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AIM:

Measuring the amount of Acetic Acid in Vinegar


by titration with. Indicator Solution.
An Objective: The goals determine acid of this
Project is to amount of Acetic in different types of
vinegar Using titration with to determine a
Colored pH indicates the end point
Introduction –
About Vinegar: -
Vinegar is Fermentation which turn Sugan a
Solution of was made from that geoethane
CCH3CH2OH), Previously fermented from. The
fermentation. Results in the of Production acid
(CH₃ COOH). There different from a types or
ethanol of acetic many Vinegars, each Starting.
different original sugar Source’s, nice, wine, salt,
etc.] of acetic acid Vany typically vinegars but in a
• The amount vinegar Can between 4 to 6 four
table UP to (18) % four pickling vinegar. Three
times higher. titration introduction: In amount this
project, I have determined the of acid a titration in
different vinegars using Common technique
Chemistry Titration measure the unknown.
Chemical in adding with solution) with a way
amount of 90 40 a Solution (the titrant) by
measured amount of Chemical known
concentration (the titrating. The titrating Solution.
titration reacts and the end point of monitored in
the titration. from and Some way. The Can not the
amount of titrating the ratio of the in the chemical
equation the reaction is Concentration. be
Calculated Solution added, two
Chemicals for the reactants.
Titration theory:
To measure Solution the acidity of we
Can add water a vinegar. Enough
hydroxyl ion.to balance out the be added
hydrogen ion .from the enact acid with
the hydroxyl ion will hydrogen ion.to
Produce Water .In anden four a titration
to work, We need three things.
1. a fitenation solution Contains hydroxyl
ion with a Precisely known
Concentration).
2. a method foun delivering a precisely
measured volume of the titrating
Solution, last
3. a means of indicating, when the end
point has been reached. Fous the
titration solution, we'll use a dilute
Solution of Sodium hydroxide (NaOH).
Sodium. Hydroxide is a Strong base
which means that it dissociates almost
completely in waters four every NaOH
molecule that we add to the Solution, we
a hydroxyl ion. Can expect to Produce
Performing titration:
To dispense an of accurately measured
volume the titrating Solution, we brunette
with a makings Volume brunette A brunette is
a will use a long tube Valve at the bottom and
graduated on the out sides to measure the
Contained in the brunette is mounted on the
ring stand, directly above the titration
Solution. Solution in the pe the brunette
tends to creep up sides of the glass. Of the
liquid tension of liquid thus meniscus liquid
the at the Sunfire
• This is due to the surface water. The
surface of the Forms a Aneasune Curve, the
called volume of the brunette always creak
from the meniscus. To in the bottom or
Indicators: In this experiment indicators
Solution Phenolphthalein Solution is the
Solution is acidic we will use a called
phenolphthalein. Colorless when the neutral.
When come slightly basics, become Phenoph
tathale in lightly purple turns pinkish, and
then as the Solution become when the
vinegary Solution. Know that the basic.
So, Stants to turn pink, cue titration is
Complete.

Apparatus: To do these experiments. We will


need the Following materials and equipment.
Vinegar three different types.
• Distilled water. Small funnel.0.5%
1.Phenolphthalein solution in alcohol’s
indication
0.1m Sodium hydroxide solution
→ 125 mL Conical Flask 25 0r 50 ml burnet
the 10 ml graduated cylinder Ring Stand
→ Bourette clamp Theory: Required amount
of be calculated using Sodium hydroxide
(NaOH) can the following Formula Molality x
molar mass x volume 1000 Molar mass of
NaOH = 40 g /mol
The acetic acid content of a be determine by
titrating a vinegar may vinegar Sample with
a solution of Sodium hydroxide of known
molas concentration (molarity)
CH3COOH (aq) + NaOH (aq) → CH3COONa
H2O
acid + base→ water+salt
At the end point in the titration stoichiometry
between the both Solution lies at lol ratio
MCH3COOH X VCN2 COOH Strength of acid
in vinegar can be determined by the
following formula Strength of acetic acid
MCH3COOH X 60 Indication:
Phenolphthalein
End point: Colorless to pink.
Experimental Procedure
Pour 1.5 ml of vinegar in an Conical Flask
2. Add distilled So that the become 20 ml.
water to dissolve the vinegar. Volume of the
Solution
3. Add 3 drops of 0.54. Phenolphthalein
solution.
4. Use the burette clamp to attach the
brunette to the ring Stand The opening at the
bottom of the burette should be just above
the height For the of the Conical flask we use
vinegar and phenolphthalein Solution
5. Use an 0.01 m Funnel to fill the burette
with Solution of Sodium hydroxide.
6. Note the starting level of the Sodium
hydroxide Solution the burette Put the
vinegar Solution to be titrated under the
burette.
7. Slowly drip the solution of Sodium
hydroxide into the vinegar Solution. Swirl the
Flask gently.to mix the Solution while
keeping the opening under neath the burette
8. At Color Same in Point a We vinegar will
see a pink Solution when the Sodium
hydroxide is added, but the Color. will quickly
mixed clay disappear as the Solution is When
this happens show the burette to drop-by-
drop and addition
9. When the vinegar solution turns pink and
cremains that color. Even the titration is
complete the brute the with mixing, Close the
tap
10. Note the reading remaining level of the
Sodium hydroxide Solution in the butterine
ban the reading bottom to the meniscus 11.
Substrate the initial level from the remaining
titura ting level to figure out Solution
12. For each titration vinegar that at least we
test, repeat the three times. How much we
have used.
Experiment: 01
Take the B. laboratory vinegar in the Conical
Flask and do the titration with NaOH as.
mentioned.
Calculations We know that
MCH3COOH* VCH3COOH =MNaOH * V NAOH
MCH3COOH =
MCH3COOH
Strength acetic acid.
Experiment 02
Take a the house hold vinegar in the Conical
Flask and do the titration with NaOH as
mention Calculations:
We know that
MCH3COOH *VCH3COOH = MNaOH *VNaOH
MCH3COOH = MNaOH* VNaOH /VCH3COOH
Strength of acetic acid.
Experiment 03.
take the wine vinegar in the conical flask
and do the titration with NaOH as mentioned.
Canulations:
We know that
MCH3COOH* VCH3COOH = MNaOH * VNaOH
MCH3COOH= MNaOH * VNaOH/ VCH3COOH

Strength of acetic acid=

Topic:
Result:

→Strength of acetic acid in laboratory


vinegar =

→Strength of acetic acid in house hold


vinegar =

Strength of acetic acid in wine vinegar =


graphically plotting various vinegar Samples
in accordance with the amount of acetic acid
Present in them we present a Stunning Order
amount of acetic acid in vinegar is
Wine Vinegar > House hold Vinegars >
Laboratory Vinegar
Precautions:
• Transiting of measured vinegar into a
measuring Flask Should be done very
Carefully.
• Measuring must be Performed care fully
• look at the meniscus of Solution at eye level
to avoid Parallax
• Look at the lowest meniscus in the light-
Colored Solution and uppers meniscus in the
dank Colored Solution because of visibility.
• Do not forget to add distilled water to the
vinegar.

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