Government Engineering College, Ajmer

Near Badliya Circle, Ajmer Rajasthan

Laboratory Manual

FOURTH SEMESTER
MATERIAL TESTING LAB

DEPARTMENT
OF
CIVIL ENGINEERING

Academic Year 2019-20

Submitted To- Submitted By-

 Govt. Engineering College, Ajmer
Department of Civil Engineering

MATERIAL TESTING LAB

List of Experiments

S.No. Experiments
1 Tensile strength test – Mild steel and HYSD bar
2 Hardness test – Rockwell hardness and Brinell hardness
3 Torsion test
4 Impact test – Izod and charpy
5 Modulus of rupture of wooden beam
6 Spring test
7 Compressive strength test - Bricks
8 Compressive strength test – Mild steel and Cast iron
9 Fatigue test
10 Compressive strength test – Cement and Concrete cubes
11 Compressive strength test – Wooden blocks

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 EXPERIMENT NO: – 01
AIM: - To determine tensile test on a Mild steel and HYSD bar
OBJECT: - To conduct a tensile test on a mild steel specimen and determine the following:
(i) Limit of proportionality (ii) Elastic limit
(iii) Yield strength (IV) Ultimate strength
(v) Young’s modulus of elasticity (VI) Percentage elongation
(vii) Percentage reduction in area.
APPARATUS: -
(i) Universal Testing Machine (UTM)
(ii) Mild steel specimens
(iii) Graph paper
(iv) Vernier Caliper
DIAGRAM: -

Universal Testing Machine

THEORY:
The tensile test is most applied one, of all mechanical tests. In this test ends of test piece are fixed
into grips connected to a straining device and to a load measuring device. If the applied load is

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small enough, the deformation of any solid body is entirely elastic. An elastically deformed solid
will return to its original from as soon as load is removed. However, if the load is too large, the
material can be deformed permanently. The initial part of the tension curve which is recoverable
immediately after unloading is termed. As elastic and the rest of the curve which represents the
manner in which solid undergoes plastic deformation is termed plastic.
A tensile test, also known as a tension test, is one of the most fundamental and common types of
mechanical testing. A tensile test applies tensile (pulling) force to a material and measures the
specimen's response to the stress. By doing this, tensile tests determine how strong a material is and
how much it can elongate. Tensile tests are typically conducted on universal testing instruments, are
simple to perform, and are fully standardized. By measuring the material while it is being pulled, we
can obtain a complete profile of its tensile properties. When plotted on a graph, this data results in a
stress/strain curve which shows how the material reacted to the forces being applied. The point of
break or failure is of much interest, but other important properties include the modulus of elasticity,
yield strength, and strain.

Ultimate Tensile Strength

One of the most important properties we can determine about a material is its ultimate tensile
strength (UTS). This is the maximum stress that a specimen sustains during the test. The UTS may
or may not equate to the specimen's strength at break, depending on whether the material is brittle,
ductile, or exhibits properties of both. Sometimes a material may be ductile when tested in a lab,
but, when placed in service and exposed to extreme cold temperatures, it may transition to brittle
behavior.

Hooke's Law
For most materials, the initial portion of the test will exhibit a linear relationship between the
applied force or load and the elongation exhibited by the specimen. In this linear region, the line
obeys the relationship defined as "Hooke's Law" where the ratio of stress to strain is a constant,

or . E is the slope of the line in this region where stress (σ) is proportional to strain (ε) and is
called the "Modulus of Elasticity" or "Young's Modulus."

Modulus of Elasticity
The modulus of elasticity is a measure of the material's stiffness which only applies in the initial
linear region of the curve. Within this linear region the tensile load can be removed from the

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specimen and the material will return to the exact same condition it had been in prior to the load
being applied. At the point when the curve is no longer linear and deviates from the straight-line
relationship, Hooke's Law no longer applies, and some permanent deformation occurs in the
specimen. This point is called the "elastic or proportional limit. From this point on in the tensile test,
the material reacts plastically to any further increase in load or stress. It will not return to its
original, unstressed condition if the load is removed.

Yield Strength
A material's "yield strength" is defined as the stress applied to the material at which plastic
deformation starts to occur.

PROCEDURE: -
• Measure the original length and diameter of the specimen.
• The length may either be length of gauge section which is marked on the specimen with a
preset punch or the total length of the specimen.
• Insert the specimen into grips of the test machine and attach strain-measuring device.
• Begin the load application and record load versus elongation data.
• Take readings more frequently as yield point is approached.
• Measure elongation values with the help of dividers and a ruler.
• Continue the test till Fracture occurs.
• By joining the two broken halves of the specimen together, measure the final length and
diameter of specimen.

OBESERVATION: -
Material: ……………………….
A) Original dimensions
Length = ------------
Diameter = ---------
Area = --------------
B) Final Dimensions:
Length = -------------------
Area = ------------------------
Diameter = -----------------

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1. Limit of proportion = . N/mm2

Load at limit of elastic limit

2. Elastic limit = Original area of cross section =……… N/mm2

Yield load
Load at limit of elastic limit
3.Yield strength = Original =……… N/mm2
Original area cross
area of section
of cross section
Maximum tensile load
4. Ultimate strength = =…. N/mm2
Original area of cross section

Stress below proportionality limit

5. Young’s modulus = Corresponding strain =……. N/mm2

Length at fracture – original length

6. Percentage elongation = original length ………%

Original area – area at fracture

7. percentage reduction in area = Original area …. %

RESULT: -
i) Average Breaking Stress =
ii) Ultimate Stress =
iii) Average % Elongation =

PRECAUTION:
• If the strain measuring device is an extensometer it should be removed before necking
begins.
• Measure deflection on scale accurately & carefully.

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 EXPERIMENT NO: - 02

AIM: - Hardness Test of Mild Steel.

OBJECT: - To conduct hardness test on mild steel, carbon steel, brass and aluminum specimens.
APPARATUS: - Hardness tester, soft and hard mild steel specimens, brass, aluminum etc.
DIAGRAM: -

Hardness Testing Machine

THEORY: -
Hardness is defined as the resistance of a material to permanent deformation such as indentation,
wear, abrasion, scratch. Principally, the importance of hardness testing has to do with the
relationship between hardness and other properties of material. For example, both the hardness test
and the tensile test measure the resistance of a metal to plastic flow, and results of these tests may
closely parallel each other. The hardness test is preferred because it is simple, easy, and relatively
nondestructive. There are many hardness tests currently in use. The necessity for all these different
hardness tests is due to the need for categorizing the great range of hardness from soft rubber to
hard ceramics.
The hardness of a material is resistance to penetration under a localized pressure or resistance to
abrasion. Hardness tests provide an accurate, rapid and economical way of determining the
resistance of materials to deformation. There are three general types of hardness measurements
depending upon the manner in which the test is conducted:

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 a. Scratch hardness measurement,
b. Rebound hardness measurement
c. Indention hardness measurement.
In scratch hardness method the material is rated on their ability to scratch one another and it is
usually used by mineralogists only. In rebound hardness measurement, a standard body is usually
dropped on to the material surface and the hardness is measured in terms of the height of its
rebound. The general means of judging the hardness is measuring the resistance of a material to
indentation. The indenters usually a ball cone or pyramid of a material much harder than that being
used. Hardened steel, sintered tungsten carbide or diamond indenters are generally used in
indentation tests; a load is applied by Pressing the indenter at right angles to the surface being
tested.
The hardness of the material depends on the resistance which it exerts during a small amount of
yielding or plastic. The resistance depends on friction, elasticity, viscosity and the intensity and
distribution of plastic strain produced by a given tool during indentation.

PROCEDURE: -
a) Rockwell Hardness Test
• Place the specimen securely upon the anvil of machine and the penetrator seated by means
of 10 kg minor load.
• The dial indicator is zeroed and then a major load of 60, 100, 150 kg is applied, forcing the
penetrator into the specimen.
• After the indicating pointer has come to the rest, the major load is removed
• After the major load removed, the pointer now indicates the Rockwell hardness number on
the appropriate scale of dial.
• The two commonest scales are the HRB and HRC scales, respectively standing for the 1/16-
inch ball with 100kg, and the diamond penetrator with the 150kg major load.

Scale Indenter Minor load kgf Major Load kgf Total Load kgf

A Diamond Cone 10 50 60
B 1/16 in. Steel ball 10 90 100
C Diamond Cone 10 140 150

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b) Brinell Hardness Test
 In this test hardened steel ball of 2.5 mm dia. is pressed into the surface of the specimen by a
gradually applied standard load 187.5 kg.
 The load is maintained for a specific time (10-30 sec.).
 The obtained impression is measured by a microscope and a Brinell hardness no(BHN) is
found out by the BHN equation.
 If the BHN is higher, then the material is said to the harder.

BHN = 2P/ПD[D-(D2-d2) (1/2)]

P= load applied on diameter in kg
D=Diameter of steel ball indenter in mm
d=Diameter of ball impression

OBESERVATION TABLE: -

Reading (HRC/HRB)
S.NO Specimens Mean
1 2 3

1 Mild Steel HRB =

2 High Carbon steel HRC =
3 Brass HRB =
4 Aluminum HRB =

Scales
• HRA for Cemented carbides, Thin steel and shallow case hardened steel
• HRB for copper alloys, aluminum alloys, malleable irons etc.
• HRC for steel, hard cast irons, case hardened steel and other material harder than 100 HRB.
RESULTS: - The hardness of the metal is found to be
1. Hard steel =
2. Unhardened steel =
PRECAUTION: -

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 Brinell test should be performed on smooth, flat specimens from which dirt and scale have
been cleaned.
 The test should not be made on specimens so thin that the impression shows through the
metal, nor should impression be made too close to the edge of a specimen.

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 EXPERIMENT No: - 03
AIM: - Torsion test on mild steel rod.
OBJECT: -To conduct torsion test on mild steel or cast iron specimens to find out modulus of
rigidity
APPARATUS: -
• A torsion testing machine.
• Twist meter for measuring angles of twist.
• A steel rule and Vernier Caliper or micrometer.
DIAGRAM:

Torsion testing apparatus and a specimen subjected to torque

THEORY: -
A torsion test is quite instrumental in determining the value of modulus of rigidity of a metallic
specimen. The value of modulus of rigidity can be found out thought observations made during the
experiment by using the torsion equation
T Cϴ q
= =
J L r

T = Torque Applied
C = Modulus of Rigidity
ϴ = Angle of Twist
I = Polar moment of Inertia
L = length of the shaft
q = shear stress
r = Distance of element from center of shaft
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PROCEDURE: -
• Select the size of the specimen and clamp it in the machine by adjusting the length of the
specimen by means of a sliding spindle.
• Measure the diameter at about three places and take the average value.
• Choose the appropriate range by capacity change lever.
• Set the maximum load pointer to zero.
• Set the protector to zero for convenience and clamp it.
• Load the machine in suitable increments.
• Plot a torque- twist (T- θ) graph.
• Read off co-ordinates of a convenient point from the straight line portion of the torque twist
(T- θ) graph and calculate the value of C by using relation.

OBSERVATIONS: -
Torque 1 2 3
Angle of twist (ϴ)in radians
Modulus of rigidity C in N/mm2

Gauge length of specimen l =…………………

Diameter of the specimen B = D =…………….

Polar moment of inertia Ip = BD3/12 =…...................

OBSERVATION TABLE: -
RESULTS: -
• Modulus of rigidity of mild steel rod is…. N/mm2.
PRECAUTION: -
• Measure the dimensions of the specimen carefully.
• Measure the Angle of twist accurately for the corresponding value of Torque.

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 EXPERIMENT No: - 04

AIM: - To study the Impact Testing m/c and Perform Izod and Charpy impact test.
APPARATUS: - Impact testing m/c, Izod and Charpy test specimens of mild steel, Aluminum,
Vernier caliper, specimen setting fixture.
THEORY: -
In manufacturing locomotive wheels, coins, connecting rods etc. the components are subjected to
impact (shock) loads. These loads are applied suddenly. The stress induced in these components
are many times more than the stress produced by gradual loading. Therefore, impact tests are
performed to determine shock absorbing capacity of materials subjected to suddenly applied
loads. These capabilities are expressed as (i) Rupture energy (ii) Modulus of rupture and (iii)
Notch impact strength.
Two types of notch impact tests are commonly-
1. Charpy test
2. Izod test
1. Izod test: -
In Izod test, the specimen is placed as ‘cantilever beam’. The specimens have V-shaped notch of
45°. The notch is located on tension side of specimen during impact loading. Depth of notch
is generally taken as t/5 to t/3 where ‘t’ is thickness of the specimen.
Specification of m/c and specimen details:
Its specifications along-with their typical values are as follows:
• Impact capacity = 164joule
• Weight of striking hammer = 18.7 kg.
• Angle of hammer before striking = 90°
• Distance between supports = 40mm.
• Striking velocity of hammer = 5.6m/sec.
• Specimen size = 75x10x10 mm.
• Type of notch = V-notch Angle of notch = 45°
• Depth of notch = 2 mm.
2. Charpy Test

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In charpy test, the specimen is placed as ‘horizontal beam’. The specimens have V-shaped notch of
45°. U-shaped notch is also common. The notch is located on tension side of specimen during
impact loading.
Specification of m/c and specimen details:
Its specifications along-with their typical values are as follows:
• Impact capacity = 300joule
• Weight of striking hammer = 18.7 kg.
• Angle of hammer before striking = 140°
• Distance between supports = 40mm.
• Striking velocity of hammer = 5.6m/sec.
• Specimen size = 55x10x10 mm.
• Type of notch = V-notch
• Angle of notch = 45°
• Depth of notch = 2 mm

DIAGRAM: -

Pendulum Impact Testing Machine

PROCEDURE: -
• Lift the hammer to an appropriate knife edge position and note the energy stored in the
hammer. For the standard Izod test the energy stored should be 164joule
• Locate the test specimen on the m/c supports.
• Release the hammer. The hammer will break the piece and shoot up the other side of the
specimen.
• Note the residual energy indicated on the scale by the hammer.

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 • Impact strength of the test specimen is the difference of the initial energy stored in
hammer and the residual energy.

OBSERVATION: -
S.No. Initial Energy (E1) Residual Energy (E2) in Absorb Energy (E1-E2)
in joule joule

CALCULATION: -
• Modulus of rupture = Rupture / Effective volume of specimen.
• Notch impact strength = Absorb energy / Effective cross section area
PRECAUTIONS: -
• The specimen should be prepared in proper dimensions.
• Take reading more frequently.
• Do not stand in front of swinging hammer or releasing hammer.
• Place the specimen proper position.

RESULT: - The impact strength of given specimen = ------ -joule/mm2.

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 EXPERIMENT NO: - 05

AIM: - To determined modulus of rupture of wooden beam simply supported at ends.

OBJECT: - To find the values of bending stresses and young’s modulus of elasticity of the material
of a beam simply supported at the ends and carrying a concentrated load at the center.

APPARATUS: -
• Deflection of beam apparatus
• Beam of different cross-sections and material (say wooden or Steel beams).

DIAGRAM: -

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THEORY: -
If a beam is simply supported at the ends and carries a concentrated load at its center, the beam
bends concave upwards. The distance between the original position of the beams and its position
after bending at different points along the length of the beam, being maximum at the center in this
case. This difference is known as ‘deflection’. In this particular type of loading the maximum
amount of deflection (δ) is given by the relation,

δ = W L3
48 EI ………… (i)

E = W L3
48 δ I ------------- (ii)

W =Load acting at the center, N

L =Length of the beam between the supports mm
E =Young’s modulus of material of the beam, N/mm2
I =Second moment of area of the cross- section (i.e., moment of
Inertia) of the beam, about the neutral axis, mm4.

BENDING STRESS:

As per bending equation, M/I = σb/Y

Where, M = Bending moment, N-mm

I = Moment of inertia, mm4
σb = Bending stress, N/mm2 and
Y = Distance of the top fiber of the beam from the neutral axis
PROCEDURE:
• Insert the bending device in the UTM.
• Measure the width and depth of wooden beam.
• Adjust the support for the required distance and clamp to the lower table.
• Fix the transverse test pan at the lower side of the lower cross head.
• Fix it on the rollers of the transverse test brackets such that the load comes at the center and
measure the length of the span of the beam between the supports for central loading.

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 • Adjust the load pointer to zero by lifting the lower table.
• While applying the load, the deflection corresponding to each load is found out from the
Vernier scale on the UTM.
• Note the maximum deflection and the maximum load.
• Find the deflection (δ) in each case by subtracting the initial reading of Vernier scale.
• Draw a graph between load (W) and deflection (δ). On the graph choose any two convenient
points and between these points find the corresponding values of W and δ by putting these in
the relation
δ = WL3/48EI

Calculate the bending stress for different loads using relation δb = My/I.

Observation Table
S. No. Load Deflection
1
2

Results: -
• The young’s modulus for steel beam is found to be----- N/mm2.
• The young’s modulus for wooden beam is found to be----- N/mm2
PRECAUTION: -
• Make sure that beam and load are placed a proper position.
• The cross- section of the beam should be large.
• Note down the readings of the Vernier scale carefully.

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 EXPERIMENT NO: - 06
AIM: - Spring Testing

OBJECT: -To determine the stiffness of the spring and modulus of rigidity of the spring wire
APPARATUS: -
Spring testing machine.
A spring
Vernier caliper,
Scale. Micrometer.
DIAGRAM: -

Closed Coiled Helical Spring

THEORY: - Springs are elastic member which distort under load and regain their original shape
when load is removed. They are used in railway carriages, motor cars, scooters, motorcycles,
rickshaws, governors etc. According to their uses the springs perform the following Functions:

1) To absorb shock or impact loading as in carriage springs.

2) To store energy as in clock springs.

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 3) To apply forces and to control motions as in brakes and clutches.
4) To measure forces as in spring balances.
5) To change the variations characteristic of a member as in flexible mounting of
motors
The spring is usually made of either high carbon steel (0.7 to 1.0%) or medium carbon alloy steels.
Phosphor bronze, brass, 18/8 stainless steel and Monel and other metal alloys are used for corrosion
resistance spring.
Several types of spring are available for different application. Springs have classified as helical
springs, leaf springs and flat spring depending upon their shape. They are fabricated of high shear
strength materials such as high carbon alloy steels spring form elements of not only mechanical
system but also structural system. In several cases it is essential to idealize complex structural
systems by suitable spring.

PROCEDURE:
 Measure the diameter of the wire of the spring by using the micrometer.
 Measure the diameter of spring coils by using the Vernier caliper.
 Count the number of turns.
 Insert the spring in the spring testing machine and load the spring by a suitable weight and
note the corresponding axial deflection in tension or compression.
 Increase the load and take the corresponding axial deflection readings.
 Plot a curve between load and deflection. The shape of the curve gives the stiffness of the
spring.

OBESERVATION
• Least count of micrometer =…. mm (Mean of three readings)
• Least count of Vernier caliper = …. Mm
• Diameter of the spring coil, D = ……mm (Mean of three readings)
• Mean coil diameter, Dm = D - d……mm
• Number of turns, n =

Observation Table: -

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 Load,W Deflection,(δ) Stiffness K = W / δ
S.NO
(N) (mm) N / mm

Mean k

Modulus of rigidity = 8wDm3/δd4

Spring index = Dm / D

RESULT: The value of spring constant k of closely coiled helical spring is found to be---------
--- N / mm.
PRECAUTION: -
• The dimension of spring was measured accurately.
• Deflection obtained in spring was measured accurate.

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 EXPERIMENT NO: - 07
AIM: - Compressive strength of brick

OBJECT: - The specimen brick is immersed in water for 24 hours. The frog of the brick is filled
with mortar to before testing for compressive Strength.

APPARATUS: Bricks, Oven, Vernier Caliper, Scale etc.

THEORY: -
Bricks are used in construction of either load bearing walls or in portion walls of frame structure. In
bearing walls total weight from slab and upper floor comes directly through brick and then it is
transfered to the foundation. In case of bearing walls the bricks are loaded with compressive nature
of force on other hand in case of frame structure bricks are used only for construction of partition
walls, layers come directly on the lower layers’ bricks. Hence for safety measures before using the
bricks in actual practice they have to be tested in laboratory for their compressive strength.

PROCEDURE: -
• Select some brick with uniform shape and size.
• Measure it’s all dimensions. (L * B * H).
• Now fill the frog of the brick with fine sand.
• Place the brick on the lower platform of compression testing machine and switch on the
motor which will lift the load cell and will compress the specimen.

OBSERVATION TABLE: -
S.No. L*B*H Area Load (N) Compressive Average
Cm3 LXB (P) Strength Compressive
Cm2 P/A(N/mm2) Strength
1
2
3

Compressive strength of brick = Maximum load at failure

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 Loaded area of brick
RESULTS: - The compressive strength of the brick is …… N/mm2.

PRECAUTIONS: -
• Measure the dimensions of Brick accurately.
• Specimen should be placed as for as possible in the of lower plate.
• The range of the gauge fitted on the machine should not be more than double the breaking
load of specimen for reliable results.

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 EXPERIMENT NO: - 08

AIM: - To Perform compression test of mild steel and cast iron on UTM.

APPARATUS: - A UTM or A compression testing m/c, cylindrical or cube shaped specimen of

cast iron or mild steel, Vernier caliper, liner scale, dial gauge (or compress meter).

THEORY: - Several m/c and structure components such as columns and struts are subjected to
compressive load in applications. These components are made of high compressive strength
materials. Not all the materials are strong in compression. Several materials, which are good in
tension, are poor in compression. Contrary to this, many materials poor in tension but very strong
in compression. Cast iron is one such example. That is why determine of ultimate compressive
strength is essential before using a material. This strength is determined by conduct of a
compression test.
Compression test is just opposite in nature to tensile test. Nature of deformation and fracture is
quite different from that in tensile test. Compressive load tends to squeeze the specimen. Brittle
materials are generally weak in tension but strong in compression. Hence this test is normally
performed on cast iron, cement concrete etc. But ductile materials like aluminum and mild steel
which are strong in tension, are also tested in compression.

TEST SET-UP, SPECIFICATION OF M/C AND SPECIMEN DETAILS:

A compression test can be performed on UTM by keeping the test-piece on base block and
moving down the central grip to apply load. It can also be performed on a compression testing
machine. A compression testing machine shown in figure, it has two compression plates/heads.
The upper head moveable while the lower head is stationary. One of the two heads is equipped
with a hemispherical bearing to obtain. Uniform distribution of load over the test-piece ends. A
load gauge is fitted for recording the applied load.

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SPECIMEN: -
In cylindrical specimen, it is essential to keep h/d ≤ 2 to avoid lateral instability due to
bucking action. Specimen size = h ≤ 2d.
PROCEDURE: -
• Dimension of test piece is measured at three different places along its height/length
to determine the average cross-section area.
• Ends of the specimen should be plane for that the ends are tested on a bearing plate.
• The specimen is placed centrally between the two compression plates, such that the centre
of moving head is vertically above the centre of specimen.

• Load is applied on the specimen by moving the movable head. The load and corresponding
contraction are measured at different intervals. The load interval may be as 500 kg.

• Load is applied until the specimen fails.

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 OBSERVATION: -
• Initial length or height of specimen h = ------mm.
• Initial diameter of specimen do = -------------mm.

S.No. Applied load (P) in Newton Recorded change in length (mm)

CALCULATION: -
• Original cross-section area Ao = -----
• Final cross-section area Af = --------
• Stress = -------
• Strain = -------
For compression test, we can
• Draw stress-strain (σ-ε) curve in compression,
• Determine Young’s modulus in compression,
• Determine ultimate (max.) compressive strength, and
• Determine percentage reduction in length (or height) to the specimen.

PRECAUTIONS: -
• The specimen should be prepared in proper dimensions.
• The specimen should be properly to get between the compression plates.
• Take reading carefully.
• After failed specimen stop to m/c.

RESULT: - The compressive strength of given specimen = -------N/mm2.

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 EXPERMENT NO: - 09

OBJECTIVE: - To determine the fatigue (endurance) limit for steel using a rotating beam fatigue
testing machine. i.e. effects of reversed and repeated cyclic bending.

Note: Since each test must run for hours or days, the data will be collected over the entire semester.
During each lab session, a sample will be left running to be removed and recorded during the next
lab session.

APPARATUS: Fatigue testing machine, standard test specimen.

THEORY: -
In many applications, materials are subjected to vibrating or oscillating forces. The behavior of
materials under such load conditions differs from the behavior under a static load. Because the
material is subjected to repeated load cycles (fatigue) in actual use, designers are faced with
predicting fatigue life, which is defined as the total number of cycles to failure under specified
loading conditions. Fatigue testing gives much better data to predict the in-service life of materials.

A steel specimen is subjected to a rotating pure bending stress. It will fail at a stress much lower
than ultimate (tensile) strength of material. This failure is due to the repeated cycle of stresses from
the maximum to the minimum in bending. By increasing the bending load, failure will occur at
fewer bending cycles. On the S-N plot (stress vs cycles to failure) plot A materials exhibit a fatigue
(endurance) limit – the stress below which the material will never fail. Plot B materials never reach
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a fatigue limit so they are given a fatigue strength – the stress for 5x107 cycles (about 20 days at
1820rpm).

DIAGRAM: -

SPECIMEN: -

PROCEDURE: -
• Install the specimen in the machine as per directions.
• Start the machine then apply the load.
• Record the start reading on the timer (hr.).
• After the specimen has failed, record the end timer reading.
• Repeat the above procedure several times at different loads.
• The machine can run unattended. It will shut itself off upon specimen failure.
In a spreadsheet, calculate the stress and cycles to failure for each load. On a semi-log graph, plot
the stress vs. cycles to failure and add a power trend line. Determine the fatigue limit and compare
the experimental fatigue limit with the estimated fatigue limit. Report the endurance ratio.
OBSERVATIONS: -

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 S.No. Load(kg) No. of cycles

RESULTS: - The fatigue limit of the test specimen is ……

28 | P a g e MT Lab CC-D.S.Dhaka
 EXPERIMENT NO: - 10

(A) AIM: To determine the compressive strength of standard cement mortar cubes compacted
by means of standard vibration machine.

APPARATUS: Vibration machine, compression testing machine and cube moulds of size
7.06 cm.

STANDARD SAND: The standard sand to be used in the test shall conform to IS: 650-1991 or
sand passing 100 percent through 2 mm sieve and retained 100 percent on 90 microns IS sieve.

2mm to 1mm 33.33 percent

1mm to 500 microns 33.33 percent
500mm to 90 microns 33.33 percent.

INTRODUCTION: The compressive strength of cement mortars is determined in order to

verify whether the cement conforms to IS specifications and whether it will be able to develop
the required compressive strength of concrete. The average compressive strength of at least three
mortar cubes (area of the face 50 cm2) composed of one part of cement and three parts of standard
stand should satisfy IS code specifications.

PROCEDURE:
Mix proportions and mixing:
1. Clean appliances shall be used for mixing and the temperature of the water and that of the

test room at the time when the above operations are being performed shall be 27 + 2oC.
2. Place in a container a mixture of cement and standard sand in the proportion of 1:3 by
weight mix it dry, with a trowel for one minute and then with water until the mixture is of
uniform color.
3. The quantity of water to be used shall be as specified below.
4. In any element, it should not take more than 4 minutes to obtain uniform colored mix.
5. If it exceeds 4 minutes the mixture shall be rejected and the operation repeated with a
fresh quantity of cement, sand and water.

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 6. The material for each cube shall be mixed separately and the quantity of cement standard
sand and water shall be as follows:
Cement 200 grams
Standard sand 600 grams
Water (P/4 + 3.0) percent of combined weight of cement and
sand, where p is the percentage of water required to produce a paste of standard
consistency.

MOULDING SPECIMENS:
1. In assembling the moulds ready for use, cover the joints between the halves of the mould
with a thin film of petroleum jelly and apply a similar coating of petroleum jelly between
the contact surfaces of the bottom of the mould and its base plate in order to ensure that
no water escapes during vibration.
2. Treat the interior faces of the mould with a thin coating of mould oil.
3. Place the assembled mould on the table of the vibration machine and firmly hold it is
position by means of suitable clamps.
4. Securely attach a hopper of suitable size and shape at the top of the mould to facilitate
filling and this hopper shall not be removed until completion of the vibration period.
5. Immediately after mixing the mortar, place the mortar in the cube mould and rod with a
rod.
6. The mortar shall be rodded 20 times in about 8 seconds to ensure elimination of entrained
air and honey combing.
7. Place the remaining quantity of mortar in the hopper of the cube mould and rod again as
specified for the first layer and then compact the mortar by vibrations.
8. The period of vibration shall be two minutes at the specified speed of 12,000 + 400
vibrations per minute.
9. At the end of vibration remove the mould together with the base plate from the machine
and finish the top surface of the cube in the mould by smoothing surface with the blade of
a trowel.
CURING SPECIMEN:

1. Keep the filled moulds at a temperature of 27 + 20 C in an atmosphere of at least 90 %

relative humidity for about 24 hours after completion of vibration.
2. At the end of that period remove them from the moulds.
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 3. Immediately submerge in clean fresh water and keep them under water until testing.
4. The water in which the cubes are submerged shall be renewed every 7 days and shall be

maintained at a temperature of 27 0C + 20C.

5. After they have been taken out and until they are tested the cubes shall not be allowed to
become dry.

TESTING:
1. Test three cubes for compressive strength at the periods mentioned under the relevant
specification for different hydraulic cements, the periods being reckoned from the
completion of vibration.
2. The compressive strength shall be the average of the strengths of three cubes for each
period of curing.
3. The cubes shall be tested on their sides without any packing between the cube and the
steel platens of the testing machine.
4. One of the platens shall be carried base and shall be self-adjusting and the load shall be
steadily and uniformly applied starting from zero at a rate of 350 Kgs/Cm2/ min.
The cubes are tested at the following periods
Ordinary portland cement 3, 7 and 28 days.
Rapid hardening portland cement 1 and 3 days.
Low heat portland cement 3 and 7 days.

CALCULATION:
Calculate the compressive strength from the crushing load and the average area over which the
load is applied. Express the results in N/mm2 to the nearest 0.05 mm2.
Compressive strength in N/mm2 = P/A =Where P is the crushing load in N
and A is the area in mm2 (5000 mm2)
PRECAUTIONS: Inside of the cube moulds, should be oiled to prevent the mortar from
adhering to the sides of the mould.

RESULT: The average compressive strength of the given cement

at 3 days N/mm2
at 7 days N/mm2
at 28 days N/mm2
31 | P a g e MT Lab CC-D.S.Dhaka
 (B) OBJECT: Determination of the compressive strength of cement concrete
specimens.

APPARATUS: Compression Testing Machine, two steel bearing platens with hardened faces
(As per IS: 516 - 1959).

Compression Testing Machine

THEORY:
Tests shall be made at recognized ages of the test specimens, the most usual being 7 and 28 days,
ages of 13 weeks and one year are recommended if tests at greater ages are required. Where
it may be necessary to obtain the early strength, test may be made at the ages of 24 hours + 1/2
hour and 12 hours + 2 hours. The ages shall be calculated from the time of the addition of water to
the dry ingredients.

Number of Specimens
At least three specimens, preferably from different batches, shall be made for testing at each
selected age.

PROCEDURE:
Specimens stored in water shall be tested immediately on removal from water and while they are
still in the wet condition. Surface water and grit shall be wiped off the specimens and any

32 | P a g e MT Lab CC-D.S.Dhaka
 projecting fines removed. Specimens when received dry shall be kept in water for 24 hours before
they are taken for testing. The dimensions of the specimens to the nearest 0.2 mm and their weight
shall be noted before testing.
Placing the specimen in the Testing Machine The bearing surfaces of the testing machine shall be
wiped clean and any loose sand or other material removed from the surfaces of the specimens
which are to be in contact with the compression platens. In the case of the cubes, the specimen shall
be placed in the machine in such a manner that the load shall be applied to opposite sides of the
cubes as cast, that is, not to the top and bottom. The axis of the specimen shall be carefully aligned
with the center of thrust of the spherically seated platen. No packing shall be used between the faces
of the test specimen and the steel platen of the testing machine. As the spherically seated block is
brought to bear on the specimen, that movable portion shall be rotated gently by hand so that
uniform section may be obtained. The load shall be applied without shock and increased
continuously at a rate of approximately 140 Kg/sq cm/min. Until the resistance of the specimen to
the increasing load breaks down and no greater load can be sustained. The maximum load applied
to the specimen shall then be recorded and the appearance of the concrete and any unusual features
in the type of failure shall be noted.

CALCULATION: The measured compressive strength of the specimen shall be calculated by

dividing the maximum load applied to the specimen during the test, by the cross sectional area,
calculated from the mean dimensions of section and shall be expressed to the nearest Kg/sq.cm.
Average of three values shall be taken as the representative of the batch provided the individual
variation is not more than + 15% of the average. Otherwise, repeat tests shall be made.
In case of cylinders, a correction factor according to the height to diameter ratio of specimen
after capping shall be obtained from the curve shown in fig. 1 of IS: 516-1959. The product of
this correction factor and the measured compressive strength shall be known as the corrected
compressive strength, this being the equivalent strength of a cylinder having a height/diameter
ratio of two. The equivalent cube strength of the concrete shall be determined by multiplying the
corrected cylinder strength by 5/4.
RESULT: Compressive strength of Concrete --------------

33 | P a g e MT Lab CC-D.S.Dhaka