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Designation: B425 − 11
Standard Specification for
Ni-Fe-Cr-Mo-Cu Alloy (UNS N08825, UNS N08221, and
UNS N06845) Rod and Bar1
This standard is issued under the fixed designation B425; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* E29 Practice for Using Significant Digits in Test Data to
1.1 This specification 2 covers nickel-iron-chromium- Determine Conformance with Specifications
molybdenum-copper alloy (UNS N08825, UNS N08221, and E1473 Test Methods for Chemical Analysis of Nickel,
UNS N06845)3 in the form of hot-finished and cold-drawn Cobalt, and High-Temperature Alloys
rounds, squares, hexagons, and rectangles.
3. Terminology
1.2 The values stated in inch-pound units are to be regarded
as standard. The values given in parentheses are mathematical 3.1 Definitions of Terms Specific to This Standard:
conversions to SI units that are provided for information only 3.1.1 bar, n—material of rectangular (flats), hexagonal, or
and are not considered standard. square solid section up to and including 10 in. (254 mm) in
width and 1⁄8 in. (3.2 mm) and over in thickness in straight
1.3 The following precautionary caveat pertains only to the lengths.
test methods portion, Section 12, of this specification: This 3.1.1.1 Discussion—Hot-worked rectangular bar in widths
standard does not purport to address all of the safety problems, 10 in. (254 mm) and under may be furnished as hot-rolled plate
if any, associated with its use. It is the responsibility of the user with sheared or cut edges in accordance with Specification
of this standard to become familiar with all hazards including B424, provided the mechanical property requirements of this
those identified in the appropriate Material Safety Data Sheet specification are met.
(MSDS) for this product/material as provided by the
manufacturer, to establish appropriate safety and health 3.1.2 rod, n—material of round solid section furnished in
practices, and determine the applicability of regulatory limi- straight lengths.
tations prior to use.
4. Ordering Information
2. Referenced Documents 4.1 It is the responsibility of the purchaser to specify all
2.1 ASTM Standards:4 requirements that are necessary for the safe and satisfactory
B424 Specification for Ni-Fe-Cr-Mo-Cu Alloy (UNS performance of material ordered under this specification.
N08825, UNS N08221, and UNS N06845) Plate, Sheet, Examples of such requirements include, but are not limited to,
and Strip the following:
B880 Specification for General Requirements for Chemical 4.1.1 ASTM designation and date of issue,
Check Analysis Limits for Nickel, Nickel Alloys and 4.1.2 UNS number,
Cobalt Alloys 4.1.3 Section—Rod (round) or bar (square, hexagonal, or
E8 Test Methods for Tension Testing of Metallic Materials rectangular),
4.1.4 Dimensions, including length,
4.1.5 Condition (see Appendix X1),
1
This specification is under the jurisdiction of ASTM Committee B02 on 4.1.6 Finish (see Appendix X1),
Nonferrous Metals and Alloys and is the direct responsibility of Subcommittee
B02.07 on Refined Nickel and Cobalt and Their Alloys.
4.1.7 Quantity—Feet (or metres) or number of pieces,
Current edition approved Oct. 1, 2011. Published November 2011. Originally 4.1.8 Certification—State if certification is required (Sec-
approved in 1964. Last previous edition approved in 2009 as B425 – 99 (2009). tion 15),
DOI: 10.1520/B0425-11. 4.1.9 Samples for Product (Check) Analysis—State whether
2
For ASME Boiler and Pressure Vessel Code applications, see related Specifi-
cation SB-425 in Section II of that code. samples for product (check) analysis should be furnished (see
3 5.2), and
New designation established in accordance with Practice E527 and SAE
J 1086, Practice for Numbering Metals and Alloys (UNS). 4.1.10 Purchaser Inspection—If purchaser wishes to wit-
4
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
ness tests or inspection of material at place of manufacture, the
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on purchase order must so state, indicating which test or inspec-
the ASTM website. tions are to be witnessed (Section 13).
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
B425 − 11
TABLE 1 Chemical RequirementsA
Element UNS N08825 UNS N08221 UNS N06845
Nickel 38.0–46.0 39.0–46.0 44.0–50.0
Chromium 19.5–23.5 20.0–22.0 20.0–25.0
IronB 22.0 min balance balance
Manganese 1.0 1.0 0.5
Carbon 0.05 0.025 0.05
Copper 1.5–3.0 1.5–3.0 2.0–2.4
Silicon 0.5 0.5 0.5
Sulfur 0.03 0.03 0.010
Aluminum 0.2 0.2 ...
Titanium 0.6–1.2 0.6–1.0 ...
Molybdenum 2.5–3.5 5.0–6.5 5.0–7.0
Tungsten ... ... 2.0–5.0
A
Maximum unless range or minimum is given. Where ellipses (...) appear in this table, there is no requirement and analysis for the element need not be determined or
reported.
B
Element shall be determined arithmetically by difference.
TABLE 2 Mechanical Properties (Rod and Bar)
Yield Strength Elongation in 2
Tensile Strength
Alloy Condition 0.2 % offset, min, in. or 50 mm or
min, ksi (MPa)
ksi (MPa) 4D , min,%
UNS N08825 Annealed: 85 (586) 35 (241) 30A
Hot-finished, cold–drawn
B B B
Forging Quality:
UNS N08221 All sizes annealed 79 (544) 34 (235) 30
UNS N06845 All sizes annealed 100 (690) 40 (276) 30
A
Not applicable to diameters or cross sections under 3⁄32 in. (2.4 mm).
B
Forging quality is furnished to chemical requirements and surface inspection only. No tensile properties are required.
TABLE 3 Permissible Variations in Diameter or Distance Between
5. Chemical Composition Parallel Surfaces of Cold-Worked Rod and Bar
Permissible Variations From
5.1 The material shall conform to the composition limits Specified Dimension, in. Specified Dimension, in. (mm)
specified in Table 1. (mm)A
Plus Minus
5.2 If a product (check) analysis is performed by the Rounds:
1⁄16 (1.6) to 3⁄16 (4.8), excl 0 0.002 (0.05)
purchaser, it shall be done in accordance with Specification 3⁄16 (4.8) to 1⁄2 (12.7), excl 0 0.003 (0.08)
B880 and the material shall conform to the product (check) 1⁄2 (12.7) to 15⁄16 (23.8), incl 0.001 (0.03) 0.002 (0.05)
analysis variations defined in Table 1 of Specification B880. Over 15⁄16 (23.8) to 115⁄16 (49.2), incl 0.0015 (0.04) 0.003 (0.08)
Over 115⁄16 (49.2) to 21⁄2 (63.5), incl 0.002 (0.05) 0.004 (0.10)
Hexagons, squares, rectangles:
6. Mechanical Properties and Other Requirements 1⁄2 (12.7) and less 0 0.004 (0.10)
6.1 Mechanical Properties—The material shall conform to Over 1⁄2 (12.7) to 7⁄8 (22.2), incl 0 0.005 (0.13)
Over 7⁄8 (22.2) to 11⁄4 (31.8), incl 0 0.007 (0.18)
the mechanical properties specified in Table 2. Over 1 1⁄4 (31.8) to 2 (50.8), incl 0 0.009 (0.23)
A
Dimensions apply to diameter of rounds, to distance between parallel surfaces of
7. Dimensions and Permissible Variations hexagons and squares, and separately to width and thickness of rectangles.
7.1 Diameter, Thickness, or Width—The permissible varia-
tions from the specified dimensions as measured on the
diameter or between parallel surfaces of cold-worked rod and
bar shall be as prescribed in Table 3, and of hot-worked rod and the allowances prescribed in Table 5 are recommended for
bar as prescribed in Table 4. normal machining operations.
7.2 Out-of-Round—Hot-worked rods and cold-worked rods 7.5 Length—The permissible variations in length of cold-
(except “forging quality”) all sizes, in straight lengths, shall not worked and hot-worked rod and bar shall be as prescribed in
be out-of-round by more than one half the total permissible Table 6.
variations in diameter shown in Table 3 and Table 4, except for 7.5.1 Rods and bars ordered to random or nominal lengths
hot-worked rods 1⁄2 in. (12.7 mm) in diameter and under, which will be furnished with either cropped or saw-cut ends; material
may be out-of-round by the total permissible variations in ordered to cut lengths will be furnished with square saw-cut or
diameter shown in Table 4. machined ends.
7.3 Corners—Cold-worked bars will have practically exact 7.6 Straightness:
angles and sharp corners. 7.6.1 The permissible variations in straightness of cold-
7.4 Machining Allowances for Hot-Worked Materials— worked rod and bar as determined by the departure from
When the surfaces of hot-worked products are to be machined, straightness shall be as prescribed in Table 7.
2
B425 − 11
TABLE 4 Permissible Variations in Diameter or Distance Between 11.1.1 All rod and bar shall be tested in full cross-section
Parallel Surfaces of Hot-Worked Rod and Bar size when possible. When a full cross-section size test cannot
Permissible Variations From be performed, the largest possible round specimen shown in
Specified Dimension, in. Specified Dimension, in. (mm)
(mm)A Test Methods E8 shall be used. Longitudinal strip specimens
Plus Minus
shall be prepared in accordance with Test Methods E8 for
Rod and bar, hot-worked:
1 (25.4) and under 0.016 (0.41) 0.016 (0.41)
rectangular bar up to 1⁄2 in. (12.7 mm), inclusive, in thicknesses
over 1 (25.4) to 2 (50.8), incl 0.031 (0.79) 0.016 (0.41) which are too wide to be pulled full size.
over 2 (50.8) to 4 (101.6), incl 0.047 (1.19) 0.031 (0.79)
over 4 (101.6) 0.125 (3.18) 0.063 (1.60) 12. Test Methods
Rod, rough-turned or ground:
Under 1 (25.4) 0.005 (0.13) 0.005 (0.13) 12.1 The chemical composition and mechanical and other
1 (25.4) and over 0.031 (0.79) 0
Forging quality rod:B
properties of the material as enumerated in this specification
Under 1 (25.4) 0.005 (0.13) 0.005 (0.13) shall be determined, in case of disagreement, in accordance
1 (25.4) and over 0.031 (0.79) 0 with the following ASTM standards:
A
Dimensions apply to diameter of rods, to distance between parallel surfaces of Test ASTM Designation
hexagons and squares, and separately to width and thickness of rectangles.
B
Spot grinding is permitted to remove minor surface imperfections. The depth of Chemical analysis E1473
these spot ground areas shall not exceed 3 % of the diameter of the rod. Tension E8
Rounding procedure E29
12.2 For purposes of determining compliance with the
specified limits for requirements of the properties listed in the
7.6.2 The permissible variations in straightness of hot- following table, an observed or calculated value shall be
worked rod and bar as determined by the departure from rounded as indicated below, in accordance with the rounding
straightness shall be as specified in Table 8. method of Practice E29:
Rounded unit for observed or
Test
calculated value
8. Workmanship, Finish, and Appearance Chemical composition nearest unit in the last right hand place of figures
8.1 The material shall be uniform in quality and condition, and tolerances of the specified limit. If two choices are possible,
(when expressed in as when the digits dropped are exactly a 5, or a
smooth, commercially straight or flat, and free of injurious decimals) 5 followed only by zeros, choose the one ending
imperfections. in an even digit, with zero defined as an even
digit.
Tensile strength and nearest 1000 psi (6.9 MPa)
9. Sampling Yield strength
Elongation nearest 1 %
9.1 Lot—Definition :
9.1.1 A lot for chemical analysis shall consist of one heat. 13. Inspection
9.1.2 A lot for mechanical properties testing shall consist of
all material from the same heat, nominal diameter or thickness, 13.1 Inspection of the material shall be made as agreed upon
and condition. between the manufacturer and the purchaser as part of the
9.1.2.1 Where material cannot be identified by heat, a lot purchase contract.
shall consist of not more than 500 lb (227 kg) of material in the
14. Rejection and Rehearing
same size and condition. A single piece weighing over 500 lb
shall be considered as one lot. 14.1 Material tested by the purchaser that fails to conform to
the requirements of this specification may be rejected. Rejec-
9.2 Test Material Selection:
tion should be reported to the producer or supplier promptly
9.2.1 Chemical Analysis—Representative samples from
and in writing. In case of dissatisfaction with the results of the
each lot shall be taken during pouring or subsequent process-
test, the producer or supplier may make claim for a rehearing.
ing.
9.2.1.1 Product (check) analysis shall be wholly the respon- 15. Certification
sibility of the purchaser.
9.2.2 Mechanical Properties—Samples of the material to 15.1 When specified in the purchase order or contract, a
provide test specimens for mechanical properties shall be taken manufacturer’s certification shall be furnished to the purchaser
from such locations in each lot as to be representative of that stating that the material has been manufactured, tested, and
lot. inspected in accordance with this specification and that test
results on representative samples meet specification require-
10. Number of Tests ments. When specified in the purchase order or contract, a
report of the test results shall be furnished.
10.1 Chemical Analysis—One test per lot.
10.2 Tension—One test per lot. 16. Product Marking
16.1 The following information shall be marked on the
11. Specimen Preparation material or included on the package, or on a label or tag
11.1 Tension test specimens shall be taken from material in attached thereto: The name of the material or UNS number;
the final condition and tested in the direction of fabrication. heat number; condition (temper); this specification number; the
3
B425 − 11
TABLE 5 Normal Machining Allowances for Hot-Worked Material
Normal Machining Allowance, in. (mm)
Finished-Machined Dimensions Distance Between
for Finishes As Indicated Below, For Rectangular Bar
On Diameter, Parallel Surfaces,
in. (mm)A for Rods for Hexagonal
and Square Bars On Thickness On Width
Hot-worked:B
Up to 7⁄8 (22.2), incl 1⁄8 (3.2) 1⁄8 (3.2) 1⁄8 (3.2) 3⁄16 (4.8)
Over 7⁄8 to 1 7⁄8 (22.2 to 47.6), incl 1⁄8 (3.2) 3⁄16 (4.8) 1⁄8 (3.2) 3⁄16 (4.8)
Over 1 7⁄8 to 2 7⁄8 (47.6 to 73.0), incl. 3⁄16 (4.8) 1⁄4 (6.4) ... 3⁄16 (4.8)
Over 2 7⁄8 to 313⁄16 (73.0 to 96.8), incl 14⁄ (6.4) ... ... 3 16
⁄ (4.8)
Over 313⁄16 (96.8) 14⁄ (6.4) ... ... 38⁄ (9.5)
Hot-worked rods, rough-turned or rough ground:C
15⁄16 to 4 (23.8 to 101.6), incl in diameter 1 16
⁄ (1.6) ... ... ...
Over 4 to 12 (101.6 to 304.8), incl in diameter 18 ⁄ (3.2) ... ... ...
A
Dimensions apply to diameter of rods, to distance between parallel surfaces of hexagonal and square bar, and separately to width and thickness of rectangular bar.
B
The allowances for hot-worked material in Table 5 are recommended for rods machined in lengths of 3 ft (0.91 m) or less and for bars machined in lengths of 2 ft (0.61
m) or less. Hot-worked material to be machined in longer lengths should be specified showing the finished cross-sectional dimension and the length in which the material
will be machined in order that the manufacturer may supply material with sufficient oversize, including allowance for out-of-straightness.
C
Applicable to 3 ft (0.91 m) max length.
TABLE 6 Permissible Variations in Length of Rods and Bars TABLE 7 Permissible Variations in Straightness of Cold-Worked
Random mill lengths: Rods and Bars
Hot-worked 6 to 24 ft (1.83 to 7.31 m) long with not Specified Diameter or
more than 25 weight % between 6 and Permissible Variations in
Distance Between Parallel
9 ft (1.83 and 2.74 m)A Lengths Indicated, in. (mm)
Surfaces, in (mm)A
Cold-worked 6 to 20 ft (1.83 to 6.1 m) long with not
Rounds: Depth of chord:
more than 25 weight % between 6 and 1⁄2 (12.7) to 2 1⁄2 (63.5), incl 0.030 (0.76) per ft (305 mm) of length
10 ft (1.83 and 3.05 m).
Hexagons, squares, rectangles:
Multiple lengths Furnished in multiples of a specified unit 12
⁄ (12.7) to 2 (50.8), 0.030 (0.76) per ft (305 mm) of length
length, within the length limits indicated
incl
above. For each multiple, an allowance
A
of 1⁄4 in. (6.4 mm) will be made for cutting, Material under 1⁄2 in. (12.7 mm) shall be reasonably straight and free of sharp
unless otherwise specified. At the bends and kinks.
manufacturer’s option, individual specified
unit lengths may be furnished.
Nominal lengths Specified nominal lengths having a range
of not less than 2 ft (610 mm) with no TABLE 8 Permissible Variations in Straightness of Hot-Worked
short lengths allowed.B Rods and BarsA
Cut lengths A specified length to which all rods and Permissible Variations,
bars will be cut with a permissible Finish
in./ft (mm/m)B
variation of plus 1⁄8 in. (3.2 mm), minus Rods and bars, hot-worked 0.050 (4.2)C
0 for sizes 8 in. (203 mm) and less in Rounds—hot-worked, rough ground or rough turned 0.050 (4.2)C
diameter or distance between parallel A
surfaces. For larger sizes, the permissible Not applicable to forging quality.
B
variation shall be + 1⁄4 in. (6.4 mm), − 0. Material under 1⁄2 in. (12.7 mm) shall be reasonably straight and free of sharp
bends and kinks.
A C
For hot-worked sections weighing over 25 lb/ft (37 kg/m) and for smooth forged The maximum curvature (depth of chord) shall not exceed the values indicated
products, all sections, short lengths down to 2 ft (610 mm) may be furnished. multiplied by the length in feet.
B
For cold-worked rods and bars under 1⁄2 in. (12.7 mm) in diameter or distance
between parallel surfaces ordered to nominal or stock lengths with a 2-ft (610-mm)
range, at least 93 % of such material shall be within the range specified; the
balance may be in shorter lengths but in no case shall lengths less than 4 ft (1220
mm) be furnished.
17. Keywords
size; gross, tare and net weight; consignor and consignee 17.1 UNS N08825; UNS N08221; UNS N06845; bar; rod
address; contract or order number; or such other information as
may be defined in the contract or order.
4
B425 − 11
APPENDIX
(Nonmandatory Information)
X1. PROCURABLE CONDITIONS AND FINISHES
X1.1 The various conditions and finishes in which rod and to a bar peeling operation and thus may not be straight.
bar are procurable are as follows: Intended generally for machining where an overhauled surface
X1.1.1 Hot-Worked, Annealed—Soft, with a tightly adher- is desired, essentially for machined step down shafts or parts
ent dark oxide. machined in short lengths of 3 ft (0.91 m) or less.
X1.1.2 Hot-Worked, Annealed, and Pickled—Same as X1.1.5 Hot-Worked, Forging Quality—Rough-turned and
X1.1.1 except descaled for removal of mill oxide. Provides for spot-ground, as necessary, for sizes 1 in. (25.4 mm) in diameter
better surface inspection than does hot-worked, annealed and over; rough ground and spot ground for sizes under 1 in. in
material and often employed where welding is involved where diameter. Material is selected from heats of known, good hot
removal of mill oxide is desired. malleability.
NOTE X1.1—Annealing prior to pickling may be required in order to NOTE X1.2—For sizes 21⁄2 in. (63.5 mm) in diameter and less,
reduce the mill oxide since uniform pickling of an unreduced oxide is cold-worked rod may be used also for forging by virtue of the fact such
difficult. rod have been overhauled for removal of mechanical surface defects prior
to cold-working. In such cases, the user should run pilot forging tests to
X1.1.3 Hot-Worked, Annealed, and Rough Ground—Similar ensure himself that such material has the desired hot malleability range.
to X1.1.1 except rough ground. X1.1.6 Cold-Worked, Annealed, and Pickled—Hotworked,
X1.1.4 Hot-Worked, Annealed, and Rough-Turned—Similar overhauled, cold-worked, annealed, descaled, and straightened.
to X1.1.1 except rough turned with a broad nosed tool similar Annealed for softness and with a dull matte finish.
SUMMARY OF CHANGES
Committee B02 has identified the location of selected changes to this standard since the last issue
(B425 - 99 (2009)) that may impact the use of this standard. (Approved October 1, 2011.)
(1) Revised Title, subsection 1.1, subsection 2.1, Table 1, and (3) Added Section 17.
Table 2; to add UNS N06845.
(2) Revised Table 1 to add new footnote A and renumber old
footnote A to B.
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.
This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above
address or at 610-832-9585 (phone), 610-832-9555 (fax), or service@astm.org (e-mail); or through the ASTM website
(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/
COPYRIGHT/).
5
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