An American National Standard

Designation: D 287 – 92 (Reapproved 2006)

Standard Test Method for

API Gravity of Crude Petroleum and Petroleum Products
(Hydrometer Method)1
This standard is issued under the fixed designation D 287; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense. This test method has been adopted for use by
government agencies to replace Method 401 of Federal Test Method Standard No. 791b.

1. Scope E 1 Specification for ASTM Liquid-in-Glass Thermometers

1.1 This test method covers the determination by means of E 100 Specification for ASTM Hydrometers
a glass hydrometer of the API gravity of crude petroleum and 2.2 IP Standards:3
petroleum products normally handled as liquids and having a Specifications for IP Standard Thermometers
Reid vapor pressure (Test Method D 323) of 26 psi (180 kPa) IP Specifications for Petroleum Hydrometers
or less. Gravities are determined at 60°F (15.56°C), or con- 3. Terminology
verted to values at 60°F, by means of standard tables. These
tables are not applicable to nonhydrocarbons or essentially 3.1 Definitions:
pure hydrocarbons such as the aromatics. 3.1.1 API gravity—a special function of relative density
(specific gravity) 60/60°F (15.56/15.56°C), represented by:
NOTE 1—The international version of this test method is described in
Test Method D 1298. API gravity, deg 5 ~141.5/sp gr 60/60°F! 2 131.5 (1)

1.2 The values stated in inch-pound units are to be regarded No statement of reference temperature is required, since
as standard. The values given in parentheses are mathematical 60°F is included in the definition.
conversions to SI units that are provided for information only 4. Summary of Test Method
and are not considered standard.
1.3 This standard does not purport to address all of the 4.1 This test method is based on the principle that the
safety concerns, if any, associated with its use. It is the gravity of a liquid varies directly with the depth of immersion
responsibility of the user of this standard to establish appro- of a body floating in it. The floating body, which is graduated
priate safety and health practices and determine the applica- by API gravity units in this method, is called an API hydrom-
bility of regulatory limitations prior to use. For specific hazard eter.
statements, see 8.3. 4.2 The API gravity is read by observing the freely floating
API hydrometer and noting the graduation nearest to the
2. Referenced Documents apparent intersection of the horizontal plane surface of the
2.1 ASTM Standards: 2 liquid with the vertical scale of the hydrometer, after tempera-
D 323 Test Method for Vapor Pressure of Petroleum Prod- ture equilibrium has been reached. The temperature of the
ucts (Reid Method) sample is read from a separate accurate ASTM thermometer in
D 1250 Guide for Use of the Petroleum Measurement the sample or from the thermometer which is an integral part of
Tables the hydrometer (thermohydrometer).
D 1298 Test Method for Density, Relative Density (Specific 5. Significance and Use
Gravity), or API Gravity of Crude Petroleum and Liquid
Petroleum Products by Hydrometer Method 5.1 Accurate determination of the gravity of petroleum and
its products is necessary for the conversion of measured
volumes to volumes at the standard temperature of 60°F
(15.56°C).
1
This test method is under the jurisdiction of ASTM Committee D02 on 5.2 Gravity is a factor governing the quality of crude oils.
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D02.02.0A on Temperature, Density, Physical Properties.
However, the gravity of a petroleum product is an uncertain
Current edition approved May 1, 2006. Published June 2006. Originally indication of its quality. Correlated with other properties,
approved in 1928. Last previous edition approved in 2000 as D 287 – 92 (2000)e1.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from the Institute of Petroleum, 61 New Cavendish St., London
the ASTM website. WIM, 8AR, England.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

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 D 287 – 92 (2006)
gravity can be used to give approximate hydrocarbon compo- they have collected on the surface of the sample, by touching
sition and heat of combustion. them with a piece of clean filter paper before inserting the
hydrometer. For field testing, make the gravity measurement
6. Apparatus directly in the sampling thief. Place the cylinder containing the
6.1 Hydrometers, of glass, graduated in degrees API as sample in a vertical position in a location free from air currents.
listed in Table 1 and conforming to Specification E 100, or the Take precautions to prevent the temperature of the sample from
IP Specifications for Petroleum Hydrometers. changing appreciably during the time necessary to complete
6.2 Thermometers, having a range from −5 to +215°F and the test. During this period, the temperature of the surrounding
conforming to the requirements for Thermometer 12F as medium should not change more than 5°F (2°C).
prescribed in Specification E 1 or Thermometer 64F of the 8.4 Lower the hydrometer gently into the sample and, when
Specifications for IP Standard Thermometers. A thermometer is it has settled, depress it about two scale divisions into the liquid
not required if a thermohydrometer is employed. and then release it; keep the rest of the stem dry, as unnecessary
NOTE 2—The ASTM Gravity Thermometer 12F has 0.5°F subdivisions liquid on the stem changes the effective weight of the instru-
and allowable 60.25°F scale error. The thermometers incorporated in ment, and so affects the reading obtained. With samples of low
thermohydrometers have 2°F subdivisions and allowable 61°F scale viscosity, a slight spin imparted to the instrument on releasing
error. assists in bringing it to rest, floating freely away from the walls
6.3 Hydrometer Cylinders, of metal, clear glass, or plastic. of the hydrometer cylinder. Allow sufficient time for the
For convenience in pouring, the cylinder may have a lip on the hydrometer to become completely stationary and for all air
rim. The inside diameter of the cylinder shall be at least 25 mm bubbles to come to the surface. This is particularly necessary in
greater than the outside diameter of the hydrometer used in it. the case of the more viscous samples.
The height of the cylinder shall be such that the length of the 8.5 When the hydrometer has come to rest, floating freely,
column of sample it contains is greater by at least 25 mm than and the temperature of the sample is constant to 0.2°F (0.1°C),
the portion of the hydrometer which is immersed beneath the read the hydrometer to the nearest scale division. The correct
surface of the sample. For field testing, a sampling thief of reading is that point on the hydrometer scale at which the
suitable dimensions may be used. surface of the liquid cuts the scale. Determine this point by
placing the eye slightly below the level of the liquid and slowly
7. Temperature of Test raising it until the surface, first seen as a distorted ellipse,
7.1 The gravity determined by the hydrometer method is appears to become a straight line cutting the hydrometer scale.
most accurate at or near the standard temperature of 60°F 8.6 To make a reading with nontransparent liquids, observe
(15.56°C). Use this or any other temperature between 0 and the point on the hydrometer scale to which the sample rises
195°F (−18 and + 90°C) for the test, so far as it is consistent above its main surface, placing the eye slightly above the plane
with the type of sample and necessary limiting conditions surface of the liquid. This reading requires a correction.
shown in Table 2. Determine this correction for the particular hydrometer in use
by observing the height above the main surface of the liquid to
8. Procedure which the sample rises on the hydrometer scale when the
8.1 For referee testing, use the long plain form of hydrom- hydrometer in question is immersed in a transparent liquid
eter (1H to 10H). For field testing, use the thermohydrometer. having a surface tension similar to that of a sample under test.
8.2 Adjust the temperature of the sample in accordance with 8.7 Observe the temperature of the sample to the nearest
Table 2. For field testing, test temperatures other than those 0.25°F (0.1°C) immediately before and after the observation of
listed in Table 2 may be used. The hydrometer cylinder shall be the gravity, the liquid in the cylinder being thoroughly but
approximately the same temperature as the sample to be tested. cautiously stirred with the thermometer (Note 3), and the
8.3 Transfer the sample into the clean hydrometer cylinder whole of the mercury thread being immersed. Should these
without splashing, so as to avoid the formation of air bubbles temperature readings differ by more than 1°F (0.5°C), repeat
and to reduce to a minimum the evaporation of the lower the temperature and gravity observations when the temperature
boiling constituents of the more volatile samples. (Warning— of the sample has become more stable. Record the mean of the
Extremely flammable. Vapors may cause flash fire.) For the thermometer reading before and after the final hydrometer
more volatile samples, transfer to the hydrometer cylinder by reading, to the nearest 1°F, as the temperature of the test.
siphoning. (Warning—Do not start the siphon by mouth.) Use
a rubber aspirator bulb. Remove any air bubbles formed, after NOTE 3—When thermohydrometers are used, stir the sample by care-
fully raising and lowering the hydrometer. It is satisfactory in this case to
read the thermometer scale after the hydrometer reading has been
TABLE 1 Available Hydrometers Scaled, Degrees API observed. Read the thermometer to the nearest 1°F (0.5°C).
API Range, deg Scale
Designation Type
Series Total Each Unit Division Error 9. Calculation
1H to 10H long plain −1 to 101 12 0.1 0.1 9.1 When gravities have been observed on opaque liquids
21H to 40H short plain 0 to 101 6 0.1 0.2 using the procedure given in 8.6, subtract the correction from
51H to 60H thermo −1 to 101 12 0.1 0.1
71H to 74H thermo −1 to 41 12 0.1 0.1 the hydrometer reading observed.
A
thermo 15 to 51 8 9.2 Correct all hydrometer readings to 60°F (15.56°C),
A
Eight-degree range thermohydrometers are available. using Tables 5A or Tables 5B of Guide D 1250.

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 D 287 – 92 (2006)
TABLE 2 Limiting Conditions and Testing Temperatures
Initial Boiling Point
Sample Type Gravity Limits Other Limits Test Temperature
Limits
Highly volatile lighter than 70° API Cool to 35°F (2°C) or lower in original closed
container.
Moderately volatile heavier than 70° API below 250°F (120°C) Cool to 65°F (18°C) or lower in original closed
container.
Moderately volatile and viscous heavier than 70° API below 250°F (120°C) Viscosity too high Heat to minimum temperature for sufficient
at 65°F (18°C) fluidity.
Nonvolatile heavier than 70° API above 250°F (120°C) Any temperature between 0 and 195°F (−18
and 90°C) as convenient.
Mixtures of nonpetroleum prod- 60 6 0.25°F (15.56 6 0.1°C)
ucts or essentially pure hy-
drocarbons

10. Report 11.1.2 Reproducibility—The difference between two single

10.1 Report the corrected hydrometer reading as degrees and independent results, obtained by different operators, work-
API (°API) or as API Gravity. ing in different laboratories on identical test material, would in
the long run, in the normal and correct operation of the test
11. Precision and Bias method, exceed 0.5° API only in one case in twenty.
11.1 The precision of this test method as obtained by NOTE 4—The precision for this method was not obtained in accordance
statistical examination of interlaboratory test results is as with RR: D02-1007.
follows: NOTE 5—This precision statement applies only to measurements made
11.1.1 Repeatability—The difference between successive at temperatures differing from 60°F (15.56°C) by less than 18°F (10°C).
test results obtained by the same operator with the same 11.2 Bias—Bias for this method has not been determined.
apparatus under constant operating conditions on identical test
material, would in the long run, in the normal and correct 12. Keywords
operation of the test method, exceed 0.2° API only in one case 12.1 API gravity; crude petroleum; hydrometer; thermohy-
in twenty. drometer; thermometer

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