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Mil PRF 85570e

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NOT MEASUREMENT
SENSITIVE

MIL-PRF-85570E
27 March 2012
SUPERSEDING
MIL-PRF-85570D
19 June 2002

PERFORMANCE SPECIFICATION

CLEANING COMPOUNDS, AIRCRAFT, EXTERIOR

This specification is approved for use by all Departments and Agencies of the Department
of Defense.

1. SCOPE

1.1 Scope. The cleaning compounds covered by this specification are used for cleaning the
exterior surface of aircraft.

1.2 Classification. The cleaning compounds covered by this specification are furnished in
the following types (see 6.2):

Type I - General purpose, aromatic solvent base


Type IA - General purpose, aromatic solvent base, aerosol
Type IW - General purpose, aromatic solvent base, pre-saturated wipe
Type II - General purpose, non-solvent
Type II RTU - General purpose, non-solvent, ready to use (RTU)
Type III - Abrasive spot cleaner
Type IV - Rubberized spot cleaner
Type V - Gel-type wheel well degreaser, low solvent (less than 10 percent)

Comments, suggestions, or questions on this document should be addressed to: Commander,


Naval Air Warfare Center Aircraft Division, Code 4L8000B120-3, Highway 547, Lakehurst, NJ
08733-5100 or emailed to michael.sikora@navy.mil. Since contact information can change, you
may want to verify the currency of this address information using the ASSIST Online database at
https://assist.daps.dla.mil.

AMSC N/A FSC 6850


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MIL-PRF-85570E

2. APPLICABLE DOCUMENTS

2.1 General. The documents listed in this section are specified in sections 3 and 4 of this
specification. This section does not include documents cited in other sections of this
specification or recommended for additional information or as examples. While every effort has
been made to ensure the completeness of this list, document users are cautioned that they must
meet all specified requirements of documents cited in sections 3 and 4 of this specification,
whether or not they are listed.

2.2 Government documents.

2.2.1 Specifications and standards. The following specifications and standards form a part
of this document to the extent specified herein. Unless otherwise specified, the issues of these
documents are those cited in the solicitation or contract.

FEDERAL STANDARDS

FED-STD-595 - Colors Used in Government Procurement/


FED-STD-595 Color Numbers 17875, 36440, and 36495

DEPARTMENT OF DEFENSE SPECIFICATIONS

MIL-C-1164 - Cloth, Terry, Cotton, Cotton and Polyester


MIL-G-21164 - Grease, Molybdenum Disulfide, for Low and High
Temperatures, NATO Code Number G-353
MIL-PRF-23377 - Primer Coatings: Epoxy, High Solids
MIL-W-81381/11 - Wire, Electric, Fluorocarbon/Polyimide Insulated, Medium
Weight, Silver Coated Copper Conductor, 600 Volts, 200
DEG C, NOMINAL 8.4 or 15.4 Mil Wall
MIL-PRF-83282 - Hydraulic Fluid, Fire Resistant, Synthetic Hydrocarbon Base,
Aircraft, Metric, NATO Code Number H-537
MIL-PRF-85285 - Coating, Polyurethane, High-Solids, Aircraft and Support
Equipment

(Copies of these documents are available online at https://assist.daps.dla.mil/quicksearch/


or https://assist.daps.dla.mil or from the Standardization Document Order Desk, 700 Robbins
Avenue, Building 4D, Philadelphia, PA 19111-5094.)

2.2.2 Other Government documents, drawings, and publications. The following other
Government documents, drawings, and publications form a part of this document to the extent
specified herein. Unless otherwise specified, the issues of these documents are those cited in the
solicitation or contract.

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CODE OF FEDERAL REGULATIONS

29 CFR 1910.1200 - Occupational Safety and Health Standards - Hazard


Communications
40 CFR - Protection of Environment
40 CFR 796.3100 - Aerobic Aquatic Biodegradation

(Copies of these documents are available online at http://www.gpoaccess.gov or from the


Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402.)

NAVAL AIR SYSTEMS COMMAND

NAVAIR 01-1A-509 - Aircraft Weapons Systems Cleaning and Corrosion Control

(This document has limited distribution. Requests for copies by U.S. Government agencies and
their contractors should be made to the Naval Air Systems Command, Code 4.3.4.2, Unit 5,
Building 2188, 48066 Shaw Road, Patuxent River, MD 20670.)

2.3 Non-Government publications. The following documents form a part of this document
to the extent specified herein. Unless otherwise specified, the issues of these documents are
those cited in the solicitation or contract.

ASTM INTERNATIONAL

ASTM D93 - Standard Test Methods for Flash Point by Pensky-Martens Closed
Cup Tester. (DoD Adopted)
ASTM D95 - Standard Test Method for Water in Petroleum Products and
Bituminous Materials by Distillation. (DoD Adopted)
ASTM D523 - Standard Practice for Specular Gloss. (DoD Adopted)
ASTM D1141 - Standard Practice for the Preparation of Substitute Ocean Water.
(DoD Adopted)
ASTM D3065 - Standard Test Methods for Flammability of Aerosol Products
ASTM E70 - Standard Test Method for pH of Aqueous Solutions with the Glass
Electrode. (DoD Adopted)
ASTM E168 - Standard Practices For General Techniques of Infrared
Quantitative Analysis. (DoD Adopted)
ASTM F483 - Standard Practice for Total Immersion Corrosion Test for Aircraft
Maintenance Chemicals. (DoD Adopted)
ASTM F484 - Standard Test Method for Stress Crazing of Acrylic Plastics in
Contact with Liquid or Semi-liquid Compounds. (DoD Adopted)
ASTM F485 - Standard Test Method For Effects of Cleaners on Unpainted
Aircraft Surfaces
ASTM F502 - Standard Test Method for Effects of Cleaning and Chemical
Maintenance Materials on Painted Aircraft Surfaces. (DoD
Adopted)
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MIL-PRF-85570E

ASTM F519 - Standard Test Method for Mechanical Hydrogen Embrittlement


Evaluation of Plating/Coating Processes and Service
Environments. (DoD Adopted)
ASTM F1104 - Standard Test Method for Preparing Aircraft Cleaning
Compounds, Liquid type, Water Base, for Storage Stability Testing
ASTM F1110 - Standard Test Method for Sandwich Corrosion Test. (DoD
Adopted)
ASTM F1111 - Standard Test Method for Corrosion of Low-Embrittling Cadmium
Plate by Aircraft Maintenance Chemicals. (DoD Adopted)
(Copies of these documents are available from www.astm.org or ASTM International, 100 Barr
Harbor Drive, West Conshohocken, PA 19428-2959.)
SAE INTERNATIONAL

SAE AMS4377 - Sheet and Plate, Magnesium Alloy, 3.0Al - 1.0Zn –


0.20Mn (AZ31B-H24) Cold Rolled, Partially Annealed -
UNSM11311. (DoD Adopted)
SAE AMS4911 - Titanium Alloy, Sheet, Strip, and Plate 6Al - 4V Annealed
- UNSR56400. (DoD Adopted)
SAE AMS5046 - Sheet Strip and Plate, Carbon Steel (SAE 1020 and
1025), Annealed. (DoD Adopted)
SAE AMS-M-3171 - Magnesium Alloy, Processes for Pretreatment and
Prevention of Corrosion on. (DoD Adopted)
SAE AMS-QQ-A-250/4 - Aluminum Alloy 2024, Plate and Sheet. (DoD Adopted)
SAE AMS-QQ-A-250/12 - Aluminum Alloy 7075, Plate and Sheet. (DoD Adopted)
(Copies of these documents are available from http://www.sae.org or from SAE International,
400 Commonwealth Drive, Warrendale, PA 15096-0001.)
2.4 Order of precedence. Unless otherwise noted herein or in the contract, in the event of a
conflict between the text of this document and the references cited herein, the text of this
document takes precedence. Nothing in this document, however, supersedes applicable laws and
regulations unless a specific exemption has been obtained.

3. REQUIREMENTS

3.1 Qualification. The cleaning compounds furnished under this specification shall be
products that are authorized by the qualifying activity for listing on the applicable qualified
products list before contract award (see 4.3 and 6.3). Cleaning compounds shall meet the
requirements in table I.

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MIL-PRF-85570E

TABLE I. Physical properties.


Property Requirement Test Method Dilution
COMPOSITION
Composition No carcinogens1/, toxic pollutants2/ Manufacturer
or ozone depleting substances3/. Certification
Type IA shall be a 1:4 dilution of a
qualified type I product in an aerosol
package. Type II RTU shall be a 1:4
dilution of a qualified Type II
product in a 32oz pump spray or 5
gallon can.
pH 7.0 to 10.0 ASTM E70 As received
and 9/
Type II RTU As received
Non-volatile content Record value 4.5.9 As received
Water content Record value ASTM D95 As received
Infrared spectrogram Record spectrogram of non-volatile ASTM E168
matter
Rubber content (type IV only) 10.0 to 15.0 percent by weight Manufacturer
particulate rubber certification
Solvent content, maximum Manufacturer As received
weight percent certification
type I, IA, and IV 10.0 percent aromatic, 32.0 percent
total solvent
type II 1.0 percent total solvent
type V 10.0 percent total solvent, no
aromatics
Net weight (Type IA) Net weight for a 16 and 20 fluid 4.5.16
ounce can shall be no less than 13
and 17 ounces respectively.
Type II RTU Nominal 32 ounces
SAFETY & ENVIRONMENTAL
Toxicity No adverse effect on the health of Manufacturer
personnel when used for its intended certification
purpose
Flash point, Pensky-Martens 140 F (60 C), minimum ASTM D93 As received
Biodegradability (types II 85 percent in 28 days, minimum 40CFR
and V) 796.3100
Flame extension (type IA only) Less than 6 inches ASTM D3065 As received
MATERIAL COMPATIBILITY
Sandwich corrosion Rating of 1 or less ASTM F1110 As received
and 9/
Type II RTU As received
Cadmium corrosion 0.20 mg/sq. cm/24hrs wt change, ASTM F1111 As received
maximum and 9/
Type II RTU As received
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TABLE I. Physical properties – Continued.


Property Requirement Test Method Dilution
Total immersion corrosion No visible corrosion and ASTM F483 As received
Al 4/ , Ti 5/ , Steel 6/ 0.04 mg/sq. cm/24hrs wt. change, and 9/
Mg 7/ maximum
0.20 mg/sq. cm/24hrs wt. change,
maximum
Type II RTU As received
Hydrogen embrittlement No failures in less than 150 hours ASTM F519, As received
when specimens are loaded to 45 type 1A and 9/
percent of fracture strength and specimens.
immersed in cleaner. Cadmium
plated in
accordance
with (IAW)
Table II,
Treatment B.
Type II RTU As received
Unpainted surfaces, effect on No streaks or stains ASTM F485 9/
Painted surfaces, effect on No softening in excess of 1 pencil ASTM F502 As received
hardness and 9/
Plastics, effect on 4.5.10 and Diluted
Acrylic, type A (Cleaner types I, No crazing after 8 hours ASTM F484 1:1 with
IA,II,II RTU, III, and IV only) distilled
Acrylic, type A (type V) No crazing after 4 hours water
Acrylic, type C No crazing after 8 hours

Type II RTU & Type III As received


Polyimide insulated wire, effect No dielectric leakage, no visual effect 4.5.11 As received
on greater than that of distilled water
Abrasiveness 4.5.1 As received
type III No more than 10 percent gloss
type IV reduction
0.5 increase in gloss, maximum
PERFORMANCE
Cleaning efficiency 4.5.4 9/
type I, II, and IV Not less than 5% of a freshly made
type II RTU control formula cleaning efficiency As received
on hydraulic fluid and grease soils
type I and IV Not less than 5% of a freshly made
control formula cleaning efficiency
on wire rope lubricant soil 8/
Cleaning efficiency, type IA only Not less than 5% of a freshly made 4.5.4 As Received
type I control formula diluted 1:4, on
hydraulic fluid and grease soils 8/

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MIL-PRF-85570E

TABLE I. Physical properties – Continued.


Property Requirement Test Method Dilution
Embedded soil cleaning Complete removal of embedded carbon 4.5.15 As received
efficiency, type III black
Cleaning of vertical surfaces, Complete removal of wire rope 4.5.5 As received
type V lubricant soil or comparable to control
Foaming properties, type I and II 80 ml liquid after 6 minutes, maximum 4.5.7 9/
Consistency 4.5.6 As received
type IV 10 to 20 cm flow in 10 seconds
type V 13 to 23 cm flow in 10 seconds
Sprayability, type I and V Uniform spray when applied from Visual As received
finger pump spray bottle or aerosol.
Type V clings to vertical panel
Service evaluation (when Satisfactory 4.5.13
required)
Leakage, type IA only Aerosol cans shall not leak nor become 4.5.17
distorted
STABILITY
Appearance Homogeneous, no foreign matter Visual As received
Low temperature stability No separation 4.5.8 As received
Accelerated storage stability No separation or effect on steel strip. 4.5.2 As received
Cleaning efficiency shall be no less
than 5% of a freshly made control
formula. 8/
Particulate matter in types III and IV
shall not settle or float appreciably.
Storage stability After one year’s storage: 4.5.14 As received
No cleaner separation, crystallization, & ASTM
or deterioration. F1104
No container incompatibility,
corrosion, distortion, or leakage.
Shall meet qualification requirements
for cleaning efficiency, sandwich
corrosion, cadmium corrosion,
total immersion corrosion,
hydrogen embrittlement, pH,
foaming properties, and appearance.
1/ As specified by the National Toxicology Program’s Annual Report on Carcinogens
2/ As specified in 40 CFR 401
3/ As specified in 40 CFR 82.
4/ Aluminum alloy: SAE AMS-QQ-A-250/12
5/ Titanium: SAE AMS4911(6Al-4V alloy)
6/ Steel: SAE AMS5046 (1020 alloy)
7/ Magnesium alloy: SAE AMS4377, Chrome Pickled: SAE AMS-M-3171, type VI
8/ Freshly made control formula is not more than six weeks old.

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9/ Unless otherwise specified dilute with distilled water (volume concentrate: volume water): type I
(1:9), type II (1:14), type III (not diluted), type IV (not diluted), type V (not diluted)

3.2 Product identification and instructions for use. All containers of cleaning compound
shall be clearly labeled with the manufacturer's name and product designation, date of
manufacture, and pH of the cleaning compound. Labels containing direction for use shall be on
each container. Labels shall contain the following instructions as applicable:

3.2.1 Type I.

EXTERIOR AIRCRAFT CLEANER, GENERAL PURPOSE, AROMATIC SOLVENT,


MIL-PRF-85570, TYPE I

Directions for use:

Light soils: Mix 1 part cleaner in 14 parts water


Moderate soils: Mix 1 part cleaner in 9 parts water
Heavy soils: Mix 1 part cleaner in 4 parts water

Apply with foam generator (see NAVAIR 01-1A-509, Section 2), spray, sponge, brush, or
cloth. Scrub, then rinse with fresh water.

3.2.2 Type IA.

EXTERIOR AIRCRAFT CLEANER, GENERAL PURPOSE, AROMATIC SOLVENT,


AEROSOL, MIL-PRF-85570, TYPE IA

Directions for use: Spray cleaner onto surface to be cleaned.


Allow up to 3 minutes dwell time.
Scrub with a brush or rub with a clean cloth.
Rinse with fresh water, if available, or wipe dry.

3.2.3 Type IW.

EXTERIOR AIRCRAFT CLEANER, GENERAL PURPOSE, AROMATIC SOLVENT,


PRE-SATURATED WIPE, MIL-PRF-85570, TYPE IW

Directions for use: Open package and remove pre-saturated cloth.


Wipe surface to be cleaned.
Allow up to 3 minutes dwell time and re-wipe.
Rinse with fresh water, if available, or wipe dry.

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MIL-PRF-85570E

3.2.4 Type II.

EXTERIOR AIRCRAFT CLEANER, GENERAL PURPOSE, NON-SOLVENT,


MIL-PRF-85570, TYPE II

Directions for use:

Light soils: Mix 1 part cleaner in 14 parts water


Moderate soils: Mix 1 part cleaner in 9 parts water
Heavy soils: Mix 1 part cleaner in 4 parts water

Apply with foam generator (see NAVAIR 01-1A-509, Section 2), spray, sponge, brush, or
cloth. Scrub, then rinse with fresh water.

3.2.5 Type II RTU.

EXTERIOR AIRCRAFT CLEANER, GENERAL PURPOSE, NON-SOLVENT,


MIL-PRF-85570, TYPE II READY TO USE

Directions for use: Spray cleaner onto surface to be cleaned.


Allow up to 3 minutes dwell time.
Scrub with a brush or rub with a clean cloth.
Rinse with fresh water, if available, or wipe dry.

3.2.6 Type III.

EXTERIOR AIRCRAFT CLEANER, ABRASIVE SPOT CLEANER (FOR GLOSS PAINT


SURFACES ONLY), MIL-PRF-85570, TYPE III

Directions for use: Apply full strength with damp cloth.


Rub with a circular motion.
Rinse thoroughly, then dry with a clean cloth.
Do not allow cleaner to dry on surface.

3.2.7 Type IV.

EXTERIOR AIRCRAFT CLEANER, RUBBERIZED SPOT CLEANER,


MIL-PRF-85570, TYPE IV

Directions for use: Apply full strength with a non-abrasive cleaning pad.
Allow 1 to 3 minutes dwell time.
Rub with a circular motion.
Rinse thoroughly, then dry with a clean cloth.
Do not allow cleaner to dry on surface.
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MIL-PRF-85570E

3.2.8 Type V.

EXTERIOR AIRCRAFT CLEANER, GEL-TYPE WHEEL WELL DEGREASER,


LOW SOLVENT, MIL-PRF-85570, TYPE V

Directions for use: Apply full strength with brush or pump spray device.
Allow 5 minutes dwell time.
Brush if necessary, then spray with fresh water to rinse.

4. VERIFICATION

4.1 Classification of inspections. The inspection requirements specified herein are classified
as follows:

a. Qualification inspection (4.3).


b. Conformance inspection (4.4).

4.2 Inspection conditions. Unless otherwise stated in the test method or paragraph herein,
standard conditions shall be a room temperature of 22 ±2° C (72 4 F) and relative humidity of
50 ±10 percent.

4.3 Qualification inspection. The qualification inspection (see 6.3) shall consist of all tests
and examinations of this specification.

4.3.1 Qualification samples.

4.3.1.1 Laboratory test samples. Each laboratory qualification sample shall consist of three
1-gallon (3.785 liters) containers of cleaning compound. Storage gallon samples shall be
constructed of the same material as those in which the manufacturer intends to supply contract
quantities of the cleaner. One gallon of each sample shall be used for the storage stability test.
Samples submitted under Type IA and Type IW shall consist of six individual units of issue.
Type II RTU samples shall consist of twelve 32 oz pump spray bottles. The samples shall be
plainly identified by securely attached durable tags or labels marked with the following
information:

MIL-PRF-85570E
Sample for qualification inspection
CLEANING COMPOUND, AIRCRAFT, EXTERIOR
Type
Name of manufacturer
Product code number
Batch or lot number
Date of manufacture

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Submitted by (name) (date) for qualification inspection in accordance with the requirements
of MIL-PRF-85570E.

4.3.1.2 Service test samples. When a service evaluation (see 4.5.13) is required by the
qualifying activity, test samples shall consist of a 5-gallon pail for types I, II, IV, and V, and one
case of twelve individual units for types IA, Type IW and Type II RTU. The cleaning compound
shall be packaged in containers that provide protection during shipment. Samples shall be
forwarded in accordance with instructions contained in the letter requesting the service
evaluation.

4.4 Conformance inspection. The conformance inspection of the cleaning compound shall
consist of all the examinations and tests specified in table II.

TABLE II. Conformance inspection.

Inspection Requirement Test Method


Appearance Homogeneous Visual
Cadmium corrosion 1/ Table I ASTM F1111
Cleaning efficiency No less than 5% of control 4.5.4
Flash point Table I ASTM D93
Non-volatile content 2 percent 2/ 4.5.9
pH 2/ 0.5 ASTM E70
Plastics, effect on Table I ASTM F484
Total immersion corrosion 1/ Table I ASTM F483
Water content ±2 percent 2/ ASTM D95
1/ 24 hour test duration for conformance testing
2/ Permitted variance from recorded qualification value.

4.4.1 Conformance test samples. Conformance test samples shall be selected in accordance
with table III. Unless otherwise specified (see 6.2), two 1-gallon (3.785 liters) composite
samples shall be subjected to the tests specified in table II.

TABLE III. Conformance samples.

Lot Size (Units) Sample Size (Units)


Up to 50 5
51 to 500 7
501 to 35,000 8
over 35,000 11

4.4.1.1 Net content. The sample unit for this examination shall be one filled container. The
sample size shall be as specified in table III. A lot (see 6.4) shall be unacceptable if the average
net content per container for all units examined is less than specified.
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4.5 Test methods. Tests shall be conducted in accordance with the conditions specified in
4.2. Control formulations for comparison purposes shall be as specified in tables IV through
VII.

TABLE IV. Type I control formulation.

Component Parts by Weight Supplier (see 6.6)


Igepal CO-630 10.0 Rhone Poulenc
Igepal CO-730 10.0 Rhone Poulenc
Monamid 150-CW 5.0 Uniqema
Dipropylene Glycol Methyl Ether 10.0 Fisher
Hexylene Glycol 8.0 Fisher
Aromatic 150 10.0 Exxon Chemical
Deionized Water 43.5 N/A
Benzotriazole 0.5 Fisher
Hostacor 2098 2.0 Clariant
Morpholine 1.0 Fisher
Total 100.0

Directions: Blend first eight components in the order given. Reduce pH to 8.0 with glacial
acetic acid. Add Hostacor 2098 and Morpholine. Blend until homogeneous.

TABLE V. Type II control formulation.

Component Parts by Weight Supplier (see 6.6)


Tomadol 91-2.5 8.5 Tomah
Tomadol 91-6 18.4 Tomah
Monamid 150-CW 15.0 Uniqema
Monateric 1000 1.0 Uniqema
Elfugin AKT 0.7 Clariant
Benzotriazole 0.7 Fisher
Hostacor 2098 0.7 Clariant
Deionized water 55.0 N/A
Total 100.0

Directions: Blend components in the order given until homogeneous. Reduce pH with glacial
acetic acid to be in the range 9.0 to 10.0.

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TABLE VI. Type IV control formulation.

Component Parts by Weight Supplier (see 6.6)


Part A:
Monamulse 653-C 7.10 Uniqema
Monamine 1-76 2.70 Uniqema
Aromatic 150 7.50 Exxon
Isopar M 7.50 Exxon
Diethylene Glycol Butyl Ether 3.55 Fisher
Decanol 1.55 Fisher
Part B:
Trisodium Phosphate Dodecahydrate 2.7 Fisher
Deionized water 55.0 N/A
Pluronic F98 1.8 BASF
Hycar 1422 10.6 BF Goodrich
Total 100.0

Directions: Blend Part A and Part B separately in the order given. Combine the two and blend
until homogeneous. After 48 hours, reduce pH to 9.5 with glacial acetic acid and blend until
homogeneous. Consistency may be adjusted to comply with the requirements of table I by
adding single drops of decanol to increase viscosity or diethylene glycol butyl ether to decrease
viscosity.
TABLE VII. Type V control formulation.

Component Parts by Weight Supplier (see 6.6)


Part A:
Tomadol 23-1 5.0 Tomah
Tomadol 91-2.5 5.7 Tomah
Tomadol 91-6 10.6 Tomah
Tomadol 91-8 10.7 Tomah
Monateric 1000 4.9 Uniqema
Prep-solve 1/ 6.7 Glidco
Isopar M 2.9 Exxon
Dipropylene Glycol 9.0 Fisher
Benzotriazole 0.5 Fisher
Part B:
Sodium Bicarbonate 1.0 Fisher
Deionized water 43.0 N/A
Total 100.0
1/ D-limonene with proprietary stabilizer.

Directions: Blend part A and part B separately until homogeneous. Gradually add part B to part
A, while blending, until homogeneous. Product may thin slightly in the first 24 hours following

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preparation. Consistency can be adjusted to conform to the requirements of table I by adding


single drops of Tomadol 91-2.5 to increase viscosity or dipropylene glycol to decrease viscosity.

4.5.1 Abrasiveness (type III and IV only). A heavy duty wear tester (see 6.6, table IX) shall
be used for this test. A block fitted with a white cotton terry cloth conforming to
MIL-C-1164 shall be inserted in the instrument holder. The combined weight of the block,
cloth, and holder shall be 1,360 ±20 grams. The area of contact with the specimen shall be 1.5
square inches. Type III and IV cleaning compounds shall be tested using panels conforming to
designation A and B in table VIII respectively. Test panel gloss shall be measured using a
60 degree calibrated glossmeter conforming to ASTM D523. The panel shall then be placed on
the wear tester. Pour 10 ml of the concentrate onto the last panel and 15 ml onto the terry cloth
attached to the cleaning block in the instrument holder. After three minutes, place the terry cloth
on the cleaning block in contact with the panel and start the tester. The cleaning block shall
travel completely across the panel and return (one cycle) at a speed of two seconds per cycle.
After 50 cycles, the test panel shall be removed and rinsed under cold, running tap water and
blotted dry with terry cloth. Repeat this procedure four times using the same panel. Each time
the procedure is repeated, a new terry cloth and additional cleaning compound shall be used. At
the completion of the fifth run, the gloss shall again be measured for conformance to table I.
When rinsing the test panel, the paint surface shall be observed for the presence of a water break.

4.5.2 Accelerated storage stability.

4.5.2.1 Preparation of test sample. A 5 oz (41.9 ml) portion of a well-shaken cleaning


compound shall be poured into a clean 12 oz (254.9 ml) pressure resistant clear glass bottle
approximately 9.5 in. (24.1 cm) in height and 2.5 in. (6.4 cm ) in outside diameter. A strip of
steel 6 x 0.5 x 0.02 in. (5.2 x 1.27 x 0.05 cm) conforming to SAE AMS5046 shall be polished
with 280-grit silicon carbide paper to remove surface contamination and then cleaned by boiling
for one minute in mineral spirits and one minute in isopropyl alcohol. The steel strip shall be
placed in the test bottle and the bottle capped. The bottle shall then be inverted to completely
coat the steel strip.

4.5.2.2 Procedure. The capped bottle containing the steel strip shall be placed in a hot water
bath held at 140 4° F (60 2° C) for 8 hours. The bath and the bottle shall then be allowed to
cool for 16 hours and the 24 hour cycle repeated each day for a total of seven days. On the
eighth day, the bottle shall be removed from the bath, uncapped, examined for separation, and
the steel strip withdrawn and examined for corrosion. The aged sample shall be tested for
cleaning efficiency in accordance with 4.5.4 or 4.5.5, as applicable.

4.5.3 Aerosol container (type IA only).

4.5.3.1 Leakage. A pressurized can of cleaning compound shall be immersed completely for
five minutes in water maintained at 130 + 3º F (54 +2º C). The can shall be observed for
emission of bubbles or distortion during this period.

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4.5.3.2 Net weight. A pressurized can of cleaning compound shall be weighed to the nearest
gram. The can shall spray for three minutes, followed by a one minute pause. This procedure
shall be repeated until the can is empty. The empty can shall then be reweighed and the weight
of the contents calculated.

4.5.4 Cleaning efficiency (types I, II, II RTU and IV).

4.5.4.1 Panel preparation. Aluminum alloy panels measuring 6 x 2.5 x 0.02 inches (15.2 x
6.4 x 0.05 cm) shall be prepared in accordance with panel B of table VIII. At least three panels
shall be used for each product tested and the control formulation. The set of panels used in one
test run shall have the same gloss readings (+0.1 gloss units) as those used for the control run.
The gloss shall be measured by 85 degree reflectance and shall be in the range of 2-5 gloss units.
The lightness value (L value in a L-a-b color system) shall be measured using a Colorimeter
(illuminant C) or equivalent as approved by the qualifying activity. Record the initial lightness
value as Li.

4.5.4.2 Soil preparation. Hydraulic fluid soil shall be prepared by blending 50 grams of
carbon black (see 6.6) and 500 grams of MIL-PRF-83282 fluid first by hand, then with a high
speed Cowles type dispersator or other high shear mixer for 15 minutes. Molybdenum disulfide
grease soil shall be prepared by blending 50 grams of carbon black and 500 grams of
MIL-G-21164 grease, first by hand, then with a mechanical grease worker for 15 minutes.

4.5.4.3 Application of hydraulic fluid and grease soils. Thoroughly mix hydraulic fluid
before using. Using a soft bristle brush, gently paint the coated surface of a test panel with the
test soil. Remove excess hydraulic fluid soil by covering the test panel with folded absorbent
tissue and exerting pressure by rolling over the tissue with a five-pound rubber cylinder. Repeat
this blotting procedure twice. Using a 0.5 inch bristle acid brush, apply 0.12 gram of grease soil
centered across the panel in a band 1.5 inches wide and perpendicular to the long dimension of
the panel. The soil is then brushed the long dimension of the panel for 12 cycles (up and down
being one cycle) with a hog bristle brush (see 6.6, table IX). Typical force applied when
brushing is equivalent to approximately 1000 grams. The brush shall be rubbed on a clean tissue
or towel in three separate places to remove excess soil before brushing the next panel. Each
freshly soiled panel shall be baked at 221 2° F (105 l° C) for 60 minutes, then cooled to room
temperature, and used within four hours. Record the soiled lightness value as Ls. The soiled
lightness values shall be in the range of 20.0 to 25.0.

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TABLE VIII. Test panel preparation.

Panel Step Material Number Thickness Drying Time Drying Time


Letter of Coats per Coat, Between Coats After Final
mil Coat
A 1 Primer, coating 1 0.6 - 0.9 1 - 2 hours at room ---
conforming to temperature
MIL-PRF-23377

2 MIL-PRF-85285 mist coat --- 15 minutes at room ---


(Color No. 17875) temperature

3 MIL-PRF-85285 wet coat 1.5 - 2.5 --- Air dry one


(Color No. 17875) week at room
temperature
plus one week
at 150° F.

B 1 MIL-PRF-23377 1 0.6 - 0.9 1 - 2 hours at room ---


temperature

2 MIL-PRF-85285 mist coat --- 15 minutes at room ---


(Color No. 36440 temperature
or No. 36495)

3 MIL-PRF-85285 wet coat 1.5 - 2.5 --- Air dry one


(Color No. 36440 week at room
or No. 36495) temperature
plus one week
at 150° F.

4.5.4.4 Application of wire rope lubricant. Spray wire rope lubricant (see 6.6) onto a test
panel and immediately wipe back and forth using a piece of non-abrasive cleaning pad to
achieve a uniform soil in the center of the panel. Bake the soiled test panels at 221 2° F
(105 l° C) for 60 minutes then cool to room temperature.

4.5.4.5 Preparation of stock solution. A 10-grain hard water stock solution shall be prepared
by dissolving 0.20 ±0.005 gram of analytical reagent grade calcium acetate monohydrate and
0.14 ±0.005 gram of analytical reagent grade magnesium sulfate heptahydrate in one liter of
distilled water.

4.5.4.6 Cleaning. The test panel shall be cleaned using a heavy duty wear tester (see 6.6,
table IX), fitted with a cellulose sponge (see 6.6) at speed setting of 5. The sponge shall be cut
such that the dimension parallel to the cleaning stroke is 3.5 inches (9 cm) and the width is 2.75
inches (7 cm). The cleaning head with the dry sponge attached shall be weighed to a mass of 600
±10 grams. Type I cleaning compound shall be prepared by diluting 1 part cleaner with 9 parts

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10-grain hard water (4.5.4.5). Type IA shall be applied from aerosol can and compared to
control formula diluted as specified in Table I. Type II cleaning compound shall be prepared by
diluting 1 part cleaner with 14 parts 10-grain water (4.5.4.5). Type IV cleaning compound shall
be tested as received. After placing a soiled test panel in the template at +45 degrees (see figure
1), the cleaning solution shall be applied to the sponge. A typical amount of diluted cleaner
applied to the sponge for wetting is 40 ml. Twenty ml of the cleaner solution is applied over
each individual test panel so that it is completely covered. To avoid cross-contamination, the
apparatus is cleaned for each new cleaner and a new sponge is used. After allowing a 30-second
dwell time, the test panel shall be cleaned using 5 cycles of the wear tester, then turned 90
degrees and cleaned for an additional 5 cycles. The panel shall then be rinsed under cold
running tap water and allowed to dry.

4.5.4.7 Evaluation. The percent cleaning efficiency for each panel shall be determined as
follows:

Lc - Ls
Percent CE =
Li - Ls
where: Percent CE = Cleaning efficiency
Li = Initial lightness
Lc = Cleaned lightness
Ls = Soiled lightness
The average of the three panels tested shall be recorded.

4.5.5 Cleaning efficiency on vertical surfaces (type V).

4.5.5.1 Panel preparation. Panel shall be at least 5 by 16 inches (12 by 40 cm) in size and
prepared as in panel A, table VIII. Spray wire rope lubricant (Sprayon No. 201, or equivalent)
onto an aluminum test panel. Immediately wipe back and forth using a non-abrasive cleaning
pad to achieve a uniform soil. Allow the soil to dry at room temperature for a minimum of 15
minutes.

4.5.5.2 Cleaning. Position the soiled test panel such that the short dimension is vertical and
the long dimension is horizontal. Apply the product to the panel using a pump-spray applicator.
After 5 minutes, rinse the test panel by spraying with distilled water using the same pump-spray
applicator.

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FIGURE 1. Template.

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4.5.6 Consistency (type IV, V). A consistometer (see 6.6, table IX) shall be used as follows:
Shake the container of cleaning compound by hand for 10 seconds. Fill the well of the
consistometer completely with the compound. Release the gate and determine the extent of flow
in 10 seconds.

4.5.7 Foaming properties (type I and II). One part of the undiluted compound shall be
mixed with 9 parts 10-grain hard water (see 4.5.4.5) for type I and 14 parts 10-grain hard water
for type II. One hundred ml of this mixture shall be placed in a 500 ml capacity blender with a
maximum 3.15 inch (9.5 cm) outside diameter. The blender shall be turned on and run for 2
minutes at 8,000 1,000 rpm. The blender shall be turned off after 2 minutes and the mixture
allowed to stand undisturbed for 6 minutes. The compound shall be observed for conformance
to table I.

4.5.8 Low temperature stability. Approximately 50 ml of the cleaning compound shall be


poured into a test tube and cooled to 0 ±9° F (-18 ±5° C) in a cold box. The sample shall be held
at this temperature for one hour. The sample shall then be removed from the cold box and the
temperature allowed to rise to standard room temperature. Invert the test tube five times and
examine the content for homogeneity.

4.5.9 Nonvolatile content. Place approximately 0.5 gram of cleaning compound into each of
three weighing dishes and record weight to within ±0.0001 gram. Place the dishes in a forced
draft oven for 1 hour at 100 4° F (38 ±2° C). Cool the dishes to room temperature in a
dessicator and reweigh to determine the percent non-volatiles.

4.5.10 Plastics, effect on. Cleaning compound shall be tested in accordance with
ASTM F484 as follows:
Types I, II, IV, V - Diluted 1:1 with distilled water
Type II RTU - As received
Type III - As received
Type IA - As received (see below)
Type IA products shall be sprayed onto the flannel patch through a metal panel with a 0.5 by 0.5
inch window which is placed directly on the patch prior to spraying. (This prevents edge
contamination which can lead to premature failures.) The edges may be taped. The amount of
cleaner applied to the patch shall be equivalent to that used for testing bulk packaged products.

4.5.11 Polyimide insulated wire, effect on. Approximately 24 inches (61 cm) of wire
conforming to MIL-W-81381/11 shall be formed into a coil. Place the coil in a 4 ounce (118 ml)
wide mouth jar. Add enough concentrated cleaning compound in the jar to completely cover the
coil of wire. Cap the jar and store it at room temperature for 14 days. Repeat this procedure
using distilled water as the test medium. At the end of the storage period, remove the coil and
rinse thoroughly with tap water at room temperature. Suspend the coil and allow it to drain until
completely dry. Each wire shall be wrapped tightly around a 0.125 inch (3 cm) mandrel and then
unwrapped slowly, noting the appearance and number of any cracks in the insulation. The wire
shall meet the requirements specified in table I. The wire shall be immersed in a 5 percent by

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weight sodium chloride solution and subjected to a one minute dielectric test of 2,500 volts
(rms).

4.5.12 Salt-coated surfaces, effect on. A test shall be conducted in accordance with
ASTM F502, with the addition that panels shall be sprayed with ASTM D1141 synthetic ocean
water and dried in a 70 ±4° F (38 ±2° C) convection oven prior to testing.

4.5.13 Service evaluation. The service evaluation tests, performed by an activity designated
by the qualifying activity, shall consist of cleaning of two or more aircraft under actual service
conditions. Test results shall be compared to the results obtained with the control formula.

4.5.14 Storage stability. A steel strip conforming to SAE AMS5046 shall be added to the
one gallon (3.785 liters) container of cleaning compound furnished for storage stability (see
4.3.1.1). The total surface area of the steel strip shall be 6 0.5 sq. inches (30.7 sq. cm). The
sample shall be stored for one year at 70 5 F (21 3 C). After the one year storage period, the
sample shall be examined for evidence of separation, crystallization, deterioration, corrosion of
the steel strip, container incompatibility, distortion, leakage, or container corrosion. Type IA
containers of cleaning compound shall be exhausted or emptied, cut open, and examined for
container incompatibility and corrosion. Type II RTU samples shall be examined for evidence of
separation, crystallization, deterioration, container incompatibility, distortion and leakage. In
addition, Type II RTU samples shall meet the qualification requirements for cleaning efficiency,
sandwich corrosion, cadmium corrosion, total immersion corrosion, hydrogen embrittlement, pH
and appearance. Type IW shall be examined for conformance to 4.5.18.

4.5.15 Embedded soil cleaning efficiency (type III only) Lightly abrade the surface of a
designation A (table VIII) test panel with 240 grit abrasive paper or cloth, then sprinkle on a
small amount of carbon black and rub it into the surface using MIL-C-1164 terry cloth, or
equivalent. If the test panel can be completely cleaned of all carbon using a non-abrasive eraser,
repeat the panel preparation using more hand pressure on the abrasive. If the test panel can not
be completely cleaned using the eraser, the above method is to be used for making test panels.
Using soiled test panels, apply undiluted type III cleaner using terry cloth. Rub the cleaner over
the soiled area for 30 seconds using moderate hand pressure and rinse thoroughly with cold tap
water. Examine for soil residue.

4.5.16 Net weight (type IA). A pressurized can of cleaning compound shall be weighed to
the nearest gram. The can shall spray for three minutes, followed by a one minute pause. This
procedure shall be repeated until the can is empty. The empty can shall then be re-weighed and
the weight of the contents calculated.

4.5.17 Leakage (type IA). A pressurized can of cleaning compound shall be immersed
completely for five minutes in water maintained at 130 +3º F (54 +2º C). The can shall be
observed for emission of bubbles or distortion during this period.

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4.5.18 Appearance and workmanship (Type IW). (Initial qualification and storage stability)

All pre-saturated wipes shall be free of visible contamination and show no signs of
degradation, discoloration, fiber deterioration or any odor not consistent with the bulk Type I
product. Flexible foil packages shall show no signs of leakage.

4.5.19 Composition.

Type IW:
Wipes shall conform to SAE AMS3819 Class II Grade A and be composed of a non-
woven material consisting of 100% Rayon or Lyocell. No gauze or cheesecloth type material is
acceptable.

Each foil package shall contain 25 wipes saturated with 1200 ml of a qualified MIL-PRF-
85570 Type I product at 1 part cleaner to 4 parts de-ionized water.

Wipe dimensions shall be 16″ x17″ and be provided in an airtight flexible foil package
with a tear strip for opening. The foil package shall be re-sealable with a press type seal or
rubber band to prevent loss of volatile and fluid components. The length of the foil package
should be long enough to allow for adequate sealing of the unused portion after opening.

Samples submitted for qualification shall be accompanied by written correspondence on


company letterhead showing qualification to 4.5.19.

Type II RTU:
The manufacturer shall have a bulk Type II product qualified prior to qualification of a
RTU product. The manufacturer is to certify the RTU product is diluted at a ratio of one part
cleaner to four parts de-ionized water (1:4).

4.5.20 Labeling (Type IW). Re-sealable foil packages should be stored at a temperature less
than 120° F (49° C) and not exposed to direct sunlight for extended periods. Do not store in
enclosed areas with minimum ventilation and a possibility of exceeding the temperature limits.
Do not freeze. Opened packages shall be used within 6 weeks.

5. PACKAGING

5.1 Packaging. For acquisition purposes, the packaging requirements shall be as specified in
the contract or order (see 6.2). When packaging of materiel is to be performed by DoD or in-
house contractor personnel, these personnel need to contact the responsible packaging activity to
ascertain packaging requirements. Packaging requirements are maintained by the Inventory
Control Point’s packaging activities within the Military Service or Defense Agency, or within
the military service’s system commands. Packaging data retrieval is available from the
managing Military Department’s or Defense Agency’s automated packaging files, CD-ROM
products, or by contacting the responsible packaging activity.

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6. NOTES

(This section contains information of a general or explanatory nature that may be helpful, but is
not mandatory.)

6.1 Intended use. The cleaning compound exceeds commercially available cleaning compounds
in order to provide for the cleaning of military aircraft high gloss and camouflage paint systems,
low gloss tactical paint schemes, and cleaning exhaust track and gun blast soils. Specifically, the
cleaning compounds are intended for use in cleaning painted or unpainted aircraft surfaces. Type I
may be used in general cleaning of aircraft, provided that local regulations do not limit the use of
aromatic solvents or volatile organic compounds. Type IA is a 1:4 dilution of Type I, packaged in
an aerosol container. Type IW is a pre-saturated wipe consisting of a 1:4 dilution of Type I. Type II
may be used in general cleaning of aircraft, for both high gloss and camouflage paint systems. Type
II RTU is 1:4 dilution packaged in a 32 oz pump spray or 5 gallon can. Type III contains a very
fine abrasive and is designed for cleaning exhaust track and gun blast soils from high gloss paint
systems. Type IV contains non-abrasive particulate rubber and can be used on low gloss tactical
paint scheme coatings to clean stubborn areas such as boot marks and smudges, as well as gun blast
and exhaust track soil. Type V can be used in wheel wells, wing butts, and other areas where
complete rinsing with water can be tolerated.

6.2 Acquisition requirements. Acquisition documents must specify the following:


a. Title, number, and date of this specification.
b. Type of cleaning compound required (see 1.2)
c. Quantity of cleaning compound.
d. Conformance test sample size, if different from 4.4.1.
e. Packaging requirements (see 5.1).

6.2.1 Unit of purchase. The unit of purchase for the cleaning compound is the U.S. gallon.
A U.S. gallon of liquid occupies 231 cubic inches (3.785 liters) at 15.6° C (60° F).

6.2.2 Container size. Container size guidelines are as follows:

Types I, II, IV, V: 5, 15, or 55 gallon


Type II RTU: 32 oz pump spray, 5 gallon
Type III: 1 quart
Type IA: 16 or 20 ounce
self-pressurized can
Type V: Optional size plastic
spray bottle

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6.3 Qualification. With respect to products requiring qualification, awards will be made
only for products which are, at the time of award of contract, qualified for inclusion in Qualified
Products List (QPL-85570) whether or not such products have actually been so listed by that
date. The attention of the contractors is called to these requirements, and manufacturers are
urged to arrange to have the products that they propose to offer to the Federal Government tested
for qualification in order that they may be eligible to be awarded contracts or orders for the
products covered by this specification. Information pertaining to qualification of products may
be obtained from the Naval Air Warfare Center Aircraft Division, Code 4.3.4.2, Bldg. 2188,
48066 Shaw Rd., Unit 5, Patuxent River, MD 20670-1908.

6.3.1 Inspection report. When authorizing the forwarding of qualification samples, the
qualifying activity will request along with the qualification sample a satisfactory Material Safety
Data Sheet (see 6.5) in accordance with FED-STD-313 and 29 CFR 1910.1200 and a report that
includes the following information:

a. The results of tests performed by the manufacturer.


b. Toxicological information necessary to evaluate the safety of the compound.
c. Weight percent of aromatic solvents, total organic solvents, water, and rubber
(for type IV).
d. Aerosol container construction and packaging company where applicable.

6.4 Definitions.

6.4.1 Batch. A batch is defined as that quantity of material which has been manufactured by
some unit chemical process and subjected to some physical mixing operation intended to make
the final product substantially uniform.

6.4.2 Lot. A lot is defined as all the cleaning compound produced by one manufacturer, at
one plant, from the same materials, and under essentially the same conditions during a
continuous operation not exceeding 24 hours. In the event the process is a batch (see 6.4.1)
operation, each batch constitutes a lot.

6.4.3 Solvent. A solvent is defined as an organic liquid having a vapor pressure of greater
than 0.1 mm Hg at 25° C.

6.5 Material safety data sheets. Contracting officers will identify those activities requiring
copies of completed Material Safety Data Sheets prepared in accordance with FED-STD-313.
The pertinent government mailing addresses for submission of data are listed in Appendix B of
FED-STD-313.

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6.6 Supplier information.


TABLE IX. Item supplier information.

Item Identification Supplier Location


5x12 Hog bristle brush Gardner WG2000B Paul N. Gardner 316 NE 1St St, Pompano
Beach, FL
954-946-9454
Optical Sensor D25A Hunter Reston, VA
Cellulose sponge Cat No. 63 3M 3M Center #223-3N-05
Minneapolis, MN
651-736-3691
Consistometer ASTM F 1080 Paul N. Gardner 316 NE 1St St, Pompano
Beach, FL
954-946-9454
Glossmeter Novo-Gloss Paul N. Gardner Pompano Beach, FL
Washability / Wear Model D10V Paul N. Gardner Pompano Beach, FL
Tester

TABLE X. Chemical supplier information.

Component Supplier Address


Igepal GAF/International 1361 Alps Road
Specialty Products Wayne, NJ 07470
973-628-3000
Monamid 76 E. 24th Street
Monateric Uniqema P.O. Box 425
Monamine Paterson, NJ 07544
Monamulse 973-345-8220
Dipropylene glycol methyl ether Fisher Scientific 711 Forbes Avenue
Diethylene glycol butyl ether Pittsburg, PA 15219-4785
Trisodium phosphate dodecahydrate 800-766-7000
Hexylene glycol
Benzotriazole
Morpholine
Sodium Bicarbonate
Sprayon #201 Sprayon Products 26300 Fargo Ave.,
Open Gear and Wire Rope Lubricant Div., Sherwin Cleveland, OH
Williams Paint Co. 216-292-7400
Tomadol Tomah 474 W. 19th St
Reserve LA 70084
608-868-6811
Hostacor 2098 Clariant 400 Monroe Road
Elfugin AKT Charlotte, NC 28205
704-331-7000
Aromatic 150 Exxon Chemical Co. 13501 Katy Freeway
Isopar M Houston, TX
281-584-7600

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TABLE X. Chemical supplier information – Continued.

Component Supplier Address


Pluronic F98 BASF 100 Cherry Hill Road
Parsippany, NJ 07054
201-316-3000
Pylam LX-6545 Pylam Products 371 Merrick Rd.,
Rockville Center, NY
516-825-4939
Hycar 1422 BF Goodrich 9911 Brecksville Road
Brecksville, OH 44141
800-337-1144 (216-447-5130)
Prep-solve Glidco Organics PO Box 389
Jackonville, FL 32201
800-231-3728
Carbon Black (Raven 1040 Pwd) Columbian Chemical 1600 Parkwood Circle, Suite 400
Co. Atlanta, GA 404-951-5700

6.7 Subject term (key word) listing.

Aerosol
Degreaser
Gel
Hazardous air pollutant
Pump dispenser
Solvent
Volatile organic compound

6.8 Changes from previous issue. Marginal notations are not used in this revision to
identify changes with respect to the previous issue due to the extent of the changes.

Custodians: Preparing activity:


Army - MR Navy - AS
Navy - AS (Project 6850-2012-003)
Air Force - 68

NOTE: The activities listed above were interested in this document as of the date of this
document. Since organizations and responsibilities can change, you should verify the currency
of the information above using ASSIST Online database at https://assist.daps.dla.mil.

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