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DEPARTMENT OF MECHANICAL ENGINEERING

LABORATORY MANUAL

CE6315 – STRENGTH OF MATERIALS LAB

YEAR / SEMESTER : II / IV

DEPARTMENT : Mechanical

ACADEMIC YEAR : 2014 – 2015 EVEN SEMESTER

REGULATION : 2013

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LIST OF EXPERIMENTS

1. Tension test on a mild steel rod

2. Double shear test on Mild steel and Aluminum rods
3. Torsion test on mild steel rod
4. Impact test on metal specimen
5. Hardness test on metals - Brinnell and Rockwell Hardness Number
6. Deflection test on beams
7. Compression test on helical springs
8. Strain Measurement using Rosette strain gauge
9. Effect of hardening- Improvement in hardness and impact resistance
of steels.
10. Tempering - Improvement Mechanical properties Comparison
(i) Unhardened specimen
(ii) Quenched Specimen and
(iii) Quenched and tempered specimen.
11. Microscopic Examination of
(i) Hardened samples and
(ii) Hardened and tempered samples.

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STRENGTH OF MATERIALS LABORATORY

GENERAL INSTRUCTION

The following instructions should be strictly followed by the students in the strength
of Materials Laboratory.

1. All the students are expected to come to the lab, with shoe, uniform etc., whenever
they come for the laboratory class.

2. For each lab class, all the students are expected to come with observation note book,
record note book, pencil, eraser, sharpener, scale, divider, graph sheets, French curve etc.

3. While coming to each laboratory class, students are expected to come observation note
book prepared for the class.

4. All the students are expected to complete their laboratory work including calculations
and get it corrected in the laboratory class itself.

5. While coming to the next lab classes are expected to submit the record note for
correction.

6. All the equipments, tools accessories and expensive. Therefore, students are expected
to handle the instruments with utmost care during the experiment.

7. The tools and accessories required for conducting the experiments can be obtained
from the technician and the same should be returned as soon as the experiment over.

8. Breakage amount will be collected from the student(S) for causing damage to the
instruments / equipments due to wrong operation or carelessness.

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TABLE OF CONTENTS

PAGE
SL.NO. NAME OF THE EXPERIMENT
NO
TENSION TEST ON MILD STEEL ROD
1 5
TORSION TEST ON MILD STEEL ROD
2 8
CHARPY IMPACT TEST
3 12
IZOD IMPACT TEST
4 14
ROCKWELL HARDNESS TEST
5 16
BRINELL HARDNESS TEST
6 18

7 DEFLECTION TEST ON BEAMS 21

TEST ON COMPRESSION SPRING
8 23
DOUBLE SHEAR TEST ON MILD STEEL AND
9 ALUMINIUM RODS 25

STRAIN MEASUREMENT USING ROSETTE STRAIN

10 GUAGE 27

EFFECT ON HARDENING – IMPROVEMENT IN

11 29
HARDNESS AND IMPACT RESISTANCE OF STEEL
TEMPERING – IMPROVEMENT MECHANICAL
PROPERTIES COMPARISON
i) UNHARDENED SPECIMEN 31
12
ii) QUENCHED SPECIMEN
iii) QUENCHED AND TEMPERED SPECIMEN

MICROSCOPIC EXAMINATION OF HARDENED

33
SAMPLES HARDENED AND TEMPERED SAMPLE
13

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TENSION TEST ON MILD STEEL ROD

Ex. No.: Date:

Aim:

To conduct a tension test on given mild steel specimen for finding the following:
1. Yield stress
2. Ultimate stress
3. Nominal breaking stress
4. Actual breaking stress
5. Percentage Elongation in length
6. Percentage Reduction in area.

Apparatus Required:

1. Universal Testing machine (UTM)

2. Mild steel specimen
3. Scale
4. Vernier caliper
5. Dot Punch
6. Hammer

Procedure:

1. Measure the length (L) and diameter (d) of the given specimen.
2. Mark the centre of the specimen using dot punch.
3. Mark two points P and Q at a distance of 150mm on either side of the centre mark so
that the distance between P and Q will be equal to 300mm.
4.Mark two point A and B at a distance of 2.5 times the rod distance on the either side of
the centre mark so that the distance between A & B will be equal to 5 times the rod
diameter and is known as initial gauge length of rod. (li).
5. Insert the specimen in the middle cross head and top cross head grip of the machince
so that the two points A and B coincide with grips.
6. Apply the load gradually and continue the applications of load. After sometime, there
will be slightly pause in the increase of load. The load at this point is noted as yield point
(Py).
7. Apply load continuously till the specimen fails and note down the ultimate load (Pa)
and breaking load (Pb) from the digital indicator.
8. Remove the specimen from the machine and join the two pieces of the specimens.
9. Measure the distance between the two points A and B. This distance is known as final
gauge length (li) of the specimen.
10. Measure the diameter of the rod at neck (dn).
11. Determine the yield stress, ultimate stress, nominal breaking stress, actual breaking
stress, percentage elongation in length and percentage reduction in area using the
following formula.

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Universal testing machine

Mild Steel Specimen

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Observation:
1. Material of the specimen =
2. Length of the specimen, L = mm
3. Diameter of the specimen, d = mm
4. Initial gauge length of the specimen Ii = mm
5. Final gauge length of the specimen Ii = mm
6. Diameter at neck dn = mm
7. Yield load. Py = KN
8. Ultimate load,Pu = KN
9. Breaking load, Pb = KN

Calculations:

1) Yield stress σy = Yield load (Py)

Initial Area (Ai)

2) Ultimate stress σu = Ultimate load (Pu)

Initial Area (Ai)

3. Nominal breaking stress, σbn = Breaking load (Pb)

Initial Area (Ai)

4. Actual breaking stress, σbn = Breaking load (Pb)

Neck Area (An)

5. % Elongation in length = Final gauge length (Ii) – Initial gauge length (Ii) x 100
Initial gauge length (Ii)

6% Reduction in area = Initial area (Ai) – Neck area (An) x 100

Initial gauge length (Ii)

Where Ai = Initial Area = πd2 /4

An = Area at neck = πdn2 / 4.

Result:
Tension test for the given specimen was conducted and the results are as follows:
1. Yield stress, σy = N/mm2
2. Ultimate stress, σu = N/mm2
3. Nominal breaking stress, σbn = N/mm2
4. Actual breaking stress, σbn = N/mm2
5. Percentage Elongation in length =
6. Percentage Reduction in area =

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TEST FOR TORSION ON MILD STEEL ROUND ROD

Experiment No: Date:

AIM:
To conduct torsion test on mild steel round rod and to determine the value of
modulus of rigidity and maximum shear stress.

APPARATUS REQUIRED:
a. Torsion testing machine
b. Vernier caliper
c. Steel rule
d. Specimen

FORMULAE USED:

Modulus of Rigidity, (C) = N/mm2

Maximum Shear Stress, (τ) = N/mm2

Where,
T Torque, N-mm
J Polar Moment of Inertia, mm4
L Gauge Length, mm
θ Angle of Twist, Radians
R Mean radius of shaft, mm

PROCEDURE:
1. Before testing, adjust the measuring range according to the capacity of the
test piece.
2. Hold the specimen in driving chuck and driven chuck with the help of
handles.
3. Adjust the angle measuring dial at zero position, black pointer at the starting
position and pen in its required position.
4. Bring the red dummy pointer in line with the black pointer.
5. Start the machine and now the specimen will be subjected to torsion.
6. Take down the value of torque from the indicating dial for particular value of
angle of twist (for every 5° of rotation).
7. Repeat the experiment until the specimen breaks into two pieces. Note the
value of torque at this breaking point.
8. Tabulate the readings and draw graph between angle of twist and torque.
9. Find the value of T/θ from the graph and find the value of modulus of
rigidity.
10. Find the maximum shear stress.

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OBSERVATION & TABULATION:
i. Gauge Length (L) = __________ mm
ii. Mean Diameter of Specimen(d):

Vernier Caliper Reading: L.C. =__________ mm

Observed Reading = Correct Reading =
M.S.R. V.S.R.
Sl. No. M.S.R. + (V.S.R. x Observed Reading ±
(mm) (Div)
L.C.) Z.C.

Mean

Mean Diameter of the specimen (d) = __________ mm.

Angle of Twist (θ) Torque (T)
Sl. No.
(Radians) (N – mm)

GRAPH:

(T/θ) = _____
T

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CALCULATIONS:

i. Polar Moment of Inertia (J) = (π/32) x d4

ii. Modulus of Rigidity, (C) = N/mm2

iii. Maximum Shear Stress, (τ) = N/mm2

RESULT

For the given mild steel round rod specimen

Modulus of Rigidity, (C) = ____________ N/mm2

Maximum Shear Stress, (τ) = ____________ N/mm2

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CHARPY IMPACT TEST

Ex. No.: Date:

Aim:
To determine the impact strength of the given specimen by conducting charpy impact
test.

Apparatus and specimen required:

1. Impact testing machine with attachment for charpy test.

2. Charpy specimen
3. Vernier caliper
4. Scale.

Procedure:
1. Measure the length (l), breadth (b), & depth (d) of the given specimen.
2. Measure the position of notch (i.e. groove) from one end (lg), depth of groove (dg)
and top width of the groove (wg) in the given specimen.
3. Lift the pendulum and keep it in the position meant for charpy test.
4. Adjust the pointer to coincide with initial position (i.e. maximum value) in charpy
scale.
5. Release the pendulum using the lever and note down the initial reading in the
charpy scale.
6. Repeat the step 3 and 4.
7. Place the specimen centrally over the supports such that the groove in opposite to
the striking face.
8. Release the pendulum again using the lever and note down the final reading in the
charpy scale.
9. Find the impact strength of the given specimen by using the following relation:
Impact strength = (Final charpy scale reading – Initial charpy scale reading)

Observation:

1. Material of the given specimen =

2. Type of notch (i.e. groove) =
3. Length of the specimen, l = mm
4. Breadth of the specimen, b = mm
5. Depth of the specimen, d = mm
6. Position of groove from one end, (lg) = mm
7. Depth of groove (dg) = mm
8. Width of groove (wg) = mm
9. Initial charpy scale reading = kg.m
10. Final charpy scale reading = kg.m

Result:
The impact strength of the given specimen is --------- Kg.m

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CHARPY IMPACT TESTING MACHINE

SPECIMEN - CHARPY TEST

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IZOD IMPACT TEST

Ex. No.: Date:

Aim:
To determine the impact strength of the given specimen by conducting Izod impact test.

Apparatus and specimen required:

1. Impact testing machine with attachment for Izod test.

2. Given specimen
3. Vernier caliper
4. Scale.

Procedure:
1. Measure the length (l), breadth (b), & depth (d) of the given specimen.
2. Measure the position of notch (i.e. groove) from one end (lg), depth of groove (dg)
and top width of the groove (wg) in the given specimen.
3. Lift the pendulum and keep it in the position meant for charpy Izod test.
4. Adjust the pointer to coincide with initial position (i.e. maximum value) in the
izod scale.
5. Release the pendulum using the lever and note down the initial reading in the izod
scale.
6. Repeat the step 3 and 4.
7. Place the specimen vertically upwards such that the shorter distance between one
end of the specimen and groove will be protruding length and also the groove in
the specimen should face the striking end of the hammer.
8. Release the pendulum again using the lever and note down the final reading in the
izod scale.
9. Find the impact strength of the given specimen by using the following relation:
Impact strength = (Final izod scale reading – Initial izod scale reading)

Observation:
1. Material of the given specimen =
2. Type of notch (i.e. groove) =
3. Length of the specimen, l = mm
4. Breadth of the specimen, b = mm
5. Depth of the specimen, d = mm
6. Position of groove from one end, (lg) = mm
7. Depth of groove (dg) = mm
8. Width of groove (wg) = mm
9. Initial charpy scale reading = kg.m
10. Final charpy scale reading = kg.m

Result:
The impact strength of the given specimen is --------- Kg.m

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IZODE IMPACT TESTING MACHINE

SPECIMEN - IZODE TEST

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ROCKWELL HARDNESS TEST

Ex. No.: Date:

Aim:

To determine the Rockwell hardness number for the given specimen.

Apparatus Required:

1. Rockwell hardness testing machine

2. Indentor
3. Test specimen
4. Stop watch

Procedure:

1. Identify the material of the given specimen

2. Know the major load, type of indenter and scale to be used for the given test specimen
from the following table.

Sl.No. Material type Major load Indenter Scale

1 Hardened steel 150kg Diamond cone 120º C
2 Mild steel 100kg 1.58mm dia, steel ball B
3 Aluminum 100kg 1.58mm dia. Steel ball B
4 Brass 100kg 1.58mm dia. Steel ball B
5 Copper 100kg 1.58mm dia. Steel ball B

3. Fix the indentor and place the given specimen on the anvil of the machine.
4. Select the major load from the knob available on the right of the machine.
5. Raise the anvil using the rotating wheel till the specimen touches the indentor and then
slowly turns the wheel till the small pointer on the dial reaches the red mark position.
Now the specimen is subjected to a minor load of 10kg.
6. Push the loading handle in the forward direction to apply the major load to the
specimen and allow the load to act on the specimen for 15 seconds.
7. Release the major load by pushing the loading handle in the backward direction and
keep the minor 10kg load still on the specimen.
8. Read the Rockwell hardness number either from ‘C’ or ‘B’ scale, as the case may be,
directly on the dial and record it.
9. Release the minor load of 10kg by rotating the hand wheel and lowering the screw bar.
10. Repeat the experiment to obtain at least 3 different sets of observations for the given
specimen by giving a gap of at least 3mm between any two adjacent indentations and
1.5mm from the edge.
11. Find the average value, which will be the rckwell hardness number for the given
specimen.

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Rockwell hardness test equipment

Observation:
Sl.No. Material Major load Indentor Scale Rockwell hardness number
(RHC…… or RHB)

Average

Result:
The Rockwell hardness number for the given specimen = RHC ----------- (or) RHB -------

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BRINELL HARDNESS TEST

Ex. No.: Date:

Aim:

To determine the Brinell hardness number for the given specimen.

Apparatus Required:

1. Brinell hardness testing machine

2. Microscope
3. Indenter
4. Test specimen
5. Stop watch

Procedure:

1. Identify the material of the given specimen

2. Know the value of P/D2 and diameter of the indenter (D) type to be used for the given
test specimen from the following table.

Sl.No. Material type P/D2value in kg/mm2 Diameter of steel ball (D)

indenter in mm
1 Steel and cast iron 30 2.5
2 Copperand Aluminum Alloys 10 2.5
3 Copper and Aluminum 5 2.5
4 Lead, Tin and Alloys 1 2.5

Where, P = Major load in kg.

3. Calculate the major load to be applied for the given test specimen by knowing the
value of PD2 and D.
4. Select the major load from the knob available on the right of the machine.
5. Fix the indentor and place the given specimen on the anvil of the machine.
6. Raise the anvil using the rotating wheel till the specimen touches the indentor and then
slowly turns the wheel till the small pointer on the dial reaches the red mark position.
Now the specimen is subjected to a minor load of 10kg.
7. Apply the major load to the specimen by pushing the loading – handle in the forward
direction and allow the load to act on the specimen for 15 seconds.
8. Release the major load by pushing the loading handle in the backward direction.
9. Release the minor load of 10kg by rotating the hand wheel and lowering the screw bar.
10. Measure the diameter of indentation (d) using the microscope.

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11. Calculate the Brinell hardness number for the given specimen using the following
formula:
Brinell hardness number = Load in kg
Spherical area of Indentation of mm2

= P kg/mm2
πD/2 [d - √ D2 – d2]
Where, P = Major load in kg.
D = Diameter of indenter in mm.
d = diameter of indentation in mm.
12. Repeat the experiment to obtain at least 3 different sets of observations for the given
specimen by giving a gap of at least 3mm between any two adjacent indentations and
1.5mm from the edge.
11. Find the average value, which will be the Brinell hardness number for the given
specimen.

BRINELL HARDNESS TEST

EQUIPMENT
BRINELL HARDNESS TESTING
MACHINE

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Observation:
Sl.No. Material P/D2value Major Diameter of Dia of Brinell
in kg/mm2 load (P) steel ball indentation hradmess
in kg indentor (D) (d) in mm number
in mm. (BHN) in
kg/mm2

Average

Result:
The Brinell hardness number for the given specimen = ----------- kg/mm2

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DEFLECTION TEST ON BEAMS

Ex. No.: Date:

Aim:

To determine the Young’s modulus of the given specimen by conducting bending test.

Apparatus and Specimen required:

1. Bending Test Attachment

2. Specimen for bending test
3. Dial gauge
4. Scale
5. Pencil / Chalk

Procedure:

1. Measure the length (L) of the given specimen

2. Mark the centre of the specimen using pencil / chalk
3. Mark two points A & B at a distance of 350mm on either side of the centre mark. The
distance between A & B is known as span of the specimen (l)
4. Fix the attachment for the bending test in the machine properly.
5. Place the specimen over the two supports of the bending table attachment such that the
points A &B coincide with centre of the supports. While placing, ensure that the
tangential surface nearer to heart will be the top surface and receives the load.
6. Measure the breadth (b) and depth (d) of the specimen using scale.
7. Place the dial gauge under this specimen at the centre and adjust the dial gauge reading
to zero position.
8. Place the load cell at top of the specimen at the centre and adjust the load indicator in
the digital box to zero position.
9. Select a strain rate of 2.5mm / minute using the gear box in the machine.
10. Apply the load continuously at a constant rate of 2.5mm/minute and note down the
deflection for every increase of 0.25 tonne load up to a maximum of 6 sets of readings.
11. Calculate the Young’s modulus of the given specimen for each load using the
following formula:

Young’s modulus, E = Pl3

48Iδ
Where, P = Load in N
L = Span of the specimen in mm
I = Moment of Inertia in mm4 (bd3/12)
b = Breadth of the beam in mm.
d = Depth of the beam in mm
δ = Actual deflection in mm.
12. Find the average value of young’s modulus that will be the Young’s modulus of the
given specimen.

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Observation:
1. Material of the specimen =
2. Length of the specimen, L = mm
3. Breadth of the specimen, b = mm
4. Depth of the specimen, d = mm
5. Span of the specimen, l = mm
6. Least count of the dial gauge, LC = mm

Sl.No. Load in Deflection in mm Young’s

T N observed Actual Modulus in
N/mm2

Average

Result:
The young’s modulus of the given wooden specimen = ---------------------N/mm2

DEFLECTION TEST – SPECIMEN SETUP

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TEST ON COMPRESSION SPRING

Ex. No.: Date:

Aim:

To determine the modulus of rigidity and stiffness of the given compression spring
specimen.

Apparatus and specimen required:

1. Spring test machine

2. Compression spring specimen
3. Vernier caliper

Procedure:

1. Measure the outer diameter (D) and diameter of the spring coil (D) for the given
compression spring.
2. Count the number of turns i.e. coils (n) in the given compression specimen.
3. Place the compression spring at the centre of the bottom beam of the spring testing
machine.
4. Rise the bottom beam by rotating right side wheel till the spring top rouches the middle
cross beam.
5. Note down the initial reading from the scale in the machine.
6. Apply a load of 25kg and note down the scale reading. Increase the load at the rate of
25kg upto a maximum of 100kg and note down the corresponding scale readings.
7. Find the actual deflection of the spring for each load by deducting the initial scale
reading from the corresponding scale reading.
8. Calculate the modulus of rigidity for each load applied by using the following formula:

Modulus of rigidity, N = 64PR3n

d4δ
Where, P = Load in N
R = Mean radius of the spring in mm (D –d /2)
d = Diameter of the spring coil in mm
δ = Deflection of the spring in mm
D = Outer diameter of the spring in mm.

9. Determine the stiffness for each load applied by using the following formula:
Stiffness, K = P/δ
10. Find the values of modulus of rigidity and spring constant of the given spring by
taking average values.

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Observation:

1. Material of the spring specimen =

2. Outer diameter of the spring. D = mm
3. Diameter of the spring coil, d = mm
4. Number of coils / turns, n = Nos.
5. Initial scale reading = cm = mm

Sl.No. Applied Load in Scale reading in Actual Modulus of Stiffness in

kg N cm mm deflection rigidity N/mm
in mm inN/mm2

Average

Result:
The modulus of rigidity of the given spring = -------------------N/mm2
The stiffness of the given spring = -------------------N/mm2

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DOUBLE SHEAR TEST ON STEEL BAR

Ex. No.: Date:

Aim:

To determine the maximum shear strength of the given bar by conducting double- shear
test.

Apparatus and specimen required:

1. Universal Testing machine (UTM)

2. Mild steel specimen
3. Device for double shear test
4. Veriner caliper / screw gauge

Description:

In actual practice when a beam is loaded the shear force at a section always comes to play along
with bending moment. It has been observed that the effect of shearing stresses compared
to bending stress is quite negligible. But sometimes, the shearing stress at a section
assumes much importance in design calculations. Universal testing machine is used for
performing shear, compression and tension. There are two types of UTM.1. Screw type2.
Hydraulic type. Hydraulic machines are easier to operate. They have a testing unit and control unit
connected to each other with hydraulic pipes. It has a reservoir of oil, which is pumped
into a cylinder, which has a piston. By this arrangement, the piston is made to move up.
Same oil is taken in a tube to measure the pressure. This causes movement of the pointer,
which gives reading for the load applied.

Procedure:

1. Measure the diameter (d) of the given specimen.

2. The inner diameter of the hole in the shear stress attachment is slightly greater than that of
the specimen.

3. Fit the specimen in the double shear device and place whole assembly in the
UTM.
4. Apply the load till the specimen fails by double – shear.
5. Note down the load at which the specimen fails (P).
6. Calculate the maximum shear strength of the given specimen by using the
following formula:
Maximum shear strength = Load at failure (P) in N
(c/s area in double shear) 2 x cross – sectional area of the bar in mm2

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Observation:

1. Material of the specimen =

2. Diameter of the specimen, d = mm
3. Cross sectional area in double shear, (A) = 2 x π d2/4 mm2
4. Shear Load taken by specimen at the time of failure (P) = ------ KN

Result:

The maximum shear strength of the given specimen = ----------------------- N/mm2

UNIVERSAL TESTING MACHINE

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STRAIN MEASUREMENT ON CANTILEVER BEAM

Ex. No.: Date:

Aim:
To determine the Strain of the cantilever beam subjected to Point load at the free end
and to plot the characteristic curves.

Apparatus required
Cantilever Beam Strainguage Trainer Kit
Weights and Multimeter

Formula used
Strain, S = 6PL / BT2E
Where,
P=Load applied in Kg.
L = Effective length of the beam in cm.
B = Width of the beam in cm.
T = thickness of the beam in cm.
E = young’s modulus = 2x109Kg/cm2.
S = Micro strain.

Theory:
When the material is subjected to any external load, there will be small change in
the Mechanical properties like thickness of the material or change in the length
depending upon the nature of load applied to the material. The change in mechanical
properties will remain till the load is released. The change in the property is called Strain
(or) material gets strained.
Strain S = ∂L/L
Since the change in length is very small, it is difficult to measure ∂L, so the strain is
measured in micro strain. Since it is difficult to measure the length, Resistance strain
gauge are used to measure strain in the material directly. Strain gauges are bonded
directly on the material using special adhesive s. As the material get strained due to load
applied the resistance of the strain gauge changes proportional to the load applied. This
change in resistance is used to convert mechanical property into electrical signal which
can be easily measured and stored for analysis.
The change in the resistance of the strain gauge depends on the sensitivity of the
strain gauge which is expressed in terms of a gauge factor, Sg
Sg = ∆R /R
The output ∆R/R of a strain gauge is usually converted into voltage signal with a
Wheatstone bridge. If a single gauge is used in one arm of Wheatstone bridge and equal
but fixed resistors is used in the other arm, the output voltage is Eo =Ei / 4(∆Rg /Rg)
Eo =1/4(EiSg ∆)

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The input voltage is controlled by the gauge size and the initial resistance of the
gauge. As a result, the output voltage Eo usually ranges between 1 to 10 ∆V / micro units
of strain.
Procedure:
1. The instrument is switched on ( i.e.,). The display glows to indicate the instrument
is ON.
2. The Instrument is allowed to be in ON position for 10 minutes for initial worm-
up.
3. From the selector switch, FULL or HALF bridge configuration is selected.
4. The potentiometer is adjusted for ZERO till the displays reads ' 000’
5. 1 Kg load is applied on the pan of the cantilever the CAL Potentiometer is
adjusted till the display reads 377 micro strains. When the weights are removed
the display should come to ZERO, in case of any variation, ZERO Potentiometer
is adjusted again and the procedure is repeated again. Now the instrument is
calibrated to read micro strains.
6. Then the loads are applied on the pan in steps of 100 gm up to 1kg. When the
cantilever is strained, instrument displays exact micro strain.
7. The readings are noted down in the tabular column . Percentages error in
readings, hysteresis and accuracy of the instrument can be calculated by
comparing with the theoretical results.

Observation:

Actual Display readings

Weigh readings
Sl.N While Error
t (using While unloading
o. loading %
(gms) formula) micro strains
micro strains
Micro strains
1 100
2 200
3 300
4 400
5 500
6 600
7 700
8 800
9 900
10 1000

% ERROR = (Actual reading – Display reading) x 100

Max Weight (gms)

Result:
Thus the strain of the cantilever beam subjected to free end loading, is obtained in micro
strains and the characteristics curves – Load Vs Strain, Output Voltage Vs Strain and
Actual Vs Display readings are plotted.

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TEMPERING- IMPROVEMENT MECHANICAL PROPERTIES COMPARISON

Ex. No.: Date:

Aim:

To perform the heat treatment tempering on the given material C-40 steel.

Apparatus required:

1. Muffle furnace: tongs

2. Given material: C-40 steel
3. Quenching medium: water
4. Rockwell test setup

Procedure:

Quenching:
It is an operation of rapid cooling by immersing a hot piece into a quenching bath.

Tempering:
It is defined as the process of reheating the hardened specimen to some temperature before the
critical range followed by any rate of cooling such are heating permit the trapped temperature
to transform and relieve the internal stresses.

1. The given specimen is subjected to Rockwell hardness test and Rockwell hardness number is
measured before hardening that the specimen is subjected to rough grinding.
2.The specimen is placed inside the combustion chamber of muffle furnace and is noted up to
830˚C
3. Then the specimen is soaked for 10 minutes at the same temperature 830˚C.
4. After soaking it is taken out from the furnace and it is quenched in the water.
5. The specimen is cooled, now the tempering is completed.
6. Again the specimen is subjected to Rockwell hardness test and Rockwell hardness number is
measured.

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Tabulation:

S.NO Specimen Material Load(Kgf) Penetration Scale RHN

Result:

The heat treatment tempering on the given material C-40 steel and its Rockwell hardness number
is measured
1. Rockwell hardness number before tempering =
2. Rockwell hardness number after tempering =

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MECHANICAL PROPERTIES FOR UNHARDENED OR HARDENED SPECIMEN

Ex. No.: Date:

Aim

To find hardness number and impact strength for unhardened, hardened specimen or
Quenched and tempered specimen and compare mechanical properties.

Material and equipment:

Unhardened specimen, Hardened or Quenched and tempered specimen, muffle furnace, Rockwell
testing machine, impact testing machine.

Procedure:

HARDENING:

It is defined as a heat treatment process in which the steel is heated to a temperature within or
above its critical range, and held at this temperature for considerable time to ensure thorough
penetration of the temperature inside the component and allowed to cool by quenching in water, oil
or brine solution.

Case (I) - Unhardened specimen

1. Choose the indenter and load for given material.

2. Hold the indenter in indenter holder rigidly
3. Place the specimen on the anvil and raise the elevating screw by rotating the hand
wheel up to the initial load.
4. Apply the major load gradually by pushing the lever and then release it as before.
5. Note down the readings in the dial for corresponding scale.
6. Take min 5 readings for each material.

Case (II) - For Hardened specimen

1. Keep the specimen in muffle furnace at temperature of 700˚ to 850˚ for 2 hours
2. The specimen is taken from muffle furnace and quenched in water or oil.3. Then above
procedure is followed to test hardness

Case (III) - For Tempered specimen

1. Keep the specimen in muffle furnace at temperature of 650˚ for 2 hours

2. Allow the specimen for air cooling after taking from muffle furnace
3. Then same procedure is followed foe the specimen

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Observation:
Rockwell hardness test:
Cases for hardness =
Cross sectional area=

Indente RHN
Load
S.No Material temperature r scale Trial trail Trail
(Kgf) Mean
detail 1 2 3
Deep
1 caseharden
ed steel
Deep
2 caseharden
ed steel

3 Mild steel

4 Mild steel

CHARPY TEST

Impact
Material and Energy Cross-sectional area
S.No strength(J/
Condition absorbed(Joules) below the notch(mm)
mm)
Mild steel-
1
unhardened
Quenched
2

Result:
Thus the hardening – heat treatment process is carried out.

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MICROSCOPIC EXAMINATION OF (i) HARDENED SAMPLES AND (ii) HARDENED
AND TEMPERED SAMPLES.

Ex. No.: Date:

Aim:
To prepare a specimen for microscopic examination.

Tools required:
Linisher – polisher grades of emery sheets (rough and Fine), disc polisher, metallurgical
microscopes.

Procedure

The specimen preparation consists of following stages:

i) Rough grinding
ii) Intermediate Polishing
Iii) Fine Polishing
iv) Etching

(i) Rough grinding:

It is first necessary for specimen to obtain a reasonable flat surface. This is achieved by
using a motor driven energy belt called Linisher-Polisher. The specimen should be kept
over the moving belt which will abrade the specimen and make the surface flat. In all
grinding and polishing operations, the specimen should be moved perpendicular the
existing scratches, so that the deeper scratches will be replaced to a shallower one. This
operation is done until the specimen is smooth, free from rust, burs, troughs and deep
scratches.

(ii) Intermediate Polishing:

It is carried out using energy paper of cogressively fine grades. The emery paper should
be of good quality. The different grades of emery paper used are 120,240,320,400 and
1/0,2/0,3/0,4/0 (Grain size from coarse to fine). The emery paper should be kept against
the specimen and moved gently until a fine matrix of uniformly spaced scratches appears
on the object. Final grade is then chosen and the specimen is turned perpendicular to the
previous direction. This operation is usually done dry.

(iii) Fine Polishing:

An approximate flat scratch free surface is obtained by the use of wet rotary wheel
covered with abrasive of alumina powder of 0.05 microns. In this operation, water is used
as lubricant and carrier of the abrasive fine scratches and very thin layer produced due to
previous operations.

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(iv) Etching:

The polished surface is washed with water and etching is done by rubbing the polished
surface gently with cotton wetted with etching reagent. After etching the specimen is
again washed and then dried, it is then placed under the metallurgical microscope to view
the microstructure of it. Thus the specimen is identified.

Result:

Thus the specimen was prepared for microscope observation for its identification.

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