IS : 261 - 1982

( Reaffirmed 1999 )
Indian Standard
SPECIFICATION FOR COPPER SULPHATE
(Second Kwision)

Third Reprint May 1997

UDC 661.856.532

@ Copyright 1982

BUREAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002

Gr 4 December I982
 I8 : 261 - 1982

Indian Standard
SPECIFICATION FOR COPPER SULPHATE
(Sc)cond Kcuision)

Inorganic Clumkds ( Mist ) Seclional Chnrnitlce, CDC 3

SHRI D. S. CHOWDIWRY ( .IllenrcLle )

DR R. M. BHATNACAR The l’crtilizcr ( 1’ & 1) ) Intlia Lkl, Sir&i
SHRI S. N. BHATTAWAKVA Tata Chemicals Ltd, l\on~tmy
YHRI S. GANAPATHY( Allenut& )
SFIRIB. N. BIIATTACHARYYA (&logical Survey 01‘ I3ltJi;l,C:aIt_utl~
SHW S. S. HONAVAR It&b Private Ltd, Ilontl~ay
SHRI J. C. DEY ( AZlenu& I )
SHRI M. V. DABHOLKAR( Alternate II )
SHRI J. S. MATHARU Directorate General 01. ‘I‘cchnical Developmcnl 1
New Delhi
SWRI R. C. BW~~TTACHARYYA ( .UernatG )
YHKI S. V. NAYAK ,J. K. Chemicals Ltd, ‘l’hanc
SHRI P. A. MENON ( Alternate )
SHRI J. K. PATWA Sarabhai M. Chemicals, Vaclotlar;l
SHRI H. H. KAVARANA ( Alternate )
SHRI A. K. RAO D. C. M. Chemical Worka, New DellG
SHRI B. K. VAHI ( Alternate )
SHRI B. K. SACHAR Ministry of Defence ( R & D )
SHRI A. D. GUPTA ( Alternate )
SHRI C. R. SANTHANAKRTSHNAN ‘l’ravancore Chemical & hlfg C:o Ltd, Mettur Darn
SHRI K. V. MANI ( Alternate )
DR H. S. SARKAR ‘Ttrc Durgapur Projects Ltd, Durgapur
SHRI P. SATYANARAYAN Development Commissioner, Small Scale lndmtrics,
New Delhi
Da E. R. SAXENA Regional Research Laboratory ( CSIK ), liydcrabad
DR MOD. ZAVAR ,JAMIL ( Alternate )
SKRI H. C. SHAH Golden Chemicals Pvt Ltd, Bombay
SHRI S. GANAPATIIY ( Alternate )

( Continued
on page2 )
0 Copyright 1982
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indiatt Col?ly/i,& Act ( XIV of 1957 ) and
reproduction in whole or in part by any means except with written permission of the
publisher shall be deemed to be an infringement of copyright under the said Act.
IS : 261 - 1982

( Contim/edJYompap I )

Alembers RCpMSCntin,~
SIIKI Y. v. SilETTY Indian Oil Corporation Ltd ( Refineries and Pipc-
lines Division ), New Delhi
DI< V. ~RINIV.28AN Glaxo Laboratories ( India ) Ltd, Bombay
SIIRI 1’. hhNSLKIIAN1 ( .i[tcWU/e )
111~ SURJIT thc:II Ministry of Defence ( DGI )
DR A. K. SEN ( .I/ter~,trle)
SIII(I N. C:. ‘I‘HAKKAR Indian Chemical Manufacturers’ Association,
Calcutta
DI:. HAKI Bui\c,wn~, Director General,BIS ( Ex-o$cioAlembcr )
Director ( CZhcm )

SHRI ni. RAKSHI GUPT.~

Assistant Director ( Chcm ), RIS

Auxiliary Cllemicals Subcommittee, CDC 3 : 18

The Dharamsi hlorarji Chemical Co Ltd, Bombay

SHRI R. S. V’YAS ( .ilternnte to

Dr M. S. Vaidya )
SImI S. 1’. .\VAD21001 Dcepak Nitrite Ltd, Bombay
SIIKIJ. T. VORA ( iillenrde )
SIIRI A. ‘r. BRAHMBHAT.~ Kalali Chemicals Ltd, Vadodnm
SHRI P. R4. SARAIYA ( Alterrrnfe)
SHRI R. K. GANDHI Tata Chemicals Ltd, Bombay
SIXRIN. K. GUHA Development Commissioner, Small Scale Industries.
New Delhi
SHRI D. P. SINCII ( rlllertlale )
SHRI M. M. KAUI. Khosla Metal Powders Ltd, Punt
SHRI S. P. KHOSLA ( A/le,~m/e )
SIIRI M. A. KOTIRIIAS~~AR Phoenix Chemical Works Pvt Ltd. Uombay
SHRI M. A. CI~JNEKAR( X/err&e )
SIIRI U. V. KUNIKULLAYA Tamil Nadu Chromates 6: Chemicals Ltd, Madras
SHRI M. N. KINI ( .Il&tmle )
SIIRI S. V. NAYAK J. K. Chemicals Ltd, Thane
SHRI P. A. MENON ( z41tertrate )
SIIRI G. P. PILLAI The Travancore Co&in Chemicals Ltd, Udyoga-
mandal
SHRI C. N. G. NAIR ( Alternale )
SHRI H. C. SHAH Golden Chemicals Pvt Ltd, Bombay
SHRI S. GANAPATHY ( Alternate I )
SHRI Y. M. RAWAL ( Alternate II )
SHRI K.M. SHAH The Mill Owners’ Association, Bombay
SHRI D. V. WITTENBAKER Waldies Ltd, Calcutta

2
 IS :261 - 1982

.hclian Stanclad
SPECIFICATION FOR COPPER SULPHATE
(Second Revision.)

0. FOREWORD
0.1 This Indian Standard ( Second Revision ) was adopted by the Indian
Standards Institution on 28 January 1952, after the clraft finalized by the
Inorganic Chemicals ( Mist ) Sectional (:ommittcc hntl Ijcen approved
by the Chemical Division Council.

0.2 Copper sulphate is used in the manufacture and processing of variolls

ludustrial products, such as fungicide mixtltres, dyeing cotton and silk,
preserving hides and wood, tanning leather, electric batteries, process
engraving, destroying algae in pools for rot proofing of jute ba.gs; and for
1he manufacture of pigments. It is also used in fine chemicals, electro-
plating, pharmaceuticals and as a reagrnt in chemical analysis. ‘l’his
standard, however, does not cover the analytical reagent grade of I he
material and the material used for electroplating, as it is covered by
IS : 4847-1979”. Pharmaceutical use of the material is being excluded
from this revision as the specifications of this grade are covered in the
1 ndian Pharmacopoeia.

0.3 So far, copper sulphate has been manufactm-ed by and large from
copper scrap only. ‘Recently, its production has started also f+om an indi-
genously available ore, namely, chalcopyrite. While preparing this revision.
it has been ensured that specification for technical grade of the material
would apply also to copper sulphate produced from chalcopyrite.

0.3.1 This revision provides for expression of the limits of copper sulphate
in terms of copper content instead of CuSO,, 5H,O. It is hoped that this
would help in overcoming controversies emanating from the loss of water
of crystallization.

0.4 For the purpose of deciding whether a particular requirement of this

standard is complied with, the final value, observed or calculated, expressing
the result of a test or analysis, shall be rounded off in accordance with
IS : 2-1960f. The number ot’ significant places retained in the rounded off
value should be the same as that of the specified value in this standard.

*Specification for copper salts for electroplating (&St revision).

tRules for rounding off numerical values ( reuiwf ).

3
IS : 261 - 1982

1. SCOPE

1.1 This standard prescribes the requirements and the methods ofsampling
and test for copper sulphate.

2. GRADES

2.1 The material shall be of the following two grades :

a) Technical ( TIEH ) - Used in dyeing cotton and silk; preserving

hides and woods; tanning leather; electric batteries; process en-
graving, destroying algae in pools; rot proofing of jute bags; and
manufacture of green and blue pigments; and fungicide mixtures
( Bordeaux mixture ) .
b) Pure-Used in fine chemicals.

3. REQUIREMENTS

3.1 Description-The material shall be in the form of blue, triclinic

crystals, blue granules or light blue powder. The material slowly effloresces
in dry air, turning to white blue powder.

3.2 The material, when iested as prescribed in Appendix A, shall comply

with the requirements given in Table 1. Reference to relevant clauses of
Appendix A is given in co1 5 of the table.

TABLE 1 REQUIREMENTS FOR COPPER SULPHATE

( Clauses 3.2, B-5.1.1, B-5.2 and B-5.3 )

REQUIREMENT METHOD OF TEST,

SL No. CHARACTERISTIC ----------1 REF TO Cl No. IN
T&I Pure APPENDIX A
(1) (2) (3) (4) (5)
i) Copper, percent by mass, Min 24.7 25.1 A-2
ii) Matter insoluble in water, 0.20 0.05 A-3
percent by mass, MUX
iii) Soluble iron and aluminium
compounds ( as Fe ), 0.30 0.15 A-4
percent by mass, Max
iv) PH value, not less than 3.0 3.5 A-5
v) Chloride ( as Cl ), percent by - 0.01 A-6
mass, Max

vi) Amga: ( as As203 ), mg/kg, - 10 A-7

vii) Lead and zinc - to pass the teat A-S

4
 I8 : 261 - 1982

4. PACKaPJG AND MARKING

4.1.1 ‘1%~ iualcrial, WIKW usc:tl as a pcsticitlc, shall also comply, with
111~p;u.king rcclrliremcnts as spccificd in 1s : 8190 ( Part I )-1976” under
the Ixsccticidcr _lct, 1968.

4.2 Marking .--The packages shall 1~ securely closed and bear legibly
and indelibly the following information :

a) Name and grade of the material;

1~) Name of the manufacturer and his recognised trade-mark, if any;
c). Gross and net mass;
(1) Da tc of mamrl&cture; and
c) IJalch number.

4.2.1 ‘l’hc packages may also be marked with the Standard Mark

NOTL - Tile use of the Standard Mark is governed by the provisions of the
Rur-eau ofIndian Standnrds Act, 1936 and the Rules and Regulations made there-
under. The Standard Mxk on products covered by an Indian Standard conveys
the assur.incc t!lnt they have been produced to comply with the requirements of that
standard under R well deiined system of inspection, testing and quality control
which is devised and supervised by BIS and operated by the producer. Standard
marked products are also continuously checked by BIS for conformity to that
standard as a further safeguard. Details of conditions under which a licence for
the use of the Standard Mark may be granted to manufacturers or producers may
be obtained from the Bureau of Indian Standards.

5. SAMPLING

5.1 The method of drawing representative samples of the material hnd the
criteria for conformity shall be as prescribed in Appendix B.

*Requirements for packing of pesticides ( Part I ) Solid pesticides

IS : 261 - 1982

APPENDIX A
( Clause 3.2 )
METHODS OF TEST FOR COPPER SULPMATE

A-O. QUALITY OF REAGENTS

A-9.1 Unless specified othcrwisc, pure chemicals and distilled water

( JCBIS : 1070-1977” ) shall be.employed in tests.
NOTE - ‘Pure chemicals’ shall mean chemicals 111;1tdo 1101 contain impurities
which affect the results of analysis.

A-l. PREPARATION OF TEST SAMPLE

A-l.1 Pow&r the material and sieve it through I*00 mm IS sieve ( .IP~
IS : ,160-19777 ) keeping the sieved material in a clean glass stoppered
wcighitq I~ottlc Jim test purposes.

A-2. COPPER

A-2.0 ‘I’wo methods are prescribed for determining copper, namely,

volumetric method and electrolytic method. The electrolytic method shall
be regarded as the referee method.

A-2.1 Volumetric Method

A-240 Outline of the Method - Copper is determined with the addition

of potassium iodide and titrating the liberated iodine against standard
sodium thiosulphate solution.

A-2.1.1 Reagents

A-2.1.1.1 Sodium carbonate -see IS : 296-1974:.

A-2.1.1.2 Potasium iodide - crystals.

A-2.1.1.3 Acetic acid-see IS : 695-19758.

A-2.1.1.4 Standard sodium thoisulphate solution - 0.1 N.

*Specification for water for general laboratory use ( second revision ).

tSpecification for test sieves: Part I Wire cloth test sieves ( secondrevision).
Part II Perforated plate test sieves ( second revision ).
$Specification for sodium carbonate, anhydrous ( secondrevision).
9Specification for acetic acid ( second revision ).

6
 IS : 261 - 1982

A-2.1.1.5 Starchindicator solution - Triturate 5 g of starch and 0.01 ;;

of mercuric iodide with 30 ml of cold water and slowly pour it with stirring
into one litre of boiling water. Boil for three minutes. Allow to cool and
decant off the supernatant clear liquid.

A-2.1.1.6 Potassium ~hiogvmztc ---crystals.

A-2.1.2 Procedure - l)issolvc about 1 g of the test sample ( .ree A-l )

accurately weighed, in 50 ml of water. Add a pinch of sodium carbonate
till a slight turbidity appears. Then add 5 ml ofacetic acid, 3 g ofpotassiunl
iodide and titrate the liberated iodine with sodium thiosulphate solution,
using starch as an indicator, until only a faint blue colour remains. Add
about 2 g of potassium thiocyanate, shake and continue the titration until
the blue colour disappears.

A-2.1.3 Calculahott

VN
Copper, percent by mass = 6.35 xX

where
I’ =volume in ml of standard sodium thiosulphate solution,
.,V =normality of standard thiosulphate solution, and
.M=ma.ss in g of the sample taken f’or the teal.

A-2.2 Electrolytic Method

A-2.2.1 Reagents

A-2.2.1.1 Dilute mlphuric acid - 33 percent ( IV/U

).

A-2.2.1.2 Urea solution - 20 pcrccnt ( ~llv ) .

A-2.2.2 Procedure - Dissolve about 1 g of the test sample, accurately

weighed in 200 ml of water. Add 5 ml of dilute sulphuric acid and heat
to 60 - 70°C. Electrolyse for 50 minutes using a platinum gauze rotating
ariode and a platinum gauze stationary cathode as given in A-2.2.2.1
and A-2.2.2.2.

A-2.2.2.1 Connect the anode and the weighed cathode to a 1%volt

electro-analyscr. Rotate the anode with the current on and test for ‘short’
across the electrodes. Stop, the rotation and raise the beaker containing
the solution until the electrodes are completely immersed. Restart the
rotation, adjust the current to 0.5 ampere till copper starts depositing the
gradually raise to 3 amperes to obtain a bright coherent deposit. Add 3 to
4 drops of urea solution half-way through the electrolysis.

7
LS : 261 - 1982

A-2.2.2.2 At the end of electrolysis, the current being still on, lower
the beaker slowly, washing the electrode with a jet of cold water from a
wash bottle. Switch off the current and stop rotation, Remove the electrodes,
wash the cathode first in rectified spirit and then in solvent ether and dry
the cathodes for live minutes and about 110°C and weigh.

A-2.3 Calculation

itl, x 100
Copper, percent by mass =M-
a
where
AJ, =mass in g of the copper deposited on cathode, and
1\1~=rnass in g of the copper sulphate taken for the test.

A-3. MATTER INSOLUBLE IN WATER

A3.f Reagents

A-3.1.1 Concentrated Sulfihuric Acid - see IS : 266-1977’.

A-3.2 Procedure - Weigh accurately about 10 g of the test sample and

dissolve in 100 ml of water. Add 3 ml of sulphuric acid and stir thoroughly
at room temperature. Filter through a tared filter paper or tared Gooch
or sintered glass crucible ( G No. 4 ). Wash the residue with water till
it is free from acid. Dry the filter paper or crucible in an oven maintained
at a temperature of 105 to 110°C till constant mass is obtained. For pure
grade, use about 20 g of the test sample.

A-3.3 Calculation

Insoluble matter, percent by mass=2 x 100

2
where
,Vl, =mass in g of the residue obtained, and
&Iz=mass in g of the material taken for the test.

A-4. SOLUBLE IRON AND ALUMINIUM COMPOUNDS ( as Fe)

A-4.0 Outline of the Method-Iron and aluminium are determined

gravimetrically by precipitation with ammonium hydroxide.

A-4.1 Reagents

A-4.1.1 Concentrated Nitric Acid - .ree IS : 2641976f.

*Specification for sulphuric acid ( second revision ).

jSpecification for nitric acid ( second revision ).
 IS : 261 - 1982

Ammonium
A-4.1.2 Chlol-idf

A-4.1.3 Dilute Ammonium Hydroxide - approximately 15 percent NH,

(m/v).

A-4.1.4 Dilute Hydrochloric Acid - 33 percent ( m/s ).

A-4.2 Procedure - Take 10 g of the test sample ( see A-l ) and add 25 ml
of water, 2 ml of nitric acid and 5 g of ammonium chloride. Make the
solution alkaline by adding ammonium hydroxide solution. Keep it on a
water bath until the precipitate has flocculated, keeping the solution
alkaline by the addition of more ammonium hydroxide, if necessary.
Filter and wash the residue with dilute ammonium hydroxide. Dissolve
the residue in hot dilute hydrochloric acid. Make the solution again alkaline
by adding ammonium hydroxide and allow the precipitate to settle. Filter
and wash the residue with water. Dry the residue, ignite and weigh till a
constant mass is obtained.

A-4.3 Calculation

70xM,
Soluble iron and aluminium compounds (as Fe) = M
percent by mass 2

where
M, -mass in g of the residue obtained, and
Mz=mass in g of the sample taken for the test.

A-5. PH VALUE

A-5.1 Procedure - Dissolve 5 g of the test sample ( see A-l ) in water

and make up the volume to 100 ml. Determine the pH with glass electrodes
using a suitablepH meter.

A-6. CHLORIDES

A-6.0 Outline of the Method - Chlorides are determined by comparison

of the opalescence produced in a solution of the material with silver nitrate
solution against the opalescence produced by a solution containing known
amount of chloride.

A-6.1 Apparatus

A-6.1.1 Smler Cylinders-50-ml capacity ( see IS : 4161-1967* ).

*Specificationfor Nesslcrcylinders.

9
IS : 261 - 1982

A-6.2 Reagents

A-6.2.1 Dilute Jfitric Acid - approximately 4 N.

A-6.2.2 Silver J&rate Solution -- approximately 5 percent ( m/v).

A-6.2.3 Standard Chloride Solution - Dissolve 0.164 9 g of ignited sodium

chloride in 1 000 ml of water. Dilute 100 ml of the solution again to one
litre. One millilitre of the diluted solution is equivalent to O-01 mg of
chloride ( as Cl ).

A-6.3 Procedure -Dissolve 0.2 g of the test sample in 50 ml of water

in a Nessler cylinder. Add 1 ml of dilute nitric acid and 1 ml of silver
nitrate solution and mix. Carry out a control test in the other Nessle~
cylinder in the same manner using 2 ml of standard chloride solution.

A-6.3.1 The limit as prescribed in Table 1 shall be taken as not having

heen exceeded if the opalescence produced in the test solution is not greater
than that produced in the control test.

A-7. ARSENIC

A-7.1 Procedure - Dissolve 1.0 g of the test sample in water and make up
the volume to about 50 ml. Carry out the determination for arsenic as
prescribed in IS : 2088-1971*, using for comparison the stain obtained
with O*OOl mg of arsenic trioxide ( as As,O, ).

A-8. LEAD AND ZINC

A-8.1 Reagents

A-8.1.1 Citric Acid

A-8.1.2 Dilute Ammonium Hydroxide - approximately 15 percent NH,

( m/u)-
A-8.1.3 Potassium Cyanide Solution - 10 per cent ( m/v ) .

A-8.1.4 Sodium Sulphide Solution - 10 percent ( m/v ).

A-8.2 Procedure - Dissolve one gram of the test sample in 10 ml of

water. Add one gram of citric acid and 10 ml of ammonium hydroxide
followed by potassium cyanide solution, dropwise, until the blue colour
is discharged. Add one drop of sodium sulphide solution. The material
shall be taken to have passed the test if not more than a slight darkening
and no opalescence is produced.

*Methods for determination of arsenic ( jir~trevision) ,

10
 IS : 261 - 1982

APPENDIX B
( Clause 5.1 )

SAMPLING OF COPPER SULPHATE

B-l. GENERAL REQUIREMENTS OF SAMPLING

B-1.0 In drawing, preparing, storing and handling test samples, the follow-
ing precautions and directions shall be observed.

B-l.1 Precaution shall be taken to protect the samples, the material being
sampled, the sampling instrunicnt and the containers for samples from
adventitious contamination.

B-l.2 ‘To draw a rcprcscntative sample, the contents of each container

selected for sampling shall be mixed as thoroughly as possible by suitable
means.

B-l.3 ‘l’lw samples shall bc placed in suitable, clean, dry and air-tight
glass or other suitable containers on which the material has no action.

B-l.4 Each sample container shall be sealed air-tight after filling and
marked with full details of sampling, the date of sampling and year of
manufacture of the material.

B-2. SCALE OF SAMPLING

B-2.1 Lot -- All the containers in a single consignment of the material of

one grade and drawn from a single batch of manufacture shall constitute
a lot. If a consignment is declared or known to consist of different grades
or batches of manufacture, the containers belonging to the same grade
and batch shall be grouped together and each such group shall constitute
a separate lot.

B-2.1.1 Samples shall be tested from each lot for ascertaining conformity
of the material to the requirements of the specification.

B-2.2 The number ( II ) of containers to be chosen from a lot shall depend

on the size of the lot ( N) and shall be in accordance with co1 1 and 2 of
Table 2.

B-2.3 The containers to be selected for sampling shall be chosen at random

from the lot and for this purpose random number tables shall be used. In
case sttch tables are not available, the following procedure may be adopted.

11
IS : 261 - 1932

Starting from an.y container, count them 1, 2, 3 . . . . . . . . . . up to r and

so on in a systematic manner, where Y is the intqra.1 part of .X/U. Every
rth container thus counted shall be taken out for drawing sarnplcs.

TABLE 2 NUMBER OF CONTAINERS TO BE SELECTED

1,0-r SILIC

(Jv)
3 to
50
51 10 200
201 to 400
-101 to 650
651 and abuvc

B-3. TEST SAMPLES AND REFEREE SAMPLE

B-3.1 Preparation of Test Samples

B-3.1.1 Draw with an appropriate sampling instrument a small portion

of the material from different parts of each container selected. Th.c total
quantity of the material drawn from each container shall bc sufficient to
conduct the tests for all the characteristics given under 3 and shall no1
exceed 1 kg.

B-3.1.2 l%oroughly mix all portions of the material drawn from the
same container. Out of these portions a small but equal quantity shall be
taken from each selected container and shall be well mixed up together
so as to form a composite sample weighing not less than 600 g. This Lompo-
site sample shall be divided into three equal parts, one for the purchaser,
another for the supplier and the third to be used as referee sample.

B-3.1.3 The remaining portions of the material from each container

( after a small quantity needed for the formation of composite sample has
been taken shall be divided into three parts, each part weighing not less
than 100 g ). These parts shall be immediately transferred to thoroughly
dried bottles which are then sealed air-tight with stoppers and labelled
with all the particulars of .sampling given under B-1.4. The material in
each such sealed bottle shall constitute an individual test sample. These
individual samples shall be separated into three identical sets of samples
in such a way that each set has an individual test sample representing
each container selected. One of these sets shall be sent to the purchaser,
another to the supplier and the third shall he used as referee sample.

12
 IS : 261 - 1982

B-3.2 Referee Sample -- The referee sample shall consist of the composite
sample (see B-3.1.2) and a set of individual samples ( see B-3.1.3 ) marked
for this purpose. It shall also bear the seals of the purchaser and the supplier.
These shall be kept at a place agreed to between the purchaser and the
supplier and shall be used in case of dispute between the two.

B-4. NUMBER OF TESTS

B-4.1 Tests for the determination of coppur sulphatc shall be conducted

on each of the individual samples for all the grades.

B-4.2 Tests for the remaining characteristics shall be conducted on the

composite sample.

B-5. CRITERIA FOR CONFORMITY

B-5.1 For Individual Samples

,
B-5.1.1 For Copper Sulphate - The test results for copper sulphate shall
be recorded and the mean and the range for these test results shall be
calculated as follows :

Mean ( X) = sum of the test results divided by the number of‘

test results,
Range ( R) = The difference between the maximum and the
minimum values of the test results.

The value of expression ( X50.6 R ) shall be calculated. If the values

of this expression lie within the limits specified for the relevant grade in
Table 1, the lot shall be declared to have satisfied the requirements for this
characteristic.

B-5.2 For Composite Sample-The test results on the composite

sample shall meet the corresponding requirements specified in Table I for
the relevant grade.

B-5.3 A lot shall be declared as conforming to the specification if it satisfies

the requirements for each of the characteristics listed in Table 1 for tFc>
relevant grade.

13
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SSales Dffice is at ‘F’ Block, Unity Building, Narashimaraja Square, 222 39 71
BANGALORE 560002

Reprography Unit, BIS, New Delhi, India

 AMENDMENT Ml. 1 JUNE 1986

Td
IS:261-19’32 SPECIFICATION FOR COPPER SULPMTE

(Second Revision)

(Pap 13, clauses B-4.1 and B-S.Z.1) - The

expression 'Copper sulphate' shall be read as 'Copper'.

(Page 13, cZause B-5.1.1 l last paragraph) -

Substitute the following for the existing paragraph:

‘The value of expression ‘(F - 0.6 R)'-shall be

calculated. If the value of this expression is
g-cater than or equal to the minim lin,itspecified
for the relevant grade in Table 1, the lot shall be
declared to have satisfied the requirement for this
characteristic.'

(CDC 3)

Reprography Unit, MS, New Delhi, India