5.1 45 01,02,03,04
spark test 5.2 44
b) Conductor resistance test 20°C 4.1.1(c) 5 01,02,03,04
II Acceptance Tests
a) Tensile test (for aluminium) IS 8130 2 01,02,03,04
b) Wrapping test (for aluminium) IS 8130 3 01,02,03,04
c) Persulphate test for tinned copper IS 8130 4 01,02,03,04
d) Conductor resistance test IS 8130 5 01,02,03,04
e) Test for thickness of insulation and sheath,diameter of 11.2, 11.3, 12.2,12.3, 6 01,02,03,04
core and sheath including ovality of sheath 13.2, 13.4, 13.5,13.6, 01,02,03,04
14.2,14.4,14.5, 14.6, 15.2, 01,02,03,04
15.4, 15.5 and
Table 3 to 8
f) Tensile strength and elongation at break of insulation Annex A and 2 7 01,02,03,04
and sheath
g) Insulation resistance Annex A 43 01,02,03,4
h) High voltage test 5.1 45 01,02,03,04
j) Flammability test 5.3 53 01,02,03,04
k) pH and conductivity 5.7 and Annex D — 01,02,03,04
m) Hot set test Annex A 30 03,04
III. Type Tests
a. Conductor
i) Conductor resistance test IS 8130 5 01,02,03,04
ii) Annealing test (for copper) IS 8130 1 01,02,03,04
iii) Persulphate test for tinned copper IS 8130 4 01,02,03,04
iv) Tensile test (for aluminium) IS 8130 2 01,02,03,04
v) Wrapping test for aluminium) IS 8130 3 01,02,03,04
b. Test for Overall Dimensions and Thickness of 11.2, 11.3, 12.2,12.3,13.2, 6 01,02,03,04
Insulation and Sheath 13.4, 13.5, 13.6, 14.2,14.4,
14.5, 14.6,15.2,15.4,15.5
and
Table 3 to 8
c. Tests on Insulation
i) Tensile strength and elongation Annex A 7 and 11 01,02,03,04
at break before and after ageing
ii) High voltage test 5.1 45 01,02,03,04
iii) Insulation resistance Annex A 43 01,02,03,04
iv) Oxygen index 5.4 58 01,02
v) Temperature Index 5.5 64 01,02
vi) Ageing in air oven Annex A 11 01,02,03,04
vii) Hot deformation Annex A 15 01,02,03,04
viii) Assessment of halogen Annex D — 01,02,03,04
7
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Table 2 ( Concluded )
Tests Requirements, Ref. to Method of Category
IS No./Clause of this Test, Ref. to
Standard Part of
IS 10810
(1) (2) (3) ( 4)
x) Cold impact test Annex A 21 01,02,03,04
xi) Hot set test Annex A 30 03,04
xii) Ozone resistance test Annex A 13 01,02,03,04
xiii)Flame retardant test 5.11 61 01,02,03,04
d. Tests on Fillers / Dummy Cores and Binder Tapes/
Identification Threads (if Any)
i) Assessment of halogen 5.7 and Annex D — 01,02,03,04
e. Tests on Sheath
i) Tensile strength and Annex B 7 01,02,03,04
elongation at break
ii) Ageing in air oven Annex B 11 01,02,03,04
iii) Oxygen index 5.4 58 01,02
iv) Temperature Index 5.5 64 01,02,
v) Ozone resistance test Annex A 13 01,02,03,04
vi) Hot deformation Annex B 15 01,02,03,04
vii) Assessment of halogen 5.7 and Annex D — 01,02,03,04
viii) Hot set test Annex B 30 03,04
f. Tests on Finished Cable
i) High voltage test 5.1 45 01,02,03,04
ii) Flammability test 5.3 53 01,02,03,04
iii) Cold bend test Annex A and B 20 01,02,03,04
iv) Cold impact test Annex A and B 21 01,02,03,04
v) Flame retardant test 5.11 61 01,02,03,04
vi) Water immersion test (effect of water on sheath 5.13 — 01,02,03,04
of cable)
vii) Smoke density test 5.6 63 01,02,03,04
8
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Table 3 ( Concluded )
12 SINGLE CORE UNSHEATHED CABLE The thickness shall comply with specified values given
WITH FLEXIBLE COPPER CONDUCTOR col 3 of Table 4.
(MAXIMUM CONDUCTOR TEMPERATURE The smallest of the measured values of thickness of
OF 70°C OR 90°C) insulation shall not fall below the nominal value (ti)
specified in the Table 4 by more than (0.1 mm +0.1 ti).
12.1 Conductor
The conductor shall comply with the requirements 12.3 Overall Diameter
given in IS 8130 for class 5conductors. The sizes The maximum overall diameter shall not exceed the
covered are 0.5 to 300 mm². limit given in col 3 of Table 4.
12.2 Insulation 12.4 Tests
The insulation shall be halogen free flame retardant Compliance with requirement of 12.1 to 12.3 shall be
compound HFI-TP 70 or HFI-XL 70 and HFI-XL 90 checked by inspection and by the test given in Table 2.
as per Annex A, applied around the conductor by the
suitable process.
Table 4 Single Core Halogen Free Flame Retardant Type Unsheathed Cable with
Flexible Conductor (Maximum Conductor Temperature 70°C or 90°C)
( Clauses 12.2 and 12.3 )
Sl No. Nominal Cross-sectional Thickness of Insulation Max. Overall
Area of Conductor (ti) Nominal Diameter
mm² mm mm
(1) (1) (2) (3)
i) 0.5 0.6 2.6
ii) 0.75 0.6 2.8
iii) 1 0.6 3
iv) 1.5 0.6 3.4
v) 2.5 0.7 4.1
vi) 4 0.8 4.8
vii) 6 0.8 5.3
viii) 10 1 7
ix) 16 1 8.1
x) 25 1.2 10.2
xi) 35 1.2 11.7
xii) 50 1.4 13.9
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Table 4 ( Concluded )
Sl No. Nominal Cross-sectional Thickness of Insulation Max. Overall
Area of Conductor (ti) Nominal Diameter
mm² mm mm
(1) (1) (2) (3)
xiii) 70 1.4 16
xiv) 95 1.6 18.2
xv) 120 1.6 20.2
xvi) 150 1.8 22.5
xvii) 185 2 25
xviii) 240 2.2 28.5
xix) 300 2.4 32
SECTION 3 SHEATHED SINGLE AND The thickness of sheath determined by taking average
MULTICORE CABLES / CORDS (ts) of number of measurements, shall not be less than
nominal value (ts) specified in Table 1 and the smallest
FOR FIXED AND FLEXIBLE WIRING of the measured values shall not fall below nominal
13 SINGLE AND MULTICORE CIRCULAR value specified in Table 5 by more than 0.15 ts + 0.1
HALOGEN FREE FLAME RETARDANT mm for single core cables and 0.2 ts + 0.2 mm for
(HFFR) INSULATED AND SHEATHED multicore cables.
CABLES WITH RIGID CONDUCTOR The colour of sheath shall preferably be black or any
(CLASS 1 AND 2) (MAXIMUM CONDUCTOR other colour as agreed between the purchaser and
TEMPERATURE 70°C OR 90°C) supplier.
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The sheath may fill the space between cores thus The preferred colour of the sheath is black.
forming a filling, but it shall not adhere to the cores. The Any other colour agreed to between the purchaser and
assembly of cores may be surrounded by a separator, manufacturer is also permissible.
which shall not adhere to cores.
The assembly of circular cord shall have a practically 15.5 Overall Dimensions
circular cross section. The maximum overall dimensions of circular cables/
The thickness of sheath determined by taking average cords shall be within the limits given in Table 7 and
of measurements shall not be less than nominal value Table 8.
(ts) specified in Table 4 and the smallest of the measured 15.6 Tests
values shall not fall below nominal value specified in
Table 7 and Table 8 by more than 0.15 ts + 0.1 mm for Compliance with the requirements of 15.1 to 15.5
single core cables and 0.2 ts + 0.2 mm. for multicore above shall be checked by inspection and by tests given
cables. in Table 2.
13
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Cables (Circular)
( Clauses 14.2, 14.4.1 and 14.6 )
Sl No. Nominal Nominal Nominal Thickness of Sheath (ts) Overall Dimensions, Max..
Cross- Thickness
Single Two Core Three Four Five Core Single Two Core Three Four core Five Core
Sectional of
core Core Core Core Core
Area of Insulation
Conductor (ti)
mm2 mm mm mm mm mm mm mm mm mm mm mm
i) 4 0.8 1.1 1.3 1.3 1.4 1.4 7.0 11.6 12.5 14.1 15.4
ii) 6 0.8 1.2 1.4 1.4 1.4 — 8.1 13.7 14.8 16.7 —
iii) 10 1 1.2 1.5 1.5 1.6 — 9.6 16.7 18.1 20.3 —
iv) 16 1 1.3 1.5 1.6 1.7 — 10.7 19.1 20.6 23.1 —
v) 25 1.2 1.3 1.7 1.7 1.8 — 12.7 22.9 24.8 27.8 —
vi) 35 1.2 1.4 1.8 1.8 1.9 — 14.2 25.9 28.0 31.4 —
vii) 50 1.4 1.5 1.9 2.0 2.1 — 16.5 30.6 33.1 37.1 —
viii) 70 1.4 1.5 2.1 2.1 2.3 — 18.8 35.1 37.9 42.6 —
14
ix) 95 1.6 1.6 2.2 2.3 2.5 — 21.4 40.5 43.7 49.0 —
x) 120 1.6 1.7 2.3 2.5 2.6 — 23.0 43.7 47.2 52.9 —
xi) 150 1.8 1.8 2.5 2.6 2.8 — 25.6 - 52.7 59.1 —
xii) 185 2 1.8 2.7 2.8 3.0 — 28.2 - 58.3 65.3 —
xiii) 240 2.2 2.0 2.9 3.1 3.3 — 31.8 - 66.1 74.1 —
xiv) 300 2.4 2.1 3.2 3.3 3.6 — 35.5 - 74.0 83.0 —
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mm2 mm mm mm mm mm mm mm mm mm mm mm mm mm mm
i) 0.50 0.60 0.9 0.9 0.9 0.9 0.9 4.3 6.9 7.3 8.0 8.7 2.6 × 5.2 5.2 7.2 × 4.9
ii) 0.75 0.60 0.9 0.9 0.9 0.9 0.9 4.5 7.3 7.7 8.4 9.2 2.8 × 5.6 5.6 7.8 × 5.2
iii) 1.00 0.60 0.9 0.9 0.9 0.9 1.0 4.7 7.6 8.1 8.8 9.6 3.0 × 6.0 6.0 8.0 × 5.4
iv) 1.50 0.60 0.9 0.9 0.9 1.0 1.0 5.4 8.9 9.4 10.4 11.4 3.3 × 6.6 6.6 8.6 × 5.6
v) 2.50 0.70 1.0 1.0 1.0 1.0 1.0 6.2 10.3 10.9 12.0 13.2 4.0 × 8.0 8.0 10.5 × 6.6
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Insulated and Sheathed Cables (Circular)
( Clause 15.2, 15.4 and 15.5 )
Sl No. 0.50 sq. mm 0.75 sq. mm 1.0 sq. mm 1.5 sq. mm 2.5 sq. mm
No. of Nominal Nominal Overall Nominal Nominal Overall Nominal Nominal Overall Nominal Nominal Overall Nominal Nominal Overall
Cores Thickness Thickness Dimen- Thickness Thickness Dimen- Thickness Thickness Dimen- Thickness Thickness Dimen- Thickness thickness Dimen-
sions of sions sions sions sions
of of of of of of of of of
Max..
Insulation Max.. Insulation Max.. Insulation Sheath (t ) Max.. Insulation Max..
Sheath Sheath s
Sheath Insulation Sheath
(ti) (ti) (ti) (ti)
(ts) (ts) (ts) (ti) (ts)
(1) (2) (3) (4) (5) (6) (7) (8) (9) (10) (11) (12) (13) (14) (15) (16) (17)
mm mm mm mm mm mm mm mm mm mm mm mm mm mm mm
i) 6 0.6 0.9 9.5 0.6 1 10.0 0.6 1 10.5 0.6 1 12.5 0.7 1.1 14.7
ii) 7 0.6 0.9 9.5 0.6 1 10.0 0.6 1 10.5 0.6 1 12.5 0.7 1.1 14.7
iii) 8 0.6 1 11.1 0.6 1 11.3 0.6 1 12.4 0.6 1.1 14.9 0.7 1.2 17.5
iv) 9 0.6 1 11.3 0.6 1.1 12.4 0.6 1.1 13.1 0.6 1.1 15.8 0.7 1.3 18.5
v) 10 0.6 1 12 0.6 1.1 12.7 0.6 1.1 13.4 0.6 1.1 16.2 0.7 1.3 18.9
vi) 11 0.6 1 12 0.6 1.1 12.7 0.6 1.1 13.4 0.6 1.1 16.2 0.7 1.3 18.9
16
vii) 12 0.6 1 12.4 0.6 1.1 13.1 0.6 1.1 13.9 0.6 1.1 16.7 0.7 1.3 19.5
viii) 13 0.6 1 13.1 0.6 1.1 13.3 0.6 1.1 14.6 0.6 1.2 17.5 0.7 1.3 20.7
ix) 14 0.6 1.1 13.1 0.6 1.1 13.3 0.6 1.1 14.6 0.6 1.2 17.5 0.7 1.3 20.7
x) 15 0.6 1.1 13.5 0.6 1.2 14.3 0.6 1.2 15.1 0.6 1.2 18.8 0.7 1.4 21.5
xi) 16 0.6 1.1 13.3 0.6 1.2 14.5 0.6 1.2 15.4 0.6 1.2 18.6 0.7 1.4 21.9
xii) 17 0.6 1.1 14.6 0.6 1.2 15.4 0.6 1.2 16.3 0.6 1.3 19.7 0.7 1.4 23.2
xiii) 18 0.6 1.1 14.6 0.6 1.2 15.4 0.6 1.2 16.3 0.6 1.3 19.7 0.7 1.4 23.5
xiv) 19 0.6 1.1 14.6 0.6 1.2 15.4 0.6 1.3 16.3 0.6 1.3 19.7 0.7 1.4 24
xv) 20 0.6 1.2 15.4 0.6 1.3 16.3 0.6 1.4 17.3 0.6 1.4 20.9 0.7 1.5 24.5
xvi) 21 0.6 1.2 15.4 0.6 1.3 16.3 0.6 1.4 17.3 0.6 1.4 20.9 0.7 1.5 25.2
xvii) 22 0.6 1.2 16.3 0.6 1.3 17.3 0.6 1.4 18.2 0.6 1.4 22.1 0.7 1.5 26
xviii) 23 0.6 1.2 16.3 0.6 1.3 17.3 0.6 1.4 18.2 0.6 1.4 22.1 0.7 1.5 26.5
xix) 24 0.6 1.2 17.1 0.6 1.3 18.2 0.6 1.4 19.2 0.6 1.4 23.2 0.7 1.5 27.4
xx) 25 0.6 1.2 17.1 0.6 1.3 19.0 0.6 1.4 19.2 0.6 1.4 23.2 0.8 1.5 28.1
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ANNEX A
( Clause 4.2.1 )
HALOGEN FREE FLAME RETARDANT INSULATED CABLES
Sl Test Unit Test Method Type of Insulation
No.
HFI-TP70 HFI-XL70 HFI-XL90
(1) (2) (3) (4) (5) (6) (7)
A General
1 Rated temperature 70°C 70°C 90°C
2 Insulation resistance constant at rated temp. MΏ.km Min. 0.037 Min. 0.037 Min. 0.037
IS 10810-
Temperature °C 70 ± 2 70 ± 2 90 ± 2
43
Test duration Hr. 1 1 1
3 Properties before ageing
3.1 Values to be obtained for the tensile strength:
7.5 10 10
- Min. N/mm2
Values to be obtained for the elongation at IS 10810-
break: 7 150 125 125
Percent
- Min.
3.2 Properties after ageing in air oven
Ageing conditions:
- temperature o
C IS 10810- 80 ± 2 135 ± 2
100 ± 2 168
- duration of treatment h 11 168 168
Value to be obtained for the tensile strength:
- Min. N/mm2 — — —
- variation, Max. Percent ± 20 ± 30 ± 30
Values to be obtained for the elongation at
break: — — —
N/mm2
-Min. ± 20 ± 30 ± 25
Percent
- variation, Max.
4 Hot Deformation Test
o
C 80 ± 2 —
Temperature —
IS 10810-
Period of test Hr. 15 4 — —
Result Percent Max. 50 — —
5 Hot set test
o
C
Temperature — 200 ± 3 200 ± 3
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ANNEX B
( Clause 4.5.1 )
HALOGEN FREE FLAME RETARDANT SHEATHED CABLES
Sl Test Unit Test Method Type of Sheathing
No.
HFS-TP70 HFS-TP 90 HFS-XL70 HFS-XL90
(1) (2) (3) (4) (5) (6) (7) (8)
A General
1 Rated temperature °C 70 90 70 90
2 Properties before ageing
2.1 Values to be obtained for the
tensile strength: N/mm2 IS 10810 10 10 10 10
- Min. (Part 7)
Values to be obtained for the
elongation at break:
- Min. Percent 100 100 125 100
2.2 Properties after ageing in
air oven IS 10810
Ageing conditions: (Part 11)
- temperature o
C 80 ± 2 100 ± 2 100 ± 2 100 ± 2
- duration of treatment h 168 168 168 168
Value to be obtained for the
tensile strength:
- Min. N/mm2 10 10 7 10
- variation, Max. Percent ± 25 ± 40 ± 30 ± 40
Values to be obtained for the
elongation at break:
- Min. Percent 100 100 125 ± 30 100 ± 40
- variation, Max. Percent ± 25 ± 40 ± 40
3 Hot deformation Test IS 10810
(Part 15)
Temperature o
C 80 ± 2 90 ± 2 80 ± 2 90 ± 2
Period of test h 4 4 4 4
Result Percent Max. 50 Max. 50 Max. 50 Max. 50
percent percent percent percent
4 Hot set test IS 10810
(Part 30)
Temperature o
C — — 200 ± 3 200 ± 3
Period under load Minutes — — 15 15
Mechanical stress N/cm² — — 20 20
Elongation under load, Max. Percent — — 175 175
Permanent Elongation, Max. Percent — — 15 15
5 Cold bend test IS 10810
(Part 20)
Temperature o
C -15 ± 2 -15 ± 2 -15 ± 2 -15 ± 2
Period of test Hr. 3 3 3 3
Result No Cracks No Cracks No Cracks No Cracks
6 Cold impact test IS 10810
(Part 21)
Temperature o
C -15 ± 2 -15 ± 2 -15 ± 2 -15 ± 2
Period of test Hrs. 3 3 3 3
Result No Cracks No Cracks No Cracks No Cracks
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ANNEX C
( Clause 8 )
SAMPLING OF CABLES
Scale of Sampling
Number of Drums/ Number of Drums/ Permissible Number of
Coils/Reels in the Lot Coils/Reels to be Defectives
taken as Samples
(1) (2) (3)
Up to 50 3 0
51 to 100 5 0
101 to 300 8 0
301 and above 13 2
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ANNEX D
( Clause 5.7 )
ASSESSMENT OF HALOGENS
D-1 REQUIREMENTS
D-1.1 The insulation and sheath shall meet the type test requirements as given in the following table:
Sl No. Test Method Measure Requirements
1 See D-2 pH and conductivity pH≥ 4.3 and
conductivity ≤ 10 µS/mm
2 IS 10810 (Part 59) Chlorine and bromine content expressed as content ≤ 0.5 percent
of HCL
3a See D-3 Presence of fluorine If negative, stop further test.
If positive, test as per 3b
D-1.2 The material shall be tested as per given sequence as per the table given below:
Sl No. Test Method Measure Requirements Outcome
Step 0 See D-3 Halogen : Fluorine, chlorine and Negative value If negative stop test – material
bromine accepted. If positive go to step 1
pH pH < 4.3 Reject the material
pH > 4.3 Evaluate conductivity
Conductivity < 2.5µ S/mm Accept no further testing required
Step 1 See D-2
> 10 µS/mm Reject material
> 2.5 <10 Chlorine bromine determination as
per See D-3
Step 2 IS 10810 (Part 59) Chlorine and bromine content >0.5 percent Reject material
expressed as hydrochloric acid (HCl)
< 0.5 percent See D-4
See D-4 Fluorine content >0.1 percent Reject material
< 0.1 percent Accept material
D-2 DETERMINATION OF DEGREE OF distances between the quartz glass tube and the first
ACIDITY OF COMBUSTION GASES FOR bottle and between subsequent bottles shall be as short
MATERIAL BY MEASURING pH AND as possible. Glass or silicone rubber tubing shall be
CONDUCTIVITY used for these connections.
NOTES
D-2.1 Test Method Principle 1 At the exit side of the quartz glass tube, as close to the end
The material under test shall be heated in a stream as possible, it is permitted to place a plug of silica wool to aid
of dry air. The evolved gases shall be trapped by collection of condensates.
bubbling through wash bottles filled with distilled or 2 A third empty bottle, of the same size as the gas washing
demineralized water. bottles, placed before the gas washing bottles may be used to
improve safety, that is to prevent suck back of water into the
The acidity of the resulting solution shall be assessed quartz glass tube.
by determination of its pH value. The conductivity of
the solution shall also be determined. D-2.2.2 Tube Furnace
The length of the heating zone of the furnace shall be
D-2.2 Test Apparatus
within the range 480 mm to 620 mm and its inside
D-2.2.1 General diameter shall be within the range 38 mm to 62 mm. It
shall be equipped with an adjustable electrical heating
The apparatus is shown in Fig.2 to Fig.6.
system.
The assembly of the components which constitute
the test apparatus shall be leak-tight. The connecting
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1
3 4
2 5
6 7 9 8
10
24
Key
1 Synthetic air or compressed air, 6 Bar magnets
filtered and dried
2 Glass tube 7 Platinum wire
3 Thermocouple 8 Combustion boat
4 Quartz glass tube 9 Standard ground joint, size in correlation to
the diameter of the quartz glass tube
5 Test specimen 10 Furnace
Fig. 2 Device for Inserting Combustion Boat and Test Specimen
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Key
1 Magnetic stirring bar h 100 mm to 120 mm
Fig. 3 Example of a Gas Washing Bottle
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2 6 4
5
7
6
9
10 12
11
Key
1 Pressure reducing valve 7 Gas washing bottles
2 Flow meter 8 Synthetic air
3 Quartz glass tube 9 Device for inserting combustion boat
containing test specimen
4 Furnace 10 Combustion boat containing test specimen
5 Needle valve 11 Magnetic stirrer
6 Thermocouple 12 Magnetic stirring bar
Fig. 4 Test Apparatus: Method 1 – Use of Synthetic or Compressed Air From a Bottle
2 3 4
5 6
10
9
7 8
11 12
13
14 15
16
Key
1 Pressure reducing valve 7 Activated charcoal 13 Device for inserting combustion boat
containing test specimen
2 Flow meter 8 Silica gel 14 Combustion boat containing test specimen
3 Quartz glass tube 9 Thermocouple 15 Magnetic stirring bar
4 Furnace 10 Gas washing bottles 16 Magnetic stirrer
5 Compressed air 11 Air filtering
6 Needle valve 12 Air drying
Fig. 5 Test Apparatus: Method 2 – Use of Laboratory Compressed Air Supply
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1 2
3 4
5
9
8
6 7
10
11 12
13
14 15
16
Key
1 Flow meter 7 Silica gel 13 Device for inserting combustion boat containing test specimen
2 Furnace 8 Thermocouple 14 Combustion boat containing test specimen
3 Ambient air 9 Gas washing bottles 15 Magnetic stirring bar
4 Quartz glass tube 10 Suction pump 16 Magnetic stirrer
5 Needle valve 11 Air filtering
6 Activated charcoal 12 Air drying
Fig. 6 Test Apparatus: Method 3 – Use of Ambient Air Sucked by Means of a Suction Pump
D-2.2.3 Quartz Glass Tube The preferred method for insertion of the combustion
boat into the quartz glass tube is shown in Fig.2.
For the test, a quartz glass tube shall be introduced
into the tube furnace. The tube shall be approximately Prior to each test, the combustion boat shall be washed
concentric to the furnace. It shall be resistant to the and calcined in a muffle furnace at approximately
action of corrosive gases. 950 °C for 4 h after which it shall be introduced into
a desiccator and cooled to ambient temperature. The
The inside diameter of the tube shall be within the
combustion boat shall then be weighed to an accuracy
range 30 mm to 46 mm. The tube shall protrude on
of 0.1 mg until two identical consecutive weights are
the entrance side of the furnace by a length of between
obtained. This weight m1 shall be recorded.
60 mm to 200 mm, and on the exit side by between
60 mm to 100 mm. The initial clearance shall allow for D-2.2.5 Bubbling Devices for Gases
thermal expansion. For the purposes of measurement of
the protrusion distances, the tube shall be regarded as At the exit of the quartz glass tube, the evolved gases
that part of essentially constant diameter. shall be trapped by bubbling through two wash bottles
NOTE — The outer diameter of the tube should be chosen with
(see Fig. 3), each containing approximately 450 ml
due regard to the inside diameter of the tube furnace. of distilled or demineralized water of a purity at least
Prior to each test the tube shall be cleaned throughout grade 3 in accordance with IS 1070.
its length by being calcined at approximately 950°C. The pH value of the water shall be 6.5 ± 1, and the
conductivity less than 0.5 µS/mm.
D-2.2.4 Combustion Boats A magnetic stirrer shall be introduced in the first gas
The combustion boat shall be made of porcelain, washing bottle to get a good swirling motion and an
fused quartz or soapstone and shall have the following effective absorbtion of the combustion gases. The tubes
dimensions: into the wash bottles shall have a maximum internal
a) external length: within the range 45 mm to diameter at their tip of 5 mm in order to aid absorption.
100 mm; The height of the liquid above the end of the tube shall
b) external width: within the range 12 mm to 30 mm; be (110 ± 10) mm in each bottle.
and NOTE — Use of a standard laboratory glass bottle of internal
diameter approximately 75 mm will enable this requirement to
c) internal depth: within the range 5 mm to 10 mm. be met.
NOTE — The dimensions of the boat should be chosen with
due regard to the inside diameter of the quartz tube.
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where a temperature of not less than 900 °C has been D-3.1 Equipment
determined by the thermocouple measurement.
a) Bunsen burner;
The combustion procedure, under the air flow condition, b) Glass test tubes of approximately 50 mm × 10 mm;
shall be continued for (30 ±1) min in the furnace.
c) Test tube holder;
WARNING —The operator should take precautions, for
example, the wearing of eye protection and suitable protective d) Evaporating basin / mortar;
clothing, because certain materials ignite quickly, and can e) Wire gauge;
cause “blow back” of hot gases. Care should also be taken
to avoid over-pressurization of the system, and to allow for f) Funnel; and
venting of exhaust gases. Guidance on the avoidance of “blow g) Filter paper.
back” is given in Note 2 of D-2.2.1.
D-3.2 Materials
D-2.4.4 Washing Procedure
a) Sample;
Following the heating procedure, all the bottles used
shall be disconnected, and the contents washed into b) Sodium metal;
a 1 000 ml volumetric flask. Using water with the c) Nitric acid ( 5 percent);
properties given in D-2.2.5, the bottles, the connecting d) Aqueous silver nitrate (5 percent);
links and, after cooling, the end of the quartz glass tube e) Freshly prepared zirconium-alizarin red S reagent;
including the silica wool (if used) shall also be washed
into the flask, and the contents made up to 1 000 ml. f) Glacial acetic acid; and
g) pH papers.
D-2.5 Determination of the pH Value and Conduc-
tivity D-3.3 Procedure
The pH shall be measured using a pH meter calibrated D-3.3.1 Sodium Fusion
as proposed by the instrument supplier.
Place 200 to 250 mg of the sample into the bottom of
The pH value of the solution shall be determined at
a small soda glass test tube. Add 10 ml of de-ionized
(25 ±1)°C in accordance with the test procedures as
water to the evaporating basin and place this in the fume
prescribed by the supplier of the measuring instrument.
cupboard behind the safety screen. Whilst holding the
Conductivity value measurements shall also be test tube firmly with the test tube holder at an angle of
performed at (25 ±1) °C in accordance with the 45o to 60o to the vertical, introduce a piece of freshly
test procedures as prescribed by the supplier of the cut, clean sodium in size of a small pea ( 200 to 250
conductivity measuring instrument. mg) into the mouth of the test tube without allowing
The pH value and conductivity value shall preferably it to come into contact with the sample directly. With
be read by using automatic temperature compensation. the safety screen in place, heat the sodium gently until
If such a facility is not available, the values shall be read it melts and runs down on to the sample leading to
when the temperature of the solution is at (25 ±1) °C. vigorous reaction when the molten sodium reaches the
sample in case of presence of halogen. Heat the test
NOTE — Automatic temperature compensation is usually
an integral feature of the pH and conductivity measuring tube gently for about a minute, then more strongly until
instruments. the lower 20 mm of the test tube glows red hot. Plunge
the red hot tube into the water in the evaporating basin,
D-2.6 Evaluation of the Test Results immediately placing the gauze on the top, to prevent
From the two test determinations undertaken, the the loss of material when tube shatters on contact with
sample shall be considered to have met the performance water. Allow any unreacted sodium to react before
requirement if both pH values are greater than or equal grinding up the solution and glass. Filter and separate
to the specified value and both conductivity values are the filtrate into two equal portions.
less than or equal to the specified value.
D-3.4 Determination of Presence of Chlorine and
D-3 DETERMINATION OF HALOGENS — Bromine
E LEMENTAL TEST To the first portion of the filtrate, add sufficient nitric
Warning — Owing to its potentially hazardous nature the
acid to make the solution acidic. Boil this total volume
fusion operation should be carried out in a fume cabinet, using till reduced by half, to remove any hydrogen cyanide
safety screen. (HCN) or hydrogen sulfide (H2S), if present, which
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would interfere with the test. Add 1 ml of silver nitrate 15 ml 2 propanol plus 35 ml water. Filter before
solution a white or yellowish precipitate indicates the use.
presence of halogen (Cl, Br), in the original sample c) Standard fluoride solution prepared from sodium
(if the liquor is decanted and the precipitate is white fluoride.
and readily soluble in dilute ammonia then chloride is
d) Dodecanol.
present).
e) 0.5 M Sodium hydroxide solution.
D-3.5 Determination of Presence of Fluorine
D-4.2.2 Procedure
To the second portion of the filtrate, acidify with glacial
acetic acid. Boil this solution until its total volume is D-4.2.2.1 General
reduced to half.
Place an accurately weighed sample of material
Add two to three drops of freshly prepared zirconium (25 mg-30 mg) in a 1 l oxygen flask using 2 to 3
lake reagent (equal volume of): drops of dodecanol on the sample to assist burning.
a) Alizarin solution : Prepared by mixing 0.05 gm Add 5 ml of 0.5 M sodium hydroxide solution as
alizarin Red – S in 50 ml distilled water. absorbant. Burn the sample and allow mist to settle.
b) Zirconium solution : 0.05gm zirconium nitrate Transfer the contents of the flask with minimum
in 10 ml concentrated hydrochloric acid (HCL) washing to a 50 ml volumetric flask and proceed
diluted with 50 ml of distilled water. with method A or B.
Heat at 40°C for one hour. The presence of fluoride is D-4.2.2.2 Method A — Ion selective electrode method
indicated by the red/pink colouration being bleached to fluoride
yellow.
Add 5 ml of recommended/buffer reagent to the
D-4 DETERMINATION OF LOW LEVELS OF sample solution and washings, and make up to the
FLUORINE mark. Construct a calibration curve for the fluoride ion
electrode according to the manufacturer’s instructions.
D-4.1 Principle Measure the fluoride concentration of the sample
solution and calculate the percentage of fluorine in the
D-4.1.1 General sample.
The sample is burnt in an oxygen flask, and the resulting D-4.2.2.3 Method B — Alizarin fluorine blue method
solution is used to measure the fluorine content. The
fluorine content may be measured using either of the Add 5 ml alizarin fluorine blue reagent to the sample
following methods: solution and washings and make up to the mark.
Allow to stand for the colour to develop. Measure the
a) Method A — A fluoride ion selective electrode, or absorbance of the solution at 630 nm using a 1 cm cell
b) Method B — Colourimetrically, by formation of with water as blank.
the blue-red oligomer fluorine blue complex.
Construct a calibration curve by suitably diluting
D-4.1.2 Apparatus the standard fluoride solution to give concentrations
in the range 0 μg/ml to 2 μg/ml. Also measure the
a) Oxygen flask; absorbance of a reagent blank using reagent and
b) Pipettes; and water only. Calculate the fluorine concentration in the
c) Volumetric flasks. sample.
NOTE — All apparatus used in the fluorine determination
should be made of polycarbonate or polypropylene, as fluoride
D-4.2.3 Using this method, it is estimated that fluorine
ions react with glassware. levels with values greater than 0.02 percent can be
detected.
For method A, ion selective electrode (fluoride) with
suitable millivolt meter and for method B, visible In order to determine total halogen content of the
spectrophotometer. material under test, the methods described below in
both a) and b) shall be used.
D-4.1.3 Reagents
D-4.3 Acid Gas Generation
a) Method A: electrode filling solution —
Buffer solution as recommended by electrode a) Tests shall be performed in accordance with the
manufacturer. method specified in IS 10810 (Part 59).
b) Method B: alizarin fluorine blue reagent — b) Tests shall be performed in accordance with the
Dissolve 2.5 g alizarin fluorine blue complex in method specified in D-2 .
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development of the activities of standardization, marking and quality certification of goods and attending to
connected matters in the country.
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BIS has the copyright of all its publications. No part of these publications may be reproduced in any form without
the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing the
standard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to
copyright be addressed to the Director (Publications), BIS.
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of
‘BIS Catalogue’ and ‘Standards: Monthly Additions’.
This Indian Standard has been developed from Doc No.: ETD 09 (11032).