Department of Chemical Engineering

Semester III Examination Scheme

Practicals

Contact H.

Credits

Units

Examination H.

Theory

Practicals
and
Sessionals

Total

1
1
1

2
3
5
5

2
3
5
5

0.5
0.5
1.0
1.0

3
3
3
3

50
50
100
100

50
50
100
100

4
16

1
4

5
20

5
20

1.0
4.0

3
-

100
400

100
400

3
3
3
3

3
3
3
3

1.5
1.5
1.5
1.5

0.5
0.5
0.5
0.5

3
3
3
3

50
50
50
50

50
50
50
50

12 12
6
16 4
12 32
26
Grand Total (A+B)
Joint award for III and IV Semester (Marks not counted for award of division)
FE
225 B *Co-curricular Activities
1
1
2
1

2.0
6.0

400

200
200

200
600

0.5

Subject Code

2
2
4
4

Branch Code

Tutorials

Marks

Lectures

BE II year (CHEMICAL), 2014

Ma
ChE
ChE
ChE

201
202
203
204

ChE

205

ChE
ChE
ChE
ChE

221
222
223
224

Subject

A
A
A
A
A

Written Papers

Mathematics-I (ChE)
Computer Programming (ChE)
Fluid Flow Operation (ChE)
Chemical
Engineering
Thermodynamics (ChE)
A Heat Transfer Operation-I (ChE)
Total (A)
B Practicals and Sessionals
B Computer Lab. (ChE)
B Fluid Flow Operation Lab.(ChE)
B Heat Transfer Operation-I Lab. (ChE)
B Chemical Process Calculations
Lab. (ChE)
Total (B)

For pass candidate must obtain:

a) 35 percent in each written paper.
b) 50 percent in each of the practicals and Sessionals, and
c) 45 percent grant total.

Department of Chemical Engineering

ChE
ChE
ChE
ChE

Units

Examination H.

Theory

Practicals
and
Sessionals

Total

Heat Transfer Operation-II (ChE)

Material Science (ChE)
Process Instrumentation and Control (ChE)
Total (A)
Practicals and Sessionals
Chemical Analysis Lab. (ChE)

1
1
2
1
5

Credits

Computer Oriented Numerical Analysis (ChE)

2
3
2
3
3
2
15

Contact H.

271
272
273
274

B
B
B
B
B

Written Papers
Mathematics-II (ChE)
Elements of Equipment Design (ChE)

2
4
3
5
3
3
20

2.0
4.0
3.0
5.0
3.0
3.0
20.0

0.5
1.0
0.5
1.0
0.5
0.5
4.0

3
3
3
3
3
3
-

50
100
50
100
50
50
400

50
100
50
100
50
50
400

3
3
3
3
Heat Transfer Operation-II Lab (ChE)
3
3
Process Instrumentation Control Lab (ChE) 3
3
Total (B)
12 12
15 5 12 32
Grand Total (A+B)
Joint award for III and IV Semester (Marks not counted for award of division)
FE
275 B *Co-curricular Activities
1 1 2
Computer Oriented Numerical Analysis Lab (ChE)

For pass candidate must obtain:

Marks

Practicals

251
252
253
254
255
256

A
A
A
A
A
A
A

Tutorials

Subject

Semester IV Examination Scheme

Lectures

Ma
ChE
ChE
ChE
ChE
ChE

Subject Code

Branch C-ode

BE II year (CHEMICAL), 2014

1.5
1.5
1.5
1.5
6.0
26.0

0.5
0.5
0.5
0.5
2.0
6.0

3
3
3
3
-

400

50
50
50
50
200
200

50
50
50
50
200
600

0.5

100

100

a)
b)
c)

35 percent in each written paper

50 percent in each of the Practicals and Sessionals, and
45 percent grant total.

Department of Chemical Engineering

BE III year (CHEMICAL), 2015

Semester V Examination Scheme

Mass Transfer Operation-I (ChE)

Process Dynamics and Control (ChE)

Chemical Process Economics (ChE)

Total (A)

2
4
5
5
3
2
21

2.0
4.0
5.0
5.0
3.0
2.0
21.0

0.5
0.5
1.0
1.0
0.5
0.5
4.0

B Practicals and Sessionals

B Fluid Particle Dynamics Lab. (ChE)
3
3
B Chemical Reaction Engineering-I
3
3
Lab. (ChE)
ChE 323 B Mass Transfer Operation-I Lab. (ChE)
3
3
ChE 324 B Process Dynamics and Control Lab (ChE).
3
3
Total (B)
12
12
Grand Total (A+B)
15
6
12
33
Joint award for V and VI Semester (Marks not counted for award of division)
ChE 321
ChE 322

Total

Practicals
and
Sessionals

1
2
2
1
6

Theory

2
3
3
3
2
2
15

Examination
H.

Units

Chemical Reaction Engineering-I (ChE)

Credits

Written Papers
Chemical Technology-I (ChE)
Fluid Particle Dynamics (ChE)

Contact H.

A
A
A
A
A
A
A

Practicals

301
302
303
304
305
306

Tutorials

Subject
Code

ChE
ChE
ChE
ChE
ChE
ChE

Subject

Lectures

Branch Code

Marks

3
3
3
3
3
3
-

50
50
100
100
50
50
400

50
50
100
100
50
50
400

1.5

0.5

50

50

1.5

0.5

50

50

1.5
1.5
6.0
27

0.5
0.5
2.0
6.0

3
3
-

400

50
50
200
200

50
50
200
600

FE

325

*Co-curricular Activities

0.5

For

pass candidate must obtain:

a) 35 percent in each written paper
b) 50percent in each of the practicals and Sessionals, and
c) 45 percent grant total.

Department of Chemical Engineering

Examination H.

Theory

Practicals
and
Sessionals

Total

351
352
353
354
355

Units

Contact H.

Written Papers
Chemical Reaction Engineering-II (ChE) 3
1 4
Mass Transfer Operation-II (ChE)
3
1 4
Chemical Equipment Design (ChE)
3
1 4
Chemical Technology-II (ChE)
3
1 4
Industrial Management (ChE)
2
1 3
Total (A)
14 5 19
B Practicals and Sessionals
ChE 371 B Mass Transfer Operation-II Lab. (ChE)
- 3
3
ChE 372 B Chemical Equipment Design Lab. (ChE) - 3
3
ChE 373 B Chemical Reaction Engineering- II Lab. - 3
3
(ChE)
Total (B)
- 9
9
ChE 374 C Seminar (ChE)
- 4
4
Total (C)
- 4
4
14 5 13
32
Grand Total (A+B+C)
Joint award for V and VI Semester (Marks not counted for award of division)
ChE
ChE
ChE
ChE
ChE

Marks

Credits

A
A
A
A
A
A

Practicals

Subject

Tutorials

Semester VI Examination Scheme

Lectures

Subject Code

Branch Code

BE III year (CHEMICAL), 2015

4.0
4.0
4.0
4.0
3.0
19.0

1.0
1.0
0.5
0.5
0.5
3.5

3
3
3
3
3
-

100
100
50
50
50
350

100
100
50
50
50
350

1.5
1.5
1.5

0.5
0.5
0.5

3
3
3

50
50
50

50
50
50

4.5
2.0
2.0
25.5

1.5
1.0
1.0
6.0

350

150
100
100
250

150
100
100
600

F FE 375 B *Co-curricular Activities

o
r pass candidate must obtain:
a) 35 percent in each written paper
b) 50 percent in each of the practicals and Sessionals, and
c) 45 percent grant total.

0.5

100

100

Department of Chemical Engineering

BE IV year (CHEMICAL), 2016

Semester VII Examination Scheme

Total

C
C

Practicals
and
Sessionals

ChE 423

Theory

B
B
B

Examination H.

ChE 421
ChE 422

Units

A
A

Credits

ChE 404
ChE 405

Contact H.

A
A
A

Practicals

A
ChE 401
ChE 402
ChE 403

Tutorials

Subject

Lectures

Subject Code

Branch Code

Marks

3
3
4

1
1
1

4
4
5

4.0
4.0
5.0

0.5
0.5
1.0

3
3
3

50
50
100

50
50
100

3
3
16

1
4

4
3
20

4.0
3.0
20.0

0.5
0.5
3.0

3
3
-

50
50
300

50
50
300

4
4
8

4
4
8

2.0
2.0
4.0

1.0
1.0
2.0

3
3
-

100
100
200

100
100
200

16

4
4
12

4
4
32

2.0
2.0
26.0

1.0
1.0
6.0

3
3
-

300

100
300

100
100
600

0.5

Written Papers
Safety in Chemical Process Plants (ChE)

Molecular Biology (ChE)

Mathematical Methods In Chemical
Engineering (ChE)
Petroleum Refining (ChE)
Elective-I (ChE)
Total (A)
Practicals and Sessionals
Chemical Technology Lab. (ChE)
Petroleum Analysis Lab. (ChE)
Total (B)
Project
Project (ChE)
Total (C)
Grand Total (A+B+C)

Joint award for VII and VIII Semester (Marks not counted for award of division)
FE
424 B
*Co-curricular Activities
1
1
2
1

For pass candidate must obtain:

a) 35 percent in each written paper
b) 50 percent in each of the practicals and Sessionals, and
c) 45 percent grant total

Department of Chemical Engineering

BE IV year (CHEMICAL), 2016

Semester VIII Examination Scheme

Total

Simulation Lab (ChE)

Total (B)
Practical Training and Tour
Industrial Tour (ChE)
Practical Training (ChE)
Total (C)

Practicals
and
Sessionals

Environmental Engineering Lab. (ChE)

Theory

C
C
C

Polymer Science Lab. (ChE)

Examination
H.

ChE 474
ChE 475

Elective-II (ChE)
Elective-III (ChE)
Total (A)

Units

Practicals and Sessionals

ChE 471
ChE 472
ChE 473

B
B
B
B

Chemical Engineering Optimization (ChE)

Credits

Written Papers
Bio Chemical Engineering (ChE)
Transport Phenomena(ChE)

Contact H.

A
A
A
A
A
A

Practicals

451
452
453
454
455

Tutorials

Subject Code

ChE
ChE
ChE
ChE
ChE

Subject

Lectures

Branch Code

Marks

3
3
3
3
3
15

1
1
1
1
4

3
4
4
4
4
19

3.0
4.0
4.0
4.0
4.0
19.0

0.5
0.5
0.5
0.5
0.5
2.5

3
3
3
3
3
-

50
50
50
50
50
250

50
50
50
50
50
250

3
3
3
9

3
3
3
9

1.5
1.5
1.5
4.5

0.5
0.5
0.5
1.5

3
3
3
-

50
50
50
150

50
50
50
150

1.5
1.5

0.25
0.75
1.0

25
75
100

25
75
100

F
D
Project (D)
o ChE 476 D
Project (ChE)
4
4
2.0
r
Total (D)
4
4
2.0
p
Grand Total (A+B+C+D)
14
4
13
32
27.0
a Joint award for VII and VIII Semester (Marks not counted for award of division)
s FE
*Co-curricular Activities
477 B
1
1
2
1
s
candidate must obtain:
a) 35 percent in each written paper
b) 50 percent in each of the practicals and Sessionals, and
c) 45 percent grant total

1.0
1.0
6.0

0.5

250
-

100
100
350

100
100
600

100

100

MA 201 A: MATHEMATICS-I
2 L, 0 T

Max. Marks 50

Differential equations and their application: Linear Differential equations of second order including variation of parameters, Simultaneous
Differential Equations.
Bessels & Legendres equation: Bessels function of first kind (Definition of Jn (X), general solution, generating function, Recurrence formulae),
Legendres Polynomials, Legendres function of first kind (Definition of Pn (X) & Qn (X), general solution, generating function, Orthogonality of
Pn (X), Recurrence formulae.
Partial differential equations: First order by Lagranges method, Partial Differential Equations of second order by Separation of variables.
One-dimensional heat & wave equations, Laplace equation in two dimensions.

2 L, 1 T

ChE 202 A: COMPUTER PROGRAMMING

Max. Marks 50

A Review of C. concept of object oriented programming using C++, data types: Elementary and drive data types, literals.
Operators and expression: operators, association and precedence rules of operators, expressions using unary, binary and ternary operators.
Conditional statement if. If else and switch. Loop: for, while and do while, break, continue, go to statements.
Function: void functions, function with return value, call by value, call by reference parameter passing, default parameters, recursive functions,
inline functions and return statements.
Classes: classes, objects, friends functions, classes within classes, constructor and destructors.
Derived classes: Single and multiple derivations of classes, types of inheritance, constructor, and destructors with inheritance classes.
Polymorphism: function and operator overloading, virtual functions.
Stream: input and output of build- in- data types, manipulators.

4 L, 1 T

ChE 203 A: FLUID FLOW OPERATIONS

Max. Marks 100

Basic principles: Units and dimensions, Properties of fluid, Classification of fluids (Newtonian and Non-Newtonian fluid, Compressible and
Incompressible fluids).
Fluid static: Fluid pressure & its measurement, Piezometers, Forces acting on immersed surfaces (Plane & Curved), Pressure diagrams.

Fluid dynamics: Laminar and turbulent flows, Conservation of mass, Continuity equation, Conservation of momentum and energy, Navierstokes
equation and its applications, Mechanical energy balance and Bernoullis equation and its applications, Orifice meter and Venturi meter, impulse
momentum equation and its application.
Dimensional analysis: Pi theorem, Dimensionless numbers and their physical significance, Similitude criterion. Introduction to boundary layer
theory: Velocity distribution, Boundary layer calculations, and Boundary layer thickness.
Flow through orifices and mouthpieces: Classification of orifices and mouthpieces, Determination of the coefficient for an orifices, Energy and head
losses of flowing liquid due to sudden changes in velocity.
Pipe Network: Specifications of standard pipes and tubes; Economic pipe diameter, Pipe fitting and valves, flow through pipes, Pressure drop,
Friction factor, Darcy-Weishbach equation, Hydraulic Gradient Line (HGL) and Total Energy Line (TEL), Pressure drop in pipe network system,
Hardy-Cross method.
Flow of compressible fluids: Isentropic expansion, Adiabatic, and Isothermal frictional flow.
Pumps, Blowers, and Compressors: Their types and basic working characteristics, their selection criteria, Cavitations, Net Positive Suction Head
(NPSH).

ChE 204 A: CHEMICAL ENGINEERING THERMODYNAMICS

4L, 1 T
Max. Marks 100
Basic concepts: Review of laws of thermodynamics and their application to engineering process, Closed and Open system, Thermodynamics
analysis chemical process. Thermodynamic properties of fluids and their inter-relationships: PVT behavior of pure substance, Viral and Cubic
equation, Equation of state, generalized correlations and acentric factor, PVT behavior of mixture, Entropy, Gibbs energy and its role as generating
function, Helmoltz Energy, Residual properties, Properties of single and two-phase systems, Relationship among thermodynamic properties.
Refrigeration cycles: Vapour absorption and Compression cycles, selection of refrigerants. Multicomponent systems: Partial molar properties,
chemical potential, Gibbs-Duhem equation, Ideal non-ideal solutions. Raoultss & Henerys laws, Fugacity and fugacity coefficient. Excess
properties of mixtures, Activity and activity coefficients, Gaseous mixtures and fundamental property relation. Phase equilibrium and stability:
General criteria for equilibrium, phase equilibrium, phase rule and its derivation, vapour liquid equilibrium (VLE), Azeatropes, Liquid- Liquid
equilibrium (LLE), and vapour- solid phase equilibrium and solid- liquid equilibrium (SLE)) (only general types, characteristics and qualitative
behavior of these equilibrium systems). Chemical reaction equilibrium: Reaction coordinate, Evaluation of equilibrium constants and effect of
temperature on them, Standard Gibbs free energy change, calculation of equilibrium conversion for single and multi-reaction systems, phase rule
and Duhem equation for reacting systems.

ChE 205 A: HEAT- TRANSFER OPERATIONS- I

4 L, 1 T

Max. Marks 100

Mechanism of heat transfer: Heat transfer rate, Flux, Coefficient and Resistance.
Thermal conductivity: Fouriers law, Conduction through flat and cylindrical walls, Spherical objects and finned surfaces, Composite walls, Heat
losses and insulation. Application of energy equation one dimension and two dimensions (series solution) steady and unsteady state conduction,
Solution of partial differential equation using numerical techniques.
Natural and forced convection: Film coefficient; Heat transfer between solid and fluids, Dimensionless analysis, laminar and turbulent flows through
pipes.
Heat transfer with phase change: Film wise and Drop wise condensation- Film wise condensation on vertical and inclined plate, Equations for
horizontal and vertical tubes, Calculations for condensers.
Radiant energy Distribution, Emissive power, Plancks law, Weins displacement law, Stephen-Boltzman law, Black body, Kirchoffs law, Gray
body, Exchange of energy between two surfaces-Large plates, Infinites cylinders, Geometric factors, Gas radiation.
Heat transfer in reactive system- Endothermic reaction, Exothermic reaction, Heat transfer in catalytic bed reactor.

Ma 251 A: MATHEMATICS II
2 L, 0 T

Max. Marks 50

Complex Variables: Basic concepts (Polar form, Powers and Roots, limit, Derivatives, etc.), Singular points, Residue theorem, Calculus of residues,
Evaluation of real-integrals, Bromwich contour integral (General Idea).
Probability and Statistics: Concept of probability, mean and variance, linear regression analysis.
Integral transforms and their applications: Laplace and Fourier transforms, Inverse transforms, Convolution, and Application to Ordinary and Partial
differential equations, Initial and Boundary value problems by operational method.

ChE 252 A: ELEMENTS OF EQUIPMENT DESIGN

3 L, 1 T
Max. Marks 100
Solid friction, a law of friction, inclined plane screw jack, friction of plate collars and clutches.
Mechanical advantages, velocity ratio and efficiency, study of simple machines. Transmission of power by bells and ropes, length of belts, tension
in belts, centrifugal tension, maximum power transmitted by belts.
Mechanics of Materials: Stress and strain-Hooks law, tension, compression, and shear, complimentary shear stress, Poisons ratio, elastic constants
and their relation for an isotropic material. Temperature stresses and composite bars, elastic and plastic behavior of structural steel in tensile and
compression tests. Principal planes, stresses and strains. Bending moment and shearing force diagrams under static loads, concentrated uniformly
distributed and uniformly varying loads on cantilever, simply supported and overhanging beams. Theory of simple bending, distribution of normal
stress due to bending, section modulus. Torsion: shear stress in solid and hollow circular shafts, angle of twist, power transmitted by shaft under
pure torsion. Combined bending and torsion.
Theories of columns, Thermal stress, Membrane stresses in shells of revolutions, Stress concentration, Theories of failures.
General Design Consideration: Design code, Design pressure, Design temperature of cylindrical and spherical shells under internal and external
pressures, Selection and design of flat plate, Spherical, Ellipsoidal conical closures.
Tall vertical vessels: Pressure, Dead weight, Wind, Earthquake and Eccentric loads and induced stresses, Combined stresses.

ChE 253 A: COMPUTER ORIENTED AND NUMERICAL ANALYSIS

2 L, 1 T

Max. Marks 50

Numerical solution of Linear Equations: Roots of Equations, Newton-Raphson method, False Position method, Bisection method, and Secant
method.
System of Linear Equations: Solutions of simultaneous equations by Gaussian-elimination, Gauss-Jordan and Gauss-Seidal method.
Interpolation: Lagranges interpolation, Newtons Forward and Backward interpolation, Difference tables.
Curve Fitting: Least square method (Polynomial, Trigonometric & Exponential).
Numerical Integration: Simpsons 1/3 rule, Trapezoidal method, Gauss Quadrature method. Numerical Differentiation
Ordinary Differential Equation: Eulers, Runge Kutta second and fourth order, Predictorcorrector method, Finite-difference method.
Classification of Partial Differential Equations: Elliptical equation, 2D Laplaces equation for steady state problems (Only general Introduction).
Characteristic Equations: Estimation of Eigen values and Eigen Vectors of matrices (Only general Introduction). Programming approach (C++
programming)

ChE 254 A: HEAT TRANSFER OPERATIONS II

3L, 2 T
Max. Marks 100
Heat exchangers: Types of Heat Exchangers, Double-pipe Heat Exchanger- Parallel and counter-current flows, Shell and Tube Heat exchangers,
LMTD, Equivalent diameter; NTU and Effectiveness, Fouling factors, Cross flow heat exchangers and its application.
Design of Shell - Tube Heat Exchangers: Calculation of heat transfer coefficient and pressure drop.
Condensation of single vapors system and type of condenser.
Vaporizers, Evaporators and Reboilers: Forced and Natural circulation vaporizers (Kettle Reboiler), Reboilers arrangements, Heat flux and
temperature difference, Single and multi-effect evaporators, BPR, Forward and Backward feeds, Calculations for chemical evaporators, Optimum
numbers of effects. Batch and unsteady state heating arrangements in jacketed and agitated vessels.

ChE 255 A: MATERIAL SCIENCE

3 L, 0 T

Max. Marks 50

Mechanical, thermal, electrical, chemical, and optical properties of materials and their measurements (General Overview and introduction to
common terms).
Atomic structure: Inter automatic attraction, Atomic co-ordination, Molecular structure, Crystalline and non-crystalline structure, Solid solutions,
Crystal imperfections (point, line and interfacial and bulk defects), Atom movement.
Mechanical Properties: Elastic deformation, Plastic deformation, tensile properties, Stress-Strain relationship, compressive, shear and torsional
deformation, Creep, hardness.

Dislocation and Strengthening: Dislocation, Slip system, Twinning, Grain-size reduction, Solid Solution strengthening, Strain Hardening, recovery,
recrystallization, grain growth.
Phase Diagrams: Fe-C diagrams, Nomenclature for steels.
Polymorphic phase transformations: Metastable phases, Micro structural and property changes in Fe-C alloys, Isothermal transformation,
Continuous cooling transformations, Tampered Martensite.
Thermal Processing: Annealing, Age hardening, Surface Hardening, Quenching and hardening.
Common engineering materials: Iron, Carbon and low alloy steels, S.S. and special steels, C.I, non-ferrous metal and alloys.
Stability in service conditions: corrosion, Oxidation, Thermal stability and radiation damage

ChE 256 A: PROCESS INSTRUMENTATION & CONTROL

2L,1T
Max. Marks 50
Introduction to process variables: Direct and Inferential measurement, On and off line measurement, Static and Dynamic characteristics of
instruments and their general classification, Error, Accuracy, Repeatability, Drift, Threshold, Zero-stability etc., Interpretation of performance
specification of transducers.
Working principle of instruments: Classification of sensors and transducers based on their principles of measurement, Building block of an
instrument- Transducer, Amplifier, Signal conditioner, Signal transmitter, Data acquisition, I/O devices (general working principle only).
Instrumentation Systems: Working principle of transducers/instruments employed for the measurement of Flow, Level, Pressure, Temperature,
Density, Viscosity, pH, Radiation, Composition, Humidity, Advantages and Disadvantages, Preparation of instrumentation diagrams,
Instrumentation of important equipments like Distillation column, Heat exchanger, etc.
Construction and characteristics of final control elements: Introduction to Pneumatic, Hydraulic and Electronic controllers, Pneumatic control
valves, Characteristics and sizing, motorized valve etc.
Signal transmission and Telemetry: Sampling, Multiplexing, Modulation and Demodulation, Basic principle of DAC and ADC, Pneumatic and
Electronic Transmitter and their Advantages and Disadvantages.

2 L, 0 T

ChE- 301A CHEMICAL TECHNOLOGY-I

Max. Marks 50

Indian Chemical Industry: An Overview

High temperature processes: Manufacture of Cement, Glass.
Chlor alkali industries.
Oil, fats, and Waxes: Vegetable oils, Animal fats and oils, Waxes.
Soaps and Detergent.
Sugar and Starch.
Paper and Pulp Industries: Different pulping processes.

3 L, 1 T

ChE- 302A FLUID PARTICLE DYNAMICS

Max. Marks 50

Flow through bed: Free and hindered settling, Flows through immersed bodies, and Flow through porous media.
Fluidization: Importance of fluidization in process industry, bubbles behavior and bed properties, Entrainment and elutriation from fluidized bed,
two phase-fluidized bed.
Filtration: Constant pressure and Constant rate filtration, Compressible cakes, Filtration rate calculation.
Particle size and shape: Measurement and analysis, Screening and screen analysis- Screen effectiveness, Working principle of industrial screening
equipments, Shape factor, Selectivity index.
Size reduction: Principal of comminution, Crushing, Grinding, Pulverization, Ultra fine grinding, Grindability, Crushing laws.
Solid handling: Storage of solids, Transport of solid Screw and belt conveyors, Pneumatic transport, Hydraulic transport and different agitators.
Filtration: Type of Rotary vacuum filter, Filter press, working principles of cyclone separator, Gravity separators, Centrifugation, Bag filters, Electro
static precipitators, Froth flotation processes.
Agitators: Types and basic principles, power calculations.

ChE 303 A: CHEMICAL REACTION ENGINEERING-I

3 L, 2T
Max. Marks 100

Introduction: Reaction rate, Type of reactions, Homogenous, and Heterogeneous reactions.

Kinetics of Homogenous Reaction: Simple reversible and irreversible reaction, Single and parallel reactions, Effects of concentration and
temperature on reaction rate, Arrhenius equations, Transition- state and collision theory.
Interpretation of Reactor Data: Data procurement and analysis, Constant volume and Varying volume Batch Reactor, Integral, and differential
methods of analysis for various types of reactions.
Designs fundamentals and behavior of Isothermal reactor: Performance equation for Ideal Batch Reactor, Space Time and Space Velocity,
Performance equation for Mixed flow reactor and Plug flow reactor, Size comparison for single reaction, Multiple reactors, Mixed flow reactors in
series, Recycle Reactors, Auto catalytic reactions, Design for parallel reactions, Multiple reactions in series and series-parallel combinations
reactions, fractional yield.
Temperature and Pressure Effects: Single and multiple reactions.

3 L, 2 T

ChE 304 A: MASS TRANSFER OPERATION-I

Max. Marks 100

Physico-Chemical basis of separation processes, Thermodynamic consideration, Stage, and Continuous contacting operation, Concept of
equilibrium states. Molecular diffusion in gases and liquids, Ficks first and second law, Mass transfer coefficient. Heat, Mass, and Momentumtransfer analogies. Film, Penetration, Surface- Renewal, Surface-Stretch Theories.
Diffusion in solids: Ficks law of solid diffusion, Types of solid diffusion.
Theory of interphase mass transfer: Individual and overall mass transfer coefficients, Steady-state co-current and counter-current process, Operating
curve, Stages and stage efficiency, Murphee efficiency.
Gas Absorption: Equilibrium solubility of gases in liquids, One component transferred material balance, Calculation of operating lines, Counter
current multistage operation, HETP dilute solution, HTU, NTU.
Distillation: Vapor-Liquid Equilibrium, Enthalpy-concentration diagrams, Differational and Extractive distillation, fractionating column, Plate and
packed column, McCabe Thile and Ponchon Savarite distillation methods, Principle of Azeotropic and extractive distillation, Multi-component
vapour liquid equilibrium, total, optimum reflux ratio and minimum reflux.
Drying: Equilibrium curve, Through Circulation and Cross circulation drying, Drying rate, Dryers and their selection.

ChE305 A: PROCESS DYNAMICS AND CONTROL

2 L, 1 T
Max. Marks 50
Laplace Transformation: Introduction, Properties of transform (Initial and Final value theorem).
Response of system: Dynamics of first, second and higher order linear, open loop and close loop system, Characteristic equation, Stability, Bode
diagram and Root locus diagram, Mode of control actions for negative feed back systems, Frequency response of system, Bode stability criterion,
Nyquist stability criterion, Design of controller, Dynamics of some complex processes, Control valves.

2 L, 0 T

ChE 306 A: CHEMICAL PROCESS ECONOMICS

Max. Marks 50

Economics of Chemical Industries in India- Demand: meaning and definition, elements, types. Law of Demand: explanation and assumptions.
Demand curve: cause of application and exceptions. Difference between want and demand, expansion and contraction of demand, increase and
decrease of demand. Factors affecting demand. Elasticity of demand: concept, type and method of measurement, determinants and its importance.
Cost estimation- elements of cost, components of cost, indirect expenses. Depreciation: its types and various method of calculating it. Obsolence,
Interest on capital, Idleness, Repairs and Maintenance. Profitability.
Economic evaluation of plant- Break-even analysis: assumptions. Break-even point theory: application. Non-linear break-even analysis.
Investment analysis- Time value of money, Interest rate, compound value, present value, annuities. Payback method, ARR, NPV, IRR. Cash flow
statement, Discounting.
Industrial financing- Sources of Business Finance: Nature and significance, types, classification. Shares: types, merits, and demerits. Debentures:
merits and demerits. Internal financing: loan financing, types, merits, and demerits. Specialized financial institutions.

ChE 351A: CHEMICAL REACTION ENGINEERING-II

3 L, 1 T
Max. Marks 100
Non ideal flow: Basic concepts of non-ideal flow, Exit age distribution of the fluid, conversion in the non-ideal reactors, Dispersion Model,
Residence Time Distribution (RTD), Chemical conversion, The conversion model and its RTD.
Introduction of Heterogeneous Reactions,
Heterogeneous Catalysis: Characteristics, Adsorption, Adsorption Isotherm, Properties, Classification, and Preparation.
Solid catalyzed reaction: Rate controlling steps, Rate equation for surface kinetic, Pore diffusion control, Porous catalyst particles, Experimental
methods for finding rates.
Transport Processes: External and Internal Transport process, Operating condition, Effectiveness factor, Effect on selectivity.
Catalyst Deactivation: Mechanism and Kinetics
Fluid particle reactions: Models, Determination for the rate-controlling step, Type of contacting.
Fluid-Fluid reactions: Kinetic and Rate expression.

3 L, 1 T

ChE 352A: MASS TRANSFER OPERATION-II

Max. Marks 100

Humidification: Vapor-Liquid Equilibrium, Vapor Gas Mixtures, Humidity charts and Calculations for humidification and dehumidification
processes (adiabatic).
Equipment for gas-liquid operations: Sparged vessels, Mechanical agitated vessels, Tray Towers, Wetted-Wall Towers, Scrubbers, Spray Towers,
Packed columns. Adsorption: Adsorption equilibrium, stage wise and Continuous adsorption, Industrial absorbers, Elution, Ion exchange.
Leaching: Principle of leaching, Batch and semi batch condition leaching, Retention of liquids after drainage, Calculation of stage in a sequence
with or without reflux.
Liquid-Liquid Extraction: Ternary Liquid-Liquid Extraction, Batch and continuous liquid-liquid extraction, Design of extraction column, Stage
calculations, Extraction with intermediate feed and Reflux, Selectivity, Rate of extraction system with complete immiscibility.
Crystallization: Equilibrium and yield, Factors governing nucleation and crystal growth rates, Controlled growth of crystal, Industrial Crystallizer.
Membrane separation: Thermodynamics basic of separation, Minimum work for separation, Types of barriers and estimation of separation factors.

ChE 353A: CHEMICAL EQUIPMENT DESIGN

3 L, 1T

Max. Marks 50

Vessel Supports: Design of skirt, lug and saddle supports. Design shell of supported vessel.
Liquid Storage Tanks: Classification, Storage tank codes, Design of shell, Bottom plates, Self-supported, and Column-supported roofs, Wind grinder,
Nozzles.
High-pressure vessels: Stress analysis of thick walled cylindrical shell, Design of monoblock.
Flanges: Types of flanges and their selection, Gaskets.
Detailed process and mechanical design: Fixed and floating head shell and tube heat exchangers, Single and multiple effect evaporators, Plate and
packed columns for distillation and absorption, Flash drum, Condenser cooling tower, Rotary drier, Fixed bed adsorption column, Cyclonic separator,
Packed and fluidized bed reactors, Crystallizer, Setting tank, Piping network

3 L, 1 T

ChE 354A: CHEMICAL TECHNOLOGY II

Max. Marks 50

Indian Chemical Industry: An overview.

Sulfur and Sulfuric acid: Production of sulfur pyrites and their use in production of sulfuric acid, DOSA and DCDA processes.
Nitrogen fertilizer and other chemical: Ammonia, Urea, and Calcium ammonium Nitrate etc. Nitric acid, Phosphatic mixed compound and other
fertilizer- SSP, TSP, NPK, UAP, DAP and Nitro phosphates, Bio-fertilizers, Phosphoric acid.
Common Salts, KCl.
Unit Process- Alkylation, Carboxylation and Acetylation, Nitration, Dehydration, Halogenations, Sulphonation, Oxidation, Ammoxidation.

2 L, 1T

ChE 355A: INDUSTRIAL MANAGEMENT

Max. Marks 50

Management and Engineering and their relation with other fields- Taylors scientific management, Fayols Principal of scientific management. Forms
of industrial enterprise: sole propertership. Partnership firms: characteristic, kinds, essentials, advantages and disadvantages. Differences between
sole propertership, Partnership, JHF and Co-ownership. Partners: types, rights, duties and liabilities. Companies: characteristics, kinds, difference
with partnership, difference between private and public companies, advantages and disadvantages.

Organization structure- role and features, organization chart and manual, their uses and limitation. Departmentation: Need and importance. Span of
management and factors affecting it. Delegation of authority and measures for effective delegation. Centralization and decentralization. Delegation
and Decentralization. Factors determining degree of decentralization. Rationale centralization and decentralization.
Personnel Management- Manpower planning and Job analysis.
Production Management- Meaning and scope. Production planning: meaning, objectives, scope, and production planning as an integral part of
cooperative planning process. Production control: meaning and importance. Quality control and SQC: meaning, importance, objective and
techniques. Work study and Productivity. Motion study: aims and procedure, micro motion study and motion economy. Time study: use and
procedure, performance rating and allowances.
Project Management: PERT and CPM techniques, Game theory.

ChE 401A: SAFETY IN CHEMICAL PROCESS PLANTS

3L, 1 T
Max. Marks 100
Introduction: Safety, hazard and Risk, accident- nature and loss statistic.
Hazards: Detection, Management, Recent trends in safety & hazard analysis, hazardous waste treatment, laws, codes and standards and case
histories & judgments.
Industrial Hygiene: Identification and evaluation .
Source Models: Introduction, spills of toxic, flammable and explosive materials, various source models.
Fires and Explosions: Distinction, definitions, characteristics and explosion hazard rating of process plant, Preventions of fire and explosions.
Hazards Identification: Checklists, surveys, HAZOP and HAZAN.
Risk Assessment: Probability Theory and failure frequency analysis.
Case studies

3 L, 0 T

ChE 402A: MOLECULAR BIOLOGY

Max. Marks 50

Introduction: Living systems and their properties, Measure biological compounds, Physiological processes, Introduction to environment, Evolution,
Ecology, Biogeography regions.
Biomolecules: Chemistry and function of the constituents of cells- water, Salts, Amino acids, Proteins and its synthesis, nucleic acids, Metabolism
of carbohydrates, Lipids, Introduction to enzymes and their action, Hormones.
Cell biology: Prokaryotic and Eukaryotic cells, Organization of plant and animal cells, Organelles- structure, Chemical composition, function.
Cellular processes and information transfer: Carbon and Nitrogen cycles in nature, Glycolysis, TCA cycle, Signal transduction, Receptor concept.
Genetics: Facts and theories of heredity, Elements of population genetics and species concept, Mendel's laws-segregation, independent assortment,
Phenotype and Genotype, Mono- and di- hybrid crosses, Chromosomes, Gene concept, DNAProtein interactions, Central Dogma-DNA
Replication, RNA Transcription and its control, RNA Processing, Protein Translation, Translation mechanism of gene expression, Genetic code,
Prokaryotic and Eukaryotic genomes, Introduction to the methods of introducing genes into the recipient cells- transformation, Transudation,
Conjugation.

ChE 403A: MATHEMATICAL METHODS IN CHEMICAL ENGINEERING

3 L, 1T
Max. Marks 50

The mathematical statement of the problem: Introduction,

Representation of the problem, Solvent extraction in two
stages, and solvent extraction in N stages, simple water
still with preheated feed, Unsteady state operation, salt accumulation in a stilled Tank, Radial heat transfer through a cylindrical conductor, Heating
a closed kettle, dependent and independent variables, parameters, Boundary conditions, Sign Conventions.
Ordinary differential equations Introduction, order and degree, first order differential equations, second order differential equations, linear
differential equations, and simultaneous differential equations.
Solution of series introduction, Infinite series, power series, simple series solutions, methods of frobenius, Bessels equation, properties of Bessel
functions.
Complex algebra introduction, The complex number, the argon diagram, principle values, algebraic operations on the argand diagram, conjugate
numbers, De Moivers theorem, the nth roots of unity, complex number series, trigonometrical exponential identities, the derivatives of a complex
variable, analytic functions, the complex variable and canohys theorem, Laurents expansion and the theory of residues.
Functions and definite integrals introduction, the error functions, the gamma function, the beta functions, and other tabulated functions which are
defined by integrals, evolution of definite integral vector analysis.

ChE 404A: PETROLEUM REFINING

3 L, 1 T

Max. Marks 50

Origin and Occurrence of Petroleum crude: status of petroleum refining industry in India, Composition, Classification and Physical properties of
petroleum, Testing and uses of petroleum products.
Petroleum refining processes: Atmospheric and Vacuum distillation, Thermal and catalytic in vapor, liquid and mixed phases, Hydro cracking,
Thermal reforming, Polyforming and plat forming, Catalytic reforming, Conversion of petroleum gases into motor fuel with reference to Alkylation,
Polymerization, Isomerisation, Hydrogenation, Production of aviation gasoline, motor fuel, kerosene, diesel oil and jet fuel.
Vacuum distillation: solvent extraction, uses of lubricating oils & waxes, Chemical & clay treatment of petroleum products, Desulphurization.

ChE 405A: ELECTIVE-I (Any one of the following.)

2 L, 0T
Max. Marks 50
1.
Phase Equilibrium and Industrial applications
General Introduction: Phases, Components, Degrees of freedom, The phase rule and its derivation

One component system: Equilibrium between liquid and vapour, vaporization curve, Le chatelier principle, Clausis clapeyron equation,
Equilibrium between solid and vapour, sublimation curve, equilibrium between solid and liquid, fusion curve, equilibrium among solid,
liquid and vapour, Allotropy or polymorphism.
Two component Systems: System consisting of two liquid phases only; ideal solutions and Raoults aw, partial and limited miscibility;
Typical systems: Phenol and water, liquid phases, systems consisting of liquid and vapour phases only, Henrys law, water and propyl
alcohol system; Systems consisting of solid and liquid phases only: KCL and AgCl systems
Three component systems: Liquid phases only, liquid and vapour phases: solid and liquid system
Systems NaCl, KCl, and H2O, KCl- K2SO4-H2O and similar systems.

2.

Energy Resources
Conventional and non-conventional energy resources: position in India, Transport, storage and environmental problems.
Solar radiation: Available solar radiation and measurements, Radiation transmission through covers and absorption by collectors, Theory of
flat plate collectors and their performance. Solar heating systems and design, Applications to solar cooling, Mechanical energy and solar
industrial process heating, Heat pumps, Solar ponds, Chemical storage systems, Photochemical conversion, solar cells.
Solids fuels: Coal, biomass, solid wastes, briquettes; Progressive of solid fuels by pyrolysis, gasification & liquefaction to secondary fuels,
Refuse derived fuels.
Coal: Origin: Classification Coal preparation; Carbonization; Coke ovens; Gasification of coal; Atmospheric and pressurized gasifiers;
Fishcer Tropsch synthesis, Methanol to gasoline conversion.
Petroleum: Origin and production of oil and gas, Petroleum refining and distillation; Cracking and reforming; Fluid catalytic cracking.
Proximate and ultimate analysis of solid, liquid and gaseous fuels: Calorific value; Antiknock rating and octane number; Cetane number;
flash point; Char value; Smoke point; viscosity; Aniline point etc.
Combustion Kinetics of solid, liquid and gaseous fuels: Ignition temperature, Types of burners.
Nuclear energy: Fission and fusion reactions; Nuclear reactor for power generation.
Hydrogen energy: Hydrogen production by photochemical decomposition of water and its storage; Fuel cells.
Introduction to wind, tidal and geothermal energy: OTEC and MHD; Energy from biomass.

3.

Biomass for Energy and Chemicals

Biomass as a source of energy, feed stock, food stuff., Biomass characterization. Solid, liquid and gaseous products from biomass, Sources
of biomass-agricultural residue, forestry waste, industrial waste. Overview of conversion technologies in particular, thermo chemical
conversion of biomass.
Combustion, pyrolysis and gasification of biomass., Design of gasifier for biomass conversion., Electricity generation and charcoal
production from biomass., Useful chemicals and energy from rice husk.

3 L, 0 T

ChE 451A: BIO CHEMICAL ENGINEERING

Max. Marks 50

Cell Growth Kinetics: Product Formation Kinetics.

Transport phenomena in cellular systems: Oxygen transfer rates, Mass transfer coefficient and interfacial area; Mechanical area, Mechanical
agitation and power requirement.
Ideal Bioreactors: Bioreactor dynamics, Multiphase bioreactors, Scale-up.
Instrumentation: Biosensors, Bioprocess control.
Thermal death kinetics: Media and air sterilization.
Enzymes and their classification: Enzymes kinetics, Inhibition, Immobilization of enzymes and whole cells, Industrial uses of enzymes,
Immobilized enzyme kinetics. Down-stream processing with emphasis on cell separation: Cell disruption: Aqueous two phase separation.
Industrial production of: ethanol, bakers yeast, penicillin, vitamins and acids.

2 L, 1 T

ChE 452A: TRANSPORT PHENOMENA

Max. Marks 50

Molecular Transport Phenomena: molecular transport of momentum, heat and mass, laws of molecular transport, Newtons law of viscosity,
Fouriers law of conduction and Ficks law of diffusion, transport coefficients-viscosity, thermal conductivity, mass diffusivity, estimation of
transport coefficients and temperature/pressure dependency.
Non-Newtonian fluids: time independent and dependent and viscoelastic fluids.
Laminar flow: Equation of continuity, motion, mechanical energy, energy and mass transport, shell balance method for momentum, heat and mass
transport, velocity distribution.
Turbulence Phenomena: Basic theory of turbulence, time averaging, intensity and correlation coefficients, equation of continuity, motion and
energy.
Diffusion Phenomena: diffusion of gases and liquids in porous solids, Knudsen diffusion.
Agitation and Mixing: introduction, agitation equipment, and power requirement.
Transport past emerged bodies: laminar and turbulent boundary layers, heat and mass transfer during boundary layer flow past a flat plate, cylinder
and spheres.
Heat, mass and momentum transfer in duct flow

Mass transfer with chemical reaction: enhancement due to reaction, determination of interfacial area.
Convective Transport: free and forced convective heat and mass transfer.

ChE 453A: CHEMICAL ENGINEERING OPTIMIZATION

2 L, 1T
Max. Marks 50
Optimization Definition of Optimization, Scope and Hierarchy of Optimization, Examples of Application, Essential Features and General
Procedure for solving Optimization Problems, Obstacles to Optimization, Classification of Models, Degrees of Freedom, Examples of Inequality
and Equality Constraints.
Objective function Economic Objective Functions, Time Value of Money in Objective Functions and Measure of Profitability.
Basic concepts of optimization Continuity of functions, NLP problem statement, Concave and Convex Functions, Necessary and Sufficient
condition for stationary points.
Optimization of Unconstrained Functions Newton and Quasi-Newton Methods of Uni-dimensional Search and Polynomial Approximation
Methods.
Unconstrained multivariable optimization Random search, Simplex Search Method, Methods using First Derivatives and Newtons Method.
Linear programming and Applications.
Applications of Optimization Optimizing Recovery of Waste Heat and Optimal Pipe Diameter.

ChE 454A: ELECTIVE-II (Any one of the following.)

3 L, 0 T
Max. Marks 50
1. Pollution Engineering
Introduction: Classification of air pollutants, Primary and Secondary pollutants, Source of air pollulation.
Atmospheric Dispersion: Meteorology, Adiabatic lapse rate, Atmospheric stability, Inversion types of inversion, maximum mixing height,
Atmospheric classes, Plumes and types of plumes under different atmospheric condition, plume rise, Gaussian dispersion curve, Point dispersion
model, Line and Area Model
Particulate Pollulation: Particulate pollulation and control equipment, centrifugal collector, Electronic precipators, Bag filter and Scrubber,
Design and Efficiency.

Water pollulation: Water quantity modeling for streams, Oxygen Demand, BOD, NBOD, CBOD Primary Treatment by Sedimentation,
Flocculation, Coagulation, Filtration, Disinfections, Waste water treatment, Biological (secondary) waste water treatment, Advance treatment
methods Nitrogen and Phosphorous Removal.
Solid waste: Collection of Solid waste. Treatment by disposal, pyrolysis.
Waste recovery system and case study.
Odour pollulation: Determination of Odour, Threshold concentration, various control method.
Noise Pollution: Measurements and units of Noise, SPL, PWL, Effect of noise, Control by equipment, SPL indicator

2. CORROSION ENGINEERING
Corrosion direct & two stage attack, electrochemical attack, environment conditioning. Higher corrosion resistance through proper selection of
material, isolation of corrosion prone materials form distructive environment, Technologies of anodisation, enamelling, rubber lining, glass
lining, refractory lining, painting and other surface protective measures. Corrosion engineering in special applications such as material transport,
pumping, filtration, condensation, boiling revetting, welding, high temperature environments etc. cost factor in cometitives corrosion
prevention/inhibition techniques

ChE 455A: ELECTIVE-III (Any one of the following.)

1. POLYMER
SCIENCE
AND
2 L, 1 T
Max. Marks 50
TECHNOLOGY.
Polymerization chemistry: Chain, Step, Addition, Condensation and miscellaneous polymerization reactions and polymerization technique.
Polymerization Kinetics: Free radical, Cationic and Anionic polymerization, Poly-condensation, Co-polymerization systems.
Microstructures of polymer molecules based on channel and geometrical structure: Transition associated properties, Factors influencing the glass
transition temperature, Degree of crystallization, Factors affecting crystallizability, Effect of crystallinity on the properties of polymers.
Polymer reactions: Hydrolysis, Acidolysis, Hydrogenation, Addition and Substitution reactions, Reactions of various specific groups,
Cyclyzation and Cross-Linking reactions, Reactions leading to graft and block copolymer.
Polymer Solutions: Process and thermodynamics of dissolution, Nature of polymer molecules in solutions, Size and shape of macromolecules in
solution, Viscosity of dilute and concentrated polymer.
Manufacturing process of important polymers: Plastic Polyethylene, Polypropylene, Polyvinyl chloride and copolymers, Polystyrene, Phenolformaldehyde, Epoxides, Urethane, Teflon, Elastomers, Rubbers, Polymeric oils Silicones, Fibers Cellulosic (Rayon), Polyamides (6:6
Nylon), Polyesters (Dacron), Acrylic, Olefin, Composite materials Ceramic and other fiber reinforced plastics, Polymer degradation Thermal
Mechanical, Ultrasonic, Photo, High-energy radiation, Oxidation and Hydrolytic degradation, Ecology and environmental aspects of polymer
industries.
Principle of polymer processing: Behavior of viscoelastic fluids, Testing and evaluation of flow behavior, Mixing of powder and viscoelastic
materials, various molding operations, Extrusion, calendaring and coating operations.
2. FLUIDIZATION ENGINEERING
Fundamentals, Industrial applsication; study, design and operation of fluidization units. Fluidization: particulate and aggregate beds. Application
of fluidization. Regimes of fluidization. Bubbling fluidized beds. Two phase theory. Heat and mass transfer between fluids and particles.
Performance of drier and reactors. Elutriation. Choking, Transport velocity. High velocity fluidized beds. Circulating fluidized beds. Design.

3. CATALYSIS
Physical adsorption: Type of adsorption isotherms, Surface area and BET and other methods of surface area measurement pore size distribution
and its determination.
Chemisorption: theory of Chemisorption, heat of Chemisorption, Chemisorption with dissociation.
Catalyst preparation, Catalyst characterization, Carrier & Supports, Promoters, Accelerators, Poison & Inhibitors.

Design of a catalyst, Catalyst for different unit processes