Conventional Vickers and true instrumented indentation

hardness determined by instrumented indentation tests

Seung-Kyun Kang
Department of Materials Science and Engineering, Seoul National University, Seoul 151-744, Korea
Ju-Young Kima)
Materials Science, California Institute of Technology, Pasadena, California 91106
Chan-Pyoung Park, Hyun-Uk Kim, and Dongil Kwon
Department of Materials Science and Engineering, Seoul National University, Seoul 151-744, Korea

(Received 16 September 2009; accepted 18 November 2009)

We evaluate Vickers hardness and true instrumented indentation test (IIT) hardness of
24 metals over a wide range of mechanical properties using just IIT parameters by taking
into account the real contact morphology beneath the Vickers indenter. Correlating the
conventional Vickers hardness, indentation contact morphology, and IIT parameters
for the 24 metals reveals relationships between contact depths and apparent material
properties. We report the conventional Vickers and true IIT hardnesses measured only
from IIT contact depths; these agree well with directly measured hardnesses within

6% for Vickers hardness and
10% for true IIT hardness.

I. INTRODUCTION sink-in of a sharp indenter. From extensive finite-

The fundamental advantage of instrumented indenta- element analysis (FEA) work on a wide range of elasto-
tion testing (IIT) over conventional hardness testing is plastic materials, Cheng and Cheng13,25,30 proposed to
that mechanical properties such as elastic modulus,1–15 measure elastic modulus and hardness without determin-
tensile properties,16–29 and hardness can be measured by ing the contact area directly by correlating these proper-
analyzing the indentation force–depth curve and without ties and the indentation work ratio. Alcala et al.,35 using
observing the residual indentation marks. However, elas- FEA, suggested a relationship between strain-hardening
toplastic deformation of materials around the indenter, exponent n and pileup/sink-in height. Cheng and Cheng
i.e., plastic pileup or sink-in,30–37 makes it difficult to also suggested a correction parameter f, the ratio of con-
determine the true contact depth in the loaded state. A tact depth (hc) to maximum indentation depth (hmax), and
contact depth can be determined by taking into account showed that f is given by the product of a function of the
the response of two major materials to an indentation, strain-hardening exponent n and the ratio of yield
elastic deflection from the initial sample surface, and strength to reduced elastic modulus (sys/Er).31,32 Choi
plastic pileup/sink-in around the indenter.30–37 The elas- et al.36 proposed a modified correction parameter f in-
tic deflection depth (hd) is given by the widely used cluding indenter tip bluntness (△hb) as:
Oliver and Pharr method3,12:

hc sys
Pmax f ¼ ¼ 1:2445ð1  0:6nÞ 1  7:2 :
hd ¼ e ; ð1Þ hmax þ Dhb Er
S ð2Þ
where Pmax and S are the maximum indentation force
and initial unloading stiffness, respectively, and e is a However, previous research on this topic has all
geometrical constant (0.75 for a conical indenter). How- or some of the following limitations that require further
ever, the plastic pileup and sink-in cannot be expressed studies:
as an analytical equation because the plastic deformation (i) The data were obtained by FEA simulation. Even
underneath the indenter is far more complex than elastic though FEA is a well-established tool, more real data are
deflection. certain to be obtained by experimental results.
Many studies30–37 have been performed to evaluate (ii) In the FEA simulations, conical indenters were
the contact depth, taking into account the plastic pileup/ used to simulate sharp indenters such as Berkovich and
Vickers indenters. While this difference does not matter
a)
Address all correspondence to this author. for true IIT hardness, it is critical when conventional
e-mail: juyoung1@snu.ac.kr Vickers hardness is measured by IIT, since it depends
DOI: 10.1557/JMR.2010.0045 only on contact depth at corners.

J. Mater. Res., Vol. 25, No. 2, Feb 2010 © 2010 Materials Research Society 337
 S-K. Kang et al.: Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

(iii) To use the proposed equations, tensile properties indenter, the projected contact depth representing the
such as strain-hardening exponent and yield strength are projected contact area may lie between the contact
required. Since the proposed equations cannot be applied depths at the center and at a corner. Third, the conven-
only with IIT for unknown materials, their applications tional Vickers hardness is given by the maximum force
are limited. divided by the four-sided pyramidal contact area, which
To explain the three different hardness values and corre- is evaluated from the diagonals of the residual indenta-
sponding contact depths in IIT using a Vickers indenter, tion marks after unloading. If the recovery in the in-
we show in Fig. 1 a schematic of contact morphology for plane direction during unloading is negligible,35 the
pileup around a Vickers indenter. First, conventional IIT diagonals evaluated
 from the contact depth at corners in
hardness (HO-P) is given by the maximum indentation force the loaded state hVc should be the same as those of the
divided by the projected contact area corresponding to residual indentation marks. Vickers hardness is repre-
the contact depth (hc,O-P) in the Oliver–Pharr method3,12,38: sented by contact depth at corners as
Pmax
HO-P ¼  2 ; ð3Þ Pmax
24:5  hc;O-P HV ¼  2 : ð5Þ
26:43  hV
c
which subtracts the elastic deflection depth hd from the
maximum indentation depth hmax. This hardness is Vickers hardness, the result of conventional hardness
measured only with IIT parameters such as maximum testing using a self-similar indenter, is widely used and
applied force and unloading stiffness, as shown in has an extensive number of databases. Nevertheless, the
Eq. (1), and thus is widely used although it does not take evaluation algorithms for Vickers hardness using IIT are
into account plastic pileup/sink-in. Second, true IIT insufficient for its industrial uses. The problem arises
hardness (Htrue) is given by the maximum from the different definitions of contact area in Vickers
  force divided
by the true projected contact area hpro : hardness and IIT hardness. Vickers hardness calculates
c
Pmax the contact area from the corner-to-corner diagonal, ig-
Htrue ¼ 2
; ð4Þ noring the difference in pileup/sink-in around the side of
24:5  ðhpro
c Þ indenter, which must be contained to derive the IIT
considering plastic pileup/sink-in. Since plastic pileup/ hardness. Thus, algorithms for evaluating not only true
sink-in is more constrained at the corners of the Vickers IIT hardness but also Vickers hardness that take into
account the real contact depth through IIT will be simple
and useful techniques in hardness testing.
In this study, we propose methods for measuring
Vickers hardness and true IIT hardness that use IIT alone
by taking into account the pileup height at the corner
and the representative pileup height, respectively. To this
end, we correlate the pileup heights with experimentally
measured IIT parameters for 24 metals over a wide range
of mechanical properties. We show that the true IIT hard-
ness and conventional Vickers hardness measured by the
proposed methods for the 24 metals agree well with the
true values within
6% for Vickers hardness and
10%
for true IIT hardness.

II. EXPERIMENTS
Twenty-four metal samples with a wide range of me-
chanical properties—Al alloys, Mg alloys, Cu alloys, Ti
alloys, Ni alloys, carbon steels, API X-grade steels, fer-
rite-based stainless steels, and austenite-based stainless
steels—were prepared for indentation tests and uniaxial
tensile tests. For the indentation tests, one side of the
samples was finely polished with 1 mm alumina powder.
IITs were conducted using the AIS 3000 instrumented
indentation system (Frontics Inc., Seoul, Korea) with
force resolution of 55 mN and displacement resolution
FIG. 1. Diagonal area and projected area at pileup and sink-in. of 100 nm and a Vickers indenter. The IITs were

338 J. Mater. Res., Vol. 25, No. 2, Feb 2010

 S-K. Kang et al.: Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

performed at constant displacement rate 0.3 mm/min plastic indentation pileup.31,32,35,36 For the metal sam-
with maximum indentation depth of 80 mm. After inden- ples, fV shows good linearity with E/sys, while it has
tation, the residual indentation marks were observed by much less relation with n. If we assume a Tabor relation-
optical microscopy to evaluate the conventional Vickers ship between yield strength and hardness (H = Csys,
hardness. The relationship between the diagonal and con- where C is plastic constraint factor of 3),9 fV can also
tact depth at the corner of the residual indent is given by be related to E/H, as shown in Fig. 3. It is notable that, in
d Fig. 3, hardness H and elastic modulus E are determined
c ¼ pffiffiffi
hV ; ð6Þ by optically measured projected area of residual impres-
2 2 tan yV sion and ultrasonic pulse-echo technique, respectively,
where yV is the half angle of the Vickers indenter, 68 . not by the E/sy data in Fig. 2. The ratio of hardness
The ratio of contact depth at the corner to maximum
indentation depth is defined as
hV
fV ¼ c
: ð7Þ
hmax
Because the elastic recovery during unloading hap-
pens mainly along loading direction and negligible
in-plane direction,35 the projected contact area at the
maximum indentation depth can be measured directly
from the area of the residual indentation mark. The pro-
jected area Apro
c was measured using an image analyzer
(NIS Elements, Nikon, Tokyo, Japan), from which the
projected contact depth hpro
c was calculated by
pffiffiffiffiffiffiffiffi
Apro
c
hc ¼
pro
; ð8Þ
2 tan yV
and the ratio of the projected contact depth to maximum
indentation depth is defined as
hpro
fpro ¼ c
: ð9Þ
hmax
Figure 1 shows the contact morphology of Vickers
indentation for material pileup around the indenter. The
contact depth at the corner hV c determines conventional
Vickers hardness, while the projected contact depth hpro c
is the parameter determining the true IIT hardness.
Uniaxial tensile tests were carried out using an Instron FIG. 2. Relation between contact depth function and tensile proper-
ties. (a) Hardening exponent and (b) ratio of elastic modulus and yield
5582 (Instron Inc., Grove City, PA) at cross-head speed strength.
1 mm/min; the gauge length and diameter of the cylin-
drical specimens were 25 and 6 mm, respectively, in
accordance with the ASTM standard.39 Elastic moduli
of the samples were measured by an ultrasonic pulse-
echo technique using a two-channel digital real-time
oscilloscope.

III. RESULTS AND DISCUSSION

To explore the relationship between plastic pileup
underneath the Vickers indenter and material plastic
properties, we show in Fig. 2 the relationship of the
contact depth function fV versus the strain-hardening
exponent n and the ratio of elastic modulus to yield
strength, E/sys, corresponding to the inverse of the yield FIG. 3. Relation between contact depth function and ratio of elastic
strain, both of which have been widely used to describe modulus and hardness.

J. Mater. Res., Vol. 25, No. 2, Feb 2010 339

 S-K. Kang et al.: Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

and elastic modulus can be expressed as the ratio of H We hmax  hf

irreversible work (Wtotal  We) to total work (Wtotal) k ¼  : ð11Þ
E Wtotal hmax
during indentation:
The ratio of elastic modulus to yield strength can thus be
H Wtotal  We represented using Eqs. (10) and (11) by the maximum
1k ¼ ; ð10Þ
E Wtotal indentation depth hmax and final indentation depth hf.12,36
Figure 4 shows the relationship between the contact
where We is the work recovered during unloading and depth function (fV) and contact depth ratio hmax/
k is a constant commonly taken as 5.36 By using linear (hmax  hf), which shows good linearity; we obtain the
indentation loading and unloading curves, Wtotal and We linear relation
are measured approximately by
hmax
fV ¼ 9:90  103 þ 1:00 ; ð12Þ
hmax  hf
which can be written as

1
c  hmax
hV 3 hmax  hf
¼ 9:90  10 ; ð13Þ
hmax hmax

where (hV c  hmax)/hmax is the normalized pileup

from the reference plane, and (hmax  hf)/hmax is the
normalized recovery depth. For a geometrically self-
similar sharp indenter such as the Vickers indenter,
the representative total strain is determined regardless
of indentation depth,9,13 so the plastic pileup is most
FIG. 4. Linear relation of contact depth function at corner and nor- likely to be related to the ratio of elastically recovered
malized recovery depth. depth to maximum indentation depth. Table I presents

TABLE I. Evaluation of contact depth at the corner and Vickers hardness using the contact depth function.

hV
c hV
c Eq. (12) Error Vickers hardness Vickers hardness Error
Materials E/sys n (mm) (mm) (%) (HV) Eq. (12) (HV) (%)
Al alloy Al6061 323.86 0.063 84.95 87.81 3.4 117.38 109.85 6.4
Al7075 136.19 0.080 84.77 83.76 1.2 173.47 177.71 2.4
Mg alloy AZ61 272.73 0.300 85.52 86.53 1.2 44.94 43.90 2.3
AZ910 229.59 0.396 83.49 85.48 2.4 58.44 55.75 4.6
Cu alloy C1010 392.46 0.029 88.26 91.24 3.4 80.30 75.14 6.4
C5101 551.17 0.328 86.52 88.85 2.7 85.66 81.22 5.2
C62400 307.01 0.259 83.61 83.48 0.2 212.68 213.36 0.3
Ti alloy Ti–10V– 95.36 0.096 79.85 82.15 2.9 360.48 340.65 5.5
2Fe–3Al
Ti–7Al–4Mo 128.18 0.055 80.32 82.70 3.0 341.86 322.40 5.7
Ni alloy Inconel 600 443.53 0.265 83.54 85.86 2.8 228.10 215.96 5.3
Carbon steel S45C 584.15 0.258 90.71 88.67 2.2 181.61 190.06 4.7
SCM21 714.93 0.222 90.03 89.40 0.7 160.11 162.36 1.4
SCM4 324.59 0.130 83.78 83.81 0.0 285.95 285.78 0.1
SKD61 574.92 0.241 89.62 87.55 2.3 189.86 198.96 4.8
SKS3 481.92 0.218 89.78 88.38 1.6 182.22 188.03 3.2
SUJ2 536.61 0.240 88.71 87.43 1.4 195.36 201.12 2.9
API steel X100 350.84 0.141 87.85 85.30 2.9 240.19 254.77 6.1
X70 348.16 0.117 87.37 86.18 1.4 216.69 222.68 2.8
Ferrite base SUS303F 560.65 0.334 87.40 87.37 0.0 175.06 175.18 0.1
stainless steel
SUS310S 720.29 0.294 93.86 93.89 0.0 129.46 129.36 0.1
SUS316L 651.07 0.309 89.77 91.18 1.6 158.28 153.40 3.1
Austenite base SUS403 628.59 0.212 90.91 91.38 0.5 165.73 164.02 1.0
stainless steel
SUS410 585.36 0.179 90.26 90.31 0.1 166.53 166.37 0.1
SUS420J2 530.18 0.207 88.61 87.29 1.5 204.08 210.26 3.0

340 J. Mater. Res., Vol. 25, No. 2, Feb 2010

 S-K. Kang et al.: Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

the corner contact depths and Vickers hardnesses directly hmax/(hmax  hf) and found a linear relation for the
measured from the profile of residual indentation marks contact depth function at the corner; Fig. 5 shows the
and evaluated only from IIT parameters using Eqs. (6) relation as
and (12), respectively. The errors in contact depth and
hardness are below
4% and
7%, respectively. hmax
fpro ¼ 1:06  102 þ 1:00 : ð14Þ
True IIT hardness is given by the maximum applied hmax  hf
load divided by the projected area in the loaded state, Table II presents true IIT hardnesses directly
which can be work for elastoplastic deformation per measured from the profiles of residual indentation marks
unit volume and mean pressure. We directly compared and evaluated only from IIT parameters using Eq. (14).
the contact depth function for projected area fpro to These results imply that the true projected contact depth
in the loaded state and true IIT hardness can be measured
without additional observation of the residual impression
and material properties. Figure 6 shows the relationship
between two different contact areas:
 diagonal
 contact area
(Adia) and projected contact area Apro
c (see Fig. 7). Apro
c
is 2% greater than Ac :
dia

c ¼ 1:02 Ac
Apro : ð15Þ
dia

Thus, when considering pileup dependent on indenter

geometry as in Fig. 1, i.e., more pileup in the center and
minimum pileup at each Vickers indenter corner, this
result implies that the true contact area, which is the
projected area at contact depth taking into account aver-
FIG. 5. Linear relation of contact depth function for projected area age pileup along the contact morphology, is slightly
and normalized recovery depth. great than projected area at corner contact depth, hV
c.

TABLE II. Evaluation of projected contact depth and true IIT hardness using the contact depth function.

hpro
c Eq. (14) True IIT True IIT hardness
Materials hpro
c (mm) (mm) Error (%) hardness (GPa) Eq. (14) (GPa) Error (%)
Al alloy Al6061 88.63 88.40 0.3 1.14 1.15 0.5
Al7075 86.75 84.08 3.1 1.75 1.86 6.4
Mg alloy AZ61 83.49 87.01 4.2 0.50 0.46 7.9
AZ910 81.82 85.89 5.0 0.64 0.58 9.3
Cu alloy C1010 91.45 92.06 0.7 0.79 0.78 1.3
C5101 84.78 89.50 5.6 0.94 0.85 10.3
C62400 82.37 83.80 1.7 2.32 2.24 3.4
Ti alloy Ti–10V–2Fe–3Al 79.86 82.40 3.2 3.81 3.58 6.1
Ti–7Al–4Mo 80.43 82.99 3.2 3.60 3.38 6.1
Ni alloy Inconel600 84.10 86.36 2.7 2.38 2.26 5.2
Carbon steel S45C 91.49 89.34 2.3 1.89 1.98 4.9
SCM21 90.53 90.11 0.5 1.67 1.69 0.9
SCM4 85.21 84.18 1.2 2.92 2.99 2.5
SKD61 90.02 88.14 2.1 1.99 2.08 4.3
SKS3 90.02 89.03 1.1 1.92 1.96 2.2
SUJ2 88.57 88.02 0.6 2.07 2.10 1.3
API steel X100 90.02 85.76 4.7 2.42 2.66 10.2
X70 90.52 86.69 4.2 2.13 2.33 9.0
Ferrite base SUS303F 87.82 87.93 0.1 1.83 1.83 0.3
stainless steel
SUS310S 95.21 94.91 0.3 1.33 1.34 0.6
SUS316L 90.36 92.01 1.8 1.65 1.59 3.5
Austenite base SUS403 92.57 92.23 0.4 1.69 1.70 0.7
stainless steel
SUS410 91.98 91.08 1.0 1.70 1.73 2.0
SUS420J2 89.50 87.87 1.8 2.11 2.19 3.7

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 S-K. Kang et al.: Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

(4) The projected area Apro has a linear relationship

with the diagonal area Adia as in Eq. (15), suggesting that
the average pileup height is slightly greater than that at
the corners of the Vickers indenter.

ACKNOWLEDGMENTS
This research was supported in part by the Seoul
R&BD Program (Grant No. TR080564) of the Seoul
Development Institute, Korea, and in part by the
Improvement of Standardization Technology Program
(Grant No. B0010740) of the Ministry of Knowledge
Economy, Korea.

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