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    Astm D 721

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    yogenm
    This document summarizes the test method and equipment for determining the oil or solvent content of petroleum waxes. The test involves dissolving the wax sample in methyl ethyl ketone, cooling to precipitate the wax, filtering, and evaporating the filtrate to determine the weight of oil residue. The required equipment includes a cooling bath, filter assemblies, flasks, regulators, meters, an evaporation apparatus, circulator, pump, thermometers, and stirrer. Spare parts and additional items like cooling material and a balance are also listed.

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    Astm D 721

    Uploaded by

    yogenm
    859 views3 pages
    This document summarizes the test method and equipment for determining the oil or solvent content of petroleum waxes. The test involves dissolving the wax sample in methyl ethyl ketone, cooling to precipitate the wax, filtering, and evaporating the filtrate to determine the weight of oil residue. The required equipment includes a cooling bath, filter assemblies, flasks, regulators, meters, an evaporation apparatus, circulator, pump, thermometers, and stirrer. Spare parts and additional items like cooling material and a balance are also listed.

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    ASTM D 721

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    This document summarizes the test method and equipment for determining the oil or solvent content of petroleum waxes. The test involves dissolving the wax sample in methyl ethyl ketone, cooling to precipitate the wax, filtering, and evaporating the filtrate to determine the weight of oil residue. The required equipment includes a cooling bath, filter assemblies, flasks, regulators, meters, an evaporation apparatus, circulator, pump, thermometers, and stirrer. Spare parts and additional items like cooling material and a balance are also listed.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    859 views3 pages

    Astm D 721

    Uploaded by

    yogenm
    This document summarizes the test method and equipment for determining the oil or solvent content of petroleum waxes. The test involves dissolving the wax sample in methyl ethyl ketone, cooling to precipitate the wax, filtering, and evaporating the filtrate to determine the weight of oil residue. The required equipment includes a cooling bath, filter assemblies, flasks, regulators, meters, an evaporation apparatus, circulator, pump, thermometers, and stirrer. Spare parts and additional items like cooling material and a balance are also listed.

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    Oil & Solvent Content of Petroleum Wax

    ASTM D 721, ASTM D 3235, ISO 2908 (obs.), DIN 51571-2 (obs.), FTM 791-5431, IP 158, JIS K2235

    Product group(s): User group(s): Scope:

    Grease, Wax Lubricating Grease, Polishes, Wax For the determination of oil or solvent extractables in petroleum waxes having a congealing point of 30 C (86 F) or higher (determined with ASTM D 938 / IP 76 / ISO 2207) and containing not more than 15% of oil.

    The oil or solvent content of a wax may have significant effects on several of its properties, such as strength, hardness, flexibility, scuff resistance, coefficient of friction, coefficient of expansion, melting point, and oil straining. The importance of these effects may be dependent upon the ultimate use of the wax.

    The sample is dissolved in methyl ethyl ketone, the solution cooled to -32C (-25F) to precipitate the wax, and filtered. The oil content of the filtrate is determined by evaporating the methyl ethyl ketone and weighing the residue.

    Ready-to-Go Unit Dry-ice or Circulator Cooling

    Oil & Solvent Content Test Equipment to be composed of: - Oil & Solvent Content of Petroleum Wax Apparatus (with Dewar cooling-bath or circulator-bath)

    Main Unit
    17-0550 Oil & Solvent Content of Petroleum Wax Apparatus Dewar (standard version with Dewar cooling bath) Oil Content: ASTM D 721 (FTM 791-5431) - JIS K2235 IP 158 (ISO 2908, DIN 51 571-2) Solvent Content: ASTM D 3235 Consisting of: 3-place cooling bath (7 liter Dewar flask with metal base), bath cover to mount filter assemblies, thermometer, electric stirrer, heat-exchanger coil (for counter-cooling by an external cooler), with openings for filling with dry ice. Supplied with: 4 filter assemblies 4 Erlenmeyer flasks 1 air pressure regulator 2 flow meters 1 evaporation apparatus 1 vacuum pump with compressor 2 thermometers (ASTM 71C) 2 thermometer for cooling bath (ASTM 5C) Power supply: 230 V, 50 Hz

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    17-0555

    Oil & Solvent Content of Petroleum Wax Apparatus Circulator (extended version with circulator-bath) Oil Content: ASTM D 721 (FTM 791-5431) - JIS K2235 IP 158 (ISO 2908, DIN 51 571-2) Solvent Content: ASTM D 3235 Consisting of: circulator with small bath (for a temperature range of -50 ... +200 C), bath cover to mount the filter assemblies and thermometer. Circulator Data: see 25-0246 Supplied with: 4 filter assemblies 4 Erlenmeyer flasks 1 air pressure regulator 2 flow meters 1 evaporation apparatus 1 vacuum pump with compressor 2 thermometers (ASTM 71C) 2 thermometer for cooling bath (ASTM 5C) Power supply : 230 V, 50 Hz

    17-0556

    Oil & Solvent Content of Petroleum Wax Apparatus - Circulator Like 17-0555 but: Power supply: 115 V, 60 Hz

    Spare Parts
    17-0561 Evaporation Apparatus, 4-place, 220 V with in hight adjustable air-inlet-divices and thermostatic temperature regulation Heating Lamp, 40 W, 230 V

    17-0569

    17-0563

    Filter Assembly Consisting of: 1 filter stick with tube and 2 spring clips

    17-0566

    Erlenmeyer Flask, with glass stopper (NS 14/23), 25 ml

    16-0775

    Flowmeter, 40 - 400 l/h, with accessories Consisting of: 1 flowmeter (mm-scale, V-shaped metal float) on a tripod-stand with leveling screws & bulb, 1 hose ( 6 mm x 1 m, silicon, clear), 1 T-piece connection ( 7.5 mm), 2 angled hose connections Note: The correlation between scale readings and flow volumes are listed in the calibration sheet. Technical Data: Range: 40 - 400 l/h Factory calibration: at 20 C and 1000 mbar ambient pressure Dimensions / Weight: 180 x 180 x 230 mm (WxDxH), 1 kg

    17-0567

    Air Pressure Regulator Consisting of:

    Page: 2 31.10.2011 17-0550.pdf data & photo not mandatory

    1 T-tube, made of glass 1 mixing cylinder with plastic stand and stopper 25-0489 Vacuum-Pump with Mini-Compressor & Accessories Consisting of: 1 oil-free diaphragm pump with filter, 1 hose ( 6 mm x 1 m, silicon, clear), 1 T-piece connection ( 7.5 mm) 1 Hoffmann-Clip Technical Data: Max. capacity: 11.5 l/min End vacuum: 240 mbar Operating pressure: 2 bar (overpressure) Dimensions / Weight: 9 x 20 x 13 cm (WxDxH), 2.2 kg Power supply: 220/230 V, 50 Hz, EU-plug

    17-0574

    Thermometer ASTM 71C / IP 72C Range: -37 to +21 : 0.5 C Length: 355 mm, Immersion: 76 mm, 7 mm Thermometer ASTM 5C / IP 1C Range: -38 to +50 : 1 C Length: 230 mm, Immersion: 108 mm, 7 mm Electric Stirrer with propeller blade Consisting of: 1 universal drive unit ( 42 x 140 mm, NS 24/29) with changeable stirring direction and an infinitely variable stirrer speed from 0 to 2300 rpm 1 stirrer with propeller impeller ( 20 x 115 mm) 1 power unit (130 x 90 x 170 mm, 1.5-15 V AC, 1.5 A) 1 coiled cord connection ( approx. 1 m) 1 wrench (size 7) for stirrer mounting Note: This stirring unit is also universal useable outside any equipments as hand-operated instrument (only 580 g). Power supply: 230 V, 50/60 Hz, EU-plug

    16-0371

    25-0042

    Order Guideline
    Minimum equipment: Spares (approx. 1 year): Additional requirements: 1x 17-0550 or 1x 17-0555 17-0563, 17-0566, Thermometer Cooling Matter, Balance

    Page: 3 31.10.2011 17-0550.pdf data & photo not mandatory

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