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Design Steps

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Important Conditions

 Pressure of the column.

 Temperature of entering liquid and gas streams.

 Humidity of the gas stream.

 Ratio of the liquid and gas stream rates.

General Design Steps


1. Entering gas (liquid) flowrate, composition, temperature, and pressure

2. Desired degree of recovery of one or more solutes

3. Choice of absorbent/(stripping agent)

4. Operating pressure and temperature

5. Number of equilibrium stages

6. Heat effects and need for cooling

7. Type of absorber (stripper)

8. Height of absorber (stripper)

9. Diameter of absorber (stripper)

10 Costing
Packed Column Design (Absorber/Stripper)
1. Entering gas (liquid) flow rate, composition, temperature, and pressure

Set from the preceding unit operation.

2. Desired degree of recovery of one or more solutes

 set by the designer.

 It may be a recovery to ensure product purity requirements

 To satisfy a purity requirement if the recovered solute is a feed stream to another unit.

3. Choice of absorbent/(stripping agent)

Ideal absorbent should:

 have a high solubility for the solute(s)

 have a low volatility to reduce loss of absorbent

 be noncorrosive

 have a low viscosity to provide a low pressure drop

 be nontoxic

 be available and not expensive

4. Operating pressure and temperature

In general , operating pressure should be high and temperature low for an absorber, to
minimize:

 stage requirements

 absorbent flow rate

 the equipment volume required to accommodate the gas flow


5. Number of equilibrium stages

Nt= [ln [(1-A-1)(y1-y2°)/(y2-y2°)+A-1]] / ln (A)

where A absorption factor = L'/mG'

y1 mole fraction of solute in entering gas

y2 mole fraction of solute in exiting gas

y2° mole fraction of solute in equilibrium with


incoming

E = Nt / Na

Where E stage efficiency

Na actual number of stages

Nt theoretical number stages

6. Heat effects and need for cooling

 the heat of solution of the solute

 the heat of vaporization or condensation of the solvent

 the change of the sensible heat between the gas and the liquid phases

 the loss of sensible heat form the fluids to internal and external cooling coils or to the
atmosphere via the tower walls

They direct whether the temperature along the absorber/stripper temperature will change or
not.
7. Type of absorber (stripper)

Absorption and stripping are frequently conducted in packed columns, particularly when:

 the required column diameter is less than 2 ft;

 the pressure drop must be low, as for a vacuum service

 Corrosion considerations favor the use of ceramic or polymeric materials

 Low liquid holdup is desirable.

8. Height of absorber (stripper)

Height of the column is based on the

 number of trays

 tray spacing

 The end lengths to allow the vapor and liquid to disengage(10 ft or 15 % extra)

H (ft) = S N + end length

9. Diameter of
absorber (stripper)

Packing Selection

Generally, the
column diameter to
packing size ratio
should be greater
than :

 30 for Raschig rings,

 15 for ceramic
saddles,
 10 for rings or plastic saddles. 

Calculate Gas flux against Selected Pressure Drop

Absorbers and Strippers = 0.2 to 0.6 in water / ft packing


                                      = 16 to 48 mm water / m packing

 Ax = Vapor Flow / G

 Diameter = [Ax / (PI/4)]0.5

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