MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC0313 Date : 27.06.2022

Invoice No.:WIF/EX/22-23/ Date :
P.O. No.: 4500630489 Line Item: 10 PO Date : 25.03.2022 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT PLUG F/
1300 VALVE 2 ULT150 F/UNION P537156 Rev D NQT/SB 7.21 : 1 896 Nos AISI 4140 BF-EOF-LRF-VD-CCP
ENDS AISI 4140 ALLOY STEEL
FMC SPEC M25070 - JSW STEEL LTD
Heat Code: MEY DU500006672 Rev B
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Ni Grain Size
F05025 0.40 0.93 0.22 0.008 0.009 1.06 0.23 0.23 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 - -
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AE-463 HT Batch No. of Q&T:- AE-465 Qty :- 896 Nos
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 7.21 : 1 890⁰C 3.20 870⁰C 3.20 OIL 32°C 55°C 580°C 5 (Air Cool)
Forging 7.21 : 1 890⁰C 3.20 870⁰C 3.20 OIL 32°C 55°C 580°C 5 (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 12.5 mm Dia, 50 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure

Note :- We hereby guarantee no weld repairs performed.
. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, heat treatment batch "AE-465" stamped near to Heat code.
The above material meets the requirement of ASTM A788 - 22

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC0313

P.O. No.:- 4500630489 Line Item: 10 PO Date : 25.03.2022 Date : 27.06.2022
BODY FORGING, ULT PLUG VALVE 2
Item : ULT150 F/UNION ENDS AISI 4140 ALLOY Material : AISI 4140
STEEL FMC SPEC M25070

Part No.: P537156 Rev D Heat No. : F05025

Drawing No.: DU500006672 Rev B Ambient Temp : 30°C
Die No.: 1300 Hardness Range:- 277 - 331 HBW
Qty.: 896 Nos Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AE-463 QT: AE-465 Sr No.09/2021-036
Reference Standard: ASTM E10 Machine Make: SAROJ
Load Applied: 3000 Kgs Calibration Agency: MTMS

Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: 'MATRIX/CAL/2021-2022/12/2040

Std Block Details: SH-0076/22 (Hardness value - 322.6 HBW)

Calibrated On: 10.12.2021
& SH-0152/22 (Hardness Value-297.8 HBW)
Entity Performing Test: WIF Sanaswadi Calibration Due On:09.12.2022
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 21 & 22.06.2022
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW

896 Nos 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 Certificate of Compliance
Customer : TechnipFMC TC No.: EC0313
Date: 27.06.2022
Die No. : 1300 Heat Code : MEY
PO No : 4500630489 Line Item No : 10
Offer Qty. : 896 Nos
Part No/ Rev : P537156 Rev D Drg No / Rev : DU500006672 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
2 ULT150 F/UNION ENDS AISI 4140
ALLOY STEEL FMC SPEC M25070

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F05025

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 16 Nos.
III. Secondary Process : Heat Treatment
A. Process Name : Normalised
Heat Lot No. : AE-463 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : AE-465 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI
Certificate No : NA Process Spec : NA

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, heat treatment batch "AE-465" stamped near to Heat
code.
The above material meets the requirement of ASTM A788 - 22
Sign with Stamp
Mr. Ajay Joshi (HEAD-MQC, HT & NDT)
 Mechanical Test Annexure
Die No.: 1300 Material Grade: AISI 4140

Heat No.: F05025 HT Lot No. : AE-465

Heat Code: MEY TC No. : EC0313

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below
L 293, 293 Ambient C-22-2671-P 1 144.04 123.14 19.62 61.67
HT Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
104 78 94 92.00
Single - 32 J Min
LE - 0.51 mm Min -29°C 1.35 1.00 1.25 1.20
%Shear - Report 70 60 65 65.00
L 1
Avg. - 27 J Min
36 28 30 31.33
Single - 20 J Min
LE - Report -40°C 0.50 0.39 0.41 0.43

%Shear - Report 30 20 25 25.00

0.5" below
Avg. - 28 J Min C-22-2671-P
HT Surface 38 42 32 37.33
Single - 18.7 J Min
-29°C
LE - Report 0.51 0.54 0.45 0.50

%Shear - Report 30 35 25 30.00

T 1
Avg. - 20 J Min
24 30 36 30.00
Single - 14 J Min
LE - Report -40°C 0.35 0.41 0.47 0.41

%Shear - Report 15 25 30 23.33

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 Mechanical Test Annexure
Die No.: 1300 Material Grade: AISI 4140

Heat No.: F05025 HT Lot No. : AE-465

Heat Code: MEY TC No. : EC0313

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below
L 293, 293 Ambient C-22-2672-P 2 145.82 123.71 19.56 61.88
HT Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
90 90 108 96.00
Single - 32 J Min
LE - 0.51 mm Min -29°C 1.12 1.13 1.30 1.18
%Shear - Report 70 70 70 70.00
L 2
Avg. - 27 J Min
88 70 40 66.00
Single - 20 J Min
LE - Report -40°C 1.02 0.88 0.57 0.82

%Shear - Report 65 60 30 51.67

0.5" below
Avg. - 28 J Min C-22-2672-P
HT Surface 48 40 40 42.67
Single - 18.7 J Min
-29°C
LE - Report 0.61 0.54 0.58 0.58

%Shear - Report 40 30 30 33.33

T 2
Avg. - 20 J Min
24 38 34 32.00
Single - 14 J Min
LE - Report -40°C 0.35 0.51 0.46 0.44

%Shear - Report 20 30 25 25.00

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory