MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC/22-23/0044 Date : 23.04.2022

Invoice No.:WIF/EX/22-23/ Date :
P.O. No.: 4500602722 Line Item: 0010 PO Date : 06.01.2022 Spec. Ref.: M25028 Rev. : B (Date:10.06.2010)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
NUT FORGING UNION 3 FIG F/
1466 P565679 Rev D 17.91 1000 Nos. AISI 4140 BF-EOF-LRF-VD-CCM
1502 MAX AISI 4140 ALLOY NQT/SB
STEEL PER SPEC M25028
15000 CWP - JSW STEEL

Heat Code: MEV DU500047082 Rev C

CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Grain Size
F04617 0.40 0.90 0.17 0.006 0.013 1.04 0.22 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 6
Max. 0.43 1.00 0.35 0.040 0.035 1.10 0.25 -
HEAT TREATMENT
Procedure :- Q00025 Rev R

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AE-120 HT Batch No. of Q&T:- A Qty :- 1000 Nos.

Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 17.91 900⁰C 3.20 870⁰C 3.20 OIL 30°C 51°C 580°C 5 (Air Cool)
Forging 17.91 900⁰C 3.20 870⁰C 3.20 OIL 30°C 51°C 580°C 5 (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 480⁰C
Max. 925⁰C 900⁰C --- 80⁰C 650⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 6.25 mm Dia, 25 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) MPI Report 4) Dimensional Report 5) Testing Annexure

Note :- We hereby guarantee no weld repairs performed.

. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, "A" stamped near to Heat code. Parts heat treated in batch number AE-121
Above material meets the requirements of ASTM A788-22

Mr. Ajay Joshi (Head - MQC, HT & NDT)

Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC/22-23/0044

P.O. No.:- 4500602722 Line Item: 0010 PO Date : 06.01.2022 Date : 23.04.2022
NUT FORGING UNION 3 FIG 1502 MAX AISI
Item : 4140 ALLOY STEEL PER SPEC M25028 Material : AISI 4140
15000 CWP

Part No.: P565679 Rev D Heat No. : F04617

Drawing No.: DU500047082 Rev C Ambient Temp : 25°C
Die No.: 1466 Hardness Range:- 277-321 HBW
Qty.: 1000 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AE-120 QT: A Machine Sr. No. 2017/09
Reference Standard: ASTM E10 Machine Make: SAROJ
Load Applied: 3000 Kgs Calibration Agency: M.M. Engineers
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: MME/CAL/072/22-23
Std Block Details: SH-2005/22 (Hardness value - 297.6 HBW) Calibrated On: 14.02.2022
Entity Performing Test: WIF Sanaswadi Calibrated Due On:13.08.2022
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 18.04.2022
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW

1000 Nos. 285 - 321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Mr. Ajay Joshi (Head - MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 MAGNETIC PARTICLE EXAMINATION REPORT

Customer : TechnipFMC

PO No. : 4500602722 Line Item : 0010 Report No : EC/22-23/0044 Date : 23.04.2022

PO Date : 06.01.2022 Test Date : 18, 19 & 20.04.2022

NUT FORGING UNION 3 FIG 1502 MAX AISI 4140

Description : Die No. : 1466 MEV
ALLOY STEEL PER SPEC M25028 15000 CWP

Part No. : P565679 Rev D Qty. : 1000 Nos.

Material : AISI 4140 Sr. No. : -

Heat No. : F04617 Heat Load No : N AE-120 QT A

Drg. No. : Stage of
DU500047082 Rev C F/NQT/SB
Examination :
Standard / Acceptance
Spec. / Q00207 Rev D , ASTM E 709 (2021) Standard / Q00207 Rev D Cl no 5.0
Procedure : Criteria :
Magnetic Particle Equipment : Magnaflux Model : AD 945DC
Calibration Date: 02.01.2022 : Calibration Due Date: 01.07.2022
Machine Sr. No : '26431017043785
Bath Concentration - 0.1 to 0.4 ml/ 100 ml Bath : 0.30 ml/ 100 ml Bath
UV-A Lamp irradiance Intensity - 1000 µWatt / cm² Minimum : 2800µWatt / cm² Make: NDT Consultant (UK) Sr no: 2137
(UV-A + LUX Meter) Calibrated on:
Ambient Visible illumination Intensity - 21.5 LUX Max. : 01 LUX 10.01.2022 Due on:10.07.2022
Type Of Magnetic Particle Material : Wet fluroscent
Magnetic Particle Used : MG 410 Magnaflux Make Batch no: 21K22 / Dec-2021
Bath Medium : Pansol 65 Carrier oil - Batch no: 605 / 2021-22
Surface Condition : As Shot Blasted
Area to be examined : 100 % of accessible Surfaces
Magnetizing Process / Method : Wet Continuous Method
Means Of Establishing Magnetization : Head Shot (Internal Conductor dia 50 mm) + Coil Shot
: 52 Gauss - Digital Hall Effect Probe Sr no:6050 Make: NDT Consultant
Observed Field Strength (Tangential)
(UK) Calibrated on: 10.01.2022 Due on:10.07.2022
Magnetization Field : Circular + Longitudinal MT Technique Sheet - MT/TS/238
Applied Current : Circular : 2800 Amp , Longitudinal : 2000 AMP
Sensitivity ensured By : Ketos Ring & SHIMS CX-230
: Within (± 3 Gauss) - Make: GNAT, DRFI Digital Gauss Meter
Residual field ensured after Demagnetization
Sr no:218001 Calibrated on:23.08.2021 Due on:23.02.2022
Result : No linear or rounded indication observed.
Remark : Material is accepted

Examined By Reviewed & Accepted By

Sign Sign
Name : Anil Thorat Name : Hemant Takawale
Cert. Type & Level - NDE Level II MT Cert. Type & Level - NDE Level II UT,MT,PT,VT As
As Per SNT-TC-1A. Per SNT-TC-1A.
Doc. No:- F-NDT-03 Rev-02 / 09 July- 2018
 Certificate of Compliance
Customer : TechnipFMC TC No.: EC/22-23/0044
Date: 23.04.2022
Die No. : 1466 Heat Code : MEV
PO No : 4500602722 Line Item No : 0010
Offer Qty. : 1000 Nos.
Part No/ Rev : P565679 Rev D Drg No / Rev : DU500047082 Rev C
NUT FORGING UNION 3 FIG 1502
Part Name : Serial No. : -
MAX AISI 4140 ALLOY STEEL PER
SPEC M25028 15000 CWP

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25028 Rev No. : B (Date:10.06.2010)
C. Material Test Report No : Mill Heat No : F04617

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 13 Nos.

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AE-120 Process Spec : Q00025 Rev R

B. Process Name : QT
Heat Lot No. : A Process Spec : Q00025 Rev R

IV. NDE
A. Process Name : MPI
Q00207 Rev D ,
Certificate No : EC/22-23/0044 Process Spec :
ASTM E 709 (2021)

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, "A" stamped near to Heat code. Parts heat treated in batch number
AE-121
Above material meets the requirements of ASTM A788-22

Sign with Stamp

Mr. Ajay Joshi (Head - MQC, HT & NDT)

 Mechanical Test Annexure
Die No.: 1466 Material Grade: AISI 4140

Heat No.: F04617 HT Lot No. : A

Heat Code: MEV TC No.: EC/22-23/0044

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW PSI PSI % %

Midwall L A-22-2146-P 149020 130811 19.44 59.21

section of
311, 321 Ambient 1
heaviest
cross section T A-22-2147-P 141675 123614 18.60 52.32

277-321 Spec. Min. 130000.00 110000.00 16.00 35.00

IMPACT TEST
QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
64 96 92 84.00
Single - 32 J Min
L LE - 0.38 mm Min 0.77 1.10 0.75 0.87
%Shear - Report 55 65 55 58.33
-29°C
Avg. - 28 J Min
60 70 56 62.00
Single - 18.7 J Min
Midwall T LE - Report 0.80 0.88 0.76 0.81
section of %Shear - Report A-22-2146-P 50 60 45 51.67
heaviest & 1
Avg. - 27 J Min
cross A-22-2147-P 46 76 60 60.67
Single - 20 J Min
section L
LE - Report 0.65 0.93 0.80 0.79
%Shear - Report 40 60 50 50.00
-40°C
Avg. - 20 J Min
52 56 56 54.67
Single - 13.5 J Min
T LE - Report 0.72 0.77 0.77 0.75
%Shear - Report 45 45 45 45.00

Mr. Ajay Joshi (Head - MQC, HT & NDT)

Authorised Signatory