Mil STD 3004c

MIL-STD-3004C
10 August 2011

SUPERCEDING
MIL-STD-3004B
w/ Change 1
14 November 2008

DEPARTMENT OF DEFENSE
STANDARD PRACTICE

QUALITY
ASSURANCE/SURVEILLANCE FOR
FUELS, LUBRICANTS AND
RELATED PRODUCTS

AMSC N/A FSC 91GP
NOT MEASUREMENT
SENSITIVE
Downloaded from http://www.everyspec.com on 2011-09-14T18:19:20.
MIL-STD-3004C

ii
FOREWORD
1. This Standard is approved for use by all Departments and Agencies of the Department of
Defense (DoD).
2. Certain provisions of this Standard are subject to international standardization agreements.
When amendment, revision, or cancellation of this Standard is proposed which would affect or
violate the international agreement concerned, the preparing activity will take appropriate
reconciliation action through international standardization channels, including departmental
standardization offices, if required.
3. The tables in this Standard are numerous; therefore, they are located at the end of Section 6,
preceding the Appendices and Index.
4. Comments, suggestions, or questions on this document should be address to DLA-ENERGY-
QA, Room 2843, Defense Energy Support Center, 8725 John J. Kingman Rd, Fort Belvoir VA,
22060-6222 or by sending your comments to the Lead Standardization Office as listed in the
ASSIST database. Since contact information can change, you may want to verify the currency of
this address information using the ASSIST Online database URL https://assist.daps.dla.mil/
Users outside the United States might find it easier to use http://assistdocs.com/ which does not
sit on a secure website.

MIL-STD-3004C
CONTENT
iii

FOREWORD ........................................................................................................................... ii

1. SCOPE
1.1 Scope ....................................................................................................................1
1.2 Applicability .........................................................................................................1
1.3 Executive Agency ................................................................................................1
1.3.1 Policy ....................................................................................................................1
1.3.2 Responsibility .......................................................................................................1

2. APPLICABLE DOCUMENTS
2.1 General .................................................................................................................2
2.2 Government Documents. ......................................................................................2
2.2.1 Specifications and Standards. ...............................................................................2
2.2.2 Other Government Documents, Drawings, and Publications. .............................6
2.3 Non-Government publications .............................................................................6
2.4 Order of precedence ...........................................................................................12

3. DEFINITIONS, ACRONYMS, and ABBREVIATIONS
3.1 Definition List ....................................................................................................12
3.2 Acronyms and Abbreviations .............................................................................20

4. GENERAL REQUIREMENTS
4.1 Personnel competency. ....................................................................................... 23
4.2 Service/contractor responsibilities. ....................................................................23
4.2.1 Sampling. ............................................................................................................23
4.2.1.1 Precautions. ........................................................................................................23
4.2.1.2 Personnel conducting sampling ......................................................................... 23
4.2.1.3 Responsibility .....................................................................................................23
4.2.1.4 Types of samples. ...............................................................................................23
4.2.1.4.1 All level sample ..................................................................................................23
4.2.1.4.2 Upper sample ......................................................................................................23
4.2.1.4.3 Middle sample. ...................................................................................................23
4.2.1.4.4 Lower sample .................................................................................................... 23
4.2.1.4.5 Top sample. ........................................................................................................23
4.2.1.4.6 Composite sample ..............................................................................................23
4.2.1.4.7 Drain sample. .....................................................................................................23
4.2.1.4.8 Bottom sample. ...................................................................................................23
4.2.1.4.9 Bottom Water sample .........................................................................................23
4.2.1.4.10 Single tank composite sample. ...........................................................................24
4.2.1.4.11 Conveyance composite sample ..........................................................................24
4.2.1.4.12 Outlet (suction) sample ......................................................................................24
4.2.1.4.13 Automatic sample ...............................................................................................24
4.2.1.4.14 Mixed sample. ....................................................................................................24
4.2.1.4.15 Spot sample ........................................................................................................24
4.2.1.4.16 Tube or thief sample. ..........................................................................................24
4.2.1.4.17 Batch/lot samples. ..............................................................................................24
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CONTENT
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4.2.1.5 Taking of samples. .............................................................................................24
4.2.1.5.1 Sampling apparatus, containers, and procedures ...............................................24
4.2.1.5.2 Sample Log Requirements .................................................................................25
4.2.1.6 Precautions. ........................................................................................................25
4.2.1.7 Size of samples. ..................................................................................................26
4.2.1.7.1 Normal sample size. ...........................................................................................28
4.2.1.7.2 Special sample size. ............................................................................................28
4.2.1.7.3 Jet fuel. ...............................................................................................................28
4.2.1.7.4 E85 sample .........................................................................................................26
4.2.1.7.5 B20 sample .........................................................................................................26
4.2.1.8 Identification of samples. ...................................................................................26
4.2.1.8.1 Markings .............................................................................................................26
4.2.1.8.2 Sample serial numbers. ......................................................................................26
4.2.1.8.3 Retained samples. ...............................................................................................26
4.2.1.9 Shipping samples to a laboratory-chain of custody requirements ......................26
4.2.1.10 Gauging and sampling JPTS cargo tanks or vessels. .........................................26
4.2.1.10.1 Contamination problems. ...................................................................................27
4.2.1.10.2 Unaccountable product loss or gain ...................................................................27
4.2.2 Testing. ...............................................................................................................27
4.2.2.1 Contamination tests ............................................................................................27
4.2.2.2 Test methods ......................................................................................................27
4.2.2.3 Testing frequency for long term storage of petroleum products ........................27
4.2.2.4 Minimum testing. ...............................................................................................27
4.2.2.5 Types of tests required. ......................................................................................27
4.2.2.5.1 Equivalent test. ...................................................................................................28
4.2.2.5.2 Predictive testing. ...............................................................................................28
4.2.2.5.3 Alternate test methods. .......................................................................................28
4.2.2.6 Testing capabilities .............................................................................................28
4.2.2.7 Calibrating test equipment .................................................................................28
4.3 Specifications .....................................................................................................28
4.4 Change in grade of fuel ......................................................................................28
4.5 Government owned property. .............................................................................28
4.6 Safety precautions. .............................................................................................29
4.7 Measurement, sampling and calibration. ............................................................29
4.8 Compliance with regulations and laws. ..............................................................29

5. DETAILED REQUIREMENTS
5.1 Waterborne operations. ......................................................................................29
5.1.1 Shipments by tanker. ..........................................................................................29
5.1.1.1 MPMS Guidelines ..............................................................................................29
5.1.1.2 Filtering requirements ........................................................................................29
5.1.1.3 Certifying statements ..........................................................................................29
5.1.1.4 Tanker and ocean-going barge inspection policy for MSC vessels ...................29
5.1.1.4.1 Responsibility .....................................................................................................30
5.1.1.4.2 Required cargo cleaning .....................................................................................30
5.1.1.4.3 Internal Tank Inspection requirements ...............................................................30
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CONTENT
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5.1.1.4.4 Suitability to load ...............................................................................................30
5.1.1.4.5 Quantity variation ...............................................................................................30
5.1.1.4.6 Responsibility for off-specification cargo ..........................................................31
5.1.1.5 Pre-loading inspection of tankers .......................................................................31
5.1.1.5.1 Vessel inspection ................................................................................................31
5.1.1.5.2 Vessel tank inspection ........................................................................................31
5.1.1.5.3 Vessel tank/internal rust test ..............................................................................32
5.1.1.5.4 Vessel loading plans ...........................................................................................32
5.1.1.5.5 Multi-port inspection ..........................................................................................32
5.1.1.5.6 Quality and quantity determination ....................................................................32
5.1.1.5.7 Vessel rejection/delay ........................................................................................32
5.1.1.6 Pre-loading procedures (shore/tanker) ...............................................................33
5.1.1.7 Loading procedures for tankers ..........................................................................33
5.1.1.7.1 Lines ...................................................................................................................36
5.1.1.7.2 Loading rates ......................................................................................................34
5.1.1.7.3 Thirty minute wait ..............................................................................................34
5.1.2 Shipments by barges and refueling craft. ...........................................................34
5.1.2.1 Pre-loading and loading inspection ....................................................................34
5.1.2.2 Product conversion .............................................................................................34
5.1.2.3 Inspection procedures for cargoes ......................................................................34
5.1.3 Receipts from tanker or barge ............................................................................35
5.1.3.1 Shore side. ..........................................................................................................35
5.1.3.1.1 Returns from USN vessels .................................................................................35
5.1.3.2 Vessel pre-discharge inspection .........................................................................35
5.1.3.3 Contaminated product. .......................................................................................36
5.1.3.4 Discharge ............................................................................................................36
5.1.3.5 Completion. ........................................................................................................36
5.1.3.6 Vessel delay ........................................................................................................37
5.1.4 Post loadingtankers and barges. .......................................................................37
5.1.4.1 Vessel samples ...................................................................................................37
5.1.4.2 Determination of quantity ..................................................................................37
5.1.4.3 Inspection documents covering tanker and barge loading .................................37
5.1.5 Ship-to-Ship transfer at Sea ................................................................................37
5.2 Pipeline operations .............................................................................................37
5.2.1 Shipments by pipelines. ......................................................................................37
5.2.1.1 Tariffs and agreements .......................................................................................37
5.2.1.2 Laboratory testing ..............................................................................................38
5.2.1.3 Markings .............................................................................................................38
5.2.1.4 Identification tests ..............................................................................................38
5.2.1.5 Multi-product pipelines ......................................................................................38
5.2.1.5.1 Product identification .........................................................................................38
5.2.1.5.2 Pumping time .....................................................................................................38
5.2.1.5.3 Pipeline transfer velocity ....................................................................................38
5.2.1.5.4 Segregation during transfer ................................................................................38
5.2.1.6 Terminal, depot and base system .......................................................................38
5.2.1.6.1 Product compatibility .........................................................................................38
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CONTENT
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5.2.1.6.2 Cleaning of pipelines ..........................................................................................38
5.2.1.6.3 Valve and pipeline control .................................................................................39
5.2.1.7 Cross Country System. .......................................................................................39
5.2.1.7.1 Turbulent flow ....................................................................................................39
5.2.1.7.2 Batch cuts and segregation .................................................................................39
5.2.1.7.3 Contaminated pipeline shipment ........................................................................39
5.2.1.7.4 System isolation .................................................................................................39
5.2.1.8 Common transfer lines and pumps for fuels. .....................................................39
5.2.1.8.1 Preferred method ................................................................................................39
5.2.1.8.2 Use of water displacement .................................................................................39
5.2.1.8.3 References ..........................................................................................................39
5.2.1.9 Segregation. ........................................................................................................39
5.2.1.10 Corrosion control. ...............................................................................................39
5.2.1.10.1 Determination of sediment (solids) ....................................................................39
5.2.1.10.2 Corrosion inhibitors ............................................................................................40
5.2.1.10.3 Aviation Turbine Fuel Additive Concentration .................................................43
5.2.1.10.3.1 Location .............................................................................................................40
5.2.1.10.4 Pressure Drop .....................................................................................................40
5.2.1.10.5 Drag Reducer Additive (DRA) ..........................................................................40
5.2.1.11 Quality surveillance pipeline procedures ...........................................................40
5.2.2 Receipts by pipeline. ..........................................................................................41
5.2.2.1 Before receipt. ....................................................................................................41
5.2.2.2 During receipt. ....................................................................................................41
5.2.2.3 Completion .........................................................................................................41
5.3 Truck and tank car operations ............................................................................41
5.3.1 Shipments by tank trucks and tank car. ..............................................................41
5.3.1.1 Tank truck and tank car service/conversion. ......................................................41
5.3.1.2 Tank truck and tank car conversion policy ........................................................41
5.3.1.2.1 Exception/quality data ........................................................................................42
5.3.1.3 Tank truck and tank car loading. ........................................................................42
5.3.1.3.1 Safety ..................................................................................................................42
5.3.1.3.2 Loading line ........................................................................................................42
5.3.1.3.3 Procedures at the loading rack ...........................................................................42
5.3.1.3.4 NATO codes .......................................................................................................43
5.3.1.3.5 Gaskets and hose connections ............................................................................43
5.3.1.3.6 Vehicle tank cleanliness .....................................................................................43
5.3.1.3.7 Product free fall ..................................................................................................43
5.3.1.3.8 Recording test results .........................................................................................43
5.3.1.3.9 Sealing ................................................................................................................43
5.3.1.3.10 Placarding ...........................................................................................................43
5.3.2 Tank truck and tank car receipts ........................................................................43
5.3.2.1 Before receipt .....................................................................................................43
5.3.2.2 Truck and tank car arrival. .................................................................................43
5.3.2.3 Truck and tank car rejection. ..............................................................................44
5.3.2.4 After discharge ...................................................................................................44
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CONTENT
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5.4 Receipts of motor gasolines, diesels and heating oils under the
post camp & station (PC&S) purchase program ................................................44
5.4.1 Truck and tank car arrival/before delivery. ........................................................45
5.4.1.1 Truck and tank car after delivery/before departure. ...........................................45
5.4.2 Barge delivery. ...................................................................................................45
5.5 Receipts from the bunkering program. ...............................................................45
5.5.1 Before bunkering. ...............................................................................................46
5.5.2 During bunkering. ..............................................................................................46
5.5.3 After bunkering. .................................................................................................46
5.5.4 Bunker Delivery Note and Statutory Sample ....................................................47
5.6 Receipts from the into-plane program. ...............................................................47
5.6.1 AIR Card ............................................................................................................47
5.6.2 Refueling units ...................................................................................................47
5.7 Receipt of aviation Secured Fuel and supporting aircraft ..................................47
5.7.1 Refueling on military installations .....................................................................47
5.7.2 Refueling at other locations ................................................................................48
5.7.3 Invoice/acquisition procedures ...........................................................................48
5.7.3.1 Contractual laboratory Invoice Procedures .......................................................48
5.7.3.2 Non-contract locations .......................................................................................48
5.8 Receipt of approved additives and injection. .....................................................48
5.8.1 Receipt of approved bulk additives ....................................................................48
5.8.1.1 Receipt of turbine fuel approved packaged additives ........................................48
5.8.2 During injection. .................................................................................................49
5.8.3 After injection. ...................................................................................................49
5.9 Bulk storage. .......................................................................................................49
5.9.1 Long-term storage. .............................................................................................49
5.9.2 Bulk tank water restriction. ................................................................................50
5.9.2.1 Corrosives in tanks. ............................................................................................53
5.9.2.2 Tank water check frequency...............................................................................50
5.9.2.3 Microbial Contamination ...................................................................................50
5.9.3 Storage tanks and piping. ...................................................................................50
5.9.3.1 Storage of similar products. ...............................................................................50
5.9.3.2 Changing product in a storage tank. ...................................................................50
5.9.3.3 Product cargo check for quality. ........................................................................51
5.9.3.4 Segregation of product. ......................................................................................51
5.9.3.5 Leaking valve contamination. ............................................................................51
5.9.3.6 Tank protective treatment. ..................................................................................51
5.9.3.7 Identification of piping system. ..........................................................................51
5.9.3.8 Settling time in tank. ..........................................................................................51
5.9.4 Control of static electricity (aviation turbine fuels, kerosene). ..........................52
5.9.5 Filtration. ............................................................................................................53
5.9.6 Internal preservation. ..........................................................................................53
5.9.7 Dispensing from curbside pumps. ......................................................................53
5.9.8 Deterioration of a product. .................................................................................53
5.9.9 Sources of contamination. ..................................................................................53
5.9.9.1 Inadvertent mixtures. ..........................................................................................53
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CONTENT
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5.9.9.2 Handling personnel. ...........................................................................................53
5.9.9.3 Rubber surface to fuel ........................................................................................53
5.9.9.4 Container sealant. ...............................................................................................54
5.9.10 Identification of transfers. ..................................................................................54
5.10 Product Governmental receipt limits (Tables I-VII). .........................................54
5.10.1 Gasoline, aviation, NATO F-18 (ASTM D 910/100 LL) and Unleaded Aviation
Gasoline ASTM D7547 ..................................................................................... 54
5.10.1.1 Knock rating. ......................................................................................................54
5.10.1.2 Color. ..................................................................................................................54
5.10.1.3 Vapor Pressure (VP) ...........................................................................................54
5.10.1.4 Corrosion. ...........................................................................................................54
5.10.1.5 Water and sediment ............................................................................................55
5.10.2 Aviation turbine fuel, NATO F-34/JP-8 (MIL-DTL-83133), F-35/Jet A-1,
Jet A (ASTM D 1655), F-40/JP-4, F-44/JP-5 (MIL-DTL-5624), JPTS
(MIL-DTL-25524), TS-1 (GOST 10227-86) .....................................................55
5.10.2.1 Existent gum. ......................................................................................................55
5.10.2.2 Vapor pressure(VP) ............................................................................................55
5.10.2.3 Corrosion. ...........................................................................................................55
5.10.2.4 Fuel system icing inhibitor (FSII). .....................................................................55
5.10.2.5 Flash point specification. ....................................................................................56
5.10.2.6 Filtration time. ....................................................................................................56
5.10.2.7 Water and sediment. ...........................................................................................56
5.10.2.8 Conductivity. ......................................................................................................56
5.10.2.9 Thermal Stability of JP-5 ...................................................................................56
5.10.2.10 Fuel Standardization Policy ...............................................................................56
5.10.2.11 Other Aviation Fuel Specifications ....................................................................57
5.10.3 Gasoline, automotive, unleaded (F-67). .............................................................57
5.10.3.1 Octane .................................................................................................................57
5.10.3.2 Color. ..................................................................................................................57
5.10.3.3 Existent gum. ......................................................................................................57
5.10.3.4 Lead content .......................................................................................................57
5.10.3.5 Copper Strip Corrosion ......................................................................................57
5.10.3.6 Vapor Pressure (VP) ...........................................................................................57
5.10.4 Automotive spark ignition engine fuel (commercial gasoline)
(ASTM D 4814) and gasohol, automotive, unleaded (A-A-52530)...................57
5.10.4.1 Octane .................................................................................................................58
5.10.4.2 Existent gum .......................................................................................................58
5.10.4.3 Lead content .......................................................................................................58
5.10.4.4 Copper Strip Corrosion. .....................................................................................58
5.10.4.5 Vapor Pressure ...................................................................................................58
5.10.4.6 Alcohol content. .................................................................................................58
5.10.4.7 Water tolerance ..................................................................................................58
5.10.5 E85 .....................................................................................................................58
5.10.6 Fuel, naval distillate, NATO F-76 (MIL-DTL-16884) ......................................59
5.10.6.1 Cetane number (ignition quality). ......................................................................59
5.10.6.2 Color ...................................................................................................................59
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CONTENT
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5.10.6.3 Flash point ..........................................................................................................59
5.10.6.4 Distillation. .........................................................................................................59
5.10.6.5 Carbon residue on 10% bottoms ........................................................................59
5.10.6.6 Storage Stability .................................................................................................59
5.10.6.7 Water and sediment ............................................................................................60
5.10.7 Fuel oil, diesel, (ASTM D 975) ..........................................................................60
5.10.7.1 RME 180 ...........................................................................................................60
5.10.7.2 RME 380 ............................................................................................................60
5.10.7.3 Water and sediment control ................................................................................60
5.10.7.4 Cetane number ....................................................................................................60
5.10.7.5 Dyed fuel. ...........................................................................................................60
5.10.7.6 Distillation ..........................................................................................................60
5.10.7.7 Cloud point. ........................................................................................................61
5.10.7.8 Carbon residue on 10% bottoms. .......................................................................61
5.10.8 Kerosene, NATO F-58 (ASTM D 3699). ..........................................................61
5.10.8.1 Color. ..................................................................................................................61
5.10.8.2 Flash point. .........................................................................................................61
5.10.8.3 Sulfur. .................................................................................................................61
5.10.9 Diesel Fuel, Biodiesel blend, B20 (ASTM D7467) ...........................................61
5.11 Aviation fuel contamination and quality standards ............................................61
5.11.1 Gasoline and turbine fuel differences ................................................................61
5.11.2 Quality fuel deliveries. .......................................................................................62
5.11.3 Fuel quality and fuel contamination. ..................................................................62
5.11.3.1 Commingling with other petroleum products ....................................................62
5.11.3.2 Contamination with water, solids, and microbiological growth. .......................62
5.11.4 Acceptable fuel. ..................................................................................................63
5.11.4.1 Free water ...........................................................................................................63
5.11.4.2 Red dye contamination .......................................................................................63
5.11.4.3 Cloudy or hazy fuel ............................................................................................64
5.11.4.4 Sediment in fuel .................................................................................................64
5.12 Ground mobility fuel contamination. .................................................................64
5.12.1 Ground mobility fuels ........................................................................................64
5.12.1.1 Automotive gasoline ..........................................................................................64
5.12.1.2 Diesel fuel ..........................................................................................................64
5.12.1.3 Aviation turbine fuel ..........................................................................................64
5.12.2 Fuel contamination and contamination prevention. ...........................................65
5.12.2.1 Contamination with other fuels (commingling). ................................................65
5.12.2.2 Contamination with water ..................................................................................65
5.12.2.3 Contamination with sediment .............................................................................66
5.12.2.4 Fuel contamination prevention. ..........................................................................66
5.13 Non-conforming product ....................................................................................67
5.13.1 Identification of a non-conforming product. ......................................................67
5.13.2 Disposition request procedures ..........................................................................67
5.13.2.1 Report of non-conforming product exceptions ..................................................69
5.13.3 Service and DLA responsibilities. ......................................................................69
5.13.3.1 Communication copies .......................................................................................70
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5.13.4 Chain of custody requirement for all samples shipped to a laboratory ..............70
5.13.5 Laboratory reports ..............................................................................................70
5.13.6 Reclamation ........................................................................................................70
5.13.6.1 Determining factors ............................................................................................71
5.13.7 Reclamation techniques ......................................................................................71
5.13.7.1 Downgrading ......................................................................................................71
5.13.7.2 Blending. ............................................................................................................71
5.13.7.3 Additive injection/mixing. .................................................................................71
5.13.7.4 Purification. ........................................................................................................71
5.13.7.5 Water removal ....................................................................................................71
5.14 Packaged products ..............................................................................................71
5.14.1 Product receipt ....................................................................................................71
5.14.2 Sampling. ............................................................................................................71
5.14.2.1 Precautions .........................................................................................................72
5.14.2.2 Personnel to conduct sampling ...........................................................................72
5.14.2.3 Responsibility .....................................................................................................72
5.14.2.4 Types of samples ................................................................................................72
5.14.2.5 Sampling apparatus, containers and procedures ................................................72
5.14.2.6 Size of samples ...................................................................................................72
5.14.2.7 Identification of samples ....................................................................................73
5.14.3 Testing. ...............................................................................................................74
5.14.3.1 Contamination tests ............................................................................................74
5.14.3.2 Test methods. .....................................................................................................74
5.14.3.3 Specification receipt limits .................................................................................74
5.14.3.4 Testing frequency. ..............................................................................................74
5.14.3.5 Minimum testing ................................................................................................74
5.14.3.6 Tests required. ....................................................................................................74
5.14.3.7 Alternate test methods ........................................................................................74
5.14.3.8 Calibrating test equipment .................................................................................75
5.14.4 Disposition procedures .......................................................................................75
5.14.5 Service and DLA responsibilities. ......................................................................75
5.14.6 Packaging and storage of packaged petroleum products....................................76
5.14.6.1 Documentation. ..................................................................................................76
5.14.6.2 Container inspection. ..........................................................................................76
5.14.6.3 Container suitability. ..........................................................................................76
5.14.6.4 Drum storage. .....................................................................................................76
5.14.6.5 Separate storage. .................................................................................................76
5.14.6.6 Stock rotation. ....................................................................................................77
5.14.6.7 Galvanized containers ........................................................................................77
5.14.6.8 Small container storage ......................................................................................77
5.14.6.9 Contamination ....................................................................................................77
5.14.6.10 Minimum container markings. ...........................................................................77
5.14.6.11 Field-filled container markings ..........................................................................77
5.14.6.12 Marking of boxes and cartons ............................................................................78
5.14.6.13 Marking of contractor supplied product .............................................................78
5.14.6.14 Marking of used drums ......................................................................................78
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5.14.7 Deterioration of products. ..................................................................................78
5.14.7.1 Lubricating oils and gear oils. ............................................................................78
5.14.7.2 Hydraulic fluids. .................................................................................................79
5.14.7.3 Greases. ..............................................................................................................79
5.14.7.4 Insulating oils. ....................................................................................................80

6. NOTES
6.1 Intended use. .......................................................................................................80
6.2 International standard agreements. .....................................................................80
6.3 Tailoring guidance. .............................................................................................80
6.4 Subject term (key word list) ...............................................................................80
6.5 Additional references .........................................................................................81
6.6 Changes from previous issue ..............................................................................83

TABLES
I Intra-Governmental receipt limits for aviation turbine fuels:
NATO F-34/JP-8 (MIL-DTL-83133), F-35/Jet A-1, Jet A,
(ASTM D 1655), F-40/JP-4 and F-44/JP-5 (MIL-DTL-5624)
and TS-1 (GOST 10227-86) ...............................84
II Intra-Governmental receipt limits for fuel system icing inhibitor,
MIL-DTL-85470, NATO S-1745 ......................................................................85
III Intra-Governmental receipt limits for fuel, naval distillate, NATO
F-76 (MIL-DTL-16884) .....................................................................................85
IV Intra-Governmental receipt limits for fuel oil, diesel,
ASTM D975 .......................................................................................................86
V Intra-Governmental receipt limits for fuel oil, diesel, NATO F-54 ...................86
VI Intra-Governmental receipt limits for gasoline, unleaded,
NATO F-67, and STANG 7090 .........................................................................87
VII Intra-Governmental receipt limits for automotive spark ignition engine
fuel, ASTM D 4814, and gasohol, automotive, unleaded, A-A-52530 ..............88
VIII Minimum frequency for testing long term storage of petroleum products ........88
IX Minimum sampling and testing requirements for petroleum products ..............89
X Tests required, aviation gasoline ........................................................................96
XI Tests required, lubrication oils ...........................................................................96
XII Tests required, aviation turbine fuels .................................................................97
XIII Support for Secured Fuel ....................................................................................97
XIV Tests required automotive gasoline ....................................................................98
XIVa Tests required E85 (ASTM D5798) ...................................................................99
XV Tests required on diesel fuels and kerosene. ......................................................99
XVa Tests required B20 ...........................................................................................100
XVI Tests required burner fuels. ..............................................................................100
XVII Tests required on Residual Marine Fuel (RME 180 Grade) ........................... 100
XVIII Tests required on Residual Marine Fuel (RME 380 Grade) ...........................101
XIX Test required on Marine Gas Oil (DMA Grade) .............................................101
XX Type B-2 tests for lubricating oils ....................................................................102
XXI Type B-2 tests for greases, semi-fluid lubricants, and other
grease-like materials ........................................................................................107
MIL-STD-3004C
CONTENT
xii

XXII Type B-2 tests for hydraulic, brake, and shock absorber fluids .......................112
XXIII Type B-2 tests for lubricants (including solid film) .........................................115
XXIV Type B-2 tests for waxes ..................................................................................117
XXV Type B-2 tests for misc. products (specialty, cutting fluids, anti-seize, etc.) ..118
XXVI Conversion chart for tank cars and trucks. .......................................................123
XXVII Minimum requirements for the preparation of tanker cargo tanks ...................124
XXVIII Minimum requirements for the preparation of barge cargo tanks. ...................126
XXIX Segregation of product movements via multiproduct pipelines,
head product .....................................................................................................127
XXX Contamination tables. .......................................................................................128
XXXI Minimum standards of filtration and water separation for petroleum
products ............................................................................................................129
C-I Significant Coal Characteristics Combustion Performance .............................161
C-II Coal Analysis ...................................................................................................166

TEST METHODS
1000 Test for the effectiveness of pipeline rust inhibitors .........................................130
1010 Visual quality surveillance test .........................................................................132
1020 Test for sulfides in water...................................................................................134
1030 Determination of small amounts of lead in fuels ..............................................136
1040 Detection of heavy hydrocarbon contamination in aviation gasoline ...............138
1050 Detection of nitrate ignition-type improvers in diesel fuel ...............................142
1060 Determination of free water in aviation and turbine fuels using
the AEL MK I or MK II fuel detector (NSN 6640-00-999-2786) ....................144
1070 Test for water reaction of aviation fuels ...........................................................146

FIGURES
1. Chromatography strip holder............................................................................140
B-1. Conductivity .....................................................................................................154
C-1. Weights and increments ...................................................................................171
C-2. Car top sampling ..............................................................................................172
E-1. Sample calculation product change record .......................................................185
F-1. Example Chain of Custody Document Page 1 .................................................187
F-2. Example Chain of Custody Document Page 2 .................................................188

APPENDIX
A Military services petroleum laboratories and fuel testing capabilities .............148
B Significance of tests .........................................................................................152
C Receipt and quality surveillance of coal...........................................................160
D Government quality surveillance of fuel ..........................................................176
E Product change record ......................................................................................183
F Petroleum sample chain of custody document .................................................186

INDEX ..........................................................................................................................189

CONCLUDING MATERIAL ...............................................................................................203
MIL-STD-3004C
1

1. SCOPE
1.1 Scope. This Standard provides DoD Policy, general instructions, and minimum procedures
to be used by the Military Services and the Defense Logistics Agency in performing quality assurance/
surveillance functions of U. S. Government-owned fuels, lubricants, and related products worldwide at
all locations except product procurement facilities which are covered by requirements contained in the
contract. Requirements for procurement needs may be derived from this document as necessary.
This Standard includes policy and responsibilities derived from Executive Agency (see 1.3 below)
documents. The information contained herein is appropriate to quality assurance where applicable (e.g.
direct delivery to customers, destination acceptance, etc.). This Standard also contains intra-
Governmental receipt limits.
1.2 Applicability. Quality assurance (QA) is a planned and systematic pattern of all actions
necessary to give confidence that adequate technical requirements are established; products and
services conform to established technical requirements; and satisfactory performance is achieved. For
the Government, Contract Quality Assurance is a method to determine if supplier of product and /or
services fulfilled its contract obligations pertaining to products and/or services provided. It includes all
actions required to ensure the Government is receiving the proper products and/or services. By
common usage, Petroleum Quality Assurance responsibility is fulfilled when the product and/or service
are accepted by the Government and the product no longer belongs to the contractor or when the
service is complete. Quality surveillance (QS), as used herein, is the aggregate of measures (blending,
stock rotation, sampling, etc.) used to determine and maintain the quality of product receipts and
Government-owned bulk petroleum products to the degree necessary to ensure that such products are
suitable for their intended use. A vigilant quality surveillance program, implemented by properly
trained personnel, is necessary to protect the original product quality and the interests of the
Government. Policy and procedures discussed for QS on receiving Government-owned fuel apply to
Military Service acceptance requirements for fuels purchased by DLA Energy under the Bulk and
Direct Delivery program groups (Bunkers & Post, Camps and Stations).
1.3 Executive Agency. Pursuant to the authority of the Secretary of Defense, DoD Directive
5101.8, DoD Executive Agent (DoD EA) for Bulk Petroleum, 11 August 2004, designates the Director,
Defense Logistics Agency (DLA), as the DoD Executive Agent (EA) for Bulk Petroleum for the
Department of Defense (DoD), with authority to re-delegate to the Defense Logistics Agency Energy.
1.3.1 Policy. The DoD EA for Bulk Petroleum will execute supply chain management for all
Bulk Petroleum owned by the Department of Defense and be responsible for all Bulk Petroleum supply
management (to include quality management). The DoD EA for Bulk fuels will be responsible for
coordination with Defense customers, other Federal Agencies, and friendly forces where the United
States is the designated fuels Role Support Nation.
1.3.2 Responsibility. In conjunction with the other DoD Components, DLA Energy will develop
standardized quality policy and procedures across the supply chain to reflect weapon systems
requirements and maximize effectiveness and efficiency.

MIL-STD-3004C
2

2. APPLICABLE DOCUMENTS
2.1 General. The documents listed in this section are specified in sections 3, 4, and 5 of this
Standard. This section does not include documents cited in other sections of this Standard nor does it
include those recommended as additional information or examples. While every effort has been made
to ensure the completeness of this list, document users are cautioned that they must meet all specified
requirements of documents cited in sections 3, 4, and 5 of this Standard, whether they are listed or not.
2.2 Government Documents.
2.2.1 Specifications and Standards. The following specifications and standards form a part of this
document to the extent specified herein. Unless otherwise specified, the issues of these documents are
those cited in the solicitation or contract.
INTERNATIONAL STANDARDIZATION AGREEMENTS
STANAG- 1110 Allowable Deterioration Limits for NATO Armed Forces Fuels,
Lubricants and Associated Products
STANAG- 3149 Minimum Quality Surveillance of Petroleum Products
STANAG- 3390 Guide Specification and Inspection Standards for Fuel Soluble
Lubricity Improvers
STANAG- 3609 Standards for Maintenance of Fixed Aviation Fuel Receipt, Storage
and Dispensing Systems
STANAG- 7036 Fuels to be Introduced Into and Delivered by the NATO Pipeline
System (NPS)
STANAG- 7090 Guide Specification for NATO Ground Fuels
FEDERAL SPECIFICATIONS
C-T-91 Tallow, Inedible
O-M-232 Methanol (Methyl Alcohol)
SS-G-659 Graphite, Dry (Lubricating)
TT-I-735 Isopropyl Alcohol
VV-C-846 Cutting Fluids: Emulsifiable Oils
VV-D-1078 Damping Fluid, Silicone Base (Dimethyl Polysiloxane)
VV-G-632 Grease, Industrial, General Purpose
VV-G-671 Grease, Graphite
VV-P-236 Petrolatum, Technical
VV-L-825 Lubricating Oil, Refrigerant Compressor, Uninhibited

FEDERAL STANDARDS
FED-STD-791 Testing Method of Lubricants, Liquid Fuels, and Related Products

MIL-STD-3004C
3

COMMERICAL ITEM DESCRIPTION
A-A-52530 Gasohol, Automotive, Unleaded
A-A-59113 Lubricating Oil, Machine Tool Sideways
A-A-59137 Lubricating Oil, Breech Block (for Naval Ordnance)
A-A-59173 Grease, Silicone
A-A-59290 Hydraulic Fluid, Arresting Gear
A-A-59354 Hydraulic Fluid, Petroleum Base, for Machine Tools
A-A- 59004 Anti-Galling Compound, Thread Lubricating, Seizing Resistant, and
Calcium Hydroxide Containing
A-A-50178 Wax, Machine Stitching
A-A-59255 Wax, Paraffin, Technical
A-A-50493 Oil, Penetrating (for Loosening Frozen Metallic Parts)
A-A-52624 Antifreeze, Multi Engine Type
A-A-58092 Tape, Antiseize, Polytetrafluorethylene
A-A-59197 Fatty Oil (for Metal-Working Lubricants)
DEPARTMENT OF DEFENSE SPECIFICATIONS
DOD-G-24508 Grease, High Performance, Multipurpose (Metric)
DOD-G-24650 Grease, Food Grade, Food Processing Equipment (Metric)
DOD-L-25681 Lubricant Molybdenum Disulfide, Silicone
DOD-L-81846 Lubricating Oil, Instrument, Ball Bearing, High Flash Point
DOD-PRF-24574 Lubricating Fluid for Low and High Pressure Oxidizing Gas Mixtures
DOD-PRF-85734 Lubricating Oil, Helicopter Transmission System, Synthetic Base
MIL-C-6529 Corrosion Preventive, Aircraft Engine
MIL-C-11796 Corrosion Preventive Compound, Petrolatum, Hot Application
MIL-DTL-3918 Lubricating Oil, Instrument, Jewel Bearing
MIL-DTL-4339 Corrosion Preventive, Soluble Oil for Water Injection Systems (NATO
Code Number C-630)
MIL-DTL-5020 Liquid, Compass, Aircraft
MIL-DTL-5624 Turbine Fuel, Aviation, Grades JP-4 and JP-5
MIL-DTL-16884 Fuel, Naval Distillate
MIL-DTL-17111 Fluid, Power Transmission
MIL-DTL-23549 Grease, General Purpose
MIL-DTL-25524 Turbine Fuel, Aviation Thermally Stable (JPTS)
MIL-DTL-46014 Lubricating Oil, Spindle
MIL-DTL-83133 Turbine Fuel, Aviation, Kerosene Type, JP-8 (NATO F-34, NATO F-35,
and JP-8+100 (NATIO F-37)
MIL-DTL-85470 Inhibitor, Icing, Fuel System, High Flash NATO Code S-1745
MIL-STD-3004C
4

MIL-G-14931 Grease, Silicone for Use with Ammunition
MIL-G-21164 Grease, Molybdenum Disulfide, for Low and High Temperatures, NATO
Code Number G-353
MIL-G-25013 Grease, Aircraft, Ball and Roller Bearing, NATO Code Number G-372,
Metric
MIL-G-25537 Grease, Aircraft, Helicopter Oscillating Bearing, NATO Code Number
G-366, Metric
MIL-G-81827 Grease, Aircraft, High Load Capacity, Wide Temperature Range
MIL-L-11734 Lubricating Oil, Synthetic (for Mechanical Time Fuses)
MIL-L-15719 Lubricating Grease (High-Temperature, Electric Motor, Ball and Roller
Bearings)
MIL-L-19701 Lubricant, All-Weather, Semi-Fluid, for Aircraft Ordnance, Metric
MIL-L-23398 Lubricant, Solid Film, Air-Cured, Corrosion Inhibiting, NATO Code
Number S-749
MIL-L-24131 Lubricant, Colloidal Graphite in Isopropanol
MIL-L-24478 Lubricant, Molybdenum Disulfide in Isopropanol
MIL-L-45983 Lubricant, Solid Film: Heat Cured (Temperature Range 125 to 250F
(51.8 to 121C)), Corrosion Inhibiting
MIL-L-46000 Lubricant, Semi-Fluid (Automatic Weapons)
MIL-L-46150 Lubricant, Weapons, Semi-Fluid (High Load-Carrying Capacity)
MIL-L-87177 Lubricants, Water Displacing, Synthetic
MIL-H-19457 Hydraulic Fluid, Fire-Resistant, Non-Neurotoxic
MIL-H-22072 Hydraulic Fluid, Catapult, NATO Code Number H-579
MIL-H-81019 Hydraulic Fluid, Petroleum Base, Ultra-Low Temperature, Metric
MIL-PRF-2104 Lubricating Oil, Internal Combustion Engine Combat/ Tactical Service
MIL-PRF-3150 Lubrication Oil, Preservative, Medium
MIL-PRF-3572 Lubricant, Colloidal Graphite in Oil
MIL-PRF-5606 Hydraulic Fluid, Petroleum Base; Aircraft, Missile, and Ordnance
MIL-PRF-6081 Lubricating Oil, Jet Engine
MIL-PRF-6083 Hydraulic Fluid, Petroleum Base, for Preservation and Operation
MIL-PRF-6085 Lubricating Oil: Instrument, Aircraft, Low Volatility
MIL-PRF-6086 Lubricating Oil, Gear, Petroleum Base
MIL-PRF-7808 Lubricating Oil, Aircraft Turbine Engine, Synthetic Base
MIL-PRF-7870 Lubricating Oil: General Purpose, Low Temperature
MIL-PRF-8188 Corrosion-Preventive, Aircraft Turbine Engine, Synthetic Base
MIL-PRF-9000 Lubrication Oil, Shipboard Internal Combustion Engine, High-Output Diesel
MIL-PRF-10924 Grease, Automotive and Artillery
MIL-PRF-12070 Fog Oil
MIL-PRF-14107 Lubricating Oil, Weapons, Low Temperature
MIL-STD-3004C
5

MIL-PRF-16173 Corrosion Preventive Compound, Solvent Cutback, Cold-Application
MIL-PRF-17331 Lubricating Oil, Steam Turbine and Gear, Moderate Service
MIL-PRF-17672 Hydraulic Fluid, Petroleum, Inhibited
MIL-PRF-18458 Grease, Wire Rope - Exposed Gear
MIL-PRF-21260 Lubricating Oil, Internal Combustion Engine, Preservative Break-in
MIL-PRF-23699 Lubricating Oil, Aircraft Turbine Engine, Synthetic Base, NATO Code
Number O-156
MIL-PRF-23827 Grease, Aircraft and Instrument, Gear and Actuator Screw
MIL-PRF-24139 Grease, Multipurpose, Water Resistant
MIL-PRE-25017 Hydraulic Fluid, Fire Resistant, Hydrogenated Polyalphaolefin Base
MIL-PRF-27601 High Temperature, Flight Vehicle, Metric
MIL-PRF-26087 Lubricating Oil, Reciprocating Compressor, Ground Support
MIL-PRF-27617 Grease, Aircraft and Instrument, Fuel and Oxidizer Resistant
MIL-PRF-32033 Lubricating Oil, General Purpose, Preservative (Water-Displacing, Low
Temperature)
MIL-PRF-46002 Preservative Oil, Contact and Volatile Corrosion-Inhibited
MIL-PRF-46010 Lubricant, Solid Film, Heat Cured, Corrosion Inhibiting NATO Code S-1738
MIL-PRF-46147 Lubricant, Solid Film, Air Cured, Corrosion Inhibiting
MIL-PRF-46170 Hydraulic Fluid, Rust Inhibited, Fire Resistant, Synthetic Hydrocarbon Base,
NATO Code No. H-544
MIL-PRF-46176 Brake Fluid, Silicone, Automotive, All-Weather, Operational and
Preservative
MIL-PRF-52308 Filter-Coalescer Element, Fluid Pressure
MIL-PRF-46167 Lubricating Oil, Internal Combustion Engine, Arctic
MIL-PRF-53074 Lubricating Oil, Steam-Cylinder, Mineral
MIL-PRF-63460 Lubricant, Cleaner and Preservative for Weapons and Weapons Systems
MIL-PRF-81329 Lubricant, Solid Film, Extreme Environment, NATO Code Number S-1737
MIL-PRF-81322 Grease, Aircraft, General Purpose, Wide Temperature Range, NATO Code
G-395
MIL-PRF-83261 Grease, Aircraft, Extreme Pressure, Anti-Wear
MIL-PRF-83282 Hydraulic Fluid, Fire Resistant, Synthetic Hydrocarbon Base, Metric, NATO
Code Number H-537
MIL-PRF-83363 Grease, Transmission, Helicopter
MIL-PRF-85336 Lubricant, All-Weather, (Automatic Weapons)
MIL-PRF-87100 Lubricating Oil, Aircraft Turbine Engine, Polyphenyl Ether Base
MIL-PRF-87252 Coolant Fluid, Hydrolytically Stable, Dielectric
MIL-PRF-87257 Hydraulic Fluid, Fire Resistant; Low Temperature, Synthetic Hydrocarbon
Base, Aircraft and Missile
MIL-T-17128 Transducer Fluid, Sonar
MIL-STD-3004C
6

MIL-W-10885 Wax, Impregnating, Waterproofing, for Laminated Paper Tubes for Small
Arms Ammunition
MIL-W-12062 Wax, Petroleum (Metric)
MIL-W-12598 Wax, Microcrystalline, Impregnating
MIL-W-13945 Wax, Hydrocarbon (for Ordnance Use)
MIL-W-20553 Wax, Desensitizing

DEPARTMENT OF DEFENSE STANDARDS
MIL-STD-161 Identification Methods for Bulk Petroleum Products Systems, Including
Hydrocarbon Missile Fuels
MIL-STD-290 Packaging and Marking of Petroleum and Related Products
MIL-STD-1548 Into-Plane Servicing of Fuels at Commercial Airports
(Copies of these documents are available online at https://assist.daps.dla.mil/, from ASSIST Shopping
Wizard (https://assist.daps.dla.mil/wizard), by phoning the ASSIST Customer Service Desk, 215-697-
6396, Mon-Fri, 0730 to 1600 EST, or by writing the Standardization Document Order Desk, 700 Robbins
Avenue, Building 4D, Philadelphia, PA 19111-5094).
2.2.2 Other Government Documents, Drawings and Publications. The following other
Government documents, drawings and publications form a part of this document to the extent specified
herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or
contract.
DOD DIRECTIVES
DoDD 4140.25 DoD Management Policy for Energy Commodities and Related Services
DOD Directive 5101.8 DoD Executive Agent (DoD EA) for Bulk Petroleum
DOD PUBLICATIONS
DODM 4140.25-M DoD Management of Bulk Petroleum Products, Natural Gas, and Coal
(Copies of these documents are available online at http://www.dtic.mil/whs/directives/index.html or from
DLA Administrative Support Center, 8725 John J. Kingman Road, STE 0119, Fort Belvoir, VA 22060-
6220)
2.3 Non-Government publications. The following documents form a part of this document to the
extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the
solicitation or contract.
AIR AND SPACE INTEROPERABILITY COUNCIL (ASIC)
AIR STD 15/04K Allowable Deterioration Limits for Stored Fuels, Lubricants, and Associated
Products
(Copies of this document are available online at http://www.dtic.mil/asic/index.htm or by writing Defense
Technical Information Center 8725 John J. Kingman Road, Suite 0944, Fort Belvoir, VA 22060-6218)
MIL-STD-3004C
7

AMERICAN GEAR MANUFACTURERS ASSOCIATION (AGMA)
ANSI/AGMA 9005 Industrial Gear Lubrication
(Copies of these documents are available online at http://www.agma.org/ from American Gear
Manufacturers Association, 500 Montgomery Street, Suite 350, Alexandria, VA 22314)
AMERICAN NATIONAL STANDARDS INSTITUTE (ANSI)
ANSI/ASQ Z1.4 Sampling Procedures and Tables for Inspection by Attributes
ANSI/NCSL Z540.3 Requirements for the Calibration of Measuring and Test Equipment
(Copies of these documents are available online at http://www.ansi.org or from American National
Standards Institute, 11 West 42nd Street, 13th floor, New York, N.Y. 10036)
AMERICAN PETROLEUM INSTITUTE (API)
API/IP MPMS API Manual of Petroleum Measurement Standards
ENERGY INSTITUTE (EI)
EI1583 Laboratory Tests and Minimum Performance Levels for Aviation Fuel Filter
Monitors
EI 1581 Specifications and Qualifications Procedures for Aviation Jet Fuel
Filter/Separators
EI 1590 Specifications and Qualification Procedures for Aviation Fuel Microfilters
HM 50 Hydrocarbon Management-Guideline for the cleaning of tanks and lines for
marine tank vessels carrying petroleum and refined products
IP 170 Determination of Flash Point Abel Closed Cup Method
IP 224 Determination of low lead content of light petroleum distillates by dithizone
extraction and calorimetric determination
(Copies of these documents are available online at http://www.energyinstitute.org.) or from Energy
Institute, 61 New Cavendish Street, London W1G 7AR, UK.

ASTM INTERNATIONAL
ASTM Manual 5 Aviation Fuel Quality Control Procedures
ASTM Sec 05/Vol 05.05 Combustion Characteristics; Manufactured Carbon and Products,
Catalysts
ASTM D56 Standard Test Method for Flash Point by Tag Closed Cup Tester (DoD
adopted)
ASTM D86 Standard Test Method for Distillation of Petroleum Products at
Atmospheric Pressure (DoD adopted)
ASTM D93 Standard Test Methods for Flash-Point by Pensky-Martens Closed Cup
Tester (DoD adopted)
MIL-STD-3004C
8

ASTM D130 Standard Test Method for Corrosiveness to Copper from Petroleum
products by Copper Strip Test (DoD adapted)
ASTM D323 Standard Test Method for Vapor Pressure of Petroleum Products (Reid
Method) (DoD adopted)
ASTM D381 Standard Test Method for Existent Gum in Fuels by Jet Evaporation
(DoD adopted)
ASTM D482 Standard Test Method for Ash from Petroleum Products (DoD adopted)
ASTM D524 Standard Test Method for Ramsbottom Carbon Residue of Petroleum
Products (DoD adopted)
ASTM D613 Standard Test Method for Cetane Number of Diesel Fuel Oil (DoD
adopted)
ASTM D664 Standard Test Method for Acid Number of Petroleum Products by
Potentiometric Titration (DoD adopted)
ASTM D665 Standard Test Method for Rust-Preventing Characteristics of Inhibited
Mineral Oil in the Presence of Water (DoD adopted)
ASTM D892 Standard Test Method for Foaming Characteristics of Lubrication Oils
(DoD adopted)
ASTM D909 Standard Test Method for Supercharge Rating of Spark-Ignition
Aviation Gasoline (DoD adopted)
ASTM D910 Standard Specification for Aviation Gasolines (DoD adopted)
ASTM D975 Standard Specification for Diesel Fuel Oils (DoD adopted)
ASTM D 976 Standard Test Methods for Calculated Cetane Index of Distillate Fuels
(DoD adopted)
ASTM D1094 Standard Test Method for Water Reaction of Aviation Fuels (DoD
adopted)
ASTM D1298 Standard Test Method for Density, Relative Density (Specific Gravity),
or API Gravity of Crude Petroleum and Liquid Petroleum Products by
Hydrometer Method (DoD Adopted)
ASTM D1364 Standard Test Method for Water in Volatile Solvents (Karl Fisher
Reagent Titration Method) (DoD adopted)
ASTM D1500 Standard Test Method for ASTM Color of Petroleum Products (ASTM
Color Scale) (DoD adopted)
ASTM D1655 Standard Specification for Aviation Turbine Fuels (DoD adopted)
ASTM D1796 Standard Test Method for Water and Sediment in Fuel Oils by the
Centrifuge Method (Laboratory Procedure) (DoD adopted)
ASTM D2013 Standard Practice for Preparing Coal Samples for Analysis (DoD
adopted)
MIL-STD-3004C
9

ASTM D2274 Standard Test Method for Oxidation Stability of Distillate Fuel Oil
(Accelerated Method) (DoD adopted)
ASTM D2276 Standard Test Method for Particulate Contaminant in Aviation Turbine
Fuel by Line Sampling (DoD adopted)
ASTM D2624 Standard Test Methods for Electrical Conductivity of Aviation and
Distillate Fuels (DoD adopted)
ASTM D2699 Standard Test Method for Research Octane Number of Spark-Ignition
Engine Fuel (DoD adopted)
ASTM D2700 Standard Test Method for Motor Octane Number of Spark-Ignition
Engine Fuel (DoD adopted)
ASTM D2709 Standard Test Method for Water and Sediment in Middle Distillate
Fuels by Centrifuge (DoD adopted)
ASTM D3237 Standard Test Method for Lead in Gasoline by Atomic Absorption
Spectroscopy (DoD adopted)
ASTM D3240 Standard Test Method for Undissolved Water in Aviation Turbine Fuels
(DoD adopted)
ASTM D3241 Standard Test Method for Thermal Oxidation Stability of Aviation
Turbine Fuels (DoD adopted)
ASTM D3487 Standard Specification for Mineral Insulating Oil Used in Electrical
Apparatus (DoD Adopted)
ASTM D3703 Standard Test Method for Hydroperoxide Number of Aviation Turbine
Fuels, Gasoline, and Diesel Fuels (DoD Adopted)
ASTM D3699 Standard Specification for Kerosine (DoD adopted)
ASTM D3828 Standard Test Methods for Flash Point by Small Scale Closed Cup
Tester (DoD adopted)
ASTM D3948 Standard Test Method for Determining Water Separation Characteristics
of Aviation Turbine Fuels by Portable Separometer (DoD adopted)
ASTM D4052 Standard Test Method for Density, Relative Density, and API Gravity of
Liquids by Digital Density Meter (DoD Adopted)
ASTM D4057 Standard Practice for Manual Sampling of Petroleum and Petroleum
ASTM D4176 Standard Test Method for Free Water and Particulate Contamination in
Distillate Fuels (Visual Inspection Procedures) (DoD adopted)
ASTM D4177 Standard Practice for Automatic Sampling of Petroleum and Petroleum
ASTM D4306 Standard Practice for Aviation Fuel Sample Containers for Tests
Affected by Trace Contamination (DoD adopted)
MIL-STD-3004C
10

ASTM D4806 Standard Specification for Denatured Fuel Ethanol for Blending with
Gasolines for Use as Automotive Spark-Ignition Engine Fuel (DoD
adopted)
ASTM D4814 Standard Specification for Automotive Spark-Ignition Engine Fuel
(DoD adopted)
ASTM D4815 Standard Test Method for Determination of MTBE, ETBE, TAME,
DIPE, tertiary-Amyl Alcohol and C1 to C4 Alcohols in Gasoline by
Gas Chromatography (DoD adopted)
ASTM D4953 Standard Test Method for Vapor Pressure of Gasoline and Gasoline-
Oxygenate Blends (Dry Method) (DoD adopted)
ASTM D5001 Standard Test Method for Measurement of Lubricity of Aviation
Turbine Fuels by the Ball-on-Cylinder Lubricity Evaluator (BOCLE)
ASTM D5006 Standard Test Method for Measurement of Fuel System Icing Inhibitors
(Ether Type) in Aviation Fuels (DoD adopted)
ASTM D5059 Standard Test Method for Lead in Gasoline by X-Ray Spectroscopy
(DoD adopted)
ASTM D5190 Standard Test Method for Vapor Pressure of Petroleum Products
(Automatic Method) (DoD adopted)
ASTM D5191 Standard Test Method for Vapor Pressure of Petroleum Products (Mini
Method) (DoD adopted)
ASTM D5304 Standard Test Method for Assessing Middle Distillate Fuel Storage
Stability by Oxygen Overpressure (DoD adopted)
ASTM D5452 Standard Test Method for Particulate Contamination in Aviation Fuels
by Laboratory Filtration (DoD adopted)
ASTM D5599 Standard Test Method for Determination of Oxygenates in Gasoline by
Gas Chromatography and Oxygen Selective Flame Ionization Detection
ASTM D5798 Standard Specification for Fuel Ethanol (Ed70-Ed85) for Automotive
Spark-Ignition Fuels
ASTM D5854 Standard Practice for Mixing and Handling of Liquid Samples of
Petroleum and Petroleum Products
ASTM D6078 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the
Scuffing Load Ball-on-Cylinder Evaluator (SLBOCLE)
ASTM D6079 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the
High-Frequency Reciprocating Rig (HFRR)
ASTM D6217 Standard Test Method for Particulate Contamination in Middle
Distillate Fuels by Laboratory Filtration
ASTM D6751 Standard Specification for Biodiesel Fuel Blend Stock (B100) for
Middle Distillate Fuels
ASTM D7224 Standard Test Method for Determining Water Separation Characteristics
of Kerosine-Type Aviation Turbine Fuels Containing Additives by
Portable Separometer
MIL-STD-3004C
11

ASTM D7371 Standard Test Method for Determination of Biodiesel (Fatty Acid
Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared
Spectroscopy (FTIR-ATR-PLS Method)
ASTM D7467 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
ASTM D7547 Standard Specification for Unleaded Aviation Gasoline
(Copies of these documents are available online at http://www.astm.org or from ASTM International, 100
Barr Harbor Drive, West Conshohocken PA 19428-2959)
EUROPEAN COMMITTEE FOR STANDARDIZATION
EN 228 Automotive fuels - Unleaded petrol - Requirements and test methods
EN 590 Automotive fuels - Diesel - Requirements and test methods
EN 15751 Automotive fuels Fatty acid methyl ester (FAME) fuel and
Blends with diesel fuel- Determination of oxidation stability by
accelerated oxidation method

(Copies of this document are available online at http://www.cen.eu/ or from CEN-CENENEC
Management Centre, Avenue Marnix 17, B-1000 Brussels).
GOSUDARSTVENNYI STANDARTY (GOST), Euro-Asian Council of Standardization, Metrology, and
Certification (EASC)
GOST 305-82 Diesel Fuel, Specifications, dated March 31, 1982
GOST 10227-86 Fuels for Jet Engines, Specifications, Revised March 1998, with
Amendments Nos. 1,2 , 3 and 4
(Copies of these documents are available online at http://global.ihs.com/ or from Customer Service and
Technical Support,15 Inverness Way East, Englewood CO 80112
UNITED KINGDOM MINISTRY OF DEFENCE (UK MOD)
STANDARD 91-91 Turbine Fuel, Aviation Kerosene Type, Jet A1, NATO Code F-35,
Joint Service Designation: AVTUR
(Copies of this document are available online at http://www.dstan.mod.uk/ or from the UK Defence
Standardization Room 1138, Kentigern House, 65 Brown Street, Glasgow G2 8EX)
INTERNATIONAL ORGANIZATION FOR STANDARDIZATION (ISO)
ISO 8217 Petroleum products Fuels (class F) Specifications for marine fuels
ISO 9001 Quality Management Systems Requirements
ISO 10012-1 Quality Assurance Requirements for Measuring Equipment Part 1:
Meteorological Confirmation System for Measuring Equipment
(Copies of these documents are available online at http://www.ISO.org/iso/iso_catalogue.htm or from the
International Organization for Standardization (ISO) 1, ch. de la Voie-Creuse, Case postale 56, CH-1211
Geneva 20, Switzerland)
MIL-STD-3004C
12

NATIONAL FIRE PROTECTION ASSOCIATION (NFPA)
NFPA 77 Recommended Practice on Static Electricity
(Copies of this document is available online at http://www.nfpa.org or from the National Fire Protection
Association, 1 Batterymarch Park, Quincy, MA 02269-9101)
SAE INTERNATIONAL
SAE AMS 1424 Deicing/Anti-Icing Fluid, Aircraft SAE Type I
SAE AMS 1428 Fluid, Aircraft Deicing/Anti-icing, Non-Newtonian (Pseudoplastic),
SAE Types II, III, and IV
SAE AMS 2518 Thread Compound, Anti-Seize, Graphite-Petrolatum
SAE AMS-G-4343 Grease, Pneumatic System
SAE AMS-G-6032 Grease, Plug Valve, Gasoline and Oil Resistant, NATO Code Number
G-363, Metric
SAE AMS-M-7866 Molybdenum Disulfide, Technical, Lubrication Grade
SAE AS 1241 Fire Resistant Phosphate Ester Hydraulic Fluid for Aircraft
SAE AS 8660 Silicone Compound NATO Code Number S-736
SAE AS 87132 Lubricant, Cetyl Alcohol, 1-Hexadecanol, Application to Fasteners
SAE J 1703 Motor Vehicle Brake Fluid
SAE J 1899 Lubricating Oil, Aircraft Piston Engine (Ashless Dispersant)
SAE J 1966 Lubricating Oils, Aircraft Piston Engine (Non-Dispersant Mineral Oil)
SAE J 2360 Lubricating Oil, Gear Multipurpose (Metric) Military Use
(Copies of these documents are available online at http://www.sae.org/ or SAE World Headquarters, 400
Commonwealth Drive, Warrendale, PA 15096)
2.4 Order of precedence. In the event a conflict between the text of this document and the references
cited herein, the text of this document takes precedence. Nothing in this document, however, supersedes
applicable laws and regulations unless a specific exception has been obtained.
3. DEFINITIONS, ACRONYMS, and ABBREVIATIONS
3.1 Definition List.

Acceptance

The act of an authorized Government by which the Government assumes for itself,
or as agent of another, ownership of existing and identified supplies tendered, or
approves specific services rendered, as partial or complete performance of the
contract on the part of the contractor.

Additives Compounds used to impart new properties to a product or to improve a property
which it already possesses. For example, mixed tertiary butylphenols (oxidation
inhibitor) when added to a gasoline improves its resistance to oxidation.
MIL-STD-3004C
13

Appearance Color, clarity, or evidence of stratification and contaminants that may be observed
by visual examination of sample.

ASSIST

B20

Acquisition Streamlining and Standardization Information System. The ASSIST-
Online database is the official source for all Defense Standardization Program
documents and contains the most current information on these documents prepared
by Department of Defense DoD. It can be accessed at https://assist.daps.dla.mil or
http://assistdocs.com/. The ASSIST database lists defense and federal specifications
and standards, defense handbooks, commercial item descriptions (CIDs), Quality
Product Lists (QPLs), adopted non-government standards (NGS) and other related
standardization documents used by the DoD.

A fuel blend consisting of 20 volume percent (vol%) of biodiesel with the remain-
ing 80 vol % a light middle or middle distillate diesel fuel meeting Specification
D975 grades No.1-D and No.2-D for any sulfur level specified. DoD mandates that
the biodiesel component of the blend conform to the requirements of ASTM
D6751. The B6 to B20 blends fall under the ASTM D7467 specification.

Ballast Water taken on board when a vessel is empty or partially loaded/ discharged to
increase draught so that the propeller is fully immersed, stability and trim are
maintained and stresses minimized.

Barrel A volume of liquid petroleum product equal to 42 U. S. gallons (USG) (159 Liters
(L)).

Biodiesel Refers to a vegetable oil or animal fat-based diesel fuel consisting of long-chained
mono-alkyl esters. Biodiesel is typically made by chemically reacting lipids (e.g.,
vegetable oil, animal fat (tallow)) with an alcohol. DoD does not allow the use of
biodiesel synthesized using tallow. Bio-diesel can be used alone, or with 6 to 20
volume percent (vol%) of biodiesel (B6 to B20) blended with petroleum diesel as
outlined in ASTM D7467. DoD only allows the use of B20 biodiesel. Biodiesel is
meant to be used in standard diesel engines and should not be confused with the
vegetable and waste oils used to fuel converted diesel engines.

Bleeding Change in physical characteristics and homogeneity of grease evidenced by
separation of oil from the grease.

Blending The procedures by which predetermined quantities of two or more similar products
are homogeneously mixed to upgrade one of the products or to produce an
intermediate grade or quality. This term is also used to define the injection of
additives, such as corrosion or icing inhibitors, into fuels.

BOCLE Test ASTM D5001, Measurement of Lubricity of Aviation Turbine Fuels by the Ball-on-
Cylinder Lubricity Evaluator (BOCLE), ASTM D5001, correlates measurement of
wear scars to lubricity/engine wear protecting capabilities of aviation fuels

Bulk products Liquid petroleum products which are normally transported by pipeline, tank car,
truck or trailer, barge or tanker, and stored in tanks or containers having a capacity
of more than 55 USG (208 L). A 500 USG (1890 L) collapsible drum is considered
a packaged item.

Bunkers Fuel intended for consumption to propel water-borne craft. Bunkers can be
distillate, such as F-76, MGO, or JP-5. Bunkers can also mean a residual fuel oil
such as Intermediate Fuel Oil 180 and Fuel Oil 380.

Burner Fuel

A petroleum distillate and residual oils used to heat homes and buildings, such as
Grade No.1-D S15; S500 or S5000; Grade No.2-D S15; S500 or S5000; and Grade
No.4-D.

MIL-STD-3004C
14

Calibration

The comparison of a measurement system or device of unverified accuracy against
one of known or greater accuracy. Used to check, detect, and correct any deviation
from required performance specifications by the unverified measurement system or
device.

Capitalization

Cargo Fuel
The process whereby the DLA division of the Defense-wide Working Capital Fund
assumes management responsibility and ownership (title) without reimbursement for
inventories financed from other DoD appropriations or funds, except as stipulated in
DoD 7000.14-R.

Fuel carried on board ship for eventual issue to consuming vessels as a bunker fuel
or turn-in to a deep-water DFSP.

Certificate of
Conformance
A statement applied to the Material Inspection and Receiving Report by the
Contractor indicating that the product being provided conforms to specification/
contractual requirements. This statement is in lieu of a Government Inspection.

Clean (clear) and
bright
The absence of visible solids, a cloud, a haze, an emulsion, or free water in the
product (some specifications define this as Appearance, Workmanship, or as
Workmanship, Finish, and Appearance). Bright is the sparkle of clean, dry product
in transmitted light.

Coalesce To unite to form one mass. A coalescer is designed to combine small water droplets
into larger ones so they will fall to the bottom of the container. Many filters in use
are combination filter/coalescers usually called filter-separators.
Commingling The mixing of two or more products of different ownership, type, or grade.

Conductivity The ability of a given substance to conduct electric current.

Contaminant A foreign substance in a product

Contaminated product A product into which one or more grades of another product has been accidentally
mixed, or a product containing foreign matter such as dust, rust, water, or emulsions
to the extent it changes the characteristics of the product.

Continuous sample A dynamic sample of fuel obtained from a pipeline in such a manner as to provide a
representative average. This sample may be collected on a continuous basis (drip
sample), or intermittently and proportional to time or flow (flow-proportional
sample).

Cracked stock A petroleum fraction obtained from a cracking process rather than from simple
distillation. In a cracking process, the hydrocarbon molecules are altered resulting
in increased quantities of low-boiling fractions.

Dedicated system An arrangement of pipeline(s), vessel(s), and/or truck(s) used exclusively to move
only one fuel type (e.g. jet fuel, diesel, etc.).

Dehydration The removal of water

Density

The density of a material is defined as its mass per unit volume. In some cases (for
instance in the U.S. oil and gas industry), density is also defined as its weight per
unit volume; although, this quantity is more properly called specific weight.

NOTE: The density of a material varies with temperature and pressure. (The
variance is typically small for solids and liquids and much greater for gases.)
Increasing the pressure on an object decreases the volume of the object and therefore
increases its density. Increasing the temperature of a substance (with some
exceptions) decreases its density by increasing the volume of that substance.

MIL-STD-3004C
15

Deteriorated product

A product in which one or more characteristics have changed to a level of quality
outside the limits of the applicable specification.

Dissolved water

Distillate Marine Fuel
/Marine Gas Oil

Water in a solution which cannot be removed by mechanical means (e.g.
filter/separator). The concentration of dissolved water varies with product
temperature, the relative humidity of air contacting the product surface, and the
chemical composition of the product.

This fuel is the petroleum distillate fuel for use in marine diesel engines and boilers.
The official name of the fuel is Distillate Marine Fuel according to the
specification ISO8217:2010(E). It is often called Marine Gas Oil (MGO) in the
industry.

Downgrading The procedures by which an off-specification or contaminated product is approved
for use as a lower grade of the same or similar product; or as a completely different
product.

Entrained water Water carried by a product which does not settle out readily. Entrained water can
be removed by mechanical means (e.g. filter/separator).

E85 Fuel blend consisting of 70 to 85 vol% denatured ethanol with the remainder of
gasoline or other hydrocarbon by volume. Used in flexible fuel ground vehicles
with automotive spark-ignition engines.

FAEE Fatty Acid Ethyl Ester; sometimes referred to as biodiesel or B100 (properties
similar to FAME).

FAME Fatty Acid Methyl Ester; sometimes referred to as biodiesel or B100.

Filtering A process of mechanically removing solids or free water from a petroleum product
using a medium such as filtering paper, clay or diatomaceous earth.

Filter-separator A mechanical device designed to remove solid contaminants and to coalesce and
separate water from fuels.
Free water Water in a petroleum product other than dissolved water. Free water may be in the
form of droplets or haze suspended in the product and/or a water layer at the bottom
of the container.

Gasohol A mixture of 90 vol% of gasoline and 10 vol% denatured ethyl alcohol (ethanol)
used as automotive gasoline.

Gauging (gaging) The act of measuring the height of product in a tank. During the process of gauging
a tank, the temperature of the fuel is also normally measured.

Gauging for water Obtaining the depth of the water bottom by taking a water cut. This is normally
accomplished by coating a plumb bob, tape, or gauging stick with water-finding
paste.

Gum Description of resin-like, fuel insoluble deposits (contaminants) formed during the
oxidative and thermal deterioration of petroleum fuels.

Homogeneity A quality or state of being homogeneous or having a uniform composition. A
product is considered homogeneous when its base components are mixed uniformly
throughout (no stratification).

NOTE: The criteria for homogeneity may not apply for post-procurement products.
For example, a sample taken from a depot tank after the receipt of a new batch may
not, in all likelihood would not, meet the repeatability precision requirements.
MIL-STD-3004C
16

Identification Tests Selected tests applied to a sample to quickly determine the type or grade of the
product represented or to determine if a quality has been altered by time or handling.

Inert-gas system A gas or mixture of gases that contain insufficient oxygen to support hydrocarbon
combustion used in cargo tanks to reduce the possibility of fire, explosion, or
product deterioration. Introducing an inert gas or, more commonly, exhaust which
has been scrubbed or filtered to remove any particulates, prevents the formation
of a flammable atmosphere in cargo tanks during cargo operations in tankers.

Innage The height of liquid in a tank or container measured from the bottom of the tank to
the top surface of the liquid.

Inspect To examine critically especially to detect flaws, errors, etc.

Interface The common boundary (or surface) of two liquids.

Intra-Governmental
receipt limits

The extent that properties of DoD-owned petroleum products may change beyond
specification requirements and remain acceptable for receipt and issue within the
DoD logistic system.
Light-ends The lower-boiling fractions of a fuel or oil.

Long Term Storage When new product has not been added to existing product in a tank for six months
or more.

Lubricity

Ability of a fluid to reduce the friction between two surfaces in motion. In fuels, it
refers to a value that is measured by a Ball-on-Cylinder Lubricity Evaluator
(BOCLE) test, scuff load BOCLE (SLBOCLE) test, or the high frequency
reciprocating rig (HFRR) test.

Marine Gas Oil
(MGO)

A distillate fuel, containing no residuals, used for vessel propulsion.

Material Inspection
and Receiving Report
(DD Form 250/250-1)

The Government document identifying the contractor, product origin, product type,
quality, quantity, and the destination of the product. The DD Form 250 document
is signed by the Government Representative while the DD Form 250-1 (waterborne
movement) is signed by the Government representative, a refinery/ facility
representative along with a vessel representative.

NOTE: For bunkers, a completed commercial report and/or order form should be
used instead of the DD Form 250, which the Government will clearly annotate with
quantity of fuel received, then sign and date the form.

Micron One micron (m, micrometer) is 1/1000 oI one millimeter or 10
-6
meter
(approximately 25,400 m equal one inch). The average human hair is about 100
m in diameter. The openings in a 100-mesh screen are 150m.

Mineral oil Lubricating oils from petroleum sources with or without additives
.
Off-specification
Product
A product which fails to meet one or more of the physical, chemical, or performance
requirements of the specification.

Outage (or ullage) The linear distance between the top surface of the liquid in a drum, tank, or tank car
and the top of the container (or ullage may refer to available fill volume of the tank
and is the difference between the full (rated) capacity and the actual contents of a
storage container). In some tanks and tank cars, it is the difference between a
reference mark and the surface of the liquid. It is important that some significant

MIL-STD-3004C
17

difference always exists in order to allow free space for content expansion in case of
a rise in temperature. This quantity in ships tanks is normally determined by outage
(ullage) gauges.

Oxygenated fuel A fuel containing a chemical compound that has oxygen as a part of its chemical
structure (e.g. alcohols, ethers) and is miscible with conventional hydrocarbon
Oxygenated fuels generally show higher octane but lower heating values than that of
hydrocarbon fuels.

Packaged product Petroleum products stored, transported, and issued in containers of 55 USG or 400
pound capacity or less but also includes 500 USG collapsible drums.

Pipeline batch The quantity of a product pumped into the pipeline in one continuous operation.

Pipeline tender A quantity of product offered or designated for pipeline shipment. It may be moved
in one or more batches.

Product equilibrium

Qualified Products
List (QPL)

When all residual movement has ceased in a storage tank after receipt of product. A
tank must be at equilibrium to be ready for final gauging or measurement after
receipt.

An electronic list in the QPD (ASSIST) of products or families of products that have
successfully completed the formal qualification process (including all specified
periodic tests) that examines, tests, and verifies that a specific product design meets
all the applicable specification requirements.

Quality

The composite of materiel attributes including performance, features and
characteristics of a product, or service to satisfy a given requirement.

Quality Assurance
(QA)
A planned and systematic pattern of all actions necessary to ensure that adequate
technical requirements are established; that products and services conform to these
established technical requirements; and that satisfactory performance is achieved.
(The generic quality assurance definition includes all actions beginning in the design
phase through procurement, storage and handling, transportation, and use.)
Contract Quality Assurance is a method the Government uses, to determine if
products and/or services a supplier provided fulfilled its contractual obligations. It
includes all actions required to ensure the Government is receiving the proper
products and/or services. By common usage, Petroleum Quality Assurance
responsibility is fulfilled when the product is accepted by the Government and no
longer belongs to the contractor or when the service is completed.

Quality Assurance
Representative
(QAR)

An organizational title assigned to the individual responsible for Government
contract QA functions. QARs have cognizance over the procurement of product
and/or services at contractor facilities (e.g. refineries, terminals, packaging plants,
laboratories, and into-plane sites). DLA Energy QARs perform both QA and in
some cases QS functions. The Military Services may use other organizational titles
for their personnel performing QA and QS functions.

Quality Product
Database (QPD)
This database consists of the officially approved electronic QPLs and may be
accessed through ASSIST website at https//assist.daps.dla.mil. Only those electronic
QPLs published in the QPD are the official source for qualified products.

Quality Status List
(QSL)
A list containing shelf-life information to determine if Type II (extendible) shelf-life
material may continue to be used.

Quality Surveillance
Program
Program of inspections, sampling, testing, and documentation established to assure
quality of Government-owned product.

MIL-STD-3004C
18

Reclamation Procedure to restore or change the quality of an off-specification or contaminated
product so it will meet the specification of the original product or a lower grade
product. The reclamation process, when properly applied, will result in down-
grading, blending, purification, or dehydration.

Relative Density The ratio of the mass of a given volume of liquid at a standard temperature to the
mass of an equal volume of pure water at a standard temperature. The standard
reference temperature must be clearly stated (e.g. Relative Density at 60 F; or
Relative Density at 20 C) when results are reported.

Repeatability Allowable differences in test result values on the same sample by the same
operator under the same test condition, using the same equipment.

Reproducibility Allowable difference in test result values on the same sample by different
technicians, laboratories, or equipment under the same test condition.

Requiring Installation

Residual Marine Fuel
(RME 180 and RMG
380 Grades)

A military installation, organization, or facility authorized to requisition and
receive material from designated distribution and storage points.

Petroleum residual fuel for use in marine diesel engines and boilers.
Sample A portion extracted from a total volume which may or may not contain constituents
in the same proportions that are present in that total volume.

Bulk Products, samples can be taken from acceptance tanks, storage tanks, delivery
trucks, intermodal containers, pipelines, barges or tankers. Samples may be taken
either manually (upper, middle, lower, all-level) or automatically (line, flow-
proportionate).

For DLA Energy contracts, samples are taken in accordance with API Manual of
Petroleum Measurement Standards (MPMS), Chapter 8, Section 1, Sampling of
Petroleum and Petroleum Products (ASTM D 4057) and/or Automatic Sampling of
Petroleum and Petroleum Products (ASTM D4177). Samples are identified by a
sample tag noting location, product, tank number, type of sample/sampler, and date
(see continuous sample).

Packaged Products, samples may be taken from drums or cans using a tube or thief
sampler. Sampling may also be accomplished by selecting an individual unit from a
collection of packaged products.

Sample Tag DD Form 2927, Petroleum and Lubricants Sample Identification Tag or equivalent
is the standard label used for petroleum and lubricant samples.

Settling time The time a product needs to remain undisturbed or un-agitated in a storage tank to
reduce the static charge of the fuel and/or to allow water and sediment to be
eliminated/reduced from the product.

Shelf life, Type I A definite non-extendable period of shelf life.

Shelf life, Type II An assigned shelf-life period that may be extended after completion of inspection,
testing, or restorative action.

Specification A detailed description of the products essential performance and/or physical and
chemical characteristics. Specifications can be classified as Federal, Military,
Commercial, or Voluntary Standard. Specifications can be categorized as
functional, design, or a performance specification. Petroleum specifications are
usually combination of functional and performance categories.

MIL-STD-3004C
19

Specification limits Boundaries or parameters that define acceptable performance for a process
expressed as a target limit, as well as an upper and lower unit.

Specific gravity See relative density.

Storage Tank A large container used for liquid (fluid) storage.

Super-clean fluid

A fluid having a specified particulate contamination limit so low that the product
is packaged in hermetically sealed containers under clean room conditions.

Surfactant Any substance, which when dissolved in water or aqueous solution, reduces its
surface tension or the interfacing tension. Also called a surface-active agent. Tends
to block removal of entrained water in fuels.

Synthetic oil

Tank Car (TC
or RTC)

Materiel not refined from petroleum sources - usually produced by chemical
synthesis.

Rail car specifically designed to transport petroleum products
Testing The determination of product physical and chemical properties. Depending on the
location, mode of storage, and transportation (see Table IX) the following type tests
are defined:

Type A Tests Complete quality conformance specification acceptance tests.

Type B-1 Tests Partial analysis checking for the principal characteristics most likely to be affected
in the course of moving the product.

Type B-2 Tests Partial analysis to verify stability of characteristics susceptible to deterioration due
of age.

Type B-3 Tests Partial analysis for contamination; in particular, for controlling the re-injection of
pipeline interface products.

Type C Tests Quick, simple, partial analysis to verify product quality and to ensure that no change
has taken place. Type C tests can be referred to as identification tests.

Thief

Tolerance

Transmix
A sampling apparatus designed so a liquid sample can be obtained from any
specified point in the container.

Allowed variations within a specified standard

A mixture of gasoline and diesel fuels resulting from various operations such as
pipeline transfers, barge transfers, cross contamination of tanks.

Truck As defined in DoDM 4140.25-M and this document, can be either a truck, tank
wagon and truck trailer.
Tank Truck (TT) A delivery truck with a capacity between 6,500 and 11,000 USG (24,600 to 41,600
L), equipped with a 15-ft (5 m) hose but usually not requiring a meter.

Tank Wagon (TW) Delivery truck with a capacity up to 5,200 USG (19,700 L) equipped with a meter,
nozzle, 100 feet (30m) of hose, and used for making multiple, small deliveries
MIL-STD-3004C
20

Truck and Trailer
(TRR)
A delivery truck usually having a 9,000 USG (34,000 L) capacity (minimum)
equipped with a 15-foot (5 m) hose. A meter is not required unless specifically
stated in contract terms and conditions.

Ullage

See outage.
Vapor pressure (VP) The measure of pressure exerted by the vaporized phase of a product on the interior
of a special container under specified test conditions
Verification Tests The testing performed by the supplier on samples verified (witnessed) by the QAR
after the supplier has completed full specification testing and certified each shipping
tanks as ready for acceptance. The scope of the testing is the minimum required to
verify that the results presented by the supplier on his full spec test report in fact
reflect the product being offered.

Volatile alkyl lead
antiknock
Volatile alkyl lead compounds (e.g. tetramethyl lead and tetraethyl lead) which
increase the octane rating when added to gasoline in small proportions.
3.2 Acronyms and Abbreviations.
ACS American Chemical Society
AFPA Air Force Petroleum Agency
AGMA American Gear Manufacturers Association
AIR Card Aviation Into-plane Reimbursement Card
AKI Anti-Knock Index
AO Anti-Oxidant additive
AMPS DLA Account Management and Provisioning System
ARP Alternate Release Procedure
ASSIST Acquisition Streamlining and Standardization Information System
APC Army Petroleum Center
API American Petroleum Institute
BBL Barrel
BDN Bunker Delivery Note
BOCLE Ball On Cylinder Lubricity Evaluator
BTU British Thermal Unit
CCAI Calculated Carbon Aromaticity Index
CEPS Central European Pipeline System
CID Commercial Item Descriptions
CI/LI Corrosion Inhibitor /Lubricity Improver additive
COCO Contractor-Owned, Contractor-Operated
CU Conductivity Unit
MIL-STD-3004C
21

DCMA Defense Contract Management Agency
DFAMS Defense Fuel Automated Management System
DFARS Defense Federal Acquisition Regulations
DFSP Defense Fuel Supply Point
DMA Diesel Marine A
DMF Distillate Marine Fuel
DoD Department of Defense
DoDSSP Department of Defense Single Stock Point
DWCF Defense Working Capital Fund
EA Executive Agency
EI Energy Institute
FAEE Fatty Acid Ethyl Ester
FAME Fatty Acid Methyl Ester
FAR Federal Acquisition Regulations
FAS Fuels Automated System
FISC Fleet Industrial Supply Center
FMD Fuels Manager Defense
FOB Free on Board
FSC Federal Supply Class
FSII Fuel System Icing Inhibitor
GOCO Government-Owned, Contractor-Operated
IFO Intermediate Fuel Oil
ISO International Organization for Standardization
IGRL Intra-Governmental Receipt Limits
JPO Joint Petroleum Office
JPTS Jet Propulsion, Thermally Stable
MDA Metal Deactivator Additive
MGO Marine Gas Oil
MPMS Manual of Petroleum Measurement Standards
MMR Motor Mid-grade, Reformulated (unleaded) gasoline
MPR Motor Premium, Reformulated (unleaded) gasoline
MRR Motor Regular, Reformulated (unleaded gasoline)
MSC Military Sealift Command
MSEP Microseparometer
MUM Motor Unleaded, Mid-grade gasoline
MIL-STD-3004C
22

MUP Motor Unleaded, Premium gasoline
MUR Motor Unleaded, Regular gasoline
NATO North Atlantic Treaty Organization
NAVSUP Naval Supply Systems Command
NGS Non Government Standards
NSN National Stock Number
POL Petroleum Oils and Lubricants
PORTS Paperless Ordering & Receipt Transaction Screen
ppm Parts Per Million
psi Pounds per Square Inch
PC&S Post, Camps and Stations
QAR Quality Assurance Representative
QAS Quality Assurance Specialist
QPD Qualified Products Database
QPL Qualified Products List
QS Quality Surveillance
RME Marine Residual Fuel Oil, such as RME-180
SDA Static Dissipater Additive
STANAG Standardization Agreement (NATO document)
ULSD Ultra Low Sulfur Diesel
USG U.S. Gallons
VP Vapor Pressure
VOL % Volume Percentage
WSIM Water Separation Index, Modified

4. GENERAL REQUIREMENTS
4.1 Personnel competency. Personnel responsible for handling fuels and lubricants 2 be thoroughly
trained and fully qualified to perform their assigned responsibilities. They shall be aware of the hazards
in handling fuels and lubricants, as well as the applicable safety and operating procedures.
4.2 Service/contractor responsibilities. The owning Service/Contracted activity shall have the
responsibility of maintaining quality and quantity of Defense Working Capital Fund products while in
their keeping (e.g. receiving, storing, sampling, testing, and releasing) and shall dispense those products
as required to using activities. The Service/Contracted activity shall develop, establish and maintain a
quality surveillance program IAW this Standard for Defense Working Capital Fund products from the
point of receipt on the installation to the point of sale. The program shall be in accordance with this

MIL-STD-3004C
23

Standard and be in effect from receipt to end-item issue. Quality problems involving Defense Working
Capital Fund product (e.g. off-spec product, downgrading of product, etc.) shall be addressed as outlined
in this Standard. Adequate sampling and testing programs can reduce or in some cases eliminate quality
problems.
4.2.1 Sampling. All samples shall be taken in accordance with ANSI Z1.4, API MPMS, Chapter 8,
Section 1, Manual Sampling of Petroleum and Petroleum Products (ASTM D 4057), and Section 2,
Automatic Sampling of Petroleum and Petroleum Products (ASTM D 4177), and/or as prescribed by
product specification or contract requirements. For Aerospace Energy Commodities (e.g. gases,
cryogenics, liquid propellant and hypergols) refer to the appropriate product specification to determine
appropriate sampling methods and procedures.
4.2.1.1 Precautions. The precautions required to ensure representative sampling are many and
depend on type of product being sampled, the type of container from which it is drawn and the sampling
procedures employed. Each procedure is suitable for sampling a specific product under definite storage,
transportation and container conditions.
4.2.1.2 Personnel conducting sampling. Because improperly taken samples can completely
invalidate a test, only trained and experienced personnel shall be assigned to sample the products. This
cannot be overstressed: No amount of laboratory work gives reliable data on a product if the sample is
not a true representation of that product.
4.2.1.3 Responsibility. This Standard shall in no way alter any assigned responsibility of the various
activities outside the continental United States for submitting special samples to a designated laboratory
or as directed by cognizant headquarters.
4.2.1.4 Types of samples. A sample is a portion of fuel taken which represents that entire batch or
delivery or a specific spot within a tank or container. The various types of samples follow:
4.2.1.4.1 All level sample. One taken by submerging a stoppered beaker or bottle to a point as near
as possible to the draw off level, then opening the sampler and raising it at such a rate that it is about
three fourths full as it emerges from the liquid.
4.2.1.4.2 Upper sample. One taken from the middle of the upper third of the tank contents.
4.2.1.4.3 Middle sample. One taken at the middle height of the tank contents.
4.2.1.4.4 Lower sample. One taken at the middle point of the lower third of the tank contents.
4.2.1.4.5 Top sample. One taken six inches below the top surface of the tank contents.
4.2.1.4.6 Composite sample. A blend of spot samples mixed in proportion to the volumes of
material from which the spot samples were obtained.
4.2.1.4.7 Drain sample. One taken from the draw off or discharge valve.
4.2.1.4.8 Bottom sample. One taken on the bottom surface of the tank, container, or pipeline at its
lowest point. The drain and bottom samples are usually obtained to check for water, sludge, scale, or
other contaminants.
4.2.1.4.9 Bottom water sample. A spot sample of free water taken from beneath the petroleum
contained in a ship or barge compartment or a storage tank.
MIL-STD-3004C
24

4.2.1.4.10 Single tank composite sample. A blend of the upper, middle, and lower samples of the
tank contents. The portion of the sample quantity to be taken at each level varies according to the type of
tank and shall be determined by applicable procedure (see 4.2.1).
4.2.1.4.11 Conveyance composite sample. A blend of individual all-level samples from each
compartment of the ship, barge, or carrier that contains the same grade of product in proportion to the
volume of product in each compartment.
4.2.1.4.12 Outlet (suction) sample. One taken at the level of the tank outlet.
4.2.1.4.13 Automatic sample. A sample taken from a pipeline conveying the product in such a
manner as to give a representative average of the stream throughout the period of transit.
4.2.1.4.14 Mixed sample. One obtained by mixing or vigorously stirring the contents of the original
container and then pouring out or drawing off the quantity desired.
4.2.1.4.15 Spot sample. A sample taken at a specific location in a tank or from a flowing stream in a
pipe at a specific time.
4.2.1.4.16 Tube or thief sample. One taken with a sampling tube or special thief, either as a core or
spot sample from a specified point in the container.
4.2.1.4.17 Batch/lot samples. One obtained from a collection of units of packaged products.
4.2.1.5 Taking of samples. A sample log should be maintained for all samples taken.
4.2.1.5.1 Sampling apparatus, containers, and procedures. Warning! All safety instructions shall be
strictly observed.
a. Approved type sample containers shall be used as specified by ASTM, API, Department of
Transportation or International Civil Aviation Organization. Samples of aviation fuel submitted
specifically for water and sediment determinations shall always be collected in clear glass bottles and
protected from exposure to sunlight. Aviation sample containers used for samples taken for thermal
stability, water separation index tests shall conform to ASTM D4306.
b. All sampling apparatus and containers shall be thoroughly clean and dry and special care shall be
taken so that no lint or fibrous material remains in or on them. Unless otherwise specified in the test
procedures, apparatus and containers shall be rinsed with a portion of the product being sampled to
ensure the sample is not contaminated with the previous material. Coated cans that have been presoaked
with a product are preferred when sampling for water reaction and for thermal stability. If not available,
then clear or amber gallon glass jugs work very well. If clear glass containers are used, then they shall be
prepared (e.g. wrapped in aluminum foil) to prevent light absorption. Sufficient liquid product shall be in
the sample lines and fittings before taking any sample. Sampling apparatus shall be cleaned immediately
after use and stored so it will remain clean until next use.
c. Unless specifically required for special testing, do not take samples through storage tank clean-
out lines, manifolds, water draw-offs, bleeder valves, or hose nozzles. Such samples will not be
representative of the product in the tank. When it is necessary to sample service station tanks and access
to such tanks cannot be gained though a manhole or sampling hatch, the tanks may be sampled through a
servicing hose after first discharging from the hose a volume of product estimated at two-times the
capacity of the piping system.
d. Containers such as drums shall be sampled with a thief. In sampling drums and cans, care shall
be taken to remove all foreign matter from the area near the enclosure before the plug is removed.
MIL-STD-3004C
25

e. Immediately after taking samples, close all sample containers tightly. Do not use sealing wax,
paraffin, rubber gaskets, pressure sensitive tapes, or similar material to seal containers. Lightweight
sample containers shall be adequately crated to withstand shipment. To prevent leakage caused by
thermal expansion of the product, do not fill any sample container above 80 percent volume capacity.
f. Samples for air shipment of turbine fuels and automotive gasoline shall be in UN1A1 cans, NSN
8110-01-371-8315 (1-gallon), with 4G fiberboard boxes, NSN 8110-01-436-7340 (drum and box
combination). The round sample can, NSN 8115-01-192-0935, is suitable for ground shipment of fuels
products, via United Parcel Service (UPS).
4.2.1.5.2 Sample Log Requirements. Each activity shall maintain a sample log, all samples
submitted will contain the following as a minimum information:
a. Sample number
b. Location sample taken (e.g. tank number, truck number, filter-separator number, etc.)
c. Type sample
d. Date sample taken
e. Name of person taking sample
f. Reason sample taken
g. Product and Grade
h. Specification (include approved waiver limits, if known)
i. Volume sample represents
j. Type tests requested
k. Date sample sent to the laboratory
l. Date results received back from the laboratory
m. Laboratory Report number
n. Laboratory Status results (e.g. on-specification, within IGRL, off-specification for
XXX test)
4.2.1.6 Precautions.
a. Samples of gasoline, jet fuel and kerosene shall be well protected from contamination and direct
sunlight by using clean, dry cans or brown bottles for leaded product. Some of these products, especially
gasoline, will change color rapidly on short exposure to sunlight and result in rapid increase in gum and
decrease in stability. Lead additives, such as tetraethyl lead, are particularly unstable in sunlight and may
appear as a gray or gray-white precipitate on the bottom of a container. If clear glass bottles are the only
containers available for sampling product containing lead, the bottles shall be covered with foil or paper
immediately after filling to avoid exposure to sunlight.
b. Samples of gasoline and jet fuel that require the vapor pressure test shall be carefully handled and
collected to preclude the loss of light-ends. Vapor pressures are extremely sensitive to evaporation losses
and to slight changes in composition. When obtaining, storing, or handling samples, observe the
necessary precautions to ensure samples are representative of the product and satisfactory for vapor
pressure tests (See ASTM D4057). Whenever practicable, arrangements should be made to maintain
MIL-STD-3004C
26

liquid fuel samples at a temperature between minus 1C and 4C (30F and 40F). This helps preserve
its characteristics from the point of sampling to the laboratory.
c. If the API gravities of fuel samples taken from the upper, middle and lower levels of a tank do not
differ by more than the reproducibility precision statement of the test method used for the type of liquid
in question, then make a composite of these samples for additional testing. If the variation is greater, test
the samples separately because the fuel may have stratified. In this case, each of the various stratified
layers shall be tested independently for conformance to the product specification.
4.2.1.7 Size of samples.
4.2.1.7.1 Normal sample size. Normally, liquid samples submitted for type A or B analysis shall not
be less than 4L (one-USG) total size; semisolids shall not be less than 2.25kg (five pounds).
4.2.1.7.2 Special sample size. Special samples and gasoline samples requiring ASTM D909 aviation
supercharge method of determining performance numbers shall be of 20L (five USG) size unless
otherwise directed.
4.2.1.7.3 Jet fuel. Samples of jet fuel requiring full specification testing shall be 8L (two USG), 4L
(one USG) of which will be used for the filtration time/particulate contamination test.
4.2.1.7.4 E85 sample. When required submit a one-gallon sample for specification conformance
testing, to include ethanol content.
4.2.1.7.5 B20 sample. When required, submit a one USG sample for specification conformance testing.
4.2.1.8 Identification of samples. Immediately after sampling, identify each sample container by
securely attaching a DD Form 2927, Petroleum and Lubricants Sample Identification Tag, or other
equivalent approved tag. Information on the tag shall include the location of the facility at which the
sample is taken, name of personnel taking the sample, grade of material, quantity represented, specifica-
tion of material when known, storage tank number and location, date sample was taken, type of sample
and reason for sample. For turbine fuel electrical conductivity (in picosiemens per meter (pS/m) units)
results, specify tank ambient temperature and request correction of conductivity value to that temperature.
4.2.1.8.1 Markings. In the case of packaged products, the complete markings shown on the
container shall be furnished. The container from which the sample was taken shall be marked with the
sample number for future identification.
4.2.1.8.2 Sample serial numbers. Each sample shall be assigned a serial number that shall be
determined by taking the calendar year as the prefix number and assigning consecutive numbers as the
samples are submitted. For example: the first sample submitted in 2003 would be 03-1, the second 03-2,
and so forth. Such sample numbers shall be shown on the sample identification tag and all shipping
documents and correspondence pertaining to the sample.
4.2.1.8.3 Retained samples. Unless otherwise specifically instructed, samples shall be retained for
45 days for reference purposes. Truck car samples will be retained for 15 days for reference purpose.
4.2.1.9 Shipping samples to a laboratory - Chain of custody requirement. In order to ensure sample
integrity a record of the chain of custody must be maintained by the sample owner until sample disposal.
Federal Express and or UPS documentation is to be on file when shipped from the DFSP. Each change
of custody shall be documented at the time and place of transfer including signature of the custodian.
4.2.1.10 Gauging and sampling JPTS cargo tanks or vessels. From or at intermediate load/discharge
ports.
MIL-STD-3004C
27

4.2.1.10.1 Contamination problems. When a partial cargo is to be loaded aboard an arriving vessel,
the QAR/Government Representative shall be required to sample/gauge all compartments loaded at
previous ports. In the case of JPTS this procedure can present a contamination problem. This type of
fuel requires special handling because it is easily contaminated. It is usually the first loaded in a multi-
product/multi-port lifting and often the last discharged.
4.2.1.10.2 Unaccountable product loss or gain. Gauging, sampling, and water-cutting of JPTS
compartments should not be conducted at intermediate terminals unless it is discharged at the
intermediate terminal or there is a clear indication of contamination or an abnormal unaccountable
quantity loss/gain. If JPTS compartments are gauged/sampled, all equipment introduced into the fuel
shall be cleaned and repetitions shall be minimized. A note shall be placed on the DD Form 250-1 or
accompanying cargo inventory report explaining complete circumstances.
4.2.2 Testing. The quality surveillance segment (testing) presented in this section is the minimum
essential for sound management of Government-owned properties. It represents the balance between
good QS practices, cost of quality, and associated risks, and the need to confirm adherence to
specification requirements through full specification testing. Only by thorough testing procedures can
premium quality surveillance be maintained.
4.2.2.1 Contamination tests. Suspected contamination of petroleum products shall be confirmed by
laboratory tests. Tests which have proved most useful in determining whether a product is contaminated
and in identifying the contaminating agents are listed under the individual products (see section 5.10).
4.2.2.2 Test methods. All laboratory tests shall be conducted in accordance with the method
prescribed in the specification covering the product. However, any special or modified method outlined
in this Standard shall be used in lieu of the specification method when products are evaluated within the
scope of this Standard. Specification and intra-Governmental receipt limits are absolute. Multiple tests
may be performed and if the results do not differ from each other by more than the amount specified for
the method repeatability, these results may be averaged to determine compliance with the specification or
established intra-Governmental receipt limits.
4.2.2.3 Testing frequency for long term storage of petroleum products. Table VIII outlines the
minimum frequency for testing petroleum and related products by broad category. Since it is the
responsibility of the cognizant QAR, petroleum officer, or supply officer to maintain strict quality
surveillance, the frequency of testing may be increased as required. Considerations for increased testing
are conditions of storage, age of stock and type of product. When a dormant product is tested, a record of
the results shall be maintained to provide a basis for determining product deterioration. Whenever
consecutive results indicate possible deterioration, testing frequency shall be increased. Once the trend
definitely reflects deterioration, the report procedures in 5.13.2 shall be followed. This is especially
important for a property such as color that presents no operational problem, but may indicate possible
deterioration.
4.2.2.4 Minimum testing. Table IX outlines the minimum sampling and testing requirements
considered necessary for determining the quality of petroleum and related products. It covers the
conditions under which a sample is taken, the type of sample, and the types of tests required to determine
whether the quality is within acceptable limits.
4.2.2.5 Types of tests required. Tables X through XXII provide a detailed breakdown of the type of
tests required for each product class. These tests are those most likely to reveal contamination/
deterioration which may have occurred during product handling or storage. Tables XVII through XXII
MIL-STD-3004C
28

designate Service and NATO prescribed B-2 tests for specific products. When a product being tested
exceeds the specification limits due to contamination, the procedures outlined in Section 5.13.1
(Identification of a non-confirming product) or 5.14.4 (Disposition instructions) are to be initiated.
4.2.2.5.1 Equivalent test. Test methods that provide analogous results and fully correlate with
standard ASTM methods, but have not yet been formally accepted by ASTM. These test methods have
been found to provide test results essentially identical to those produced by ASTM testing methods.
4.2.2.5.2 Predictive testing. Analytical techniques using instruments, equipment, and other methods
to predict fuel and lubricant test values using compositional data typically determined by standard or wet
chemistry methods.
4.2.2.5.3 Alternate test methods. The use of alternate test methods to measure physical properties of
fuel is allowed, provided that: the test results are presented in the format required in the specification; the
test device has a demonstrated reliability and repeatability equal or better than called for by the ASTM
method; and the device has been approved for use by the military services.
4.2.2.6 Testing capabilities. All terminals (commercial and military) receiving bulk products and
facilities storing packaged products shall be equipped and capable of performing tests required by Table
IX. When the capability does not exist at the terminal or facility, other laboratories, either commercial or
military, may be used. Appendix A lists petroleum testing facilities available to military and commercial
users.
4.2.2.7 Calibrating test equipment. All laboratories shall calibrate testing and measuring equipment
to the accuracy necessary to ensure the equipment is within allowable tolerance limits. ISO 10012-1,
Part I shall be used.
4.3 Specifications. Each JPO and petroleum product laboratory shall maintain an up-to-date file of
Government fuel and lubricant specifications (both Military and non-Government specifications and
standards). It is not practical to include complete specification limits in this Standard, as specifications
are subject to change with variations in product availability and technical developments. Copies of this
Standard can be obtained through regular channels from ASSIST Online website:
https://assist.daps.dla.mil/. Limits cited in this Standard are for Service use of fuel, not for procurement
documents.
4.4 Change in grade of fuel. Any change in grade of fuel requires notification to DLA Energy prior
to the change. Where product has been found to be off-specification, the DLA Energy Quality
Operations Division (DLA Energy-QA) is notified IAW section 5.13.2 of this standard. Disposition
instructions may be a change in grade. DLA Energy-QA performs internal coordination with the
Inventory Management Division (DLA Energy-FI), Program Budget Division (DLA Energy -RB) and the
Inventory & Distribution Division (DLA Energy -BI) within DLA Energy. In addition it will be
coordinated with the respective Service Control Point (SCP). Disposition instructions are provided by
DLA Energy -QA. A change in grade may be requested for other reasons, such as product availability,
fuel no longer needed, etc. In these circumstances the activity having physical possession of DWCF fuel
shall request concurrence from DLA Energy-FI. They will coordinate acceptability of the change with
DLA Energy -QA and determine the inventory impact with DLA Energy-BI before making a decision on
acceptance. DLA Energy -FI provides disposition in these cases.
4.5 Government-owned property. Contractors are obligated to adequately protect Government-
owned property located on their premises for use on, or in connection with a contract. The periodic

MIL-STD-3004C
29

inventory and reporting of such property is a contractual requirement. The amount of Government-
owned petroleum products in pipelines will be reported as a separate item in stock reports.
4.6 Safety precautions. Throughout this Standard there are general safety precautions and
instructions that apply to fuel handling and laboratory operations to ensure personal safety/health and the
protection of Government property. Occupational Safety and Health Administration, Department of
Labor and standard commercial safety practices shall be observed.
4.7 Measurement, sampling and calibration. For measurement, product sampling and calibration of
storage tanks and meters requiring the API Manual of Petroleum Measurement Standards: Chapter 2
covers tank calibration (strapping). Chapter 3 covers tank gauging. Chapter 5 covers measurements by
meters. Chapter 7 covers temperature determination. Chapter 8 covers sampling. Chapter 9 covers
density determination. Chapter 11 covers volume correction and conversion factors. Chapter 12 covers
procedures for calculating the net quantities from the gross measurements. Chapter 17 covers marine
measurement.
4.8 Compliance with regulations and laws. Many petroleum products are considered hazardous
materials and are regulated as such. Users of this Standard must be aware of regulations and laws
governing the products that they are handling. In the event of a conflict between this Standard and a law
or regulation, the law or regulation takes precedence.
5. DETAILED REQUIREMENTS
5.1 Waterborne Operations. This section applies to all movements of product belonging to or to
be accepted by the Government.
5.1.1 Shipments by tankers. This section covers pre-loading and loading procedures for tankers.
Those procedures for barges and refueling craft are covered in 5.1.2. Post loading of tankers and barges
is addressed in 5.1.4.
5.1.1.1 MPMS Guidelines. QARs utilize the following guidelines/sections of MPMS Chapter 17,
Marine Measurement during the applicable phase of each operation:
a. Section 2 - Measurement of Cargoes On Board Tank Vessels.
b. Section 6 - Determining Fullness of Pipelines between Vessel and Shore Tanks.
c. Section 8 - Pre-Loading Inspection of Marine Vessel Cargo Tanks.
5.1.1.2 Filtering requirements. Fuel and lubricant deliveries from fleet replenishment vessels shall
be filtered according to filtration standards for the particular product involved, unless these filtration
requirements are waived by the receiving ship. Replenishment vessels shall always take action to remove
water from their cargoes.
5.1.1.3 Certifying statements
1
5.1.1.4 Tanker and ocean-going barge inspection policy for MSC vessels. The following applies to
vessel cleaning, gas freeing, inspecting and quantity variations between MSC and DLA-ENERGY. It
. Statements of quantity and quality shall accompany all shipments.
The DD Form 250-1 is prepared under the supervision of the cognizant Government QAR (or Military
Service designated personnel) to cover marine petroleum shipments and receipts of Government
inspected products.

1
NOTE: References to the QAR include Military Service personnel designated to perform these functions.
MIL-STD-3004C
30

applies only to MSC controlled vessels. Table XXVII is only guidance to be used by QARs for the
inspection of MSC vessels.
5.1.1.4.1 Responsibility. Vessel owners/operators are responsible for providing vessels suitable to
load and deliver the intended cargo and for determining the need-to-clean vessel cargo tanks. This
determination is made by monitoring vessel cargo history and by what cargo is to be loaded. The process
for monitoring cargo history and identifying when vessel cargo tanks will require cleaning will be
developed by tanker owners/operators for each vessel. Copies of the DD Form 250-1 and test reports
shall be forwarded to vessels by the loading quality representative should early departure preclude
obtaining a copy upon loading completion.
5.1.1.4.2 Required cargo cleaning. MSC vessel cargo tanks shall be cleaned whenever the
following conditions exist (exceptions to these requirements shall be coordinated with DLA-ENERGY-
QA prior to the proposed cargo loading):
a. The vessel cargo tanks held ballast between the prior cargo discharge and the scheduled follow-on
cargo.
b. The cargo to be loaded is JP-5, and the previous cargo was other than JP-5.
c. The cargo to be loaded is JP-5, JP-8 or JPTS and the previous cargo was F-76.
d. The initial loading of a spot or time charter.
e. The vessel has been in dry dock, or repairs have been performed on the cargo tanks.
f. The cargo to be loaded is MOGAS and previous cargo was F-76.
g. The cargo to be loaded is other than MOGAS and the previous cargo was MOGAS.
5.1.1.4.3
5.1.1.4.4 Suitability to load. Vessels should arrive at the required port ready to load the intended
cargo. Vessels shall certify that cargo tanks are suitable for loading the intended cargo by including the
following statement in the Notice of Readiness: All compartments, lines and pumps to be used are
suitable for loading and delivering the intended cargo. Vessels shall also provide the quality
representative with soundings of product / water onboard and validated onboard quantities (OBQ) prior
to loading.
Internal Tank Inspection requirements. QARs will inspect vessels that are loading their
first DoD cargo under any MSC charter, or that have not maintained segregated ballast conditions, or that
have been dry docked or had repairs made to their cargo system. MSC will provide notification to the
QAR prior to loading regarding vessels that have been in dry dock or had repairs done to their cargo
system. MSC shall make the request for inspections at the repair facility to the next load port. They may
request assistance from a QAR closer to the facility if deemed necessary and acceptable. Any party may
request inspection, given proper notification to MSC. When MSC requires a vessel inspection by a QAR,
the request shall be forwarded from MSC to the cognizant Region and DLA-ENERGY-QA. This
notification shall be done prior to loading the intended cargo, allowing adequate time for the quality
representative to be present for an internal tank inspection. Otherwise, an inspection will not be
performed.
5.1.1.4.5 Quantity variation. Investigations shall be conducted by a MSC representative and DLA-
ENERGY Quality personnel for variations exceeding the following (shore-to-shore, loading to final
destination): 0.2 % volume for cargoes not requiring cleaning, gas-freeing, drop/strip; 0.3 % volume for
cargoes requiring drop/strip only; 0.5 % volume for cargoes requiring cleaning, gas-freeing, drop/strip.
MIL-STD-3004C
31

The Manual of Petroleum Measurement Standard, Chapter 17.5, Guidelines for Cargo Analysis and
Reconciliation, shall be used.
5.1.1.4.6 Responsibility for off-specification cargo. Tanker owner/operators are responsible for off-
specification product cargoes when the vessel is identified at fault. The Tanker owner /operator shall be
given the opportunity to secure the services of an independent petroleum surveyor in the event a
discrepancy would be suspected or identified. A representative sample taken at the custody transfer point
shall be used to determine source of contamination.
5.1.1.5 Pre-loading inspection of tankers. The following actions shall be taken prior to approving
tankers for loading:
5.1.1.5.1 Vessel inspection.
a. When a vessel internal cargo tank inspection is required (see 5.1.1.4 for tanker inspection policy
for MSC vessels), the QAR shall assure vessel conditioning has been performed in accordance with
Table XXVII. Before entering vessel tanks the QAR shall confirm that tanks are gas and vapor free and a
fresh air pack is available. Should validation of the confined space condition require the services of a
Marine Chemist, it is normally the vessel owner/operator who is responsible for obtaining these services.
MSC vessels and charters are not on-hire or back-in-service until the QAR accepts the vessel as suitable
to load.
b. When a vessel does not require internal cargo tank inspection, the QAR shall validate that the
vessel has either properly cleaned and/or stripped. The QAR shall validate the vessel certification, as
required in section 5.1.4.3, is written on the Notice of Readiness. The QAR shall validate the liquid
measurements are reflected on the OBQ arrival certificate. The QAR shall randomly validate the water
content in all cargo tanks by witnessing water cuts on the gauge tape.
5.1.1.5.2 Vessel tank inspection. When requested to perform an inspection a QAR shall personally
enter and inspect the vessels cargo tanks prior to loading to determine suitability for loading. The QAR
shall also check systems and lines to assure that they are drained and properly isolated and that any
overboard discharge, sea suction and isolation valves are sealed and tagged with serially numbered seals
provided by the contractor. All seal numbers shall be recorded on the shipping documents. All cargo
valves shall be in the open position prior to physically entering the cargo tanks.
a. In cases of multi-port loadings, the QAR at the initial loading port is responsible for physically
inspecting all vessel cargo compartments. Consequently, the QARs at subsequent loading ports shall not
enter any cargo tanks and where possible, empty tanks shall then be visually inspected from the deck.
b. All cargo tanks containing liquids shall be ullaged and sampled, and samples shall be retained.
Where cargo tanks to be filled have on-board quantity (OBQ) from a previous cargo/parcel, the product
previously loaded shall be ullaged, sampled and tested to the extent deemed necessary for conformance to
the applicable specification prior to topping off. Cargo tanks not being topped off (if any) that have been
loaded at a previous port shall be ullaged and sampled. These samples are to be held in the event loading
difficulties result in commingling of products.
2
c. Tanks used for loading must be coated with an approved epoxy. Coating must be adherent: no
flaking, peeling, or blistering.

2
NOTE: This ullaging and sampling does not apply to tanks containing JPTS. Special tank preparations and cargo handling is required for
JPTS, to prevent contamination.
MIL-STD-3004C
32

d. Cargo tanks that contain heating coils shall be checked to assure that the coils are tight and no
liquid/steam can escape from the coils. One way to validate this is by performing a pressure tightness
check on the system. Coils containing yellow metals (copper, bronze, etc.) are not permitted for aviation
turbine fuel use. The QAR shall report any vessel found to contain coils with yellow metals to MSC
PMO5, DLA-ENERGY Regional Quality Manager and DLA-ENERGY-QA. This precludes chartering
that vessel for a cargo of aviation turbine fuel.
e. It is mandatory that JPTS be loaded in tanks in which the last product carried was JP-5, JP-4,
kerosene, non-aromatic solvent, unleaded gasoline, or arctic diesel. Prior to loading JPTS, tank cleaning
requirements are: tanks must be machine washed with hot water, if cleaning chemical and/or salt water is
used, the final wash must be with fresh water. Tank bottoms, interior bulk heads and internals must be
completely free of sediment, scale and other contaminants. Tanks must be dry and all liquids completely
removed from the tanks lines after cleaning, must be flushed with fresh water, drained and free of all
water. Loading and unloading system must be completely isolated. This will be accomplished by
completely separate piping systems or by use of blinds. Valves will not be depended on to effect
isolation. No common lines will be used. Steam smothering lines should have at least two valves that
can be sealed from the main line to the tanks, or a blind installed that can be readily removed. Each tank
will have its own individual vent. If ship has a common vent system, tanks used for JPTS must be
isolated from balance of the vent system.
5.1.1.5.3 Vessel tank/internal rust test. When considered necessary and where safety precautions
permit, the QAR will require that samples of the rust be taken from selected cargo tanks and tested with
the product to be loaded or with a similar solvent. This procedure is performed to determine the effect
upon the corrosiveness and gum characteristics of the product. The rust shall be pulverized and added to
a sample of the product to be loaded, or to a similar product, in proportions of 5 to10 grams of rust per
100 mL of the liquid. After shaking the mixture vigorously for at least one minute, it shall be filtered
free of rust and tested for color, corrosion and residue.
5.1.1.5.4 Vessel loading plans. Loading plans shall be reviewed to determine their suitability,
giving consideration to bulkheads, lines, tank capacities, and ships trim. In the case of split cargoes, the
QAR shall ensure the vessel is physically suitable for handling two or more grades of product
simultaneously without contamination. The QAR shall ensure all bulkheads are secure and the vessel has
double valve separation or line blanks. If valves are used, such valves shall be lashed and sealed in
proper position against misuse. Initial and normal pumping rates shall be agreed upon before starting. If
differences cannot be resolved locally, they shall be referred to MSC. Prior to loading, all water shall be
removed from the vessel pipelines and cargo tanks.
5.1.1.5.5 Multi-port inspection. When a vessel is scheduled for a multi-port loading, the inspector
at the first loading point shall inspect, if practical, all of the ships cargo tanks to determine their
suitability for the scheduled product. The vessel shall not be approved for loading part of the cargo
unless all cargo tanks are considered suitable for the respective products. QARs at the subsequent
loading point(s) shall be advised by appropriate means of the results of the previous tank inspections.
This does not preclude rejection by QARs at subsequent loading points if conditions warrant such action.
5.1.1.5.6 Quality and quantity determination. Vessel movements must not be expedited at the
expense of quality and quantity determinations, regardless of pressure or protests. Full support shall be
given the QAR for reasonable actions taken to assure quality and quantity.
5.1.1.5.7 Vessel rejection/delay. For MSC (Military Sealift Command)-controlled vessels, DLA-
ENERGY-QA will be notified immediately to discuss the reason for rejection and/or need for re-
MIL-STD-3004C
33

cleaning. The QAR shall follow up the DLA-ENERGY-QA notification with a report to the cognizant
DLA-ENERGY Region, DLA-ENERGY-BI and MSC on vessel rejection or delays in loading
operations. The report shall contain pertinent details, including length of delay anticipated for tank
cleaning and product availability. For CONUS locations, telephone MSC Washington, D.C. at 202-685-
3121 (FAX: 202-685-5362). All calls shall be confirmed by a message to Commanding Officer, MSC
(COMSC), Washington, D.C. with the local MSC representative and DLA-ENERGY as information
addresses. For locations outside CONUS, a priority message shall be dispatched to COMSC,
Washington, DC, with the same information addressed as for CONUS. Rejection or delays shall be well
documented including dates, times, circumstances, personnel, discussion, etc. They shall be detailed on
the DD Form 250-1 with supporting documentation included. Contract administrative documentation, to
include DD-250-1, of these cargoes shall be kept for 6 years from date of completion IAW the FAR.
5.1.1.6 Pre-loading procedures (Shore/Tanker).
a. Assure sampling, testing and approval of shore tank prior to loading aboard the vessel (see Table
IX).
b. Check loading lines to determine they are properly isolated and do not contain product
detrimental to the cargo. Drain free water from each tank to be used through the water draw-off line.
c. Assure loading lines are full. In some cases, especially underwater lines, the lines may be
required to be empty prior to loading. Witness opening and closing shore tank gauges, and opening and
closing meter readings (when used).
d. Determine the position and setting of the swing line in the shore tank (where applicable) to
prevent loading of any free water or sludge from the tank bottom. Water shall be drawn from the tank
bottom through the water draw-off if it is anticipated that there is any possibility of loading the water
with the cargo.
e. Review the cargo layout and loading plan. The QAR and the master of the vessel (or his
designated representative) shall concur on the cargo layout and loading plan.
f. Inspection (to include checking the vessels log on nature of previous cargoes and the vessels
condition: leaks, previous rejections and excessive delays, for instance) and approval or rejection of the
vessel cargo tanks.
g. Assure sea suction and overboard discharge valves are closed and sealed prior to loading. In the
case of split cargoes, those valves essential to cargo isolation shall be sealed with serially numbered seals
and their numbers recorded on shipping documents.
h. Assure all parties are aware of sampling procedures for first-in prior to commencing. Check
cargo first-in and line samples analyses to verify quality of product moving to the vessel.
5.1.1.7 Loading procedures for tankers. Product quality and isolation shall be assured in shore
tanks and all lines used in loading. The line fill, approximately 2,000 to 5,000 barrels, shall first be
pumped into one or two cargo tank(s) on the vessel. Request the ships officer to switch from this tank to
other tank(s) and continue loading. A sample shall be drawn (after a 30-minute wait) from the first tank
and tests performed to determine if the quality of the product being loaded is satisfactory. Further
sampling and testing shall be conducted to the extent deemed necessary by the QAR. If at any time
during loading there is an indication of contamination, the loading shall be stopped until the cause and
extent of the contamination has been determined. When loading aviation turbine fuel or kerosene,
loading procedures (from COMSCINST 3121.3) shall be as follows:
MIL-STD-3004C
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5.1.1.7.1 Lines. If the vessel does not have segregated ballast, prior to loading, all lines shall be
dropped and water removed from cargo tanks. If simultaneous ballasting or de-ballasting must be
performed during cargo operations, record this fact and the reason(s) for it on the Material Inspection and
Receiving Report. A description of the degree of segregation that was maintained during the operation
should also be recorded.
5.1.1.7.2 Loading rates. Initial loading shall be at a rate not in excess of three feet/one meter per
second (about 1,500 barrels per hour through a 12-inch line) through loading lines into the cargo tanks
until the discharge outlet has been covered by at least three feet of the product. Thereafter, the normal
loading rate may be resumed. The loading rate of three feet per second applies to the flow into each tank.
The total loading rate shall not exceed the sum of the allowable rates for the individual tanks being filled.
If there is evidence of turbulence or splashing of the product in a cargo tank after the discharge outlet is
covered by the specified three feet of product, the reduced loading rate shall be continued until turbulence
ceases.
5.1.1.7.3 Thirty minute wait. Ullages, water soundings, temperatures and samples, including the
first-in samples, shall not be taken from any cargo tank until at least 30 minutes after flow into the tank
has ceased in order to dissipate static charge built up during the fuel movement. In the meantime,
loading of other tanks may proceed.
5.1.2 Shipments by barges and refueling craft. This section covers pre-loading and loading
procedures for barges and refueling craft. Those procedures for tankers are covered in 5.1.1. Post
loading procedures for tankers and barges are addressed in 5.1.4.
5.1.2.1 Pre-loading and loading inspection. Precautions and procedures outlined in 5.1.1.4, 5.1.1.5,
5.1.1.6, and 5.1.1.7 are applicable to barges and refueling craft to the extent possible, except rust samples
shall be taken only if the last cargo carried indicates this action to be necessary and can be taken under
safe condition.
5.1.2.2 Product conversions. Table XXVIII covers conversion from one product to another.
5.1.2.3 Inspection procedures for cargoes. Key operations in loading of barges and refueling craft
include the following:
a. Sampling, testing, and approving shore contents prior to loading aboard the vessel (see Table IX).
b. Checking loading lines to determine that they are properly isolated and do not contain product
detrimental to the cargo.
c. Ensuring lines are full. Obtaining opening and closing shore tank gauges. Obtaining opening and
closing meter readings where necessary.
d. Determining the position of the swing line in the shore tank, where applicable, and setting it at a
position to prevent loading of any free water or sludge from the tank bottom. Water shall be drawn from
the tank bottom through the water draw-off if it is anticipated that there is any possibility of loading
water with the cargo.
e. Checking the cargo layout and loading plan. The QAR and the master of the vessel (or his
designated representative) shall concur on the cargo layout and loading plan. The QAR shall assure that
the loading plan is for the ordered quantity. If differences exist between the vessel, shore facility and/or
the QAR, the matter must be resolved expeditiously prior to commencement of loading. This may
require confirmation from the ordering office. Allowable variances from the ordered quantity per the
MIL-STD-3004C
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contract are only acceptable if based on a condition of manufacturing, loading or shipping. Neither
product suppliers nor vessels should be targeting more or less than the original ordered quantity.
f. Inspecting (to include checking the vessels log on nature of previous cargoes and leaks, for
instance) and approving or rejecting the vessel and individual cargo tanks. Prior to loading aviation
turbine fuels, vessels shall have the tanks receiving the product stripped and mucked to remove residual
contaminants and moisture (IAW MSC Policy 98-01 and Table XXVII). These procedures shall be
applied to barges (over 30,000 barrels size) and refueling craft to the maximum extent possible.
g. Closing and sealing sea suction and overboard discharge valves prior to loading. In the case of
split cargoes, those valves essential to cargo isolation shall be sealed with serially numbered seals and
their numbers recorded on shipping documents.
h. Checking/analyzing first-in and line samples to verify quality of product moving to the vessel.
i. Sampling and testing of contents of vessels cargo tanks during and after loading (see Table IX).
5.1.3 Receipts from tanker or barge. This section excludes fuels which are delivered directly into a
vessels fuel tank (the process of bunkering - see 5.5). It also excludes barge receipts under the post
camps and station program (see 5.4). For F.O.B. Destination contracts, the product supplier may have a
representative present at the discharge facility in order to witness quantity and quality procedures
performed at the destination receipt facility.
5.1.3.1 Shore side. Before commencing with a receipt of fuel, personnel shall assure that the shore-
side is ready for discharge to ensure the quality of the product in the receipt tank(s) subsequent to
receiving the product. The terminal shall be aware of the time of the vessels arrival. Personnel shall
assure line condition is full and properly isolated in accordance with MPMS. Free water shall be drained
from the tank through the water draw off line. Shore tanks shall then be gauged and temperatures
determined in accordance with the MPMS. Personnel shall determine net quantity before discharge. If
necessary, samples shall be taken of the line to assure product is the same as that being discharged (e.g.
when the line contains unlike product in a non-dedicated system or when problems were experienced
with the previous receipt). If additives are to be injected into the product during discharge, personnel
shall assure injectors are in working order and that required additives are in proper quantity and quality.
5.1.3.1.1 Returns from USN vessels. Test representative samples sent from the vessel cargo/bunker
tanks to assure product quality. In some circumstances the vessel may elect to defuel to a barge to
consolidate all product and expedite repairs or operational re-deployment. JP-5 shall be tested to type B-
1 series tests plus thermal stability. F-76 shall be tested to type B-1 series test plus storage stability.
Request disposition instructions for off-specification fuel from DLA-ENERGY-QA IAW section 5.13.2.
5.1.3.2 Vessel pre-discharge inspection. Paperwork onboard the vessel shall be examined to
confirm product type, quantity and quality, and the presence of free water. If there is any indication the
product does not conform to the quality requirements, discharge shall not be commenced until the
disposition instructions have been received in accordance with this Standard (see 5.13.2). Personnel shall
verify that seal numbers as compared to the DD Form 250-1 are intact. A meeting shall be held with
vessel personnel prior to discharge to discuss procedures and pumping rates to be used. Tank
gauging/temperature determination shall be witnessed for record and net quantities shall be calculated. If
variations of 0.5 % volume are indicated on an individual barge gauging comprising a shipment of two or
more barges, then that barge shall be discharged separately and separate shore tank gauges taken.
Monitor all-level tank samples and testing as stipulated in Table IX, Serial 5b. Additional testing shall be
performed if required to assure split cargoes have not been commingled. The remainder of the composite
MIL-STD-3004C
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sample shall be retained until discharge is complete and the shore tank is tested. Product is normally
discharged when laboratory tests show conformance to specification requirements.
5.1.3.3 Contaminated product. If the product is suspected of being contaminated, it shall be
sampled prior to off load and submitted to a laboratory for a minimum of B-3 series analysis. If testing
facilities are not readily available, but a visual examination shows contamination, then DLA-ENERGY
shall be notified (see 5.13.2). Disposition instructions are provided based on the circumstances (product
contaminated, contaminant, the configuration of the discharge facility, the urgency for the product) and
options available (availability of filter-separators, product isolation ashore, product blending capability
ashore, or possibility of product remaining on vessel for disposition at another facility). Prompt action
shall be taken to reduce vessel lay time costs.
5.1.3.4 Discharge. Once authorization for discharge has been given, the vessel notifies the shore
when ready to commence and ensure communication is maintained between ship and shore for the entire
operation. Personnel shall ensure that line samples are being taken as required (Table IX, Serial 5b) and
shall monitor logs as well as line sample results.
5.1.3.5 Completion. Upon finishing the discharge, personnel shall determine product Remaining
On Board (ROB), calculate net quantity received ashore, investigate any quantity discrepancies, sample
and test product after settling, complete discharge DD Form 250-1, and gather any other applicable
documents to include ullage sheets, bunker reports, etc. Any delays in discharging and/or investigation
results shall be reported to DLA-ENERGY.
a. After the vessel is unloaded, the Government Representative shall examine each cargo tank to
determine if any product is remaining onboard. Cargo tanks containing product(s) ROB shall be gauged
and the amounts determined by the correct applicable procedures such as capacity tables and wedge
formula. If it is impossible to obtain accurate figures, the quantities should be estimated. The quantity,
the cargo tank number involved and pertinent information or reason for incomplete discharge shall be
entered on the DD Form 250-1, Tanker/Barge Loading/Discharge Report. If it is not the final destination
port, the Government Representative at the next discharge port shall be notified of any unusual
conditions, gauges, or losses identified.
b. Shipping and handling losses or gains, as cited in DoDM 4140.25-M, shall be recorded by the
destination Government Representative on the DD Form 250-1, indicating the cause of the loss/gain to
the extent possible. The destination Government Representative remarks, concerning the loss or gain,
shall be confined to observations and evaluations made at the receiving terminal. Tank gauges, line
capacities and ship ullages shall be checked as necessary in attempting to account for the loss or gain
(DoDM 4140.25-M along with paragraph 5.1.1.4.6 of this document establishes loss or gain criteria). If
the loss or gain cannot be accounted for at the final discharge point, the Government Representative shall
immediately communicate with the QAR at the loading point(s) and simultaneously with the Government
at each intermediate discharge point (if any) to determine possible reasons for the loss or gain. Each
Government Representative queried shall advise final destination of his findings within 15 calendar days.
The final destination Government Representative shall consolidate the data and forward it to the account-
able property officer. Corrected DD Form 250-1(s) shall be initiated and distributed as appropriate.
c. The required inspection documents shall consist of DD Form 250-1 (Tanker/Barge Discharge
Report), DD Form 250-1 Continuation Sheet, the shore tank ullage or innage report, the vessel ullage or
innage report, bunker reports (if any), laboratory test results sheets and such other documents as required.
Distribution of these documents should be made in accordance with DFARS and/or contractual
requirements.
MIL-STD-3004C
37

5.1.3.6 Vessel delay. For MSC-controlled vessels - report to the cognizant DLA-ENERGY Region,
DLA-ENERGY-BI and MSC on delays in discharge operations, with pertinent details, including length
of delay anticipated. For CONUS locations, telephone MSC Washington, D.C. at 202-685-3121 (FAX:
202-685-5362). All calls shall be confirmed by message to Commanding Officer, MSC (COMSC),
Washington, D.C. with the local MSC representative and DLA-ENERGY as information addresses. For
locations outside CONUS, a priority message shall be dispatched to COMSC, Washington, DC, with the
same information addresses as for CONUS.
5.1.4 Post-loading - tankers and barges. This section covers post loading of tankers and barges.
Procedures for pre-loading and loading of tankers are in 5.1.1.6 and 5.1.1.7. Those procedures for barges
and refueling craft are covered in 5.1.2.1.
5.1.4.1 Vessel samples. Government shall witness sampling of vessel cargo tanks. The
Government Representative shall monitor cargo tank gauging and temperature determination, and water
cuts as time permits. If possible, water shall be stripped ashore before the tanker is released. Maintain
surveillance of the stripping operation. Failing this, advise the master to strip water out of the cargo
tanks into vessel slop tanks. Report fuel loss during the stripping operation.
5.1.4.2 Determination of quantity. Government Representative shall witness shore tank gauging
(opening and closing). The Government Representative shall independently determine shore and vessel
net quantities, and ship/shore losses or gains. If a ship/shore loss or gain is determined, the Government
Representative will re-compute to confirm the numbers and conduct an investigation if there is still a loss
or gain and the variance is outside the allowed variance (see 5.1.1.4.5 for tolerances).
5.1.4.3 Inspection documents covering tanker and barge loading
3
5.1.5 Ship-to-Ship Transfers at Sea. Issuing and receiving vessels are responsible for performing
quality checks before, during and after a transfer. The issuing vessel will strip water from the tank just
prior to the transfer to assure water and sediment are not transferred. Line samples will be taken and
checked for appearance every thirty minutes during the transfer by the receiving vessel.
. Government Representative
shall assure completion of the required inspection documents that includes a DD Form 250-1,
Tanker/Barge Loading Report, Continuation Sheet, ullage or innage report and such other documents as
may be required. If the product is loaded from more than one tank, list the tests applicable to each tank in
separate columns headed by the tank number. The date the material in each tank was approved and
quantity loaded from each tank shall be indicated in the appropriate column. The QAR may require
additional testing if the situation so warrants. Assure distribution of these documents is made according
to DFARS.
5.2 Pipeline operations.
5.2.1 Shipments by pipelines. This section applies to all movements of product belonging to or to
be accepted by the Government, except movements of Contractor-owned product where quality is
verified after receipt at a terminal and prior to delivery to the Government. The movement of petroleum
products via multi-product pipelines presents many problems in the control of quality and the operation
requires close surveillance. This section furnishes guidance related to quality of petroleum products
shipped in pipelines. This does not apply to bunker fuel where the mode of delivery is pipeline.
5.2.1.1 Tariffs and agreements. Carriers tariffs outline the normal responsibilities of the pipeline
company. Supplemental agreements are usually entered into between the Government and the carriers,

3
It is recommended that laboratory tests report sheets be attached separately vice transcribing results onto the DD 250-1.
MIL-STD-3004C
38

which further elaborate on the extent of the carriers responsibilities. Copies of these agreements shall be
made available to cognizant quality assurance offices by either the DLA-ENERGY Region or prime
contractors as applicable. These documents shall be reviewed by the QARs concerned and the provisions
thereof shall be used in product quality surveillance.
5.2.1.2 Laboratory testing. Products shall be tested in accordance with the appropriate Table IX-
XXV before entry into and after discharge from a pipeline. For pipelines carrying aviation turbine fuels
and automotive gasoline, laboratory facilities shall be made available to perform identification tests on
products at terminals along the pipeline system.
5.2.1.3 Markings. Single and multi-product pipelines, pumps, and valves shall be marked to clearly
identify the grade of a product being carried. These markings shall be placed adjacent to all operating
accessories such as valves, pumps, regulators and manifolds. MIL-STD-161 provides guidance on color
markings and titles. However, due to security issues, military style markings may be replaced by an
acceptable alternative when required by the security office.
5.2.1.4 Identification tests. When products are transferred through a multi-product pipeline,
identification tests are required in accordance with Table IX.
5.2.1.5 Multi-product pipelines. Pipelines are to be used wherever possible for one grade of fuel
only. However, multi-product pipelines are often used between bulk terminals.
5.2.1.5.1 Product identification. The product entering a multi-product pipeline or discharging from
it shall be identified by a flag or sign on the connections to the multi-product pipeline.
5.2.1.5.2 Pumping time. Pumping shall normally be continuous until product has been cutoff.
5.2.1.5.3 Pipeline transfer velocity. Product velocities in pipelines shall be maintained to minimize
mixing of product.
5.2.1.5.4 Segregation during transfer. Preferred procedures for segregating products during
movement are shown in their order, see the following:
a. Turbulent flow without plugs between products.
b. Hydrocarbon plug between products or grades.
c. Mechanical plugs (batching balls) between products or grades.
d. Disposal of Water-Mixed Product. Provision shall be made for removal and disposal of mixed
product and water.
5.2.1.6 Terminal, depot, and base system.
5.2.1.6.1 Product compatibility. Before the pipeline transfer is started, it shall be determined
whether the product in the line (line fill) is the same as the issue/transfer tank product or can be included
in the transfer.
5.2.1.6.2 Cleaning of pipelines. Incomplete flushing or cleaning of multi-product pipelines is a
potential source of contamination. Pipelines are cleaned using various methods, most of which involve
various types of pigs. These create large quantities of scale, sediment and water called pig clouds.
Isolation of these pig clouds is required so as to preclude a major contamination of working tanks. The
preferred method of receiving a pig cloud is into a truck(s) to capture the largest portion of the cloud.
Containment in a small tank is next or into a tank that is already scheduled for cleaning in the next three
months.
MIL-STD-3004C
39

5.2.1.6.3 Valve and pipeline control. Proper blinding off of connecting lines and correct valve
control during transfer will minimize the possibilities of pipeline contamination.
5.2.1.7 Cross-country system.
5.2.1.7.1 Turbulent flow. The maintenance of turbulent flow during multi-product movements and
a packed line when shipments are static is mandatory to ensure a minimum of transmix.
5.2.1.7.2 Batch cuts and segregation. Both improper batch cuts and product segregation are
potential sources of contamination.
5.2.1.7.3 Contaminated pipeline shipment. Rust contamination during pipeline shipments can result
from inadequate corrosion inhibition or scraping of the pipeline.
5.2.1.7.4 System isolation. Isolation of the system from all inter-connecting lines by suitable blinds
or two block valves with an open bleeder valve between will minimize the possibility of product
contamination.
5.2.1.8 Common transfer lines and pumps for fuels.
5.2.1.8.1 Preferred method. It is preferable to utilize separate pipelines, valves and pumps for each
type and grade of fuel in order to maintain the quality of liquid fuels.
5.2.1.8.2 Use of water displacement. Except where approved hydraulically-operated water
displacement systems are employed, displacement by water is not recommended.
5.2.1.8.3 References. Detailed information on the operation, maintenance and inspection of
facilities used in dispensing and storing fuels may be found in appropriate departmental directives and
manuals.
5.2.1.9 Segregation. The segregation of product in military multi-product pipelines is accomplished
by maintaining turbulent flow, by the use of a batching plug or buffer batch of a suitable hydrocarbon.
During movements with turbulent flow, constant surveillance shall be maintained to ensure minimum
flow rates required for turbulent flow. Even though commingling occurs under all conditions at the
interface between products, the objective is to control the length of the transmix and ensure its proper
disposition. The resultant transmix will vary in amount with factors like pumping rate, distance and
contour of the line, line pressure and number of pumping stations. Cuts into terminal storage shall be
made in accordance with Table XXIX. If this schedule cannot be followed because of operational
requirements or limited capacities of a terminal, cuts shall be made in a manner ensuring delivery of an
on-specification product to the consumer. No other product shall be commingled with grades JP-5, JP-8,
JPTS or aviation gasoline (all grades).
5.2.1.10 Corrosion control. Fuels transported by pipeline are subject to contamination by rust,
sediment (solids), water and surfactants. Periodic checks shall be made to determine the extent of
internal deterioration of the pipelines.
5.2.1.10.1 Determination of sediment (solids). An increase in solids content in petroleum products
while in transit through a system can indicate rust buildup in the system. Particulate buildup may also be
the result of insoluble agglomerates formed from fuel oxidation processes. The amount of solids may be
determined by ASTM D 2276, D 5452, or D 6217 as applicable. Solids content of product samples taken
at the shipping and receiving points or at periodic intervals at the receiving point will provide data for
comparison.
MIL-STD-3004C
40

5.2.1.10.2 Corrosion inhibitors. Fuel for military aircraft and ground vehicles may contain
approved corrosion inhibitors to reduce corrosion of the pipeline and handling systems. Corrosion
inhibitors also enhance fuel lubricity, which is required for some aircraft components. All aviation
turbine fuel will normally be supplied by the manufacturer with a corrosion inhibitor. It is permissible to
inject approved oil soluble corrosion inhibitors into aviation turbine fuel being moved by pipeline to
effectively control pipeline corrosion, subject to the limitation indicated in to ensure proper protection,
the inhibitor effectiveness shall be checked at various points along the line. This can be accomplished by
a visual inspection of the steel coupons that have been installed in the fuel stream in the pipeline, or by
determining metal loss from change in weight of the specimens (see Test Method 1000 of this Standard
for rating level). Another method is making a visual inspection of steel rods or strips that have been used
in specific laboratory tests on fuels taken from the pipeline.
5.2.1.10.3 Aviation Turbine Fuel Additive Concentration. In the event corrosion inhibitor shall be
added, only those inhibitors listed in the current Qualified Products List for MIL-PRF-25017, and those
approved for that product shall be permitted. Care shall be taken to ensure approved concentration in the
product is not exceeded. Excessive inhibitor will lower the water separation rating. Only corrosion
inhibitors listed in STANAG-3390, Guide Specification and Inspection Standards for Fuel Soluble
Lubricity Improvers, are approved for use in the NATO pipeline system.
5.2.1.10.3.1 Location. To locate information, link to the Qualified Products List at
https://assist.daps.dla.mil/quicksearch then type the QPL number (25017) and hit enter. Page down to
Revision History and click on View QPL data. Another screen will appear and chick on MIL-PRF-
25017 Category 1. To get concentration for each additive you click on source notes
5.2.1.10.4 Pressure drop. A gradual reduction in product flow rates while maintaining a constant
pumping pressure can be caused by increased internal corrosion in the pipeline system. A continued
increase in pumping pressures to maintain normal product delivery rates may also be indicative of
internal corrosion buildup. Such evidence shall be brought to the attention of the responsible authorities.
5.2.1.10.5 Drag Reducer Additive (DRA). Drag reduction additives (DRAs) improve flow in
pipelines by reducing turbulence. The present DLA Energy policy is that no DRA will be added to any
military aviation turbine fuel, motor gasoline or automotive diesel. To ensure the absence of DRA in
government owned fuels, if a pipeline company is injecting DRA into commercial product, the DRA
injection must be stopped two (2) hours before and resumed two hours after the expected government
fuel batch has passed the injection point. This will preclude the inadvertent inclusion of DRA into the
government fuel and should exclude the DRA in any transmix.
5.2.1.11 Quality surveillance pipeline procedures. QARs should:
a. Assure products to be tendered through the pipeline conform to the applicable specification or
standard.
b. Maintain surveillance over the pipeline operations during the transfer to another carrier and at key
points in the system during the movement of tenders. Examine records of pumping rates, progress of
tenders, and extent of transmix, gravity and color determinations.
c. Witness the cutting of tenders or batches into pipeline receiving tanks. In emergency
circumstances where witnessing batch cuts are impossible, a review of the product change record shall be
made when the sampling and testing of the receiving tank are witnessed.
d. Verify the quality of product in pipeline receiving tankage after receipt of the tender or batch.
Select the identification tests to be performed for verification of product quality (See Table IX).
MIL-STD-3004C
41

e. Maintain familiarity with procedures used to protect or condition the pipeline interiors.
f. Where necessary, evaluate the characteristics of the transmix to determine its disposition. The
procedures for this evaluation, a suitable form for recording data and a sample of the calculations
involved are shown in the product change record form (See Appendix E).
5.2.2 Receipts by pipeline.
5.2.2.1 Before receipt. Before commencing receipt of fuel, personnel shall assure that the quality of
the product in the receipt tank(s) subsequent to receiving the product. The terminal shall be aware of the
time and quantity of the pipeline tender. Personnel shall assure line condition is full and properly
isolated. Tanks shall then be gauged, temperatures taken and a net quantity determined before receipt of
product in accordance with the MPMS or other applicable publication. If necessary, samples shall be
taken of the line to assure product is the same as that being received. If product is to be injected during
receipt into the tank, personnel shall assure injectors are in working order and that required additives are
the proper type and in the proper quantity and quality.
5.2.2.2 During receipt. To the maximum extent possible, personnel shall witness batch cuts to
assure they are in accordance with contract or operating agreement (e.g.: heart, mid-point, etc.). If line
samples are being taken during receipt, assure that each sample is being properly taken. Personnel shall
monitor samples taken throughout the receipt of the tender for contamination (e.g. water, increased
sediment, secondary products).
5.2.2.3 Completion. Upon completion, personnel shall determine quantity by gauging the receipt
tank(s) used, measuring temperatures and calculating net quantity received. Personnel shall investigate
any quantity discrepancy in excess of that cited in DoDM 4140.25-M and allow receipt tanks time to
settle before sampling and testing. Receipt tanks shall be sampled and tested in accordance with ASTM
D 4057 (MPMS, Chapter 8.1 or other applicable publication) and Table IX of this Standard. Personnel
shall assure samples are retained as called for in the quality control plan or established quality
procedures. The DD Form 250 shall be completed and signed.
5.3 Truck and tank car operations.
5.3.1 Shipments by tank truck and tank car.
5.3.1.1 Tank truck and tank car service/conversion. Tank cars and trucks shall be continuously kept
in the same grade of service to minimize the possibility of contamination. If this is impracticable, each
vehicle shall be processed for a change in grade in accordance with Table XXVI of this Standard, except
as outlined in the conversion policy below.
5.3.1.2 Tank truck and tank car conversion policy. The following policy is in effect concerning
cleaning requirements of commercial trucks when switching from gasoline to Aviation Turbine Fuel.
Trucks are required to be steam cleaned after carrying gasoline and prior to carrying jet fuel. DLA-
ENERGY Region Commanders may approve exceptions to this policy for Aviation Turbine Fuel,
provided that the transportation officer can verify that trucks and tank cars which previously carried
turbine fuels are not available and that there is a definite need to forgo cleaning as required by this
Standard. This need to forgo the cleaning would be based on having to load out of a specific facility to
accomplish a specific mission
4

4
Each facility shall be a separate request and a separate evaluation. Facilities shall not be combined in this instance.
. The transportation officer shall then forward a request for exception to

MIL-STD-3004C
42

the Region Commander, identifying: the need not to clean trucks and tank car; the risks to product
quality; and the procedures to be established to abide by the requirements cited below. A complete file
should be kept at the region facility for which an exception has been requested. As a minimum the file
should include: identification of the facility, the initial request by the transportation officer, identification
of quality controls to be in place; approval or disapproval by the Region Commander, and the collected
data. Exceptions for each facility shall be re-certified by each new commander, transportation officer,
and quality manager after initial implementation. All problems with customer rejection of product, or at
the facility with off-specification product, shall be reported to DLA-ENERGY-QA. Exceptions shall be
curtailed any time loss of quality control is indicated.
5.3.1.2.1 Exception/quality data. As outlined above, the following data should be collected as part
of any exception concerning cleaning requirements switching from gasoline to turbine fuels. The
following data shall be collected and requirements met for each DFSP for which an exception is
requested:
a. The JP-8 received at the DFSP shall have sufficient headroom difference between the minimum
JP-8 specification requirement and actual flash point in the issue tank so that some product degradation
can be tolerated. The DFSP issue tank shall have minimum 10 C headroom above the specification or
equal to or greater than 48 C (118 F).
b. DFSP personnel shall examine each truck and tank cars previously carrying gasoline to determine
if the truck (to include its pumps and piping) have been completely drained and dried. There are no
exceptions to a drained and dried truck after it has carried gasoline.
c. Test a conveyance composite for density and flash point prior to release of the truck. DFSPs shall
collect and monitor flash point data.
d. Regardless of headroom, only minus 5 C flash point degradation shall be tolerated at the DFSP
level. Results beyond this shall require DFSP personnel to identify the cause of the degradation (e.g.
gasoline remaining in the manifold/piping) and discuss with the trucking company methods to preclude
recurrence. Failure to correct the situation would require the steam cleaning requirement to be reinstated.
e. As a precautionary measure, the DFSP shall submit truck composite samples for B-1 plus ASTM
D3241 oxidative stability testing every 30 days for the first three months. Barring any problems, samples
shall then be continued quarterly for the first year and then tested as deemed necessary by the QAR. This
is a precaution against interactions with new reformulated gasolines, or any possible contamination
picked up during transport of JP-8.
5.3.1.3 Tank truck and tank car loading.
5.3.1.3.1 Safety. Appropriate safety measures shall be taken during loading and unloading
operations. Blanking caps shall be fitted to all filling and discharge connections not in use.
5.3.1.3.2 Loading line. Prior to loading, the contents of the source tank and the loading line to the
fill rack shall be checked in accordance with Table IX.
5.3.1.3.3 Procedures at the loading rack. Upon arrival at the loading rack, trucks and tank cars shall
be inspected for mechanical condition and suitability to transport the product. Dome covers shall be
opened, bottom outlet caps on tank cars removed, and the bottom outlet valves fully opened. This allows
residues from previous cargoes to drain completely into a suitable container. The outlet valves shall be
inspected and if found defective shall be repaired or replaced prior to loading.
MIL-STD-3004C
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5.3.1.3.4 NATO codes. In NATO countries, wherever possible, the vehicle should be clearly
marked with the NATO code numbers of the product being carried.
5.3.1.3.5 Gaskets and hose connections. Care shall be taken to ensure gaskets and hose connections
are maintained in good condition so fill and discharge connections will be air and fluid tight.
5.3.1.3.6 Vehicle tank cleanliness. Each truck or tank car shall be inspected for cleanliness and
suitability to receive product. Interiors, including domes, shall be free from loose rust, scale, or dirt and
shall be dry (water-free) prior to loading.
5.3.1.3.7 Product free-fall. For top-loading facilities, care shall be taken to prevent fuels other than
residuals from free-falling or splashing during loading operations by inserting the discharge hose or
loading arm fill pipe to the bottom of the tank. The fill rate shall be slow until hose or fill pipe is covered
by six inches of product. Prior to loading, particular attention shall be given to the outlet and safety
valves to ensure they are properly seated and in operable condition.
5.3.1.3.8 Recording test results. The contents of each tank car and truck shall be sampled for the
check tests (Table IX) upon completion of loading. Test results shall be recorded and retained for one
year. Retained samples of the truck/car loading shall be held until product has been received and tested
by the using facility.
5.3.1.3.9 Sealing. Where sealing is required domes and/or unloading valves in the case of tank cars
and all openings in the case of truck loadings shall be secured and sealed with serially numbered seals
immediately after filling. Serially numbered seals and the API gravity at 60 F or density at 15 C shall
be noted on shipping documents.
5.3.1.3.10 Placarding. Trucks and tank cars shall be properly placarded, identifying cargo being
carried prior to departure from the loading facility.
5.3.2 Tank truck and tank car receipts. This section excludes tank truck and tank car receipts of
motor gasoline, diesel and heating oil under the post, camps and station program (see 5.4).
5.3.2.1 Before receipt. Before commencing a truck or tank car receipt of fuel, personnel shall
assure that the receipt tank is ready and that the quality of the fuel in the receipt tank(s) has been
determined subsequent to receiving the product. The terminal/facility shall be aware of the time and
quantity of the arriving trucks. Personnel shall assure line condition is full and properly isolated to
receipt tank. Normally, lines are dedicated, however, if not, line condition shall also be checked. Receipt
tank(s) shall then be gauged, temperatures taken and a net quantity determined in accordance with
MPMS or other applicable publication, before fuel receipt. If necessary, samples shall be taken of the
line to assure product is the same as that being received. If product is to be injected with additives while
discharging into the tank, personnel shall assure injectors are in working order and that required additives
are the proper type and in proper quantity and quality.
5.3.2.2 Truck and tank car arrival. Personnel shall check accompanying paperwork to assure the
fuel to be unloaded is the proper type and quantity. Validate the product grade in the truck is the same
grade as in the receipt tank. Validate that the receiving point is identical to that on the shipping papers.
If not redirect the truck to the correct off-loading location. If being used, truck hoses shall be checked to
assure they are clean and dry for use. Seals, when placed at the load point, shall be checked to assure
they are intact and correspond to the numbers on the shipping manifest/DD Form 250. Afterward,
personnel shall break seals, sample and test each compartment in accordance with Table IX
(workmanship). Shipment must be accompanied by the test report for the product carried from the
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loading point. Provided all conditions mentioned are satisfactory, the product may be discharged into
receipt tanks.
a. Where seals are required, the conveyance will be checked to determine if the required seals are
broken or missing, the product shall not be unloaded until it is determined that the quality and quantity is
satisfactory. Demurrage charges, if any, shall be referred to the cognizant DLA-ENERGY Region.
Where tampering is evident, the shipper shall be notified immediately.
b. If water is present, it shall be drawn off prior to unloading. Fuels which have a cloudy
appearance or have an unusual color shall not be accepted until laboratory tests indicate they are suitable
for use.
c. At Navy, Marine Corps and Army terminals, personnel shall compare the density at 15 C (API
Gravity at 60 F), with the density at 15 C (API Gravity at 60 F) reported on the DD Form 250. Both
shall agree within
2 kg/m
3
(0.5 degrees API).
d. In the event water has collected in the bottom outlet valve of a tank car and has frozen, prevent-
ing the free movement of the valve, a steam jet, hot water or hot cloths may be used for thawing the ice.
5.3.2.3 Truck and tank car rejection. If truck is rejected, a receiving organization shall first notify
the origin shipping point and quality representative, identifying the product, truck number and reason for
rejection of the product. Activities shall notify their service control point as soon as possible after
rejection of vehicle.
5.3.2.4 After discharge. Personnel shall examine truck or tank car to determine if all product has
been discharged into receipt tanks. Installation of a VISI-Flow gauge on the receipt system is another
method enabling determination of full discharge. When all trucks/cars have been discharged, personnel
shall annotate the receipt quantity on the DD Form 250. Quantity is determined by calibrated meter or
gauging receipt tank(s). When tank gauging is the method used for determining receipt quantities, the
temperature shall also be measured and net calculations performed correcting the quantity received to 60
F (15 C). Personnel shall investigate any quantity discrepancy in excess of that cited in DoDM
4140.25-M. Time shall be allowed for the product to settle in the receipt tank before sampling and
testing. Personnel shall sample and test receipt tanks in accordance with the MPMS, Chapter 8 or other
applicable publication and Table IX. Samples shall be retained as called for in the quality control plan or
established quality procedures.
5.4 Receipts of motor gasoline, diesel and heating oil under the post, camps & station (PC&S)
purchase program. Under DLA-ENERGY purchase programs, products required at the base level are
normally provided under PC&S contracts. The following products are normally procured under PC&S
contracts, mostly to non- Government specifications: Fuel oils (FO #2, #4, #6, etc.), Gasolines (MUR,
MUM, MUP, MMR, MRR, MPR, Gasohol, E85, etc.), diesel fuels (DF-2, DL-1, DL-2, 1-D, 2-D, No.
1/2/4-D, B20, DS-1, DS-2 etc.) and aviation turbine fuel (JP-8, Jet A, Jet A-1, TS-1, etc.). Product is
usually delivered directly by the contractor, via truck or tank car to the requiring activity. On fuels, other
than aviation, which are delivered via truck or tank car to U.S. Government installations for their use and
consumption, Government inspection for identity and quantity will be performed by the receiving activity
in order to accept the fuel on behalf of the Government. Note: Trucks may or may not be sealed after
loading based upon contract requirements. Normally CONUS does not require trucks to be sealed while
OCONUS may require sealing due to security requirements. Whenever the item calls for delivery into or
by barge, for either origin or destination contracts, the Contractor shall keep the QAR informed of the
loading date and source of supply along with any changes thereto as far in advance of the loading date as
MIL-STD-3004C
45

is possible to permit necessary inspection by the U.S. Government. The U.S. Government reserves the
right to perform quality inspection at all times and places if warranted.
5.4.1 Truck and tank car arrival/before delivery. Product may be delivered to one location (by truck
and tank car fill-to-the-mark or meter) or delivery may be made to several locations (by tank wagon,
meter). If unable to take an all-level sample from the truck compartment prior to discharge, then an in-
line sample taken after line displacement during discharge may be used. Responsible base personnel
shall examine accompanying paperwork, assuring the correct product, quantity and location. Verify seal
numbers prior to discharge where seals are applicable. Validate the product grade in the truck is the same
grade as in the receipt tank. Validate that the receiving point is identical to that on the shipping papers.
If not redirect the truck and tank car to the correct off-loading location. Tank compartments shall be
sampled (all-level) and examined for workmanship. Gasoline, diesel fuel and particularly aviation
turbine fuel shall not contain visible water and sediment. Burner fuels shall not contain more than a trace
of water or sediment. Excessive sediment may plug the burner tip degrading fuel atomization. Water can
cause rough burning, corrode the fuel handling system and result in the production of microbiological
growth. The type of equipment and type of burner fuel will determine the allowable limits of water and
sediment in the fuel. If sample testing indicates an off specification product, product shall not be
accepted. The problem shall be reported immediately after the rejection of the truck, info to the
appropriate service control point, to the DLA-ENERGY contracting officer (PC&S: DLA-ENERGY-
PEA (703-767-9509); DLA-ENERGY-PEC (703-767-9520); DLA-ENERGY-PLB (703-767-9536);
DLA-ENERGY-PLC (703-767-9511) and DLA-ENERGY-QA (703-767-8362). These are commercial
numbers; the DSN is 427-XXXX, using the last four numbers of the phone numbers above. The
facsimile number is 703-767-8506 for DLA-ENERGY-BP and 703-767-8747 for DLA-ENERGY-QA.
5.4.1.1 Truck and tank car after delivery/before departure. For direct delivery to one location - once
off-loading has been completed, the truck shall be examined to determine if any product is Remaining On
Board (ROB). This shall be annotated on the bill of lading. If multiple drops are being made using a
meter, the tank wagon shall also be examined, simply as a check, especially if all quantities are supposed
to be delivered.
5.4.2 Barge delivery. Product being delivered by barge shall be sampled and tested in accordance
with Table IX, Serial 5 and the appropriate table (Table X Table XXV) depending on the type of fuel.
5.5 Receipts from the bunkering program. This section applies to commercial bunker fuels (such as
MGO or IFO) from commercial suppliers at ports under DLA-ENERGY Bunkers Contract. The
commercial supplier shall provide and maintain an inspection system acceptable to the Government
covering supplies under this program. The Government has the right to inspect and/or test supplies called
for under this program. Unless otherwise noted, inspection will be performed by the receiving activity
based on documents required to be supplied by the commercial supplier at the time of delivery.
Acceptance of these supplies will take place at destination notwithstanding that inspection by the
Government may take place elsewhere prior to acceptance. Note that within the DLA-ENERGY Bunkers
Program, DLA-ENERGY does not normally perform inspection at source, rather the receiving vessel is
expected to perform both inspection and acceptance functions. Acceptance on behalf of the U.S.
Government is normally made by the vessel representative. The products provided under the bunker
program may either be under DLA-ENERGY contracts or purchased directly by the vessel. The products
are delivered to the vessels via barge, pipeline or truck when the vessels are moored to the docks. They
are delivered to the vessels via barge when they are at anchor. The vessel personnel perform quality and
quantity checks. Additional testing of bunker samples may be through a DLA-ENERGY, MSC or vessel
contract. Vessels requesting participation in the DLA-ENERGY bunker test program shall submit their
MIL-STD-3004C
46

request through Navy/Coast Guard channels to DLA-ENERGY-QA. The requirements for a bunker test
program include the following: (1) A flange with a sample valve (sample collar) is required to be on each
bunker line to be used for receiving bunkers, (2) A composite sample is taken at the sample point, split
three ways between the supplier, vessel and testing laboratory, (3) Sample containers/mailers are
provided to the vessel for taking and sending a sample to the authorized testing laboratory, (4) Test
results are provided back to the vessel within a specified time frame and (5) When problems are
encountered during the delivery and cannot be resolved within the limits of the contract, the contracting
office shall be contacted immediately for assistance.
5.5.1 Before bunkering. Validate that the product to be delivered is exactly as ordered. This can be
accomplished by taking a representative sample of the offered product and performing as a minimum of
type C tests, receiving a certificate of analysis of the product to be tendered, or by validating that the
shipping documents indicate the correct product and grade are being delivered. Validate quantity to be
received conforms to ordered amount. The vessel personnel have the option to witness manual gauges
whether from a shore tank or bunker barge. To prevent fraud, especially on deliveries by bunker barges
without delivery meters, the vessel personnel shall witness the product and water gauges for all tanks
aboard the bunker barge. This shall include all slop and void spaces that could hold cargo. As deliveries
are net volume or by weight, assure a temperature is taken from each cargo and slop tank. Confirm with
the vessel which tanks will be issued to the vessel. When participating in a bunker test program, vessel
personnel shall assure that the sample collar is properly affixed at the manifold, the sample valve is clean,
sufficiently cleaned sample containers are on hand to obtain the drip sample and a sufficient number of
containers are on hand to make the required distribution of the samples.
5.5.2 During bunkering. If possible, new bunkers should be segregated until test results have been
received and indicate that the product is satisfactory for use. Validate at the commencement of the
delivery that the product conforms to specification requirements by taking a sample at the flange. Check
the appearance and gravity (if capability exists). Save at least two quarts of any product suspected of
being off-specification for future analysis. Stop the delivery and investigate when problems develop.
Sample several times during the delivery for a visual inspection for water, sediment or other
contaminants separate from the in-line composite drip sample taken. When participating in a bunker test
program, start the composite drip sample as soon as the delivery commences so as to obtain a fully
representative sample of the entire bunker delivery. Collect the sample as per instructions provided in the
kit. Should sampling indicate a problem on a DLA-ENERGY Bunker contract that cannot be resolved
locally, discontinue bunkering and notify the DLA-ENERGY- Contracting Officer at (703) 767-8461; or
by facsimile to (703) 767-8506. Problems of a quality nature shall also be reported to DLA-ENERGY-
QA directly at (703) 767-8742; or by facsimile to (703) 767-8747.
5.5.3 After bunkering. Validate quantity issued by the supplier and compare vessel receipt figures
against supplier issue figures to confirm that any quantity difference is within acceptable tolerances. If
manual gauges are used, the vessel has the option of witnessing the after delivery gauges. In order to
prevent fraud, witness the after delivery bunker barge water and product gauges from every tank gauged
before bunkering commenced. Maintain a record of the before and after bunker barge gauge readings.
As deliveries are net volume or by weight, assure a temperature is taken from each cargo and slop tank.
Assure all tanks that were not intended for delivery have not received or issued any product, water or
slops during the delivery. For vessels participating in a bunker testing program, follow the instructions in
the kit on preparing and dividing the sample into aliquots for shipment to the testing facility and retain
samples. Normally one aliquot will be sent to the laboratory, one signed for by the supplier and one
retained on the vessel. If the bunker supplier will not accept the sample, annotate in the vessels log that
MIL-STD-3004C
47

the sample was refused and retain the contractors sample also. Retains can be put back into a bunker
tank after quality results are received and indicate the product conforms to specification requirements.
When non-conforming product is indicated, notify the contracting officer providing full documentation
on the receipt and the vessels desired action for disposition of the non-conforming product.
5.5.4 Bunker Delivery Note and Statutory Sample. MARPOL 73/78, Annex VI, Regulation 14 and
Regulation 18, requires that a Bunker Delivery Note (BDN) and a representative sample of the delivery
be presented to the vessel receiving the bunkers by the supplier. Active duty Navy vessels that have
taken the military exemption to these regulations will not accept the samples. MSC will accept samples
from both commercial and DLA Energy suppliers. Copy of the BDN to be issued to MSC Vessels.
5.6 Receipts from the into-plane program. DLA-ENERGY contracts are established to service
DoD/Federal Civilian aircraft at commercial airports throughout the world. Product is supplied directly
to the customer and can be either commercial (Jet A/A-1) or Military (JP-8). Additives such as FSII are
provided as per location requirements. Procedures for into-plane servicing are covered under MIL-STD-
1548. Problems under Into-Plane contracts shall be reported to the DLA-ENERGY contracting officer
(DLA-ENERGY/PHC, 703-767-8469/540-288-3030; FAX: 703-767-8506). Problems of a quality nature
shall also be reported directly to DLA-ENERGY-QA (703-767-8736/562-256-2509; FAX: 703-767-
8747).
5.6.1 AIR Card. The AIR Card is used to obtain fuel at commercial locations. It identifies the
airplane for billing purposes. Use of the AIR Card does not guarantee fuel quality at locations and
contractors not contracted to DLA-ENERGY under the Into-Plane Program.
5.6.2 Refueling units. When refueling units containing turbine fuel are converted to JP-8, JP-5 or
commercial jet fuel service, refer to Table XXVI of this Standard for appropriate guidance. When the
type of turbine fuel to be serviced is different from the type in the aircraft tanks, the fuel shall be serviced
at half the normal delivery rate to minimize hazards of static electricity. Kerosene fuel such as Jet A, Jet
A-1, JP-8, JP-5, and TS-1 are classified as the same type. A different type would be wide-cut fuel, such
as JP-4 or Jet B. Supplies of aviation fuel for use in Secured Fuels are sealed and secured in accordance
with AFI 31-101, Volume I.
5.7 Receipts of aviation Secured Fuels and support aircraft. Secured fuel is used on any aircraft on
which the President of the United States is a passenger. The below procedures apply only to secured
fuels. Support aircraft shall be serviced the same as any other transient aircraft. JP-8 is the primary fuel
for use in these aircraft. If JP-8 is not available, alternate fuels (commercial Jet A-1, commercial Jet A or
JP-5, and TS-1) may be used. In Table XIII, Support for Secured Fuels, Commercial Jet A-1 includes
fuels identified by other National Specifications like the Russian GOST specification TS-1 and Chinese
specification No. 3 Jet Fuel. Whenever Secured Fuels are used, tests listed in Table XIII shall be
conducted on representative samples taken downstream of the final filtration from refueling units or
hydrant servicing equipment prior to issuing fuel. The sample location will be under normal operating
pressure and continuous flow.
5.7.1 Refueling on military installations. The Secured Fuels Advance Team will contact the Base
Fuels Officer and the Air Force Service Control Point to coordinate fuel support and testing. Those tests,
within the capability of the base laboratory, shall be performed on base. Testing beyond the capability of
the base laboratory shall be performed at the area laboratory. If time does not permit testing at the area
laboratory, the Service Control Point will contact the appropriate DLA-Energy Region Quality Manager
for guidance in contacting a local laboratory for testing on a service contract basis. Information on
MIL-STD-3004C
48

laboratories under contract for testing services can be found on the DLA-ENERGY Web page at
http://www.desc.dla.mil/DCM/DCMPage.asp?pageid=39 and click on the Contracts List.
5.7.2 Refueling at other locations. The Secured Fuels Advance Team will contact the appropriate
DLA-Energy Region Quality Manager for fuel support and testing. The Region Quality Manager will
assign a Quality Assurance Representative (QAR), who will, in conjunction with the Secured Fuels
Advance Team, locate a fuel source and make necessary arrangements for sampling and testing. The
QAR will contact the Secured Fuels Advance Team with test results in the most expedient manner.
5.7.3 Invoice/acquisition procedures.
5.7.3.1 Contractual Laboratory Invoice procedures. For testing done at contract locations, a DLA-Energy
QAR will validate invoices and submit invoices for payment per laboratory contractual requirements.
5.7.3.2 Non-contract locations. The DLA Energy QAR will validate the certificates of analyses with the
statement, These services were performed and validated and include the QARs signature and date.
The certificates of analysis, invoices and W-9, Request for Taxpayer identification Number and
Certification (applicable to U.S. Companies only) will go to DLA-ENERGY-Quality Operations Division
who will in turn submit to DFAS-CO for payment. DLA-ENERGY-Quality Operations Division will
track the expenditures for Secured Fuels laboratory testing. Send invoices to the Defense Logistics
Agency Energy, ATTN: (Laboratory Program Manager), DLA-ENERGY-QUALITY OPERATIONS,
RM 2843, 8725 John J. Kingman Rd., Fort Belvoir, VA 22060-6222.
5.8 Receipt of approved additives and injection. Fuel is usually delivered to base level fully
additized. This requires product to have additives injected either at the refinery, GOCO or COCO
terminals, before shipment or en-route, such as when product is injected by commercial pipelines just
prior to delivery. Finally, product can be injected at the base level, either upon receipt or during a
transfer within the facility. In most cases the product to be injected is jet fuel, being injected with FSII,
CI/LI, or SDA. The +100 additive is normally injected as part of the base operation into a dedicated
refueler. Injection equipment is usually permanently installed, with injectors tapped into the
receiving/transfer line, and supplied by a bulk additive tank. Responsible base personnel shall assure
injection equipment is in working order and that the rate of injection of the additive into the product is
correct.
5.8.1 Receipt of approved bulk additives. Bulk additives are stored in smaller storage tanks (e.g.:
1,000 - 5,000 USG). Additives are delivered by truck (also inter-modal containers for OCONUS)
directly from the producer. Upon arrival by truck or inter-modal container, paperwork shall be examined
by receiving personnel to assure the proper additive is being received. Because of safety consideration,
sampling of additives such as FSII shall be done with safety equipment and the knowledge of the
Material Safety Data Sheet (MSDS). Because of cleanliness considerations, additive sampling
equipment shall not be used to sample other products. Arriving trucks shall be examined to determine if
seals are intact. Truck pumps and hoses shall be clean and capped. Product tank compartments shall be
sampled and tested for workmanship and density to determine if any contamination has occurred. The
density of additives must be determined in accordance with product specification. Once accomplished,
product may be discharged into the proper storage tank. If unable to take an all-level sample from the
truck compartment prior to discharge, then an in-line sample taken during discharge may be used for
testing.

MIL-STD-3004C
49

5.8.1.1 Receipt of turbine fuel approved packaged additives. Packaged additives should be inspected
upon arrival for correct identification, content, packaging and damage. Containers should be in good
condition upon arrival, and proper paper work should be supplied by the vendor. Packaged additives
should be stored under cover, preferably in warehouses or open sheds. In the situation where storage
must be outside, containers must be off the ground on pallets or dunnage and covered with tarpaulins for
protection from the elements. Additives that are in drums should be stored on their sides with proper
bracing and blocking if necessary. Bungs should be in horizontal position so leaks may be detected.
Drums should never be stored in a vertical position outdoors as water will collect on the drum heads, and
could seep through bungs. The proper packaging, storage, and stock rotation (in which the oldest material
is issued first) will help to minimize losses due to deterioration.
5.8.2 During injection. To assure the correct additive concentration, personnel shall monitor the
quantity of additives expended and compare it to the target concentration and to the quantity of product
injected. This can be done by comparing the difference in ullage of the additive tank to the quantity of
product injected at regular intervals. Even when monitoring equipment exists that provides the injection
rate, a manual check shall be accomplished to assure proper injection rate. This can be accomplished
weekly, monthly, etc. depending on the amount of injection being performed and the accuracy of the
manual checks. To ease injection calibration accuracy, it is beneficial to premix product with additive
prior to injecting into lines, storage tanks, and conveyances.
5.8.3 After injection. Product that has been injected shall be sampled and tested once
receipt/transfer has been completed. Personnel shall consider outside temperatures, especially for
additives such as SDA. Lower temperatures tend to lower SDA readings and higher temperatures tend to
raise the readings.
5.9 Bulk storage. Quality surveillance of bulk products shall begin upon receipt and continue as
long as the product is in physical possession of the storage facility. Table IX is referenced for minimum
sampling and testing for normal turnaround products and Table VIII outlines frequencies for the testing
of products in a static long term storage (see 5.9.1). Sediment and water are the most common types of
contaminants found in storage and dispensing systems. Their presence can cause serious problems in the
systems, particularly in the operation of aircraft. Positive action shall be taken to prevent and eliminate
their occurrence.
5.9.1 Long-term storage. A product will be considered under dormant conditions (long term
storage) when either the product has remained in storage for a period as indicated in Table VIII without a
turnover of at least two-thirds of the tank content or if new product has not been received into existing
stocks for 6 months. Product stored in collapsible containers shall be tested every month as a minimum.
When new tanks are put into service and product added (recommended one (1) meter to the new tank),
then B-1 testing is to be conducted. Product shall then be monitored for deterioration by requiring B-2
testing to check product stability. This frequency can be maintained as long as deterioration is not
detected. However, when deterioration does begin (e.g. in gasolines when the oxidation stability
decreases or gum level increases; in diesel fuel when the particulate contamination increases), the
frequency of testing shall be increased, such as from six months to four months. As the deteriorating
characteristics approach intra-Governmental receipt limits (see Tables I-VII), product shall either be
consumed on an expedited basis, or rotated so that it can be consumed elsewhere before exceeding the
intra-Governmental receipt limits. The rate of deterioration cannot be predicted as storage locations
throughout the world differ in temperature and environment, and the products stored are produced
differently from refinery to refinery. Therefore, each product in long-term storage shall be regularly
sampled and tested with an increase in testing frequency when deterioration begins.
MIL-STD-3004C
50

5.9.2 Bulk tank water restriction. The use of fuel tanks with water bottoms is prohibited unless
specifically authorized by the appropriate technical authority. Bulk fuel tanks shall be drained of water
after each product receipt, a minimum of weekly thereafter and prior to each issue. Floating roof tanks
shall be checked more frequently during periods of heavy rain or melting snow. Underground fuel tanks
shall be checked more frequently when the water table is high and during periods of excessive rain or
melting snow.
5.9.2.1 Corrosives in tanks. In instances where water bottoms in storage tanks cannot be
completely removed the water layer shall be checked monthly for the presence of hydrogen sulfide.
Hydrogen sulfide, that sometimes forms as a result of bacterial action on sulfates present in the water (see
Test Method 1020 in this Standard), is corrosive and will cause the product to fail the copper strip
corrosion requirement of the specification.
5.9.2.2 Tank water check frequency. Water checks shall be made daily on issue tanks and weekly
on static tanks or each time a tank is gauged, whichever occurs first. When water is found it shall be
drained as soon as possible.
5.9.2.3 Microbial Contamination. Microbes can exist in extremely small pockets of water. This
growth can be corrosive creating pinpoint holes in metal. Microbial growth cycles can result in
contamination that clogs filter. A good water removal program is an important maintenance function.
5.9.3 Storage tanks and piping.
5.9.3.1 Storage of similar products. Storage tanks should continue in one type fuel to the extent
practicable. The contents of receiving storage tanks shall always be identified before the receipt of fresh
product.
5.9.3.2 Changing product in a storage tank.
a. When storage tanks are changed from one type of fuel to another, tanks shall be inspected,
cleaned if required and re-inspected to ensure elimination of excessive rust or sludge. See STANAG-
3609 and applicable contract clauses for guidance on this subject.
b. When conversion to E85, tanks selected will be inspected, cleaned, and certified for compatibility
and use of E85 by the MAJCOM Fuels Engineer.
1. Initial Fill Procedures (All Tanks) - fill the tank with E85 that has been tested. For the initial fill
allow 48 hours settling time.
2. Displace twice the volume of the dispensing line prior to obtaining a sample. Collect sample
into a wide mouth container and visually inspect for particulates, water, and phase separation.
3. Should the sample fail the visual examination, flush the dispensing line until samples are clear
and free of visible particles.
4. Test for ethanol content according to ASTM D5798.
c. Ground diesels may switch between summer and winter grades for cloud and pour point purposes.
These changes do not require cleaning/inspection between grade changes. In order to promote the
swiftest conversion during summer when converting to winter grade, the storage tank shall be brought as
low as possible before the conversion begins. Product should not be purchased during a summer grade
period for storage when the use of the product is primarily for winter use. Careful planning and ordering
procedures must be developed to assure the storage tank will be prepared for the winter use season.
MIL-STD-3004C
51

1. Conversion from low to ultra low sulfur diesel/ B20 will require the removal of all existing
diesel fuel from the tank to the maximum extent possible. Empty tank with service pump to
remove remaining product, clean tank. Install a 10 micron maximum filter on pumps.
2. After the initial B20 receipt, dispense at least twice the piping fill quantity through the pump
to purge the system.
d. Conversion to Ultra-Low Sulfur Diesel (ULSD) Tank. The U.S. Environmental Protection
Agency has mandated that diesel fuels shall contain no more than 15 ppm by mass sulfur. Many diesel
vehicles built after 2007 will contain emission control devices that will be deactivated by higher levels of
sulfur. These devices when overwhelmed with sulfur will result in the vehicle shutdown. It is very
important that fuel storage tanks be properly converted into ULSD service. The policy for converting a
storage tank(s) to ULSD is found at http://www.desc.dla.mil/DCM/DCMPage.asp?PageID=479 under the
DLA-ENERGY Policy Document Number DLA-ENERGY-I-15, Conversion of Low Sulfur Diesel
Storage to Ultra Low Sulfur Diesel (ULSD).
5.9.3.3 Product cargo check for quality. To the extent practical, product shall be discharged into a
single, low-innage shore tank. After discharging and checking for quality, identical products may be
combined in common tankage. Gasoline storage tanks shall be kept as full as possible to minimize
evaporation losses. These losses are excessive in partially filled cone roof tanks during extended storage.
5.9.3.4 Segregation of product. Grades of product shall be segregated from one another and
whenever feasible all issues made through a segregated system. Segregation of different grades and
products shall be by some positive means such as a blank flange, spectacle plate, spool piece, double
valve with open drain, or double block-and-bleed valve. Segregation by a single valve is not sufficient.
5.9.3.5 Leaking valve contamination. To minimize the danger of contamination from leaking
valves, one of the following precautions is recommended:
a. Use of blank flanges between valves.
b. Removal of a section of pipe between two valves.
c. Introduction of a bleeder valve (normally open) between two valves. A catch basin (drip pan)
shall be placed under the bleeder valve and monitored on an established schedule to detect leaks. Failure
to perform this inspection may result in liquid overflowing the catch basin creating an environmentally
unsafe condition.
5.9.3.6 Tank protective treatment. Before an internal protective treatment is applied to any tankage
(e.g. coating), approval from the responsible DLA-ENERGY or service technical authority is required.
5.9.3.7 Identification of piping system
5
5.9.3.8 Fuel settling time in tank. Settling time is required for determination of quantity
measurement for official receipt quantities, sampling for tank certification after receipt or permitting the
tanks issue.
. Piping systems shall be marked to clearly identify the
grade of a product being carried. These markings shall be placed adjacent to all operating accessories
such as valves, pumps, regulators and manifolds. MIL-STD-161 provides guidance on color markings
and titles. In NATO countries the NATO code numbers for the product grade shall be included in the
marking or identification system.

5
NOTE: In certain situations security requirements may dictate what markings are not allowed.
MIL-STD-3004C
52

a. For quantity measurements in tanks greater than 2,000 barrels, a settling time of thirty minutes
minimum is required for products that have little to no water (anticipated water level in the tank is less
than or equal to one-eighth of an inch). For tanks less than 2,000 barrels allow a minimum settling time
of five minutes. For products that retain water and/or sediment (e.g. crude, IFOs, etc), allow a minimum
of twenty-four hours of settling in bulk storage tanks before taking a custody transfer measurement upon
receipt. Take a provisional gauge after a minimum of thirty minutes of settling noting it as a preliminary
gauge for receipt purposes.
b. For sampling and issuing functions, the following settling times and issues apply. After fuel
stocks have been added, allow maximum possible settling times in order to permit reasonable settlement
of waters and solids. For aviation fuel a minimum tank settling period of 8 hours prior to issue or transfer
is required for tanks greater than 2,000 barrels. For tanks 2,000 barrels, or less, a settling time of thirty
minutes minimum is required. Observe a longer settling period if mission requirements allow. Prior to
issue or transfer following the settling period, drain the tank water removal systems.
c. For ground fuel tanks greater than 2000 barrels minimum settling time is one hour per foot of
product received. For ground fuel tanks 2000 barrels, or less, a minimum of 30 minutes settling time is
required. Observe a longer settling time if mission requirements allow. This settling period is not
necessary when fuel handling system cleanliness has been assured by design to eliminate the ingestion or
generation of corrosion products or contaminants and when transfers to the system are made through a
properly monitored filter apparatus.
d. The settling period does not apply to bulk storage aboard ships. A settling period of thirty
minutes aboard ships is recommended for static dispersing.
5.9.4
a. In filling any empty tank, the initial fuel flow rate shall not exceed three feet (one meter) per
second through a receiving line until the roof of a floating-roof tank is afloat, or a minimum of three feet
/one meter above the level of the tank filling line is reached (see 5.1.1.7.2).
Control of static electricity (aviation turbine fuels, kerosene). The following are certain
hazards and precautions emphasized in the handling of aviation turbine fuel:
b. Agitation of the fuel surface and air, and entrainment of air and water in fuel shall be avoided.
c. The fuel stream into storage tanks shall be horizontal rather than toward the bottom of the tank.
d. NFPA 77 states that removal of outer garments is particularly dangerous in work areas where
there may be flammable or explosive atmospheres that are ignitable with low electrical energy. Because
some materials exhibit static phenomena, especially under low humidity conditions, the outer garments
used in these areas shall be suitable for the work area. Recommend that outer garments not be donned or
removed where a flammable or explosive atmosphere may exist.
e. The sampling device shall always be bonded to the tank before the sampling hatch is opened.
f. Personnel shall wait a minimum of thirty (30) minutes after receipts of any type of fuel to allow
electrostatic charges to dissipate before gauging or sampling. (See 5.9.3.8 for exceptions for small tanks).
g. Other ignition sources of concern are the cell phone and other portable electronic devices (PED).
Cell phones or other PEDs should not be used in and around areas where flammable vapors are a risk,
unless they have been tested, approved and labeled as intrinsically safe. If at all possible the use of cell
phones and other PEDs should be avoided while working in areas exposed to flammable vapors.
MIL-STD-3004C
53

5.9.5 Filtration
6
5.9.6 Internal preservation. If any fuel equipment or facility is likely to be out of service for four
months or more, then pumps, fans, motors, etc. shall be given adequate protection either in place, or by
transfer or storage. Tanks shall be isolated, cleaned, dried and sealed. Water-displacing fluids shall not
be used for the internal protection of aviation fuel tanks, as they are difficult to remove completely and
they affect the water reaction property of the fuel. However, such fluids may be used as directed for
tanks used for other products.
. Filtration equipment of a proper type shall be a part of some fuel handling
systems (see Table XXXI). The equipment shall be inspected for condition and performance capability
in accordance with applicable standards (i.e. MIL-PRF-52308, EI Specification 1581, etc.) or the
equipments operations and maintenance manuals. Micronic filtration equipment conforms to EI
Specification 1590. The location of this equipment is to be in accordance with civil engineering design
criteria. In commercial installations the requirements for any maintenance of this equipment are to be
consistent with the terms of the contract. Because filter-separators generate static electricity their
location in the system shall permit a 30-second relaxation time in product travel between the filtration
equipment and receiving containers. The 30-second relaxation time applies only to systems designed for
fuel without SDA. Systems designed to deliver fuel with 50 pS/m or greater concentration of SDA need
not comply with the 30-second relaxation time.
5.9.7 Dispensing from curbside pumps. The provision for bulk storage tanks are applicable except
for conditions outlined in 5.9.2.1.
5.9.8 Deterioration of a product. Characteristics of petroleum products change as the product ages
and storage conditions may accelerate the change. The degree of deterioration can be determined only by
laboratory testing, which shall be accomplished periodically as set forth in Table IX.
5.9.9 Sources of contamination.
5.9.9.1 Inadvertent mixtures. The principle sources of bulk product contamination are: failure to
properly identify product in receiving vehicle to proper receipt tank, carelessness in making line
connections; error in valve operation during transfer of bulk products; use of contaminated tanks;
incomplete cleaning or flushing of product lines; leakage between compartments of a tanker or through
partially closed or defective valves. Consequently, every precaution shall be exercised to prevent the
inadvertent mixing of different grades of product as well as contaminating the product with foreign
materials like water and sediment. Mixture of products can often be detected by changes in appearance,
color, gravity, or odor. Laboratory analysis will detect mixtures when not visually detectable. See 5.11
and 5.12 for sources of contamination.
5.9.9.2
5.9.9.3 Rubber surface to fuel. Refers to characteristics of elastomeric or rubber compounds that
change during exposure to fuel. Seal swelling, an interaction between the fuel media and elastomer
materials, is desirable (to a point) as a means to prevent leakage.
Handling personnel. Contamination may also result from accident, inability or failure to
follow prescribed procedures, carelessness, or sabotage. Proper identification and strict control of the
entire handling and dispensing system shall be maintained to minimize contamination at bulk storage
terminal and user activities.

6
Note: "The DLA Energy will provide direct funding and/or reimbursement for filter elements, coalescer cartridges, and pre-filter elements at Defense Fuel
Support Points (DFSPs) and facilities that manage Defense Working Capital Fund (DWCF) bulk petroleum products."
MIL-STD-3004C
54

5.9.9.4 Container sealant. Fuel containers with bullet hole sealing properties may be particularly
hazardous if the fuel should penetrate to the sealing media. Long hose lines shall not be kept full of
product. The initial throughput of a hose system equal to the volume of the hose shall be checked for
excessive contamination. Extra precautions shall be taken to clean the system or containers if it has been
used to store or transport diesel fuel or other lightly inhibited material, such as commercial motor
gasolines.
5.9.10 Identification of transfers. Identification shall be made on all product transfers. Testing shall
be conducted on all product transfers except for transfers of approved stocks from fully segregated
systems (pipeline, tank car or truck) and provided that a grade change is not involved. Details of
sampling and testing requirements are shown in Table IX.
5.10 Product Intra - Governmental receipt limits (Tables I-VII).
5.10.1
5.10.1.1 Knock rating. The knock value for ratings of 100 or below is stated in terms of octane
number and in terms of performance numbers for those above 100.
Gasoline, aviation, NATO F-18 (ASTM D 910/100 LL) and Unleaded Aviation Gasoline
ASTM D7547.
5.10.1.2 Color. Aviation gasoline may change color for such reason as mixing with gasolines of
another color, contamination, or prolonged exposure to light. A visible cloudy or hazy appearance may
accompany the color change. This indicates the presence of suspended water, precipitated lead salts, or
other particulate matter. A definite yellow case or darkening of color may be caused by the presence of
lubricating oil, diesel fuel, heating oil, or other petroleum products of similar nature. Off-color gasoline
shall not be used until analysis is performed to determine product usage.
a. Color standards prepared in 4-ounce bottles from fresh, uncontaminated stocks and compared
with the questionable gasoline may provide initial information regarding contamination.
b. Confirmation of contamination shall be obtained from the results of other tests. The type of
testing to be performed would depend on the type of contamination suspected, e.g.: commingling,
cleanliness, water and sediment.
5.10.1.3 Vapor pressure (VP). Vapor pressures can be tested using various methods. A common test
is called the Reid Vapor Pressure (RVP) test measuring the vapor pressure created in a defined volume of
air to volume of fuel at 100 F.
a. A VP above 7.0 psi (49 kPa) indicates contamination by a more volatile product. Additional tests
and complete investigation of the previous history of the gasoline may identify the contaminating agent.
A possible cause of such contamination could be commingling with automotive gasolines which
generally have higher VPs.
b. A VP below 5.5 psi (38.5 kPa) may indicate weathering (loss of volatile fractions) or
commingling with other products having a lower VP. Disposition of a weathered gasoline shall be made
on the basis of other pertinent tests such as distillation range, knock rating, gum and lead content.
5.10.1.4 Corrosion. A gasoline having a copper strip rating of ASTM 2a or greater is corrosive.
This may be caused by the presence of other petroleum products or by corrosive materials having been
extracted from sulfur-impregnated rust present in transport or storage systems or sulfate reducing
bacteria.
MIL-STD-3004C
55

5.10.1.5
5.10.2 Aviation turbine fuel, NATO F-34/JP-8 (MIL-DTL-83133), F-35/Jet A-1, Jet A (ASTM
D1655) and F-40/JP-4, F-44/JP-5 (MIL-DTL-5624)
Water and sediment. These characteristics shall be controlled within the transportation,
storage, handling and servicing systems in order to avoid serious problems in the operation of aircraft and
resultant degradation of the supply readiness position.
7
5.10.2.1 Existent gum. The existent gum shall not exceed 7.0 mg per 100 ml of fuel and shall be dry
in appearance. The preferred vaporizing medium for aviation turbine fuel is steam, however, the existent
gum test (ASTM D 381) may be performed using air as the vaporizing medium at the following operating
temperatures: Bath: 232-246 C; Test well: 229-235 C. However, it must be noted that specification and
contract requirements shall be followed as product and product characteristics may change.
and TS-1(GOST 10227-86).
5.10.2.2 Vapor pressure. In requesting disposition for JP-4 which does not meet the VP intra-
Governmental receipt limits (see Table I), the recommended alternate use or disposition shall take into
consideration the results of other tests such as the distillation range, existent gum and freezing point.
5.10.2.3 Corrosion. An aviation turbine fuel which has a copper strip corrosion rating of 2a or
greater will not be used in aircraft. The fuel shall be segregated and handled in accordance with
instructions in 5.13.
5.10.2.4 Fuel system icing inhibitor (FSII). One type of FSII is approved for inhibiting ice formation
in turbine fuels. Diethylene glycol monomethyl ether (DIEGME) with a flash point of 85 C (185 F) has
been identified as the type FSII to be purchased for all jet fuels. FSII lowers the freeze point of entrained
or free water present in turbine fuels or in fuel systems. The amount of FSII added to turbine fuels in the
wholesale system shall be adjusted to ensure delivery of the fuel with a minimum FSII content of 0.10
vol %, for all grades of turbine fuels. FSII does not readily dissolve into the fuel so it must be dispersed
as fine droplets. A proportional-flow injection system is recommended with shearing devices such as
meters or mixers downstream of the injector. FSII will not fully disperse in wet fuel (fuel containing
free water) even with proper additive injection equipment. In fuel containing free water, the FSII will
preferentially solubilize in the water resulting in a lower than expected concentration of FSII in the fuel
and water bottoms containing high FSII concentrations. It is recommended a filter-separator system be
installed upstream of the FSII injection point if the free water content cannot be maintained below 30
ppm by volume during the injection process. The FSII content of turbine fuels shall be verified when a
storage tank is designated as an issue tank or when delivery into the bulk tank. Fuel stored in floating
roof issue tanks shall be checked for FSII content after each heavy rain. Underground storage tanks shall
be checked during periods of heavy rain, melting snow and other periods of high water tables. It should
not be allowed to remain in tank bottoms or filter-separator sumps. In FSII treated fuel, the water at tank
bottoms and sumps should be carefully drained daily or more frequently if warranted. It is also important
to prevent water and moist air from entering the FSII additive tanks because the water dissolves rapidly
into the additive. FSII that contains an excessive amount of water will not readily disperse into the fuel
and can settle in the aircraft fuel tank causing corrosion and deterioration of the tank lining materials.
Therefore, a desiccator or other drying mechanism shall be used in the air vent to prevent entrance of
moist air into the FSII storage tank. FSII, either by itself or mixed with water, can be corrosive to epoxy
linings or aluminum vessels under certain conditions. Because of its corrosive nature FSII should be
stored in stainless steel or Teflon coated tanks. Since laboratory testing has shown long-term stability of
FSII is questionable even if stored in stainless steel containers, it is recommended FSII stocks be rotated

7
NOTE: See T.O. 42B1-1-16, Chapter 6, for JPTS (MIL-DTL-25524) test limits.
MIL-STD-3004C
56

as frequently as possible, FSII should be checked one month after delivery. Bulk FSII stocks should be
fully retested for quality conformance every 12 months as a minimum. Warning: FSII has been
determined to be a health hazard. Therefore, special precautions shall be taken to avoid exposure when
handling glycols (for example, while sampling and testing). Refer to the manufacturers MSDS for
safety precautions.
5.10.2.5 Flash point specification. JP-5, JP-8, Jet A and Jet A-1 fuel exposed to systems which have
recently contained gasoline/naphtha or which have been contaminated by the same is likely to be
rendered off-specification for flash point. This is critical non-compliance for JP-5 because of the safety
factors involved in handling fuel aboard vessels at sea. For JP-8, Jet A and Jet A-1 the flash point non-
compliance is a ground handling safety issue. The extent of the severity for aviation turbine fuels used at
land-based locations is based on the degree of flash deterioration.
5.10.2.6
5.10.2.7 Water and sediment. These characteristics shall be controlled within the transportation,
storage, handling and servicing systems in order to avoid serious problems in the operation of aircraft and
resultant degradation of the mission readiness position.
Filtration time. Control of this property is essential to prevent rapid differential pressure
buildup in filtration equipment and possible migration of finely divided solids into aircraft. Degradation
of filterability may occur in transportation and storage systems and is particularly prevalent when fuel is
exposed to saltwater and metallic contaminants.
5.10.2.8 Conductivity. Conductivity is a measure of its electrical conductance in fuels. By
increasing conductance of the fuel, rapid dissipation of an electrostatic charge can be accomplished.
Except for direct deliveries to a using activity from a refiner, the static dissipater additive (conductivity
additive) most likely will be injected in the JP-4 or JP-8 at the terminal making delivery to the using
activity. The conductivity unit (CU) specification requirement for JP-4 and JP-8 is 150-600 picosiemens/
meter (pS/m). For JP-8 with the thermal stability improver additive (JP-8+100) the CU limit is 150-700
pS/m. The CU limit for Jet A-1 is 50-600 pS/m. Readings of CUs shall be taken at ambient temperature
or 29 C (85 F), whichever is lower. If the sample is tested in a laboratory, results shall be corrected to
the ambient temperature of the tank in accordance with ASTM D 2624.
5.10.2.9
5.10.2.10 Fuel Standardization Policy. The fuel standardization policy (also known as the Single
Fuel Policy) mandates the use of a kerosene base fuel as the single fuel on the battlefield, for both aircraft
and ground vehicles/equipment. DoDM 4140.25-M states this policy in great detail. In most cases, this
fuel is JP-8. Primary fuel support for sea-based aircraft shall be a high flash kerosene-based fuel, JP-5.
In overseas theaters where the predominant fuel is in support of the Navy, JP-5 may be substituted for JP-
8, as approved by the Combatant Commander, JP-8 and JP-5 have been tested in all types of tactical
vehicles and equipment and can be used interchangeably in most cases with diesel fuel. JP-8 when used
in tactical equipment is currently exempt from the sulfur limits required by the EPA when used in ground
vehicle equipment for on-grade use in the United States DoD.
Thermal Stability of JP-5. Most Navy/MSC ships have copper-nickel piping which results
in copper leaching into JP-5 that causes oxidation stability testing failures by ASTM D3241. This fuel
due to failure of oxidative stability testing is not suitable to be returned to DLA-ENERGY-owned bulk
JP-5 stock ashore. Naval Air System Command (NAVAIR) has determined that this product can be
burned at sea by shipboard aircraft. Ships carrying JP-5 with non-conforming MIL-DTL-5624 thermal
stability results due to copper contamination (no other known cause) may transfer that JP-5 to other ships
for use at sea without DLA-ENERGYs disposition.
MIL-STD-3004C
57

5.10.2.11 Other Aviation Fuel Specifications. Use of Other Aviation Fuel Specifications DLA-
ENERGY may obtain aviation turbine fuel conforming to the National specification of another country, if
DoD primary fuels (JP-8, JP-5) are not available. All alternate fuel approvals must be processed through
the Service Control Points.
5.10.3 Gasoline, automotive, unleaded (F-67).
5.10.3.1 Octane. Gasolines having an octane or performance number below the intra-Governmental
receipt limits, specified in Table VI shall be re-sampled and the knock rating verified before considering
it below the intra-Governmental receipt limits.
5.10.3.2 Color. F-67 gasolines are normally clear and bright but may undergo a color change due to
mixing with dyed fuels (aviation gasolines, certain commercial leaded gasolines, or high sulfur diesel
fuels). A cloudy or hazy appearance that may accompany the color change is usually caused by
suspended water or precipitated lead salts or other particulates. A yellow cast may be caused by
contamination with diesel fuel, lubricating oil, or other petroleum products.
5.10.3.3 Existent gum. Existent gum shall not exceed 7.0 mg/100 mL of gasoline (F-67).
5.10.3.4 Lead content. The maximum amount of lead permitted, by STANAG 7090, Guide
Specification for NATO Ground Fuels, is 0.013 g/L for unleaded gasolines (F-67). Lead content in
gasoline may be restricted to a lower limit by local regulation. Lead content be determined by ASTM
D3341 or ASTM D5059 (Test Method C).
5.10.3.5 Copper Strip Corrosion. Gasoline with a corrosion rating of ASTM 2a or greater shall be
segregated and reported as prescribed in 5.13.
5.10.3.6 Vapor Pressure (VP). Vapor pressures are determined by class as well as geographic and
climatic conditions. They may also be regulated by national authorities. The following intra-
Governmental receipt limits are for guidance only:
a. Class 1. Minimum 33 kPa; maximum 72 kPa.
b. Class 2. Minimum 43 kPa; maximum 82 kPa.
c. Class 3. Minimum 53 kPa; maximum 92 kPa.
d. Class 4. Minimum 58 kPa; maximum 97 kPa.
e. Class 5. Minimum 68 kPa; maximum 107 kPa.
5.10.4 Automotive spark ignition engine fuel: commercial gasoline (ASTM D 4814) and gasohol,
automotive, unleaded (A-A-52530). Under authority of the Clean Air Act, gasolines marketed in the
United States, territories and possessions may have restrictions on vapor pressure limits and have
mandates for the use of gasoline-oxygenate blends for the purpose of controlling emission. An oxygen-
ate is a hydrocarbon that contains an oxygen atom embedded in a chain of hydrogen and carbon atoms.
Oxygenates are usually alcohols or alcohol-derived ethers and are added to gasolines to increase its
oxygen content. The increased oxygen content results in a cleaner, more efficient fuel. The restrictions
vary by region and time of year. Oxygenated Gasoline is sold in designated areas during the winter
months when the carbon monoxide problem is the most serious. Reformulated Gasoline is an oxygenated
fuel sold in designated areas year round to control emission. Reformulated Gasoline differs from
Oxygenated Gasoline in the amount of oxygenate (2.0% by mass compared to 2.7%). Some states,
notably California, may have more restrictive regulations. Fuels using ethanol (ethyl alcohol) as the
oxygenate are exempt from EPA mandated vapor pressure limits. Many States now require a blend of 10
MIL-STD-3004C
58

vol % ethanol to either meet the oxygenate requirements or to fulfill a requirement to reduce consumption
of petroleum based fuels. Therefore the fuel may be designated as gasoline, not gasohol, and still contain
10 vol % ethanol. The States that do not require ethanol in their gasolines still refer to the 10 vol % blend
as gasohol. This is on a State-by-State basis.
5.10.4.1 Octane. Gasolines having an octane or performance number below the intra-Governmental
receipt limits, specified in Table VII, shall be re-sampled and the knock rating verified before considering
it below the intra-Governmental receipt limits.
5.10.4.2 Existent gum. Existent gum shall not exceed 6.0 mg/100 ml of gasoline. Values for
gasohol are based on those of the base gasoline. Commercial gasoline may contain detergent and
multifunctional additives designed to maintain engine fuel system cleanliness. These additives can
contribute to high unwashed gum levels. Generally, the values will be reduced to acceptable levels by
the heptane wash.
5.10.4.3 Lead content. The maximum amount of lead permitted in the U. S. by the Clean Air Act is
0.013 grams /L for unleaded gasoline. Gasohol is considered an unleaded gasoline. Gasoline containing
more than the prescribed lead content may be blended with gasoline of a lower lead content so the
resultant blend conforms to the requirements. Lead content shall be determined by ASTM D 5059.
5.10.4.4 Copper Strip Corrosion. Gasoline with a corrosion rating of ASTM 2a or greater shall be
segregated and reported as prescribed in 5.13.
5.10.4.5 Vapor pressure. Values for gasohol are based on those of the base gasoline. Blending to
meet the VP limit is permissible provided the resultant blend meets all specifications and inter-
Governmental receipt limits.
a. Class AA is for use in ozone non-attainment areas within the U.S. as defined by the EPA. The
intra-Governmental receipt limit for VP is 57 kPa (8.3 psi) maximum.
b. Class A is for use at temperatures of 43 C (109 F) and above. The intra-Governmental receipt
limit for VP is 65 kPa (9.4 psi), maximum.
c. Class B is for use at temperatures between 36 C (97 F) and 43 C (109 F). The intra-
Governmental receipt limit for VP is 72 kPa (10.4 psi), maximum.
d. Class C is for use at temperature between 29 C (84 F) and 36 C (97 F). The intra-
e. Class D is for use at temperatures between 21 C (70 F) and 29 C (84 F). The intra-
f. Class E is for use at temperatures below 20 C (68 F). The intra-Governmental receipt limit for
VP is 107 kPa (15.5 psi), maximum.
5.10.4.6 Alcohol content. Total ethanol content in gasohol shall not exceed 11 vol % as determined
by ASTM D4815.
5.10.4.7 Water tolerance. Gasohol shall not separate into two phases with the addition of water up to
0.1% by volume at various temperatures based upon class of fuel. Test Method is in ASTM D4814.
5.10.5 E85. This liquid fuel is handled in a manner similar to that of gasoline, the chemical
properties of alcohol are different than those of gasoline and must be recognized when establishing a fuel
handling standard. To reduce the chance for failure or contamination of alcohol equipment and systems,
MIL-STD-3004C
59

select proper materials and control composition. Ethanol is not compatible with aluminum, and all
aluminum products must be removed from a gasoline dispensing system that will be used to dispense
E85. The ASTM standard specification for blended ethanol fuel is designated as ASTM D5798. This
ASTM specification covers fuel blends for different seasons and geographical areas. In accordance with
the EPA regulations, all commercial grades of gasoline must contain certain additives, detergents, and
corrosion inhibitors. In a finished blend of E85, any additive that was found previously in gasoline is now
contained in E85 (although at reduced levels). While the adding detergent to the hydrocarbon component
of E85 is necessary, it is not necessary to add detergent based on the alcohol portion of the product.
Overuse of additives with E85 may result in poor vehicle operation. The most common form of
hydrocarbon used in the blending of E85 is unleaded gasoline. The hydrocarbon blended with the ethanol
in E85 must meet the same standards as gasoline.
5.10.6
5.10.6.1 Cetane number (ignition quality). If the F-76 does not contain ignition improvers as
determined by ASTM D613 in this Standard, the cetane number may be estimated by means of the
calculated cetane index as outlined in ASTM D 976.
Fuel, naval distillate, NATO F-76 (MIL-DTL-16884).
5.10.6.2 Color. Most F-76 fuels are considerably lighter in color than the maximum allowed (ASTM
3 Color) in MIL-DTL-16884. Darkening of color on the ASTM scale generally indicates product
deterioration or contamination with another product. If the color exceeds ASTM 4 Color, then type B-2
tests, as outlined in 4.2.2.5 and Table XV shall be performed. If the product passes all the tests except
color, then the technical authority shall be contacted prior to use. F-76 shall contain no dye of any kind.
MGO, a similar fuel, may contain dye.
5.10.6.3 Flash point. Because F-76 is a standard product in shipboard operation; flash point is a
critical safety factor. Flash point of F-76 shall conform to the specification requirement of 60 C (140
F), minimum.
5.10.6.4 Distillation. F-76 failing to meet the distillation intra-Governmental receipt limit may be
used ashore in low-speed stationary diesel engines or as boiler fuel provided all other specification and
intra-Governmental receipt limits are met. This fuel must also meet local sulfur limits.
5.10.6.5 Carbon residue on 10% bottoms. This test is useful in determining contamination with
higher temperature boiling range material in F-76. An increase in carbon residue and a darkening of
color in stored F-76 indicate either contamination with another product or deterioration of the F-76. The
addition of ignition improvers will also increase the carbon residue (see Test Method 1050 in this
Standard). If it has been determined that ignition improvers have not been added, then the fuel shall be
completely tested for specification requirements to determine if other characteristics of the fuel have been
altered because of contamination. If the increase in carbon residue is caused by age deterioration, the
product shall be used as soon as possible.
5.10.6.6 Storage Stability. This provides insight into the anticipated time frame that the F-76 will
remain stable in storage. After procurement, the results are not limiting, rather high storage stability
results are viewed with other characteristics such as particulate content, carbon residue and color to
determine whether the F-76 requires immediate consumption or can be held in stock longer. F-76 with
high storage stability numbers may be placed on restricted issue. Normally this restriction applies to
issues to submarines.

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5.10.6.7 Water and sediment. These contaminants shall be held to an absolute minimum to prevent
corrosion and wear of fuel pumps and severe corrosion of shipboard gas turbine blades and diesel engine
injectors. If a sample fails ASTM D 4176 because a slight haze was observed, the product must meet the
requirements of ASTM D 2709 (0.05 vol % max). If the sample fails ASTM D 4176, procedure 1,
because it contains visible sediment or particulate matter, but meets the specification requirement of 10
mg/L (max) IAW ASTM D 5452 or ASTM D 6217 the product is considered acceptable provided all
other requirements are met. Controls are discussed in other sections of this Standard on bulk
transportation, bulk storage, fuel contamination and quality standards.
5.10.7 Fuel oil, diesel (ASTM D 975). Diesel fuel consists of a mixture of cracked and straight-run
stocks. This produces a fuel of good handling characteristics and availability. Recent innovations in
engine and vehicle design and increasing engine performance requirements impose greater emphasis on
fuel stability and cleanliness. In addition, the relatively low turnover rates of diesel fuel in non-tactical
situations require a fuel that resists deterioration over time.
5.10.7.1 RME 180. Marine Fuel Oil, the commercial denomination (IFO 180) is an intermediate Fuel
Oil 180 produced from heavy and medium oil fractions mixture, obtained from primary and secondary
crude oil processing. This product is used as combustible for maritime vessels. For testing requirements
see Table XVII.
5.10.7.2 RME 380. Marine Fuel Oil, the commercial denomination (IFO 380) is an intermediate Fuel
Oil 380. Along with RME 180 (IFO 180) RME 380 (IFO 380) are the most common intermediate fuel oil
grades for maritime vessels (commercially). For testing requirements see Table XVIII.
5.10.7.3 Water and sediment control. Diesel fuel shall be delivered to consuming vehicles through
filters or filter separators in order to keep water and/or sediment contamination to the absolute minimum
while preventing corrosion and wear of fuel pumps and injectors. Whether a filter or a filter-separator is
required, it will be based on the operational requirements at the specific location. For ASTM D975 diesel
fuel, Test Method ASTM D2709 is used for Grades No. 1-D, and No. 2-D (all sulfur levels) and Test
Method ASTM D1796 is used for Grade No. 4-D.
5.10.7.4 Cetane number. If the diesel fuel does not contain ignition improvers as determined by Test
Method 1050 in this Standard, the cetane number may be established by means of the calculated cetane
index listed in ASTM D 976 or ASTM D 4737. However, if estimated, the value shall be reported as a
cetane index. The cetane index should never be reported as the cetane number, as the two are not
equivalent.
5.10.7.5 Dyed fuel. The Internal Revenue Service requires that a red dye be added to all non-taxable
diesel fuel marketed in the United States, territories and possessions. This will generally include fuel that
exceeds the sulfur limit for on-road use (Grades No. 1-D, No. 2-D and No. 4-D). Non-dyed fuels (Grades
Low Sulfur No. 1-D and Low Sulfur No. 2-D) may acquire a reddish tinge due to cross contamination
with dyed fuels. Such fuels may be downgraded to off-road use. Use of red dyed fuel for on-road use is
a Federal offense
8
5.10.7.6 Distillation. Diesel fuel failing to meet the distillation intra-Governmental receipt limit may
be downgraded for use in low-speed stationary diesel engines as heating fuel provided all other
specification and intra-Governmental receipt limits are met.
.

8
NOTE: Under United States regulations if Grades Low Sulfur No. 1-D and Low Sulfur No. 2-D are sold for tax exempt purposes, then at or
beyond terminal storage tanks they are required by 26 CFR Part 48 to contain the dye Solvent Red 164 at a concentration spectrally equivalent
to 3.9 pounds per thousand barrels of the solid dye standard Solvent Red 26.
MIL-STD-3004C
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5.10.7.7 Cloud point. The cloud point is the temperature at which paraffinic wax crystals start to
appear. It is the lower operating limit for diesel fuel. Cloud point of diesel fuel varies with location and
season. The cloud point of the fuel should be below the expected lowest ambient temperature. Diesel
fuels with too high a cloud point may be blended with similar or kerosene fuels (1-K kerosene, JP-5, JP-
8) with lower cloud points to obtain a usable product. Blending for cloud point shall also take into
consideration the locality sulfur requirements as EPA mandated sulfur maximums cannot be exceeded.
5.10.7.8 Carbon residue on 10% bottoms. This test is useful for the determination of the presence of
burner fuels or other higher boiling range materials in the diesel fuel. An increase in carbon residue and a
darkening of color in stored diesel fuel indicate either contamination with another product or
deterioration of the diesel fuel. The addition of ignition improvers will also increase the carbon residue
(see Test Method 1050 in this Standard). If it has been determined that ignition improvers have not been
added, then the fuel shall be completely tested for specification requirements to determine if other
characteristics of the fuel have been altered. If the increase in carbon residue is caused by age
deterioration the product shall be used as soon as possible.
5.10.8 Kerosene, NATO F-58 (ASTM D 3699)
5.10.8.1 Color. Kerosene may be clear or colored, may darken with age. This normally has no
appreciable effect upon its operational capacity. However, even a slight color change brought about by
contamination with other products may seriously affect its intended use.
5.10.8.2 Flash point. A flash point below intra-Governmental receipt limit precludes use of kerosene
for its intended purpose, since the explosion danger becomes too great.
5.10.8.3 Sulfur. Sulfur limits for Grade 1-K kerosene (intended for use in non-flue connected
heaters) shall not be allowed to exceed intra-Governmental receipt limits as a health hazard may result.
5.10.9 Diesel fuel, biodiesel blend, B20 (ASTM D7467). Biodiesel (B100) is a fuel comprised of
mono-alkyl esters of long chain fatty acids derived from vegetable oils or animal fats. B20 is a blend
ratio of 80 vol % petroleum-based diesel fuel (ASTM D975) with 20 vol % biodiesel blend stock
(ASTM D6751) which requirements are listed in ASTM D7467. A B20 product must be pre-blended
prior to delivery. It is not acceptable to attempt blending into a Government tank during the delivery.
5.11 Aviation fuel contamination and quality standards. Delivery of clean aviation fuels to user
equipment is essential. Effort has been directed by both the military and industry toward development
and improvement of handling and surveillance procedures, equipment, and devices to ensure delivery of
clean aviation fuels. The necessity for clean fuel became evident when aviation turbine fuels began
causing problems in the modern engine. The purpose of this section is to emphasize the importance of
this requirement and to provide guidance to field operating personnel.
5.11.1 Gasoline and turbine fuel differences. Although information herein pertains to both aviation
gasoline and turbine fuel, cleanliness requirements for turbine engines are more restrictive than for piston
engines. High pressure, complex metering equipment built to close tolerances provides precise fuel
metering over a wide range of altitude, speed and power. Dirt and water contamination become more
critical for turbine engines and because of high fuel consumption rates contamination accumulates more
rapidly. Fine contaminants may block engine fuel supply systems and may erode critical parts of the
engine and fuel control system. Free water freezing at high altitudes may plug screens causing engine
flameout. Saltwater will especially cause fouling of the fuel quantity probe and corrosion within the fuel
system. The separation of contaminants from aviation turbine fuel, particularly grades JP-5 and JP-8, is
complicated because of higher viscosity and higher relative density, thereby increasing the required
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settling time. Aircraft engine filters are not designed to remove the fine or excessive amounts of
contamination; therefore, fuel cleanup shall be accomplished on the ground rather than in the aircraft.
5.11.2 Quality fuel deliveries. It shall be reemphasized that personnel responsible for delivery of
fuel shall take all steps necessary to ensure fuel delivered to aircraft is clean, bright, on-specification and
water-free. Samples may be taken and inspected visually as frequently as necessary. If specification or
intra-Governmental receipt limits are exceeded, it is obvious that improvement in fuel handling is
urgently required. Identifying the source of contamination to prevent future occurrences is the most
important aspect of determining necessary corrective action. While changing filter-separator elements
may appear to resolve the problem, this action provides only temporary relief if excessive solids or water
exists upstream of the filter-separator. Existing and potential problem areas shall be promptly identified
and brought to the attention of responsible personnel (Test Method 1010 in this Standard describes a
quality surveillance test procedure).
5.11.3 Fuel quality and fuel contamination. The main causes of fuel contamination are
commingling with other petroleum products and contamination with water; solids and microbiological
growth (see Table XXX).
5.11.3.1 Commingling with other petroleum products. This type of contamination usually results
from inadvertent mixing with other petroleum products during transportation and storage. Commingling
may be detected by color or odor change, but normally requires laboratory tests ranging from a simple
gravity test to a knock rating test in a laboratory engine.
5.11.3.2 Contamination with water, solids, and microbiological growth. This type of contamination
can frequently be detected visually since it is not miscible with the fuel. Table XXX of this Standard
provides a list of possible contaminants along with a description of each types appearance,
characteristics and effects on aircraft performance. For additional information refer to ASTM Manual on
Fuel and Fuel System Microbiology Fundamentals, Diagnosis, and Contamination Control.
a. Water in fuels may be either fresh or salt and may be present either as dissolved or free water.
Dissolved water is that which has been absorbed by the fuel and is not visible. Free water may be in the
form of a cloud, emulsion, droplets, or in larger amounts in the bottom of a tank or container. Any form
of free water can cause icing in the aircraft fuel system, malfunctioning of fuel quantity probes and
corrosion of fuel system components. Saltwater will promote corrosion much more rapidly than fresh
water (Test Method 1060 in this Standard describes the determination of free water in jet fuels).
b. Sediment appears as dust, powder, flakes, granular or fibrous materials. Total sediment includes
both organic and inorganic materials. If the total sediment as determined by tests is ashed, only the
inorganic portion remains. Presence of applicable quantities of fibrous materials is indicative of filter
element breakdown, either because of a ruptured element or mechanical disintegration of the filter
element in the fuel system. Usually a high metal content consisting of relatively large particles indicates
a mechanical failure. Sediment or solid contamination can be separated into two categories: (1) coarse
sediment and (2) fine sediment (See Test Method 1010 in this Standard).
(1) Coarse sediment is sediment that easily settles out of the fuel or can be removed by adequate
filtration. Ordinarily, particles ten (10) microns in size and larger are regarded as coarse sediment.
Coarse particles clog fuel orifices and become wedged in sliding valve clearances and valve shoulders,
causing malfunctions and excessive wear of fuel controls and metering equipment. They also clog nozzle
screens and other fine screens throughout the fuel system.
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(2) Fine sediment may be defined as particles smaller than ten microns. To a limited degree, this
sediment can be removed by settling, filtration and centrifuging. Particles of this size accumulate in fuel
controls appearing as a dark shellac-like surface on sliding valves. These particles may be centrifuged
out in rotating chambers as sludge-like matter resulting in sluggish operations of fuel metering equip-
ment. Fine particles are not visible to the naked eye as distinct or separate particles. However, they will
scatter light and may appear as point flashes of light or as a slight haze in fuel.
c. Microbiological growth consists of living organisms that grow at the fuel water interface. These
organisms include yeast, fungus and bacteria, all of which can cause problems associated with
microbiological contamination of aviation turbine fuels. Products of microbiological organisms and
fungus hold rust and water in suspension and are effective stabilizing agents for fuel/water emulsions.
These suspensions cling to glass and metal surfaces and may cause erroneous readings in fuel quantity
systems, sluggish fuel control operations and sticking of flow dividers. Microbiological growth is
generally found wherever pockets of water exist in fuel tanks. It has a brown, black or gray color and a
stringy, fibrous-like appearance. The presence of microbiological growth in fuel being delivered to
aircraft is a reliable indication of failure of fuel filtration equipment, inadequate water stripping of storage
tanks and a need for more frequent cleaning of fuel storage tanks.
d. Media Migration. The active media in all filter monitor (fuse) cartridges is water absorbent
materials know as super-absorbent polymer. Filter monitor cartridges qualified to EI 1583 4
th
edition
or earlier editions may allow small quantities of this material to pass or migrate into the fuel as the fuel
flows through the filter monitor. A portion of this material can then exit the downstream side of the filter
monitor entrained in the fuel. Although FSII has been proven to accelerate the media migration process,
media migration occurs in the absence of any FSII additive. Initially super-absorbent polymer material
takes the form of small solid particulates. These particles form a gel when exposed to water and/or fuel
additives. Since both the FSII additive and super-absorbent polymer have very high affinities for water,
both FSII and any migrated fragments of super-absorbent polymer may be found in water bottoms. Filters
employing super-absorbent polymer are no longer used at Navy shore based facilities or at any Air
Force fuels activity.
e. Samples representative of fuel serviced to aircraft shall contain no more than ten fibers when a
quart sample is visually examined. More than ten fibers indicate the filter or filter-separator elements are
not functioning properly and that corrective action shall be taken. Meticulous cleaning of the quart
sample bottle is necessary to properly determine fibrous content of the fuel.
5.11.4 Acceptable Fuel.
5.11.4.1 Free water. For product to be acceptable for fueling aircraft, it shall not only meet
specification/intra-Governmental receipt limits requirements, but be clean, bright and contain no more
than 10 ppm by volume of free water (for Navy requirements, see Note 1 of Table XXXI. The terms
clean and bright are independent of the normal color of the fuel. Some of the common colors
experienced are water white to various shades of straw. A cloud, haze, specks of sediment, or entrained
water indicates the fuel is unsuitable for use and that there is an existing breakdown in fuel handling (e.g.,
equipment or procedures). Once a breakdown has been identified, steps shall be taken to find the source
of the problem so that it may be corrected immediately.
5.11.4.2 Red dye contamination. Aviation turbine fuels are not to contain dye of any kind. The
current test for examining for possible contamination of jet fuel with a dye is the white bucket test (no
dilution permitted), identified in ASTM Manual 5. In this test a portion of jet fuel is placed into a white
MIL-STD-3004C
64

bucket and examined for any color change which may be attributable to the dye. Under current policy if
any red or pink color is visually detected the product is not acceptable for use or downgrade.
5.11.4.3 Cloudy or hazy fuel. Ordinarily, a cloud in the fuel indicates the presence of water, but a
cloud can also be caused by excessive amounts of fine sediment or a finely dispersed stabilized emulsion.
Fuel containing a cloud from either cause is not acceptable for use. For JP-8, JP-5, and JP-4 at the time
of government acceptance, the finished fuel or finished fuel blend shall be visually free from undissolved
water, sediment or suspended matter, and shall be clear and bright. In case of dispute, the fuel shall be
clear and bright at 21 C (70 F) and contain no more than 1.0 mg/L of particulate matter. For F-76,
product shall be clear and bright and contain maximum of 0.05 percent volume or less of water and
sediment.
5.11.4.4 Sediment in fuel. Visible specks or sediment granules in the fuel indicate a particle size
larger than forty microns. The presence of any appreciable number of such particles indicates a filter-
separators malfunction, a source of contamination downstream of the filter-separator, or an improperly
cleaned sample container. Sediment ordinarily encountered is an extremely fine powder, rouge, or silt.
In a sample of clean fuel (one taken after a filter), no sediment should be visible.
5.12 Ground mobility fuel contamination. Many of the elements found in aircraft engines are also
found in ground-based engines (e.g.: burner cans and injectors) and are just as prone to failure due to fuel
contamination. This is especially true with the increased use of turbine engines to replace compression
ignition piston engines in ground equipment/vehicles, the more sophisticated fuel delivery systems found
in current compression ignition engines, and the introduction of certain alternative fuels. The purpose of
this section is to provide information on the nature of the contaminants common to ground mobility fuels
and to give guidance to field operating personnel as to the procedures necessary to prevent or eliminate
fuel contamination. Whenever specification or intra-Governmental receipt limits on fuel contamination
are exceeded, the probable cause shall be investigated and appropriate corrective action taken. Such
corrective action shall be completed before the fuel is allowed to reach the using vehicle or equipment.
5.12.1 Ground mobility fuels. The general types of ground mobility fuels are diesel fuel and
aviation turbine fuel (JP-8/JP-5, and Jet A/A-1), however, some specialized equipment still use
automotive gasoline. The use of aviation turbine fuel as a ground mobility fuel is mandated by the Fuel
Standardization policy of DoDM 4140.25-M. JP-8 is kerosene based fuel and is an acceptable substitute/
alternate for diesel fuel. Using JP-8 is essentially no different than operating diesel engines with diesel
fuel products. All three fuels require a high degree of attention to basic housekeeping rules to ensure
delivery of a clean, dry product and each type has its own unique problems.
5.12.1.1 Automotive gasoline. Gasoline has a tendency to form gum deposits in storage. Gasohol,
a gasoline and alcohol blend, is sensitive to small quantities of free water.
5.12.1.2 Diesel fuel. Because of its higher content of naturally occurring and added surfactants
along with a higher viscosity when compared to gasoline, diesel holds water droplets in suspension that
resist removal by coalescence. Biodiesel blends can reduce exhaust emissions; however, water
absorption occurs at a greater rate. It should be noted biodiesel blends have not been approved for use in
tactical/combat vehicles deploying for overseas combat areas.
5.12.1.3 Aviation turbine fuel. Being able to issue aviation turbine fuel as a ground and aviation
product may simplify storage, quality control and distribution while supporting the Fuel Standardization
policy directed by DoDM 4140.25-M. JP-8 conditions must be maintained IAW the JP-8 specification
requirements. The use of commercial jet fuels are not recommended for use as ground fuel unless the
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fuel is additized with corrosion inhibitor/lubricity approver additives IAW QPL-25017 concentration
levels. Unless under emergency conditions, the appropriate Service Control Point shall be contacted for
guidance and/or assistance prior to using unadditized commercial jet fuels for ground fuel applications.
a. The particulate matter requirement for JP-8 is 1.0 mg/L, but may be issued with 10.0 mg/L for
product used as a diesel product for ground use.
b. Fuel conductivity must be between 150 and 600 pS/m for JP-8.
c. JP-8, as a ground fuel, does not meet current Federal, State and local regulations for ultra low
sulfur diesel (ULSD) for either on-road or off- road usage in commercial vehicles. If JP-8 is designated
for ground fuel use, consult Federal, State and local regulations to determine allowed sulfur content.
DoD tactical vehicles and equipment are exempt from environmental sulfur limits imposed on diesel use.
However, non-tactical diesel equipment is not exempt. Therefore, product used for commercial equip-
ment must comply with the environmental regulations for the commercial equipment. In many countries,
including the US, ultra-low sulfur diesel is required. Many US made commercial vehicles made after
2007 will include a pollution control device that is sensitive to total sulfur contents greater than 15 mg/kg
(ppm by volume). Using a fuel with higher sulfur content will cause the device to fail and preclude
further operation of the equipment. For these commercial vehicles JP-8 fuel is not recommended for use
in whole or as a blending stock, as the sulfur content of the final blend will likely be higher than what is
required.
5.12.2 Fuel contamination and contamination prevention. Ground fuel contaminants include those
caused by the commingling of other fuels, by the introduction of sediment and water, and by the products
of fuel deterioration.
5.12.2.1 Contamination with other fuels (commingling). Contamination of this type usually results
from an accidental mixing of different types of fuel during storage or transportation or from refueling
vehicles or equipment with the wrong fuel. It may also occur in smaller quantities from improper
batching in pipelines or from failure to adequately clean fuel tanks when switch loading. The effects of
commingling vary with the amount and type of fuels, as the following examples illustrate:
a. Contamination of diesel fuel with gasoline or a low flash point turbine fuel will lower the flash
point of the diesel and create a safety hazard, and lower the cetane value.
b. Contamination of motor gasoline, gasohol, or oxygenated gasoline with diesel fuel will reduce the
antiknock index (average of research and motor octane numbers) and will cause increased engine
deposits, as well as decreased storage stability. It will also expand the flammability limits over that of
neat gasoline.
c. Contamination of unleaded gasoline with leaded gasoline will result in damaging the catalytic
converter in the using vehicles equipped with emission control systems. In many cases it will also void
warranties.
5.12.2.2 Contamination with water. Water in fuel may be either fresh or salt and may be either
dissolved or free water. Dissolved water is water that has been solubilize in the fuel and is invisible. It
usually does not pose a threat to engines as the amount is generally less than 100 ppm by volume.
However, decreasing the fuel temperature can cause dissolved water to come out of solution to form free
water. Free water may be in the form of an emulsion, fine droplets in suspension, or in larger quantities
that separate and sink to the bottoms of a tank or container. Free water in ground fuels can cause stalling,
injector fouling and other engine malfunctions as well as being a cause of corrosion. In cold weather free
water may cause blockage of fuel lines by freezing. Diesel fuel contains high levels of surfactants,
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usually left as refinery residuals or those introduced in additive systems. These surfactants keep water
droplets in suspension and resist separation by coalescence. If gasohol is exposed to water, it will tend to
separate into two phases with the aqueous alcohol phase on the bottom. If this lower phase is delivered
to the engine, serious malfunction will result. Water in fuel can arise by condensation, leakage, seepage
of ground water into underground storage tanks, or from rain leaking into storage or vehicle tanks.
5.12.2.3 Contamination with sediment. Sediment may be in the form of dust, powder flakes,
granular material, fibrous material, agglomerates, sludge, or slime. Sediment includes both organic and
inorganic matter. The sediment may be denser than fuel (tending to sink) or lighter than fuel (tending to
float). If the fuel container or tank has a water bottom, some or all of the sediment may be present at the
fuel and water interface.
a. Inorganic sediment includes metallic and rust particles, siliceous material, and mineral fibers such
as fiberglass. Coarse sediment (greater than ten microns) may clog fuel lines and damage fuel injector
pumps and other engine components. Fine sediment may form a sludge-like material degrading the
operations of fuel pumps and metering equipment. The composition of the sediment usually reveals its
source. Metallic particles may be present as a result of mechanical failure further up the fuel system.
Rust particles are usually from tanks and pipelines. Fiberglass fibers may indicate the breakdown of
filter/coalesce elements.
b. Organic sediment consists primarily of the deterioration of products of fuel and of microbio-
logical debris. The deterioration products take the form of brown to black insoluble material, gums and
sludge that can clog filters and screens. Gums are the products of oxidation and polymerization of
unsaturated hydrocarbons frequently found in gasolines and distillate fuels. Microbiological organisms
include bacteria, yeasts, fungi and protozoa. Bacteria and fungi are the prime categories usually found in
fuel systems. Bacteria are single-cell organisms that can live in the presence of free oxygen (aerobic), or
in the absence of oxygen (anaerobic). Fungi are larger than bacteria and grow to form fungal mats.
Fungi produce spores that can germinate in the presence of water. The organisms can grow in strings,
mats, or globules and usually appear black, green, or brown. They are frequently seen on the surface of
filter coalescer elements. All microbiological species require the presence of water. Growth takes place
at the fuel/water interface where organisms feed on the fuel and can get trace elements as well as
moisture from the water layer. Many bacteria and fungi can produce acids and other metabolic products
which can promote corrosion of metal surfaces. The mats and globules can block fuel systems.
5.12.2.4 Fuel contamination prevention. The following practices and procedures are recommended
to minimize the possibilities of fuel contamination.
a. The use of filter-separators, meeting the performance requirements of MIL-PRF-52308 or EI
1581, is mandatory for aviation and ground fuels issued. Delivery of fuels through a filter-separator
should reduce the water and sediment contamination to a minimum and prevent corrosion, wear and
deposits in the using equipment and vehicles. Furthermore, the life of the engine-mounted filters will be
extended and fewer fuel blockage incidents will occur. Filter-separators are not recommended for use
with gasohol as they facilitate water/fuel contact and can encourage phase separation.
b. All fuel tanks, from the using vehicle/equipment back to the bulk storage tank, shall not be
allowed to accumulate water bottoms. Fuel tanks shall be drained regularly. This deprives
microorganisms of water essential to their growth, reduce corrosion in the fuel system and prevent
freezing of fuel lines in cold weather.
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c. Fuel operating tanks (fixed tanks dispensing fuel directly to using vehicles and equipment) and
bulk storage tanks shall be inspected in accordance with STANAG 3609. Ground fuel tanks are
inspected whenever fuel samples approach or exceed intra-Governmental receipt limits, or when they
show evidence of excessive rusting and sludging, microbiological growth, or liner deterioration.
d. The empty space at the top of the fuel tank breathes through the vent during periodic temperature
and pressure cycles. As a result, moisture laden air is drawn into the tank where water can condense on
the metal surfaces to cause corrosion and support microbiological growth. Keeping the vehicle full will
reduce the volume of air and minimize the chance of condensation.
e. FSII meeting the requirements of MIL-DTL-85470 may be added to diesel fuels at a
concentration up to 0.15 vol % to cope with small amounts of water contamination (entrained water), or
to keep separated water from freezing. A diesel fuel additive (MIL-S-53021) is available to control the
growth of microorganisms and the deterioration of diesel fuel remaining in storage tanks or intended for
storage (pre-positioning of material). This additive is a combination antioxidant, metal deactivator,
detergent, corrosion inhibitor and biocide that is intended primarily for use in those fuels for vehicles and
equipment destined for depot storage or for pre-positioning material in a fully fueled storage condition. It
must be emphasized that additives are not substitutes for good housekeeping and proper maintenance of
fuel tanks. Additives are only preventative measures and cannot restore fuel that has already deteriorated
past its intra-Governmental receipt limits. Only those additives authorized by the fuel specification
preparing activity shall be added.
5.13 Non-conforming product.
5.13.1 Identification of a non-conforming product. A product is deemed to be non-conforming
when:
a. A product being accepted by an authorized Government Representative either at origin on an
F.O.B. Origin contract basis or at destination on an F.O.B. Destination contract basis determined by
inspection and/or tests not to conform to the procurement contract specifications; or,
b. For DLA-ENERGY-owned product determined by inspection and/or tests not to conform to the
procurement specification as amended by the Intra-Governmental Receipt Limits (IGRL) contained in
Tables I-VII, MIL-STD-3004.
c. For DLA-ENERGY product determined by inspection and/or test to fall between the product
specification and the IGRL, the product is deemed acceptable for use but a report of non-conformance is
still requested to improve product quality. Issuance of fuel meeting only the intra-Governmental receipt
limit should be used as a safety net to continue issuing product to customers when a problem has been
identified and corrective action is being taken to prevent recurrence. A product found to meet the IGRL
limits after shipment of on-specification product from a DFSP means that a problem has been
encountered within the transportation system that requires attention.
d. Reports of non-conforming product are categorized as Customer/Depot Complaints. DLA-
ENERGY-QA manages the Customer/Depot Complaint Program for DLA-ENERGY.
5.13.2 Disposition request procedures. It is DLA policy to issue only those supplies and services
that fully conform, in all respects, to the procurement specification requirement.
a. When product does not meet specification limits, the facility having physical possession of the
product shall provide pertinent details to DLA-ENERGY-QA for bulk products or DLA AVIATION for
packaged products.
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b. Based on these details DLA-ENERGY-QA or DLA AVIATION will provide a decision
concerning the products use, rehabilitation, or disposition. The facilities shall also inform the cognizant
DLA-ENERGY Region. Service facilities shall coordinate with their service control point prior to
reporting to DLA-ENERGY.
c. For DLA-ENERGY contract locations, DLA-ENERGY may provide rehabilitation direction to
the contractor after coordinating with the Service Technical Office and end user to ensure that the end
result is a specification/intra-governmental receipt limits product which is being issued. At Service run
GOGOs and Service contracted sites, DLA-ENERGY shall coordinate with the Service Technical Office
and end user to ensure that all parties are aware of the disposition actions.
d. When fuel does not meet specification requirements at the time of shipment to an end user for any
characteristic(s) that does not have an intra-Governmental receipt limit (see Tables I-VII), and
rehabilitation is not possible, DLA-ENERGY-QA will obtain a waiver from the applicable Service
technical office prior to shipment to the end user.
e. Where a characteristic does have an intra-Governmental receipt limit and the product does not
meet this limit, DLA-ENERGY-QA shall obtain a waiver from the applicable Service Technical Office
prior to shipment to an end user.
f. In the case of out-of duty hour emergent requests, DLA-ENERGY-QA shall provide disposition
instructions and if possible notify the applicable Service technical office prior to shipment. If it is not
possible to contact the Service technical office prior to shipment, then the contact shall be made as soon
as practical.
g. When Service-owned product does not meet intra-Governmental receipt limits set forth in this
Standard; they will contact the using Services technical office (see 5.13.3) for a decision concerning its
use or disposition.
h. Report of Customer/Depot Complaint and request for disposition instructions shall be sent through
channels to DLA-ENERGY-QA. The DLA-ENERGY-QA office Program Manager if known can receive
the report by e-mail. If the DLA-ENERGY-QA office Program Manager is unknown the request shall be
sent to the email box as specified at http://www.desc.dla.mil/DCM/DCMPage.asp?pageid=79 or by
facsimile (703-767-8747). The email address of the DLA-ENERGY-QA office box is as of the date of this
documents approval desc.bqoffice@dla.mil. The Report shall contain, as a minimum, the following
details:
(1) Specification and Grade of product non-conforming.
(2) Quantity of non-conforming product by storage tank/conveyance.
(3) Location where non-conforming product is held.
(4) Date of Receipt.
(5) Name of manufacturer, contract number, batch number, qualification number, date of
manufacture, as applicable.
(6) Type of container or storage.
(7) Accountable military department.
(8) Need for replacement product.
(9) Detailed laboratory test results and if known, degree of contamination and contaminating
materials. Test results reported shall include all known characteristics and whether results are within
MIL-STD-3004C
69

specification. The appropriate Type A or B test results performed on stock just prior to identification of
contamination problem shall also be included.
(10) Recommended alternate use, disposition, or proposed recovery measures, if appropriate.
Facility capabilities to rehabilitate the non-conforming product assist in expediting disposition
instructions.
5.13.2.1 Report of non-conforming product exceptions. For non-conforming product found on
F.O.B. destination procurements contracts prior to off-load, the activity having acceptance
responsibilities shall reject the non-conforming product. The activity shall notify the DLA-ENERGY
contracting/quality operations personnel or the military service contracting personnel by telephone or
message in order to report the circumstances pertaining to the delivery in question. All information as
stated in paragraph 5.13.2 (h.) above is required. Disposition of the product on the conveyance is
required prior to releasing the conveyance back to the contractor. The supplier needs to contact the
contracting officer (or in some cases the DLA-ENERGY contracting office may contact the supplier).
DLA-ENERGY shall coordinate with the concerned technical facility of the military department(s) in
resolving the shipment and shall advise the receiving facility accordingly. In overseas areas the JPO and
DLA-ENERGY Regions shall be advised by DLA-ENERGY of the problem and its resolution. If a
military service contract is involved, the responsible service shall take the above action.
5.13.3 Service and DLA responsibilities. The following are the responsible technical organizations
of the Services and DLA for petroleum and related products.
a. Army
Mailing Address: U.S. Army Petroleum Center
Room 0522 Mail Stop 6241
8725 John J. Kingman Rd.
Ft. Belvoir, VA 22060-6241

Message Address: USAPC Ft Belvoir Va//AMXPC//
Telephone: Commercial: (703) 767-0649
DSN: 427-0649
b. Navy
Mailing Address: Director
NAVSUP Energy
Attn: Code PS
8725 John J. Kingman Rd., Suite 3719

Message Address: NAVSUP Energy BELVOIR VA
Telephone: Commercial: 703-767-7334/7341
DSN: 427-7334/7341
c. Air Force
Mailing Address: Commanding Officer
Air Force Petroleum Agency
J. Kingman Road, Stop 6232,
Room 1227
MIL-STD-3004C
70

Message Address: AFPA WRIGHT PATTERSON AFB,
OH//PTOT//
Telephone: Commercial: 937-255-8070
DSN 785-8070
Email: afpet.afth@wpafb.af.mil

d. DLA-Energy Message Address: DLA-Energy-QA, Room 2843
8725 John J. Kingman Rd

Message Address: DLA-Energy
FT BELVOIR VA//DLA-ENERGY-QA,
Telephone: Commercial: 703-767-8736/8395
DSN: 427-8736/8795

e. DLA- Aviation Message Address: DLA-Aviation
Richmond, VA 23297
Attn: DLA-E-JDTA
Richmond, VA 23297

Message Address: DLA-Aviation
VA//DLA AVIATION-JDTA//
Telephone: Commercial: 804-279-5173
DSN: 695-5173

5.13.3.1 Communication copies. DLA-ENERGY-QA or DLA AVIATION, cognizant JPO, and
cognizant DLA-ENERGY Region shall be furnished copies of all communication regarding disposition
of Government-owned, off-specification product in overseas areas.
5.13.4 Chain of custody requirement for all samples shipped to a laboratory. In order to ensure
sample integrity a record of the chain of custody must be maintained by the sample owner until sample
disposal. Chain of custody documentation must be used for all samples forwarded where there is a
contractual issue in question. Each change of custody shall be documented at the time and place of
transfer including signature of the custodian. Chain of custody documentation shall be forwarded to
DLA-ENERGY-QA for inclusion into the Customer Depot Complaint (CDC) file. DLA-ENERGY-QA
determine product disposition and sample disposal and notify sample owner(s) accordingly.
Documentation and samples representing legal/potential legal disputes shall be maintained until release
by DLA-ENERGY-G. See Appendix F for a sample form that may used to record sample chain of
custody.
5.13.5 Laboratory reports. While laboratories are authorized to provide recommended disposition
instructions for non-conforming Defense Working Capital Fund product, only DLA-ENERGY Quality
Division can provide official disposition.
5.13.6 Reclamation. This is the procedure that restores or changes the quality of a contaminated or
off-specification product so it will meet the specification of the original product or a lower grade product.
MIL-STD-3004C
71

The process of reclamation, when properly applied, will result in downgrading, blending, purification, or
dehydration.
5.13.6.1 Determining factors. The following factors shall be carefully considered before
reclamation is recommended:
a. Contaminating agents present and source of contaminants.
b. Degree of contamination.
c. Probable end use of petroleum product in present condition with consideration given to laboratory
analysis, purchase specification, established intra-Governmental receipt limits and safety factors.
d. Feasibility of removing or nullifying undesirable effects of contaminants so the petroleum product
may be used.
e. Actual location and quantities of off-specification or contaminated petroleum product.
f. Probable need for reclaimed petroleum product.
g. Availability of time, materials, equipment and labor necessary to reclaim the off-specification or
contaminated product.
5.13.7 Reclamation techniques.
5.13.7.1 Downgrading. Downgrading is the procedure by which an off-specification or slightly
contaminated petroleum product is approved for use as a lower grade of the same or similar petroleum
product.
5.13.7.2 Blending. Blending is that procedure by which predetermined quantities of two or more
similar petroleum products are mixed to produce a petroleum product of intermediate grade or quality.
5.13.7.3 Additive injection/mixing. The inclusion of an additive, such as MIL-S-53021 (for
automotive diesel fuel) along with other techniques such as blending to bring the characteristics of former
off-specification product back into the range of on-specification or intra-Governmental receipt limits.
5.13.7.4. Purification. The removal of contaminating agents by filtration or dehydration.
5.13.7.5 Water removal. Water Removal is accomplished primarily by filtering or settling process.
Water in most light petroleum products will settle out if allowed to stand undisturbed from 6 to 24 hours.
If the light product is in a storage tank, the excess water may be withdrawn through the water draw-off
valve. If the product is in a small container, the water may be separated by filtering and decanting into
another container or by siphoning off the water.
5.14 Packaged products. This section covers receipt and storage of packaged petroleum products for
direct delivery and stock locations. It also addresses the sampling and testing requirements and the
significance of those tests. (See MIL-STD-290, Packaging, Packing and Marking of Petroleum and
Related Products, for detailed requirements and methods.)
5.14.1 Product receipt. Products are delivered under DLA AVIATION contract either by direct
delivery that comes from the contractors facility directly to the customer, or from a depot storage
facility.
5.14.2 Sampling. All samples shall be taken in accordance with standard procedures described in
API, MPMS, Chapter 8, Section 1 or ASTM D 4057, or as prescribed by product specifications or
contract requirements and ANSI Z1.4.
MIL-STD-3004C
72

5.14.2.1 Precautions. The precautions required to ensure a representative sample are many and
depend on type of product being sampled, the type of container from which it is drawn and the sampling
procedures employed. Each procedure is suitable for sampling a specific product under definite storage,
transportation and container conditions. Warning: All safety instructions shall be strictly observed.
5.14.2.2 Personnel to conduct sampling. Because improperly taken samples can completely
invalidate a test, only trained and experienced personnel shall be assigned to sample the products. This
cannot be overstressed: No amount of laboratory work will give reliable data on a product if the sample
is not a true representation of that product.
5.14.2.3 Responsibility. This Standard shall in no way alter any assigned responsibility of the
various activities outside the continental United States for submitting special samples to a designated
laboratory or as directed by cognizant headquarters.
5.14.2.4 Types of samples. A sample is a portion of a packaged petroleum product taken which
represents that entire batch or delivery. The various types of samples are as follows:
a. Tube or thief sample is one obtained with a sampling tube or special thief, either as a core, or spot
sample, from a specified point in the container.
b. Batch or lot sample is one obtained from a collection of units of package products.
5.14.2.5 Sampling apparatus, containers, and procedures.
a. Approved type samplers shall be used as specified by ASTM/API procedures. All sampling
apparatus and containers shall be thoroughly clean and dry, and special care shall be taken so no lint or
fibrous material remains in or on them.
b. Apparatus and containers shall be flushed three times with 10 to 20 % of the volume of the
sample container of the product being sampled to ensure the sample is not contaminated with the
previous material unless otherwise specified in the test procedures. For each flush, the container shall be
closed and shaken for 10 seconds and product replaced for the next flush. All cans shall be thoroughly
flushed to ensure complete removal of soldering flux. Sampling apparatus shall be cleaned immediately
after use and stored so it shall remain clean until next use.
c. Containers such as drums shall be sampled with a thief. In sampling drums and cans, care shall
be taken to remove all foreign matter from the area near the enclosure before the plug is removed.
d. Close all sample containers tightly, immediately after taking the sample. Do not use sealing wax,
paraffin, rubber gaskets, pressure sensitive tapes, or similar material to seal containers. Light sample
containers shall be adequately crated to withstand shipment. To prevent leakage caused by thermal
expansion of the product, do not fill any sample container above 80 % volume capacity.
e. The one gallon sample can, NSN 8110-01-371-8315, is suitable for fuel products and the one
gallon sample can, 8110-00-178-8292, is suitable for grease products.
5.14.2.6 Size of samples.
a. Except for liquid units of issue greater than 1-gallon and semi-solids greater than 6.5-pound can
or container, all samples shall be submitted in the original unopened container. When instructed to take
a sample, the sample size shall be as follows:

MIL-STD-3004C
73

(1) Liquid
Unit of Issue Sample Size
Less than 1 quart 1 gallon (USG)
1-quart can Four 1 quart cans
1-gallon can 1-gallon can
Any unit of issue larger than 1
gallon
1 gallon
(2) Semi-solid
Unit of Issue Sample Size
Less than 1 pound 4 pounds
1-pound can Four 1-pound cans
5 pound can or container One 5-pound can or
container
6.5-pound can or container one 6.5-pound can or
container
Any unit of issue larger than 6.5
pounds
5 pounds
b. For container sizes not listed in the tables above, contact the appropriate focal point for
instructions.
5.14.2.7 Identification of samples. Identify each sample container immediately after sampling by
securely attaching a DD Form 2927, Petroleum and Lubricants Sample Identification Tag or the
equivalent. The link for DD Form 2927 is:
http://www.dtic.mil/whs/directives/infomgt/forms/forminfo/forminfopage3398.html
Information on the tag shall include the following:
a. Product and Type
b. Date Received
c. Installation
d. Sample Number
e. Laboratory Number (If known)
f. Specification Number with revision
g. National stock number (NSN)
h. Contract number
i. Product batch, lot number or emulsion number
j. Contractor/Manufacturer/Supplier
k. Quantity
l. Sample Source
m. Fill/Delivery/DOM date
MIL-STD-3004C
74

n. Submitters sample number
o. Sampled by
p. Date Sampled by
q. Organization, Address, telephone, fax number and email of submitter/POC
r. Test Series, Sample Type and Sample Information and Special/Additional Information
s. Qualification number (if available)
t. In the case of packaged products, the complete markings shown on the container shall be
furnished. The container from which the sample was taken shall be marked with the sample number for
future identification.
5.14.3 Testing. The quality surveillance segment (testing) presented in this section is the minimum
essential to sound management of Government-owned properties. Only by thorough testing procedures
can premium quality surveillance be maintained.
5.14.3.1 Contamination tests. Suspected contamination of petroleum products shall be confirmed
by laboratory tests. Tests which have proved most useful in determining whether a product is
contaminated and the identification of the contaminating agents are listed under the individual products.
(See 5.10)
5.14.3.2 Test methods. All laboratory tests shall be conducted in accordance with the method
prescribed in the specification covering the product, except any special or modified method outlined in
this Standard which shall be used in lieu of the specification method when products are evaluated within
the scope of this Standard.
5.14.3.3 Specification receipt limits. Specification receipt limits are absolute. Multiple tests may be
performed and if these tests do not differ from each other by more than the amount specified for the
reproducibility of the method, the results may be averaged to determine compliance with the specification
limits.
5.14.3.4 Testing frequency. For current testing frequency requirements refer to DLIS Total Item
Record (TIR).
5.14.3.5 Minimum testing. Table IX outlines the minimum sampling and testing requirements
considered necessary for determining the quality of petroleum and related products. It covers the
conditions under which a sample is taken, the type of sample and the types of tests required to determine
whether the quality is within acceptable limits.
5.14.3.6 Test required. Tables X-XIX are a series of charts providing a detailed breakdown of the
type of tests required for each class of product. These tests are those most likely to reveal deterioration
which may have occurred during product handling or storage. Tables XX-XXV designate Service and
NATO prescribed B-2 tests for specific products.
5.14.3.7 Alternate test methods. The use of alternate test methods to measure physical properties is
allowed, provided that: test results are presented in the format required in the specification; the test
device has a demonstrated reliability and repeatability equal to or better than that called for by the
American Society for Testing and Materials (ASTM) and the device has been approved for use by the
military services. The types of alternate tests are listed below:
MIL-STD-3004C
75

a. Equivalent tests are test methods that provide analogous results and fully correlate with standard
ASTM methods but have not yet been formally accepted by ASTM. These test methods have been found
to provide test results that will be essentially identical to those results produced by ASTM testing
methodologies.
b. Predictive testing involves the use of instrumental and other types of analytical techniques to
predict lubricant test values using compositional data that typically is determined by standard or wet
chemistry methods.
5.14.3.8 Calibrating test equipment. All laboratories shall calibrate testing and measuring
equipment to the accuracy necessary to ensure the equipment is within allowable tolerance limits. See
ANSI/NCSL Z540-1.
5.14.4 Disposition procedures. Prior to submission of samples for testing or prior to reclassification
of condition codes, the storage activity shall consult the DoD Quality Status List (QSL) published by
DLA AVIATION to determine the status of the particular batch/lot number under a specific contract.
a. If the extension data is listed in the QSL, then the stock shall be updated accordingly.
b. If the QSL indicates condition code H, then the stock shall be disposed of through Defense
Reutilization and Marketing Office (DRMO) in accordance with local procedures.
c. If the item is not listed in the QSL, then the appropriate focal point shall be contacted.
5.14.5 Service and DLA responsibilities. The following are the responsible technical organizations
within the Services and DLA for packaged petroleum products:
a. Army U.S. Army Petroleum Center
8725 John J Kingman Rd.
Ft. Belvoir, VA 22060
DSN: 427-0659
FAX DSN: 427-0669
Commercial: (703) 767-0659

b. Navy NAVSUP Energy
Attn: Code PS
8725 John J. Kingman Rd., Suite 3719
DSN: 427-7341
FAX DSN: 427-7389
Commercial: (703) 767-7341
c. Air Force Air Force Petroleum Agency
ATTN: AFPA/PTPT
2430 C Street, Building 70, Area B
Wright Patterson AFB, OH 45433-7632
DSN: 785-8050
FAX: DSN 785-8051
Commercial: (937) 255-8050

MIL-STD-3004C
76

d.-DLA

FSC 9150 only DLA-Aviation
ATTN: DLA-JDTA
8000 Jefferson Davis Highway
Richmond, VA 23297-5000
DSN: 695-5173
FAX DSN: 695-4370
Commercial: (804) 279-5173

FSC 9110 or 9160 DLA-Troop Support
700 Robbins Avenue
Philadelphia, PA 19111-5096
DSN: 442-5515
FAX DSN: 442-5520
Commercial: (215) 697-5515
5.14.6 Packaging and storage of packaged petroleum products. The care and preservation of
packaged oils and lubricants in a ready-for-issue condition, from supplier to user, is an important
responsibility of the military services. The appropriate military activity shall prescribe the procedures
and establish the requirements in each phase of the storage program. These shall be predicated on the
type of item, type of storage, anticipated length of storage, probable end use and other factors.
5.14.6.1 Documentation. Care of packaged products in storage is a program of such magnitude that
detailed procedures cannot be included in this Standard. Reference shall be made to appropriate
departmental publications. Pertinent highlights are cited in the following paragraphs.
5.14.6.2 Container inspection. Containers shall be inspected before being placed in storage and
periodically thereafter. These inspections shall be made more frequently if required by local conditions.
If containers are received in an unsuitable condition and repackaging is necessary, the product shall be
fully inspected by a Government at the repackaging facility. Under no circumstances shall product be
accepted without Government inspection if it has been repackaged by the railroad or trucking company.
5.14.6.3 Container suitability. Before filling, all containers shall be inspected to ensure they are
clean, free of loose rust, paint flakes and contaminants and are suitable for receiving the product.
Meticulous cleanliness of the container and filling equipment shall be ensured since many products
require a high degree of cleanliness and have been micronically filtered. In addition to those mentioned
in 5.14.7.2, the specifications for other super-clean fluids are MIL-PRF-7808, DOD-PRF-85734, and
MIL-PRF-23699. Containers shall be appropriately marked prior to filling and shall be closed
immediately after filling.
5.14.6.4 Drum storage. Except in an emergency, containers shall not be stored in direct contact with
the ground. Drums shall be stored on their sides on dunnage with proper blocking and bracing. Bungs
shall be in a horizontal position so leaks may be detected and/or eliminated. Drums shall never be stored
vertically outdoors as water shall collect on drum heads, seep through bungs and contaminate the product.
5.14.6.5 Separate storage. For identification purposes different products and grades shall be stored
separately. Stocks of similar dates of filling shall be stored together whenever possible. Oldest stocks
shall be used first.
MIL-STD-3004C
77

5.14.6.6 Stock rotation. Where feasible, packaged products opened for spot checking or storage
control testing shall be used as soon as possible. When this cannot be done the containers shall be re-
closed tightly, marked as having been previously opened and be included in the next issue if possible. To
minimize deterioration of a product due to age, excessive corrosion of containers, and/or deterioration of
packing and markings, (excluding other quality considerations), the oldest package petroleum products
shall be issued first. Fill dates on the containers and the condition of the package are the governing
factors.
5.14.6.7 Galvanized containers. Internally galvanized containers shall not to be used.
5.14.6.8 Small container storage. Containers smaller than the 55-gallon drum shall be stored under
cover, preferably in warehouses or open sheds. In emergency situations containers shall be stored
outside, off the ground on pallets or dunnage and covered with tarpaulins for protection from the
elements.
5.14.6.9 Contamination. Many things can happen in the filling, handling, storage and dispensing of
packaged petroleum products. Some of the more detrimental things include contamination, deterioration
of quality, inadvertent use of incorrect products, damage to equipment, loss of identity and loss of product.
Improper storage conditions can lead to contamination, deterioration of identification markings and
excessive corrosion of metal containers. Refilling of previously used containers without first cleaning and
remarking can lead to contamination on issue. The use of an incorrect grade product in unmarked
containers can result in incorrect applications with resultant loss of life and equipment. Improper loading,
blocking, or bracing of packaged products in transportation equipment will almost always result in
container damage and often the loss of product.
a. Water is a common source of contamination which can render packaged products unsuitable for
use. Rough handling or improper application of plugs and gaskets will permit breathing and result in
condensation of water vapor inside the package. Reasonable protection against atmospheric conditions
will reduce water contamination.
b. Packaged petroleum products shall be properly protected from initial filling until ultimate
consumption. Leaving containers open or unprotected at the final point of application of the product
often results in contamination. Extreme care shall be taken at dispensing points to protect product
quality. Instructions concerning disposition of product remaining after partial use of container contents
shall be followed.
5.14.6.10 Minimum container markings. It is essential that containers for petroleum products are so
marked that:
a. The products may be properly identified.
b. The origin and age of the product may be determined at any time.
c. Any hazard associated with the use or handling of the product is clearly indicated as flammable,
toxic, or corrosive.
5.14.6.11 Field-filled container markings. The following minimum markings are required for all
containers of petroleum products filled under field conditions:
a. National stock number
b. Nomenclature
c. Specification with revision and amendment number (if applicable)
MIL-STD-3004C
78

d. Qualification Number (if applicable)
e. Contractor and contract number
f. Product batch, lot number or emulsion number
g. NATO code (if applicable)
h. Military symbol (if applicable)
i. Date of filling
j. Weight or volume of contents
k. Filling activity/ telephone number
l. Safety and use markings (when applicable)
5.14.6.12 Marking of boxes and cartons. Minimum markings shall also be shown on boxes and
cartons.
5.14.6.13 Marking of contractor supplied product. Packaged oils and lubricants supplied by
contractors shall be marked in accordance with MIL-STD-290, or in accordance with provisions of the
contract.
5.14.6.14 Marking of used drums. When used drums are refilled in the field all old drum markings
shall be completely obliterated and drums thoroughly cleaned before being filled. The filled drums are to
be marked as required in 5.14.6.11. Total capacity is 57.2 USG; however, to allow for adequate vapor
space the drums shall be filled as follows:
a. 54 USG, maximum, for products which flash at 27 C (81 F) or less.
b. 55 USG, maximum, for products which flash over 27 C (81 F).
5.14.7 Deterioration of products.
5.14.7.1 Lubricating oils and gear oils. Most of these oils are procured as packaged products;
however some are also procured and shipped in bulk. Those composed entirely of mineral oils, including
those with additives such as viscosity index improvers, pour point depressants, or detergents, are very
stable. If the package remains unbroken and airtight, the oil will remain on-specification for a long
period of time. Storage guides and factors contributing to deterioration and contamination of packaged
oils are contained in 5.14.6. Guides and precautions pertinent to sampling are discussed in 5.14.2.
a. Most existing specifications for oils do not establish a quantitative limit for water content since
none should theoretically be present. At the time of packaging, water content is at a negligible level.
However, it is possible for a container to breathe air through the closures over a period of time, thus
introducing atmospheric moisture into its contents. Very small amounts of water can usually be detected
by cloudy or hazy appearance.
b. Engine lubricants and gear oils are required to pass ASTM D 892, Foaming Characteristics of
Lubricating Oils, which limits the amount of aerated foam in terms of foam tendency and foam stability.
This tendency towards foaming is undesirable since it reduces lubricant flow to bearings/gears and
decreases the thickness of the fluid film under hydrodynamic lubrication environments. To eliminate
this, trace amounts of antifoam additives are added which shall be uniformly dispersed to be effective for
controlling foam. Under storage conditions these dispersed antifoam additives may coalesce or stratify,
which decreases their effectiveness significantly by allowing high foaming values under ASTM D 892.
MIL-STD-3004C
79

In actual use environments the high mechanical shear induced by gear/bearing activity re-disperses the
antifoaming agent so satisfactory foaming control is attained. To ensure against premature failing of
samples because of the coalescence tendency, ASTM D 892 includes a pre-agitation requirement prior to
sample analysis that involves mixing in a Waring-type blender.
5.14.7.2 Hydraulic fluids. Some hydraulic fluid specifications such as MIL-PRF-5606, MIL-PRF-
6083, MIL-PRF-17672, MIL-PRF-46170, MIL-PRF-83282 and MIL-PRF-87257 contain particle
contamination limits which are so low the products are required to be packaged under clean room
conditions. Very slight amounts of dirt, rust, and metal particles will cause them to fail the specification
limit for contamination. Five gallon and fifty-five gallon containers are opened by removing bungs.
Quart and gallon containers are usually packaged in hermetically sealed containers, which should be
opened by means of a piercing type device. To minimize external contamination, it is recommended that
these containers are opened at the top of the vertical side rather than on the top. The act of opening any
container may allow more contaminants into the fluid than the specification allows. In opening the
container for use or evaluation it is extremely important that the can be opened and handled in a clean
environment. The area of the container to be opened shall be flushed with filtered solvent (petroleum
ether, mineral spirits or isopropyl alcohol). The device used for opening the container shall be
thoroughly rinsed with filtered solvent. After the container is opened, a small amount of the material is
poured from the container and disposed of prior to pouring the sample for analysis. Once a container is
opened, the unused portion shall be discarded. Military hydraulic fluids, particularly those using ester-
synthetic hydrocarbon base stocks, can absorb water. The amount of water absorbed shall be controlled
in order to prevent corrosion and other hydraulic system problems.
5.14.7.3 Deterioration of grease is usually indicated by bleeding or a change in texture, but neither
constitutes assurance the grease is beyond specification limits. Tests such as penetration, dropping point
and oil separation are necessary to make the determination.
a. Penetration is a method of measuring the consistency of grease. Consistency provides a means
for classification of greases in accordance with the National Lubricating Grease Institute (NLGI)
classification system. Most grease specifications contain a storage stability requirement which specifies
that after a certain period of time under prescribed environmental conditions, the grease shall comply
with all specification requirements except an expanded penetration. If the penetration is within the
storage stability limits, the grease is satisfactory for use.
b. Dropping point indicates the temperature at which grease passes from a semisolid to a liquid state
under the conditions of the test. It is not necessarily indicative of service performance. A change in
dropping point is an indication the consistency of the grease has changed.
c. Oil separating from grease, commonly known as bleeding, is characteristic of most grease. The
amount of bleeding varies with the composition of the grease, the size of the container and storage
conditions. A film of free oil does not preclude satisfactory use of grease. However, where an excessive
amount of free oil (pourable) is present, the grease shall not be used unless laboratory analysis confirms
its continued conformance to specification requirements.
d. Incompatibility between the seal elastomer and the grease may result in the failure of seals to
retain lubricating grease and exclude contamination. The deterioration of elastomer seals results in
failure of lubricity and causes a shortened bearing life.
e. Grease is formulated with various types of base oils, viscosity additives and thickeners. Some of
these greases freeze at extreme cold weather conditions that may result in failure of bearings and
MIL-STD-3004C
80

equipment. Most military greases will operate down to minus 54 C (minus 65 F), which reflects one of
the militarys global operability requirements. This property is often determined using the bearing torque
test or other rheological tests.
5.14.7.4 Insulating oils. Special precautions shall be taken to maintain insulating oils in first class
condition. Insulating oil is required to have a high dielectric strength. It shall be moisture free and
contain no foreign matter. If it is necessary to store insulating oils outdoors the containers shall be
protected from the weather. Containers shall not be opened or unsealed before the oil is actually required
for use. If necessary to open for test, the utmost precaution shall be taken against the entrance of
moisture or other foreign matter.
6. NOTES
(This section contains information of a general or explanatory nature that may be helpful, but is not
mandatory.)
6.1 Intended use. The purpose of this Standard is to establish common requirements for maintaining
quality during the receiving, storing and issuing of government-owned bulk and packaged petroleum
products and coal. This Standard is military unique because it covers internal government procedures for
the handling and storage of government-owned fuels under conditions not found in the commercial world
such as long term storage and special testing requirements.
6.2 International standardization agreement implementation. This standard implements NATO
STANAGS 1110, 3149, 7036, and AIR-STD-ACS (FG) 4021. When changes to, revision, or
cancellation of this standard are proposed, the preparing activity must coordinate the action with the U.S.
National Point of Contact for the international standardization agreement, as identified in the ASSIST
database at https://assist.daps.dla.mil (see Foreword, Paragraph 2).
6.3 Tailoring guidance. To ensure proper application of this Standard, invitations for bids, request for
proposals and contractual statements of work should tailor the requirements in sections 4 and 5 of this
Standard to exclude any unnecessary requirements.

6.4 Subject terms (key words) list.
Aviation turbine fuel
Barge
Bulk storage
STANAG
Coal
Diesel
F-76
Gasoline
Greases
Intra-Governmental receipt limits
Jet fuel
JP-5
JP-8
Packaged products
Petroleum
Sampling of petroleum
MIL-STD-3004C
81

Secured Fuels
Tanker
Truck
Waxes
6.5 Additional references. The following references are included to identify where additional
information may be found.
STANAG
STANAG 1110 Allowable Deterioration for NATO Armed Forces Fuels, Lubricants and
associated products
STANAG 1135 Interchangeability of Fuels, Lubricants and associated products used by the
Armed Forces of the North Atlantic Treaty Nations
STANAG 1385 Guide Specification (Minimum Quality Standards) for Naval Distillate Fuels
(F-75 and F-76)
STANAG 3149 Minimum Quality Surveillance of Petroleum Products
STANAG 3390 Guide Specification and Inspection Standards for Fuel Soluble Lubricity
Improvers
STANAG 3609 Standards for Maintenance of Fixed Aviation Fuel Receipt, Storage, and
Dispensing Systems
STANAG 3682 Electrostatic Safety Connection Procedures for Aviation Fuel Handling and
Liquid Fuel Loading/Unloading, Operations during Ground Transfer and
Aircraft Fueling/Defueling
STANAG 3747 Guide Specifications (Minimum Quality Standards) for Aviation Turbine
Fuel (F-34, F-35, F-40 and F-44)
STANAG 3967 Design and Performance Requirements for Aviation Fuel Filter Separator
Vessels and Coalescer and Separator Elements
STANAG 4107 Mutual Acceptance of Government Quality Assurance and Usage of the
Allied Quality Assurance Publications
STANAG 7036 Fuels to be Introduced into and Delivered by the NATO Pipeline Systems
(NPS)
STANAG 7063 Method of Detection and Treatment of Fuels Contaminated by Micro-
Organisms
STANAG 7090 Guide Specifications for NATO Ground Fuels

DEPARTMENT OF DEFENSE HANDBOOKS
MIL-HDBK-113 Guide for the Selection of Lubricants, Functional Fluids, Preservative, and
Specialty Products for Use in Ground Equipment Systems
MIL-HDBK-114 Fuels, Mobility, User Handbook
MIL-HDBK-844 Aircraft Refueling Handbook for Navy/Marine Corps Aircraft
UFC 3-460-01 Petroleum Fuel Facilities

MIL-STD-3004C
82

(Copies of this document are available online at https://assist.daps.dla.mil/ or from the Standardization
Document Order Desk, 700 Robbins Avenue, Building 4D, Philadelphia, PA 19111-5094.)
FEDERAL REGULATIONS
29 CFR Hazardous Communications Standard 29 Code of Federal Regulations
paragraph 1910.1200
(This publication is available from the Superintendent of Documents, US Government Printing Office
Washington DC 20402)
OTHER GOVERNMENT DOCUMENTS
AFI 31-101 The Air Force Installation Security Program
AFJMAN 23-209 Storage and Handling of Hazardous Material
AFMAN 23-110 USAF Supply Manual
CINCLNTFLT/ CINCPACFLT 4026 Fuel Management Afloat Manual
DLAI 4145.11/AFJMAN 23-209/TM 38-410/
MMCO 4450.12A/NAVSUP PUB 573/ Storage and Handling of Hazardous Materials
FM 10-13 Supply and Service Reference Data
FM 10-67-1 Concepts and Equipment of Petroleum Operations
FM 10-67-2 Petroleum Laboratory Testing and Operations
FM 10-70-1 Petroleum Reference Data
FM 101-10-1 Staff Officers Field Manual Organization, Technical and
Logistical Data Materials, Construction Effort, and
Personnel Requirements for Petroleum Storage and
Distribution; Vehicle Fuel and Lubricants Data; Bulk
Carrier Capacities; Estimating Class III Requirement;
Gasoline and Oil Supply Data for Various Organization
Units
NAVAIRINST 10350 (Series) Utilization of Aircraft Engine and Helicopter
Transmission Lubricating Oils
NAVAIR 00-80T-109 Aircraft Refueling NATOPS manual
NAVDOCKS P-342 Fuel Storage Tank Cleaning at the Shore Establishment
(Finished Product Tanks)
NAVPERS 10883 Fundamentals of Petroleum
NAVPETOFFINST 4025. Bulk Fuel and Lubricant Sources
NAVPETOFFINST 4025.2 Handling, Storing, Recycling, and/or Disposing of
Contaminated Low-Flash Petroleum Product
NAVSHIPS 0900-016-0010 Manual Cargo Tank cleaning
NAVSEA S9086- SN-STM-000/CH 541 Petroleum Fuel Storage and Use Testing
NAVSUP Manual, Volume II Supply Ashore
MIL-STD-3004C
83

NAVSUP Manual, P-485 Navy supply Systems Command Manual Afloat Supply
Procedures
NWP 38G Change 3 (Limited Distribution) Replenishment at Sea
UFC 3-460-03 Operations and Maintenance: Maintenance of Petroleum
Systems
(DLA and other Federal agencies may obtain copies of these documents from DLA Administrative
Support Center, 8725 John J. Kingman Road, STE 0119, Fort Belvoir, VA 22060-6220. The military
services should order these publications from their publication distribution office).
Air Force Technical Orders (T.O.)
T.O. 36-1-191 Technical and Managerial Reference for Motor Vehicle Maintenance
T.O. 36Y31-1-1 Removal of Rust and Sediment from Fuel and Oil Servicing Truck and
Trailer Tanks and Application of Coating, Interior, Fuel and Water
Resistant
T.O. 37A-1-101 USAF Fuel, Water, and Lubricant Dispensing Equipment
T.O. 37A2-2 Series Hose Carts, Type MH-1 and MH-2
T.O. 42B-1-1 Quality Control of Fuels and Lubricants
T.O. 42B1-1-1 Fuels for USAF Piston and Turbine Support Equipment and
Administrative Vehicles
T. O. 42B1-1-14 Fuels for USAF Aircraft
T.O. 42B1-1-15 NATO/ASIC Interchangeability of Aviation Fuels, Lubricants, and
Allied Products
T.O.42B1-1-22 Quality Control of Aviation Gasoline
T.O. 42B2-1-1 Uses and Grades of Aircraft Engine Lubricating Oils
T.O. 42B2-1-3 General - Fluids for Hydraulic Equipment
(Copies of these T.O.s can be obtained from the ETIMS Catalog listed online at
https://www.my.af.mil/gcss-af61/ETIMS/index.jsp or from DLA Administrative Support Center, 8725
John J. Kingman Road, STE 0119, Fort Belvoir, VA 22060-6220. The military services should order
these publications from their TO distribution system).
6.6 Changes from previous issue. Marginal notations are not used in this revision to identify changes
with respect to the previous issue due to the extent of the changes.
MIL-STD-3004C
84
TABLE I. Intra-Governmental receipt limits for aviation turbine fuels: NATO F-34/JP-8 (MIL-DTL-
83133), F-35/Jet A-1, Jet A (ASTM D1655), F-40/JP-4 and F-44/JP-5 (MIL-DTL-5624) and TS-1
(GOST 10227-86)
1

TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
2
ASTM TEST
METHOD
Existent Gum, mg/100 mL, max 7.0 14 D381
3

Vapor Pressure, kPa, @ 37.8
o
C (JP-4) 14.0-21.0 10.5-22.5 D323
Distillation, vol % recovered, @ 205
o
C,
min. (JP-5)
10 7 D86
Distillation, residue, vol %, max (JP-5,
JP-4)
1.5 2.0 D86
Flash point,
o
C, min
JP-5
JP-8,Jet A, Jet A-1
TS-1

60
38
28

60
38
28
D56, D93, or D3828
4

Microseparometer rating D3948, D7224
With (additives):
AO & MDA
AO & MDA & FSII
AO & MDA & CI/LI
AO & MDA & FSII & CI/LI

90
85
80
70

60
5

Particulate matter, mg/L, max D2276, D5452, or
Appendix B of MIL-DTL-83133

Aircraft servicing (AF/Army/Navy) 1.0 0.5/2.0/2.0
Intra-Governmental transfer 1.0 2.0
6, 7

Intra-Governmental transfer to USAF 1.0 1.5
Filtration time, minutes, max.
JP-4 10 15 Appendix A of MIL-DTL-5624
JP-5 (No reducer ring) 15 20 Appendix A of MIL-DTL-5624
JP-8 15 20 Appendix A of MIL-DTL-5624
FSII, Vol. %, D5006
JP-4, JP-5, JP-8, TS-1 0.10-0.15 0.09-0.20
Conductivity, pS/m (JP-4, JP-8) 150-600
8
50-700 D2624
Appearance C&B C&B
9

Peroxide Number, mg/kg (ppm), max
10
8.0 16.0 D3703
NOTES:
1 All required tests must be performed (see Tables XII-XIII). For test requirements not in this table specification limits
apply
2 For limits for Secured Fuels see Table XIII.
3 See 5.10.2.1
4 Test Method ASTM D56 may give results up to 1
o
C (2
o
F) below the ASTM D93 results. ASTM D3828 may give results
up to 1.7
o
C (3
o
F) below the ASTM D93 results. Method IP170 is also permitted; may give results up to 2.2
o
C (4
o
F below
the ASTM D93 results.
5 Microseparometer will not be run if turbine fuel contains static dissipater additive. Intra-Governmental Receipt Limit is
60, only for fully additized product (except static dissipater). Lower-than-spec results with other additive combinations
will require identifying the situation and communicating with DLA-ENERGY-QA.
6 Where products may be received through a fixed-placed filter vessel, the limits apply to the sample taken after the receipt
filter. Samples taken before the receipt filter are for information purposes only. Notify the local OAR for any
investigation and/or corrective action (info the DLA-ENERGY Region Quality Manager).
7 For Navy use only. Particulate matter of 8.0 mg/L, maximum, is acceptable for usage on transfers from shore tankage to
pier side manifolds; fleet oilers, barges, tankers, and U. S. Naval vessels.

MIL-STD-3004C
85
TABLE I. Intra-Governmental receipt limits for aviation turbine fuels: NATO F-34/JP-8 (MIL-DTL-83133),
F-35/Jet A-1, Jet A (ASTM D 1655), F-40/JP-4 & F-44/JP-5
(MIL-DTL-5624) and TS-1 (GOST 10227)
1
- Continued
TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
2
ASTM TEST
METHOD
NOTES:
8 The conductivity must be between 150 and 600 pS/m for JP-8 (F-34) and JP-4 (F-40); and 50-600 pS/m for Jet A, Jet A-1 (F-35), at
ambient temperature of 29.4
o
C (85
o
F), whichever is lower, unless otherwise directed by the procuring activity. JP-8 with thermal
stability improver additive, the conductivity limit must be between 150 and 700 pS/m at ambient temperature or 29.4
o
C (85
o
F),
whichever is lower, unless otherwise directed by the procuring activity. The US Navy does not use conductivity additives.
Conductivity additive is only added to JP-5 when product is used for issue or purging of Air Forces tactical aircraft.
9 Clear and Bright at ambient temperature, as measured where the sample is taken. If the product is not Clear and Bright at ambient
temperature, this test will be conducted at 70 F. An investigation would become necessary should the product Iail at 70 F. Steps
should be taken (particularly pipeline operations) to confirm that hazy conditions are a result of water and not air. To make this
determination: collect a sample of the product in question in a clean, clear glass bottle, place the sample on a flat surface and
ascertain as to whether the bubbles in the product rise or fall. In cases where the bubbles rise, the hazy condition is a result of air in
the product and should not be a cause for rejection. Further investigation may be warranted, but this simple test may prevent
unfounded product rejections.
10. Only for Jet A stored in long term storage in accordance with Table VIII.
TABLE II. Intra-Governmental receipt limits for fuel system icing inhibitor, MIL-DTL-85470, NATO
S-1745
1
TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
ASTM TEST
METHOD
Total water, mass. %, max. 0.10 0.40 D1364
NOTES:
1 All required tests must be performed (see Table XXII, B-2 requirements). For test requirements not in Table XXII,
specification limits apply.
TABLE III. Intra-Governmental receipt limits for fuel, naval, distillate, NATO F-76, (MIL-DTL-16884)
1
TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
ASTM TEST
METHOD
Color, ASTM, max. 3 4
2
D1500
Ash, mass %, max. 0.005 0.010 D482
Distillation D86
3
90% evaporation, C 357 360
End point, C 385 388
Water & sediment, vol. %, max. 0.05 0.1 D2709
Particulate contamination, mg/L, max. 10.0 15.0
4
D6217 or D5452
Storage Stability total insoluble,
mg/100 mL max.
3.0
1.5
6.0
5
3.0
6

D5304
D2274
NOTES:
1 All required tests must be performed (see Table XV). For test requirements not in this table specification limits apply.
2 See 5.10.6.2.
3 As the end point of the distillation is approached, if either a thermometer reading of 385 C or a decomposition point is
observed, discontinue the heating and resume the procedure as directed in ASTM D86.
4 Shoreside-use only.
5 Storage Stability results greater than 3.0 mg/100 ml. shall be reported to DLA-ENERGY-QA.
6 Storage Stability results greater than 1.5 mg/100 ml. shall be reported to DLA-ENERGY-QA. This test is performed on the
finished product. When ASTM D2274 is utilized, the test period shall be extended from 16 hours to 40 hours.

MIL-STD-3004C
86

TABLE IV. Intra-Governmental receipt limits for fuel oil, diesel, ASTM D975
1
TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
ASTM TEST
METHOD
Ash, mass %, max 0.01 0.025 D482
Distillation, C D86
90%, vol., Recovered
Grade No.1-D S15 or No.1-D
S500
288 293
Grade No.2-D S15 or No.2-D
S500

min. 282 277
max. 338 343
NOTES:
TABLE V. Intra-Governmental receipt limits for fuel oil, diesel, F-54
1

TEST
REQUIREMENTS
SPECIFICATION
LIMITS
RECEIPT
LIMITS
ASTM TEST
METHOD
Ash, mass %, max 0.01 0.025 D482
Color, max 5 6 D1500
Particulate contamination, mg/L, max. 10 20 D6217
EN12662
2

Flash Point, C (F), min 56(133) 55 (131) D93
Distillation, D86
%v/v recovered at 180
o
C (356
o
F),
max vol.,

10

12

% v/v recovered at 340
o
C (644
o
F)
min

95

93

Oxidation Stability, mg100mL,max
3

1.5 2.5 D2274
EN12205
3

NOTES:
2. Total contamination requirement for F-54 is max 24 g/m
3
as per EN12662.
3. Total oxidation stability n requirement for F-54 is max 25 g/m
3
as per EN12205.

MIL-STD-3004C
87
TABLE VI. Intra-Governmental receipt limits for gasoline, unleaded, NATO F-67, and STANAG 7090
1

TEST
REQUIREMENTS
SPECIFICATION
LIMITS (/F-67)
RECEIPT
LIMITS
ASTM TEST
METHOD
Color Clear Note
2
Note
3

Existent gum, mg/100mL, max. 5 7 D381
Octane number, motor/research, min. 85.0/95.0 D2700/D2699
Vapor Pressure, kPa D5191
Class A 45.0-60.0 43.0-62.0
Class B 45.0-70.0 43.0-72.0
Class C/C1 50.0-80.0 48.0-82.0
Class D/D1 60.0-90.0 58.0-92.0
Class E//E1 65.0-95.0 63.0-97.0
Class F/F1 70.0-100.0 68.0-102.0
Distillation, vol %, evaporated D86
Class A @ 70
o
C
@100
o
C
@150
o
C
Final boiling pt. (
o
C)
20.0-48.0
46.0-71.0
75.0, min
210
18.0-50.0
44.0-73.0
73.0,min
204

Class B @ 70
o
C
@100
o
C
@150
o
C
Final boiling pt. (
o
C)
20.0-48.0
46.0-71.0
75, min.
210
18.0-50.0
44.0-73.0
73.0, min
204

Class C/C1 @ 70
o
C
@ 100
o
C
@ 150
o
C
Final boiling pt. (
o
C)
22.0-50.0
46.0-71.0
75.0, min.
210
20.0-52.0
44.0-73.0
73.0, min.
204

Class D/D1 @ 70
o
C
@100
o
C
@150
o
C
Final boiling pt. (
o
C)
22.0-50.00
46.0-71.0
75.0,min
210
20.0-52.0
44.0-73.0
73.0, min.
204

Class E/E1 @ 70
o
C
@100
o
C
@150
o
C
Final boiling pt. (
o
C)
22.0-50.0
46.0-71.0
75.0, min.
210
20.0-52.0
44.0-73.0
73, min.
204

Class F/F1 @ 70
o
C
@100
o
C
@150
o
C
Final boiling pt. (
o
C)
22.0-50.0
46.0-71.0
75.0, min.
210
20.0-52.0
44.0-73.0
73.0, min.
204

NOTES:
1 All required tests must be performed (see Table XIV). For test requirements not in this table specification limits
apply.
2 See paragraph 5.10.3.2.
3 Test method is Method 103.6 in FED-STD-791.

MIL-STD-3004C
88
TABLE VII. Intra-Governmental receipt limits for automotive spark ignition engine fuel, ASTM D 4814
and gasohol, automotive, unleaded, A-A-52530
1

TEST REQUIREMENTS SPECIFICATION
LIMITS

RECEIPT LIMITS
ASTM TEST
METHOD
Existent gum, mg/100mL, max
2
5 6 D381
Antiknock index, min
3

Limited Grade 87 86
D2700/D2699
Regular Grade 89 88
Premium Grade 91 90
Vapor Pressure, kPa, max
1, 2

D4953, D5190,
D5191
Class AA 54 57
Class A 62 65
Class B 69 72
Class C 79 82
Class D 93 96
Class E 103 107
Alcohol, contents, vol. %, max
4
10 11 D4815 / D5599
Water tolerance, C See Table X8.1
ASTM D4814
+1 from maximum
temperature for
phase separation, C
listed in Table X8.1
ASTM D4814
Note
5

NOTES:
1 All required tests must be performed (see Table XIV). For test requirements not in this table specification limits
apply.
2 Value shown for gasohol based on the values of the base gasoline. (see 5.10.4.5 for VP).
3 Average of research and motor octane numbers or (R+M)/2.
4 These requirements only apply to gasohol.
5. Maximum temperature allowable before separation into two phases by addition of 0.1 % water.
TABLE VIII. Minimum frequency for testing long term storage of petroleum products
PRODUCT
DESCRIPTION
MINIMUM TESTING FREQUENCY
(MONTHS)
BULK PACKAGED
Gasoline, Aviation 6 6
Gasoline, Automotive
2
6 12
Turbine Fuels, Aviation
2
6 12
Diesel Fuels 6 12
Kerosene 6 12
Fuels, Burner 6 12
Fog Oils 6 12
NOTES:
1. A product is considered dormant when either one of the two conditions exit-the product has remained within a
storage tank for the period indicated without turnover of at least two-thirds of the tank content or stocks where new
product has not been received into existing stocks for 6 months.
2. Product stored in collapsible containers shall be tested every month as a minimum.

MIL-STD-3004C

89

TABLE IX. Minimum sampling and testing requirements for petroleum products.
SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS 9
1 Upon procurement at: refineries,
blending installations, etc. and at
main installations including
national depots & ocean-
importing points on establishment
of new batches.
Bulk Before acceptance of
new material and after
establishment of new
batch.
Upper, middle, and lower
composite, or all-level
composite from each
storage tank.
A

Samples shall be retained
IAW solicitation, contract
and/or QCP requirements.
2 / Storage tanks and pipelines, for
Pipeline Shipments or Vessel
Loadings of Government Stocks.
For all stock locations and
operations, at the direction of
the QAR, and with the
concurrence of DLA-
ENERGY-QA, additional
sampling and testing maybe
required as the conditions
warrant.
2a Storage tanks Bulk Before shipment or
loading
composite from each
storage tank.
Appearance, API
gravity, color, flash
point, particulate
content, filtration
time, FSII, water
reaction (as
applicable)
Government-owned stocks in
tanks that have been tested
previously within 90 days
need only Type C. Referee
sample will be retained.
3 Pipelines Bulk Before start of loading
and after line pack
operations
Line sample C for Dedicated Line.
B for Common Line
Test results should be within
reproducibility of shipping
tank
3a Pipelines Bulk Immediately after start
of shipment or loading
Line sample, downstream
of filter
C
3b Pipelines Bulk Hourly after starting
shipment or loading
of filter
Visual, plus additive
analysis for FSII &
SDA, if line injected

3c Pipelines Bulk During Loading or
Shipment
Representative line
Composite IAW API
MPMS, Chapters 8.1 or
8.2.
Retained composite Sample to be retained as
Referee. Testing to be
conducted will be based on
the situation.
MIL-STD-3004C

90

TABLE IX. Minimum sampling and testing requirements for petroleum products. - Continued
SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS 9
4 Vessel loading
4a Tankers and barges
First-In
Bulk After receipt of line
displacement or 1 meter
in tank whichever is
greater
Spot C-plus
Particulate if
sample fails
appearance, and
additive
analysis for
FSII & SDA, if
line injected

4b Tankers and barges Dock
Pipeline

Bulk
Before Start of
Loading/After Line Pack
Operations
Line Sample C Test results should be within
reproducibility of shipping tank.
4c Tankers and barges Bulk After loading All-level from each
compartment
a. Appearance
and density

b. C

c. Conductivity
and FSII, as
appropriate
a. For Government owned product
only

b. Navy underway replenishment /
fueling at sea

c. (Only) For procurement and
government owned product where
SDA and FSII additives are line
injected, and ships composite fails
SDA and FSII additives values.
(Test each compartment). For
intermediate discharges, sample
remaining compartments and
retain till discharge at destination.
Volumetric composite of
cargo tanks
B-1 Vessel may sail after C Tests;
Remainder of tests to be completed
before arrival at next load or
discharge port.
MIL-STD-3004C

91

TABLE IX. Minimum sampling and testing requirements for petroleum products. Continued

SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS 9
4d Yard Oilers Bulk After Loading Volumetric composite of cargo tanks API, flash,
BS&W
Normally yard oilers are in dedicated
service and carry ships fuels.
5 Vessel discharge
5a Tankers and barges
(multi-product cargo)
Bulk Prior to discharge All level from each tank C If on-spec, discharge authorized.

Volumetric composite of each cargo
on board.
B-1 These tests will be performed prior to
or during discharge of cargo. In the
event the capability for testing does not
exist at the discharge point, a
composite sample from the vessel will
be retained, type B-1 tests performed
on an all-level sample taken from the
receiving tank. If receiving tank fails
spec requirements, perform B-1 tests
on the tanker retain composite sample
to determine the cause of the off-spec
problem.
5b

Dock/discharge
manifold header

Bulk

During discharge

a. Sample IAW API MPMS, Chapter
8, commencing one half hour after
start of discharge and each hour after
until completion of the discharge.
One-half quart to be taken each time.
Sample to be composited after
completion of discharge.

b. Also, USG at one hour, midpoint,
and one hour prior to completion.
a. Particulate
and Retained
composite

b. Particulate
3

a. Retained for referee tests.

b. For barge receipts directly into A.F.
bases, refer to agreement of minimum
standards.
5c After receipt of fuel by
waterborne transport.
Bulk After receipt of
fuel.
Upper, middle, and lower composite,
or all-level Composite. (from each
storage tank)
Type B-1 Also, Thermal Oxidation Stability
testing after turbine fuel receipt by
tanker.
5d Shipboard JP-5
De-fuels for return to
Defense Working
Capital Fund inventory
Bulk Before Discharge Upper, middle, and lower composite
or all-level composite (from each
storage tank).
Type B-1 plus
thermal
oxidation
stability testing

MIL-STD-3004C

92


SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS 9
5e Shipboard F-76
De-fuels for return to Defense
Working Capital Fund inventory
Bulk Before Discharge Upper, middle, and lower
composite or all-level
composite (from each
storage tank).
Type B-1

6

Pipeline/TC/TT receipts.

6a During pipeline
receipt
Bulk During receipt at
custody transfer point
Representative Line
sample, IAW API MPMS,
Chapter 8
(5 gallon minimum)

Retain sample for 45 days.
Retained sample to be used as
referee sample if testing of
receipt tank fails.

6b After receipt of fuel via multi
product pipeline
Bulk After receipt of fuel Upper, middle, and lower
composite. (from each
storage tank)
Type B-1

6c TC/TT receipt Bulk Prior to discharge Representative sample
from each compartment
Visual
6d TC/TT receipt Bulk During receipt at
custody transfer point
Line sample, after line
displacement
Type C
11
First TC/TT of the day will
sampled from each supplier or
new batch.
6e After receipt of fuel via a
dedicated mode.
Bulk After receipt of fuel. Upper, middle, and Lower
composite. (from each
storage tank)
Type C, except
on initial filling
or change of
grade then, B-1
is required.

7 Transfers within installation or
depot

7a Receiving Tank: Through a
dedicated system.
Installations
and Depots
After receipt of fuel Upper, middle, and lower
composite.
Type C Samples will be retained for 45
days for referee purposes.
7b Through a common system. Installations
and Depots
After receipt of fuel. Upper, middle, and lower
composite.

Type B-1 Samples will be retained for 45
days for referee purposes.
MIL-STD-3004C

93


SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS 9
7c Receiving Tank/Initial fill or
Product Conversion
Installations
and Depots
Initial fill or product
conversion/
composite, or all- level
composite
Type B-1
8 Long term storage wherever
located.
Bulk Periodically, as required by
Table VIII.
composite or all-level
composite (see remarks).
B-2 or A (see
remarks)
a. Separate samples; upper, middle,
and lower shall be taken and tested
to establish homogeneity. If
homogenous these samples shall be
mixed for required tests. If not,
perform B-2 tests on each level of
product.
b. Additional tests may be
performed at the discretion of the
owning or custodial authority, with
regard to type of product, age of
stock, conditions of storage, etc..
9 Filling Points for road and
rail tank car containers, or
other equipment.
Bulk Daily on first container
filled, and on changeover to
fresh feed tank after comple-
tion of line displacement
from the fresh feed tank.
of filter
Type C
9 Filling Points for road and
rail tank car containers, or
other equipment.
Bulk Daily on first container
filled, and on changeover to
fresh feed tank after comple-
tion of line displacement
from the fresh feed tank.
of filter
Type C
10 In rail tank cars, Inter-Modal
Containers (ISO-Containers),
and road tank vehicles and
refuelers used in over the
road transportation
Bulk Both after loading and
before discharge
All level sample from the
rail car or vehicle.
Appearance on
each
compartment
Type C on
composite
Note
5
Road vehicles with multi-
compartments shall have sample
obtained (proportional) from each
compartment sufficient to permit a
quart sample. If product contains
additives (FSII and /or SDA), which
have been line injected, then each
mode of transportation shall be
tested for FSII.
MIL-STD-3004C

94


SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2,4
REMARKS9
11 Tanks containing interface
mixtures from pipeline for re-
injection.
Bulk Before re-injection Upper, middle, and lower
composite.
Type B-3 Re-injection of interface product
is to be under the technical
control of the pipeline authority,
or IAW with O.A.
12 Packaged fuel stocks wherever
stored
Packaged (a) Periodically as
required by Table VIII.
(see remark)
(b) When contamination
or deterioration of
product is suspected.
(c) When identity is
uncertain.
Representative sample
IAW API MPMS, Chapter 8
Type B-2
6
Where an agreed inspection
period has not been stipulated
the product is to be inspected at
least annually.
13 Refueler trucks, skid mounted
refuelers, or other dispensing
equipment.

Note: If the product is
Capitalized these instructions are
to be followed. If the product is
non Capitalized then individual
service technical guidance is to be
followed.
Bulk (a) Daily

(b) Monthly
7

(a) Drain sample taken
from sump.

(b) Line sample,
downstream of filter. After
re-circulation of fuel.
See remarks (a) Check for (visual) color and
appearance.,

(b) Laboratory analyses for
water & Sediment
10

14 Collapsible fabric tanks (bags)
and drums on the establishment
of tactical refueling systems.

followed.
Bulk (a) Initial fill and before
issue

(b) Daily - before issue

(c) Monthly
7

(a) After the filter-separator

(b) After filter-separator.
Note: After re-circulation of
fuel prior to the first
refueling of the day.

(c) After filter separator
See Remarks

(a) API, visual check for
appearance, water, sediment and
fiber (Aqua-Glo or AEL and
filter membrane color rating for
turbine fuels)
(b) Visual check for color,
appearance, free water (Aqua-
Glo or AEL for Turbine
Fuels)and particulates (AEL or
equivalent)
(c) Laboratory analysis for water
and sediment.
10

MIL-STD-3004C

95


SERIES
LOCATION OF
STOCKS
TYPE
STORAGE
WHEN
SAMPLED
TYPE
SAMPLE
1

TESTING
REQUIRED
2
REMARKS
15 Collapsible fabric tanks (bags)
and drums used for wholesale and
retail other than series 13 above
(Aviation and Ground fuel)
followed.
Bulk (a) Initial fill-before
issue-Note: after
recirculation of fuel

(b)Daily-before use,
Note: after recirculation
of fuel prior to the first
refueling of the day.

(c)Monthly
7

(a)After the filter-separator

(b)After the filter-separator

(c)After the filter-separator
B-1

(b) C and See
Remarks

(c) See Remarks

(b) Aviation Turbine Fuels
containing additives be
checked for FSII and
conductivity.

(c) Laboratory analysis for
sediment and water.
10
NOTES:
1. Use the API MPMS for sampling methods (see 4.7).
2. See Tables X through XXII for the types of test required on the various products. The legend for the types of testing required is as follows:
a. Type A Test - Complete specification, Water separation index, modified, testing is not performed if the fuel contains conductivity additive (DO NOT PERFORM DOWNSTREAM
OF SDA INJECTION.
b. Type B-1 Test - Partial analysis comprising the checking of principal characteristics most likely to have been affected in the course of moving the product.
c. Type B-2 Test - Partial analysis to check characteristics susceptible to deterioration because of age.
d. Type B-3 Test - Partial analysis for contamination; in particular, for controlling the return (or reintroduction) of pipeline interface products.
e. Type C Test Quick, simple, partial analysis for verification of product quality, to ensure that no change has taken place.
3. The average particulate content of the 3 fuel samples should not exceed 2 mg/L; however, the first and last samples are obtained under severe discharge conditions they may show high
particulate content. Solid contamination while extremely objectionable is a physical contaminant which can be removed under proper conditions with proper equipment, and since the product at
this point is Government owned, discharge operations will not be discontinued for this reason. However, the contracting officer, DLA Energy, and the Quality Assurance Representative at the
loading point will be advised of any high particulate results obtained. This information will be used for future planning purposes and for determining possible cleaning actions necessary on the
vessel involved. This note is not applicable to internal Navy transfers.
4. Flash Point at the receiving point is not required for product that is to be use by the U.S. Army. This fuel is tested in accordance with Army quality surveillance program AR 710-2.
5. If unable to take an all-level sample from the compartment prior to discharge, then take an in-line sample at or near the off-loading header during the discharge, immediately upon product
displacement of the receipt manifold/hose.
6. No receiving tests are necessary on packaged products, provided the containers are intact and markings adequately identify the product.
7. Filter-separator performance is to be checked every 30 days.
8. For retaining of samples (storage) see E28 Contractor Inspection Responsibilities.
9. Testing maybe complete specification testing or an individual test based on the request of the Government Representative.
10. When laboratory tests of material from dispensing and handling equipment show evidence of free water or a sediment level exceeding 0.5 mg/L for aviation fuels (2.0 mg/L for U.S. Army
and U.S. Navy), or 10.0 mg/L for diesel fuel, that equipment shall be re-sampled and dead lined pending laboratory confirmation of the initial results. If the second laboratory analysis confirms the
presence of free water or sediment exceeding the above limits, improvement in fuel quality must be made.
11. For aviation delivery, FSII and SDA will be tested where capability exists.

MIL-STD-3004C

96

TABLE X. Tests required aviation gasoline.

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST
Appearance
1
X X X X
Particulate matter
2,3
X X X
Color (Visual) X X X X
Density or API gravity X X X X
Distillation X X X
Copper strip corrosion X X X
Existent gum X X
Vapor pressure X X
Water reaction

X X X
Lean mixture rating
4
X X X
Rich mixture rating
4
X X
Lead content X X
Potential gum X
NOTES:
1 Obtain sample in a clear round one quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check
for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of
the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of
contaminated fuel).
2 Perform only if visual sediment is present.
3 AVGAS samples will be checked for solids and water. When no laboratory is available to perform these tests, solids will
be determined visually upstream of filter-separators and by the particle assessment method downstream of the filter separator.
4 Perform only if Lead content was performed and failed the specification requirement. If the capability does not exist to
perform this test at the terminal, a sample will be sent to the nearest Service laboratory that does have the capability. In the
event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be
made; however, when laboratory results indicate failure, notify DLA-ENERGY-QA.

TABLE XI. Tests required lubrication oils
1, 2
PROPERTIES B-1 TEST C TEST
Appearance (to include visual sediment & water) X X
Emulsion test
X
3

Gravity X X
Viscosity
X
4,

Flash point X
Foam test X
Water (by centrifuge) X
4
X
5

Solid contaminants X
NOTES:
1. For application of these tests see Table IX.
2. B-2 tests are listed in Tables XVII-XX.
3. Only if the specification has this requirement.
4. For MIL-PRF-17331 and MIL-PRF-9000 viscosity is not required unless the tank has
been dormant for 3 months and water (by centrifuge) is only required if the oil fails
appearance because of water contamination (cloudiness).
5. Is only required if the oil fails appearance because of water contamination (cloudiness).

MIL-STD-3004C

97

TABLE XII. Tests required aviation turbine fuels.

PROPERTIES B-1
TEST
B-2
TEST
B-3
TEST
C
TEST
Appearance
1
X X X X
Color (visual) X X X X
Particulate matter X X X
Distillation X X X
Freezing point X X X
Existent gum X X X
Vapor pressure (JP-4 only) X X X
Flash point (except JP-4) X X X X
Water reaction
6
X X X
Lead content (If contaminated with leaded fuels suspected) X X X
Fuel system icing inhibitor
2
X X X
Filtration time X X X
Water separation index (JP-4 and JP-8)
3, 4
X X X
Conductivity (JP-4 and JP-8)
5
X X X
Thermal stability (B-1 requirement applies only to JPTS
and marine mode receipt tank sample)
X X
Color (Saybolt) X
Acid number X
NOTES:
1 Obtain sample in a clear round one quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the
point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of the contaminant (a spot larger than 3
mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).
2 If product contains FSII, product should be check on delivery into a bulk storage tank and every month thereafter if stock remains dormant,
and no deliveries have been made into the tank.
3 If the capability does not exist to perform this test at the terminal, a sample will be sent to the nearest Service laboratory that does have the
capability. In the event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be
made, however, when laboratory results indicate failure, notify DLA-ENERGY-QA.
4 Water separation index, modified, testing is not performed if the fuel contains conductivity additive.
5 If fuel contains conductivity additive, CU readings should be taken within two minutes of sampling.
6 Not performed on JP-5.
TABLE XIII. Support for Secured Fuels.
1

JP-5 Jet A Jet A-1 JP-8
CHARACTERISTIC
LIMITS

Min.

Max.

Min.

Max.

Min.

Max.

Min.

Max.
Gravity, API @ 60 F
D 1298/D 4052
36 48 37 51 37 51 37 51
Density at 15 C (kg/m
3
) 788 845 775 840 775 840 775 840
Weight: lb/USG
Calculated
6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0
Distillation (C)
D 86

10% Recovered 205 205 205 205
20% Recovered RPT RPT
50% Recovered RPT RPT RPT RPT
90% Recovered RPT RPT RPT RPT
Final Boiling Point 300 300 300 300

MIL-STD-3004C

98

TABLE XIII. Support for Secured Fuels.
1
- Continued

JP-5 Jet A Jet A-1 JP-8
CHARACTERISTIC
LIMITS

Min.

Max.

Min.

Max.

Min.

Max.

Min.

Max.
Freezing point, C
D 5972/D 2386
-46 -40 -47 -47
Flash point, C
D 93/D 56
60 38 38 38
Particular Matter (mg/L)
D 5452
0.5 0.5 0.5 0.5
Conductivity (pS/m)
D2624

Report Report 50 700
Copper strip corrosion
D 130
1 1 1 1
Water reaction

D 1094
1b
Existent gum (mg/100 mL)
D381
7.0 7.0 7.0 7.0
FSII, (vol %)
2

D 5006
0.07 0.20 0.07 0.20
Thermal Stability
D 3241

Change in pressure drop,
mm Hg

25

25

25

25
Heater tube deposit, visual
rating
<3 <3 <3 <3
Appearance
4

NOTES:
1. DLA Energy Aviation Refueling Quality Assurance Procedures Related to Secured Fuel Support posted on DLA
Energy website (ELA Energy-Quality Assurance page) shall be used when conducting Secured Fuel missions.
2. Only FSII which meets specification MIL-DTL-85470, Inhibitor, Icing, Fuel System, High Flash, and NATO Code
Number S-1745 is to be used.
3. Water: Fuel must be clear and free of water on visual examination. Sample will be taken downstream of final filtration
of refueler or hydrant servicing equipment.

TABLE XIV. Tests required automotive gasoline.

Appearance X X X X
Color X X X X
Water and Solids (Visual Check) X X X X
Distillation X X X
Vapor pressure X X
Copper strip corrosion X X
Existent gum X X
1

Knock rating (RON and MON)

X
2
X
2

Oxidation stability X
Water tolerance
3
X X X
NOTES:
1 Unwashed gum, without solvent wash, shall not increase by more than 2 mg as compared to the original product. In
the event of gum increase exceeding 2 mg, a Type A test, as defined in the legend, will be run.
2 Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the
case of pipeline, this test shall be performed when considered necessary.
3 Gasohol only.
MIL-STD-3004C

99

TABLE XIVa. Tests required E85 (ASTM D5798)
1
.

Appearance X X X
Water X X X X
Ethanol Volume X X X X
Vapor Pressure X X X X
Higher Alcohols X
Sulfur X X
Acidity X
Solvent Washed Gum X X
pH X
Unwashed Gum X
Copper X X
NOTES:
1. For cleaning see 5.9.3.2

TABLE XV. Tests required diesel fuels and kerosene.
Appearance
1
X X X X
Color X X X X
Density and API gravity X X X X
Distillation X X
Flash point X X X X
Carbon residue
2

(F-76 only)

X

X

Cloud point X
Pour point X
Copper strip corrosion X
Cetane index X
3

Viscosity X
Water & sediment by centrifuge X
Particulate
(F-76 only)

X

X

Storage stability (F-76 only) X
Sulfur
4,5,6
X
NOTES:
1 For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D 4176,
procedure 1, then the product must meet the requirements of ASTM D 2709, 0.05 percent volume of water and sediment,
maximum. The fuel is acceptable for appearance if the water and sediment content is 0.05 percent volume or less. If the
sample fails ASTM D 4176, procedure 1, because it contains visible sediment or particulate matter, but meets the
requirement of 10 mg /L, maximum, in accordance with ASTM D 5452 or ASTM D 6217, then the fuel shall be considered
acceptable provided all other requirements are met.
2 Only required if change in color and/or density occurs after procurement.
3 Cetane Index can only be run if no ignition improvers are present. Otherwise, Cetane number shall be given.
4 Kerosene. Grade No.-1K only, if intended for non-flue connected burner.
5 Test to be performed if equipment is available.
6 Sulfur testing is required for ULSD or LSD believed contaminated with a higher sulfur content fuel.

MIL-STD-3004C

100

TABLE XVa. Test required on B20
Appearance
1
X X X X
Distillation

X X
Flash Point X X X X
Cloud Point or LTFT/CFPP X
Viscosity X
Copper Strip Corrosion X
Water and Sediment X
Sulfur X
Ramsbottom Carbon Residue X X
Particulate Content X X
Acid Number X
Ash Content X
Biodiesel Content X X X
Oxidation Stability X
NOTES:
1 Obtain a sample in a clear round one quart bottle, swirl the bottle vigorously so a vortex is formed. Visually check for
sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of
contamination.
TABLE XVI. Tests required burner fuel oils

B-1 TEST B-2 TEST B-3 TEST C TEST
Flash point X X X X
BS&W
1
(centrifuge)
X X X X
Density/API Gravity X X X X
Viscosity X X
Ash X
Carbon Residue X
Sediment by extraction X
Pour point X
TABLE XVII. Tests required on Residual Marine Fuel (RME 180 Grade)
Kinematic Viscosity X X X X
Density at 15
o
C

X X X X
Flash Point X X X X
CCAI X
Hydrogen Sulfide X
Acid Number X
Total sediment aged X X
Carbon Residue X
Sulfur X
Pour Point X
Water X X
Ash X
Sodium X

MIL-STD-3004C

101

TABLE XVIII. Tests required on Residual Marine Fuel (RME 380 Grade)
PROPERTIES B-1
TEST
B-2
TEST
B-3
TEST
C
TEST
Kinematic Viscosity X X X X
Density at 15
o
C X X X X
Flash Point X X X X
CCAI X
Sulfur X
Hydrogen Sulfide X
Acid Number X
Total sediment aged X X
Sulfur X
Pour Point X
Water` X X
Ash X
Sodium X

TABLE XIX. Test required on Marine Gas Oil (DMA Grade)
Kinematic Viscosity X
Density at 15 degree C X X X
Flash Point X X X X
Cetane Index X
Sulfur X
Oxidation Stability X X
Acid Number X
Carbon Residue X X
Sulfur X
Pour Point X
Appearance X X X X

MIL-STD-3004C

102

TABLE XX. Type B-2 tests for lubricating oils
CHARACTERISTICS SPECIFICATION
A-A-59113 A-A-59137 ANSI/AGMA
9005
DOD-L-81846 DOD-PRF-24574 DOD-PRF-85734 MIL-L-3918
Appearance / workmanship X X
Color X
Viscosity @ 100 C X
2
X X
2
X X
2

Viscosity @ 54 C
Viscosity @ 40 C X X X
2
X X
2
X
2

Viscosity @ -40 C X
Viscosity @ -54 C X
Relative density
Flash point X X X X X
Pour point X X X X X
Neutralization number (acid/base) X X
Corrosion & oxidation stability X X X
3

Evaporation loss X X X
Precipitation number
Ash
Emulsion
Foam test X X
Water content
Particulate content / trace sediment X X
Trace metals X
Carbon residue
Sulfur
Hydrolytic stability X
Minimum retest frequency (months) 36 24 24 24 36 36 24
Visual check frequency (months) 12
Military symbol(s) None None None None None None None
NATO Code Numbers None None None None None None None
MIL-STD-3004C

103

TABLE XX. Type B-2 tests for lubricating oils. Continued
MIL-L-11734 MIL-DTL-
46014
MIL-PRF-2104 MIL-PRF-3150 MIL-PRF-6081 MIL-PRF-6085 MIL-PRF-6086
Appearance / workmanship X X X X X
Color X X
Viscosity @ 100 C X
2
X
Viscosity @ 54 C X
Viscosity @ 40 C X
2
X
2
X X
2
X
2

Viscosity @ -40 C X
Viscosity @ -54 C X
3
X X
Relative density
Flash point X X X X X
Neutralization number (acid/base) X X X
Corrosion & oxidation stability X
3
X X X
3

Evaporation loss X X
Precipitation number X
Ash
Emulsion
Foam test X X
Water content
Trace metals
Carbon residue
Sulfur
Hydrolytic stability
Visual check frequency (months) 12 12 12 12 12
Military symbol(s) None None OE/HDO-10,
OE/HDO-30,
OE/HDO-40,
OE/HDO-15/40
OE/HDO-5/40
PL-M None OAI OGL, OGR
NATO Code Numbers None None O-237, O-238,
N/A, O-1236, N/A
O-192 O-133 O-147 O-153, O-155
MIL-STD-3004C

104

MIL-PRF-7808 MIL-PRF-7870 MIL-PRF-9000 MIL-PRF-17331 MIL-PRF-21260 MIL-PRF-23699 MIL-PRF-26087
Appearance / workmanship X X X
Color X X
Viscosity @ 100 C X X X X X X
2

Viscosity @ 54 C
Viscosity @ 40 C X X
2
X X X
2

Viscosity @ -40 C X X
Viscosity @ -54 C X
2

Relative density
Flash point X X X X X X X
Pour point X X X X X X
Neutralization number (acid/base) X X X X X
Corrosion & oxidation stability X X X
Precipitation number X X
Ash X
Emulsion X
Foam test X X X
4
X X X
Water content X
Particulate content / trace sediment X X X
Trace metals X X
Carbon residue X
Sulfur
Visual check frequency (months) 12 12 12 12
Military symbol(s) None None 9250 2190-TEP PE-10, PE-30,
PE-40, PE-15/40
None None
NATO Code Numbers O-148, O-163 O-142 O-278 O-250 C-640, C-642,
N/A, N/A
O-152, O-154,
O-156
None

MIL-STD-3004C

105

MIL-PRF-32033 MIL-PRF-46167 MIL-PRF-53074 MIL-PRF-87100 SAE J 1899 SAE J 1966
Color X
Viscosity @ 100 C X X X
2
X X
Viscosity @ 54 C
2

2

Relative density X X X
Flash point X X X X X X
Pour point X X X X X X
Neutralization number (acid/base) X X X X
Copper strip corrosion X X X X
Corrosion & oxidation stability
Ash X X X
Emulsion
Foam test X X X
Water content
Particulate content / trace sediment X X X
Trace metals X X
Carbon residue
Sulfur
Minimum retest frequency (months) 24 24 36 36 36 36
Visual check frequency (months) 12 12 12
Military symbol(s) PL-S OEA-30 5190, 5230 None Type II
Type III
1065, 1080, 1100, 1120
NATO Code Numbers O-190 O-183 None None None None

MIL-STD-3004C

106

MIL-PRF-32033 MIL-PRF-46167 MIL-PRF-53074
Appearance / workmanship X
Color
Viscosity @ 54 C
Viscosity @ -40 C
Viscosity @ -54 C X
Relative density
Flash point X X X
Pour point X X
Neutralization number (acid/base) X X
Evaporation loss X
Ash X
Emulsion
Foam test X
Water content
Particulate content / trace sediment
Trace metals
Carbon residue X
Sulfur
Minimum retest frequency (months) 24 36 24
Military symbol(s) GO-75/90, GO-80/90,
GO-85/140
RCO-2,
RCO-3, RCO-4
LAW
NATO Code Numbers O-186, O-226, O-228 O-283, O-290 O-157
MIL-STD-3004C

107

TABLE XXI. Type B-2 tests for greases, semi-fluids, lubricants, and other grease-like materials.
A-A-59173 DOD-G-24508 DOD-G-24650 MIL-G-14931 MIL-G-21164 MIL-G-25013
Odor X X X X
Penetration (un-worked) X
Penetration (worked) X X X X X
Worked stability X X X
Dropping point / melting X X X X X
Oil separation X X X
Evaporation loss / bleed X X X X X
Oxidation stability (100 hours) X
Rust preventive properties X X X
Water resistance X X X X
Fuel resistance
Free-acidity / free alkali
Molybdenum disulfide content X
Boiling water immersion
Water stability / emulsification
Water content
Dirt (particles) X X X X
Load carrying capacity

X
5
X
5

Minimum retest frequency (months) 24 24 24 24 24
Visual check frequency (months)
Military symbol(s) None None None None GMD None
NATO Code numbers None None None None G-353 G-372

MIL-STD-3004C

108

TABLE XXI. Type B-2 tests for greases, semi-fluids, lubricants, and other grease-like materials. - Continued
MIL-PRF-32033 MIL-PRF-46167 MIL-PRF-53074 MIL-L-15719 MIL-L-19701
Odor X X
Penetration (un-worked) X X X
Penetration (worked) X X X X
Worked stability X X X X
Dropping point / melting X X X X
Oil separation X X X
Rust preventive properties X X X X
Fuel resistance
Boiling water immersion X
Water content
Dirt (particles) X X X

X
5

Military symbol(s) None None None HTG None
NATO Code Numbers G-366 None None None None

MIL-STD-3004C

109

TABLE XXI. Type B-2 tests for greases, semi-fluids, lubricants, and other grease-like materials. - Continued
MIL-L-46000 MIL-L-46150 MIL-PRF-10924 MIL-PRF-18458
1
MIL-DTL-23549 MIL-PRF-23827
Odor X X
Worked stability X X
Dropping point / melting X X X
Oil separation X X X X
Copper strip corrosion X X X X X
4

Rust preventive properties X X X X
Water resistance X
Fuel resistance
Boiling water immersion X
Water content
Dirt (particles) X

X
5
X
5
X
5
X
5
X
5
X
5


Military symbol(s) LSA None GAA None None None
NATO Code Numbers O-158 None G-403 None None G-354

MIL-STD-3004C

110

TABLE XXI. Type B-2 tests for greases, semi-fluids, lubricants, and other grease-like materials. . - Continued
MIL-PRF-24139 MIL-PRF-27617 MIL-PRF-81322 MIL-PRF-83261 MIL-PRF-83363 MIL-PRF-85336
Odor X X
Penetration (un-worked) X X
Worked stability X X X X
Dropping point / melting X X
Oil separation X X X X
Evaporation loss / bleed X X X X X X
Oxidation stability (100 hours) X X X
Rust preventive properties X X
Fuel resistance X
Molybdenum disulfide content
Water stability / emulsification X
Water content
Dirt (particles) X X

X
5
X
5
X
5
X
5

Military symbol(s) None None None None None None
NATO Code Numbers None G-397, G-398,
G-399, G-1350
G-395 None G-396 None

MIL-STD-3004C

111

TABLE XXI. Type B-2 tests for greases, semi-fluids, lubricants, and other grease-like materials. . - Continued
SAE AMS-G-4343 SAE AMS-G-6032 VV-G-632 VV-G-671
2
VV-P-236
3
Appearance / workmanship X X X X
Odor X
Penetration (un-worked) X X
Penetration (worked) X X X
Worked stability
Dropping point / melting X X X X X
Oil separation X
Evaporation loss / bleed X X
Copper strip corrosion X X X X X
Oxidation stability (100 hours)
Rust preventive properties X
Water resistance
Fuel resistance
Free-acidity / free alkali X X
Molybdenum disulfide content
Water content X
Dirt (particles) X

X
5

6
12
Military symbol(s) None None None None None
NATO Code Numbers G-392 G-363 None G-412 S-743
NOTES:
1 Also volatile matter.
2 Also ash content.
3 Also neutralization number, viscosity & flash point.
4 Per time cited in specification.
5 If capability exists.
6 Examine each 6 months for hardening.

MIL-STD-3004C

112

TABLE XXII. Type B-2 tests for hydraulic, brake, shock absorber fluids

A-A-59290 A-A-59354 MIL-DTL-17111 MIL-H-19457
1
MIL-H-22072 MIL-H-81019
Color X X X
Composition
Viscosity @ 54 C X
Viscosity @ 40 C X
2
X X X X
2
X
Viscosity @ 25C
Viscosity @ -40 C X
2

Viscosity @ -54 C X
Low temperature stability
Flash point X X
Pour point X X X
Neutralization Number (acid/base) X X X X
Copper strip corrosion X
Corrosion & oxidation stability X
pH X X
Evaporation loss X X X
Water content X X X X
Foam test X X X X
Particulate content / trace sediment X
Ash X
Precipitation number X X
Rust prevention X
Emulsion X
Lubricity (steel-on-steel) X
4
X
4

Gel time
NATO Code None None H-575 H-580 H-579 None

MIL-STD-3004C

113

TABLE XXII. Type B-2 tests for hydraulic, brake, shock absorber fluids. - Continued
MIL-PRF-5606 MIL-PRF-6083 MIL-PRF-46170 MIL-PRF-17672 MIL-PRF-27601 MIL-PRF-46176 MIL-PRF-83282
Color X X X
Composition
Viscosity @ 100 C X X X X X
Viscosity @ 54 C
Viscosity @ 40 C X X X X X X
Viscosity @ 25C
Viscosity @ -40 C X X X X X
Viscosity @ -54 C X X X
2

Low temperature stability
Relative density
Flash point X X X X X X X
Neutralization Number (acid/base) X X X X X X
pH
Water content X X X X X X
Foam test X X X X X X
Particulate content / trace sediment X X X X X X
Ash X
Rust prevention
Emulsion X
Lubricity (steel-on-steel) X
4
X
4
X
4
X
4

Gel time
Visual check frequency (months) 12 12
Military symbol(s) OHA OHT FRH 2075-T-H, 2110-T-H, 2135-T-H None BFS None
NATO Code Numbers H-515 C-635 H-544 H-573 None H-547 H-537
MIL-STD-3004C

114

TABLE XXII. Type B-2 tests for hydraulic, brake, shock absorber fluids. Continued

MIL-PRF-87257 SAE AS 1241 SAE J 1703 VV-D-1078
Appearance / workmanship X X
Color X
Composition
2
X
Viscosity @ 54 C
2

Viscosity @ 25C X
Low temperature stability X
Relative density X X
Flash point X X
3
X
Pour point X X
Neutralization Number (acid/base) X X X
pH X
Evaporation loss
Water content
Foam test X X
Ash
Rust prevention
Emulsion
Lubricity (steel-on-steel)
Gel time
Minimum retest frequency (months) 24 36 24 24
Military symbol(s) None None None None
NATO Code Numbers H-538 None H-542 S-1714, S-1716, S-1718, S-1720, S-1724,
S-1726, S-1728, S-1732
NOTES:
1 Also, hydrolytic stability.
2 Per temperature in specification.

3 Fire point test characteristic also required.
MIL-STD-3004C

115

TABLE XXIII. Type B-2 tests for lubricants, (including solid film).
CHARACTERISTICS

SPECIFICATION
A-A-59004 DOD-L-25681 MIL-L-23398 MIL-L-24131 MIL-L-24478 MIL-L-45983 MIL-L-87177
1

Color
Odor X
Viscosity @ 100 C X
Viscosity @ 40 C X
Viscosity @ 0 C
Viscosity @ -54 C
Boiling point
Flash point X X
Pour point
Density / relative density
Composition X
Oil content X
Particle size X
Solids content X X
Ash X
Adhesion
Thermal stability
Endurance life

X
3

Minimum retest frequency (months) 12 24 Note
4
12 12 Note
4
24
Military symbol(s) None None None None None None None
NATO Code Numbers None S-1735

S-749 None None None None

MIL-STD-3004C

116

TABLE XXIII. Type B-2 tests for lubricants, (including solid film).- Continued
CHARACTERISTICS

SPECIFICATION
MIL-PRF-3572 MIL-PRF-46010 MIL-PRF-46147 MIL-PRF-63460 MIL-PRF-81329 SAE AS 87132
Color
Odor
Viscosity @ 100 C X
2

Viscosity @ 40 C
Viscosity @ 0 C X
2

Viscosity @ -54 C X
Boiling point
Flash point X X
Pour point X X
Density / relative density
Composition X
Oil content
Particle size X
Solids content X
Ash X
Adhesion X
Thermal stability X
Endurance life X

X
3

Minimum retest frequency (months) 24

Note
4
Note
4
36 Note
4
36
NATO Code Numbers None None None S-758 S-1737 None
NOTES:
1 Also, dielectric strength.
4 Discard 12 months from date of manufacture.
5 Discard 6 months from date of manufacture.

MIL-STD-3004C

117

TABLE XXIV. Type B-2 tests for waxes
A-A-50178 A-A-59255 C-T-91 MIL-W-10885 MIL-W-12062 MIL-W-12598 MIL-W-13945 MIL-W-20553
Odor X X X
Color X X
Melting point / solidification point X X X X X
Softening point X X X
Penetration X X X X X
Viscosity @ 100 C X X X X
Oil content X X X
Flash point X X X X
Ash X X
Water content X
Neutralization Number (acid/base) X X X X
Saponification number X X X
Volatile matter X
Minimum retest frequency
(Months)
36 36 48 36 36 36 36 36
Military symbol(s) None None None None None None None None
NATO Code Numbers None None None None None None None None

MIL-STD-3004C

118
TABLE XXV. Type B-2 tests for misc. products (specialty, cutting, anti-seizing, etc)
MIL-PRF-
32033
MIL-PRF-
46167
MIL-PRF-
53074
A-A-59197 ASTM D 3487
Viscosity @ 100 C
Viscosity @ 54 C
2
X
Viscosity @ 20 C
Viscosity @ -40 C
Viscosity @ -54 C
Relative density X
Distillation
Flash point X X X
Fire point
Pour point X X
Freezing point
Penetration (un-worked)
Penetration (worked)
Melting point
Protection
Corrosion X
Neutralization Number (acid/base) X X
Acidity
Lead corrosion
pH
Stability
Evaporation / bleed
Residue on evaporation
Ash
Foaming
Emulsification properties
Contamination / sediment
Water content X X
Dielectric strength X
Film appearance
Drying Rate
Particle size (fineness)
Surface and interface tension X
(months)
36 36 24
4

NATO Code Numbers None S-750 S-1736 None None

MIL-STD-3004C

119
TABLE XXV. Type B-2 tests for misc. products (specialty, cutting, anti-seizing, etc) - Continued
MIL-DTL-
4339
MIL-C-6529 MIL-C-11796 MIL-DTL-
5020
MIL-DTL-85470
1

Viscosity @ 100 C
Viscosity @ 54 C
Viscosity @ 40 C X
2

Viscosity @ 20 C
Viscosity @ -40 C
Viscosity @ -54 C
Relative density X
6

Distillation X
Flash point X
Fire point
Pour point
Freezing point
Melting point X
Protection X
Corrosion X X X
Neutralization Number (acid/base)
Acidity X
Lead corrosion
pH X X
Stability X X
Evaporation / bleed
Ash
Foaming
Emulsification properties X
Water content X
Dielectric strength
Film appearance
Drying Rate
Surface and interface tension
(months)
48 36 36 48 18
7
Military symbol(s) None None None FDC None
NATO Code Numbers C-630 C-608, C-
609, C-610
C-633 S-712 S-1745

MIL-STD-3004C

120
MIL-PRF-
8188
MIL-PRF-
12070
MIL-PRF-
16173
MIL-PRF-
46002
MIL-PRF-87252
Viscosity @ 100 C X X X X
Viscosity @ 54 C
Viscosity @ 20 C
Viscosity @ -40 C X
Viscosity @ -54 C X
Relative density
Distillation
Flash point X X X X
Fire point X
Pour point X
Freezing point
Melting point
Protection X
2

Corrosion X X X
Neutralization Number
(acid/base)
X
Acidity
Lead corrosion X
pH
Stability X
Evaporation / bleed X
Ash X
Foaming
Contamination / sediment X
Water content X
Film appearance X
Drying Rate X
(months)
36 12 36 24 24
Visual check frequency
(months)

Military symbol(s) None SGF-2 None None None
NATO Code Numbers C-638 None C-620, C-632 None S-1748

MIL-STD-3004C

121
MIL-T-
17128
SAE AMS
1424
SAE AMS
1428
SAE AMS
2518
SAE AMS-M-
7866
Viscosity @ 100 C X
Viscosity @ 54 C
Viscosity @ 40 C X
Viscosity @ 20 C X
Viscosity @ -40 C
Viscosity @ -54 C
Distillation
Flash point
Fire point
Pour point X
Freezing point X X
Melting point
Protection
Corrosion X X X
Neutralization Number
(acid/base)
X
Acidity
Lead corrosion
pH X X
Stability
Ash
Foaming
Water content
Dielectric strength
Film appearance
Drying Rate
Particle size (fineness) X
(months)
36 Note
5
Note
5
36 36
Visual check frequency
(months)
12
NATO Code Numbers None S-1717 S-1719, S-1723 S-720 S-740

MIL-STD-3004C

122
SAE AS 8660 O-M-232 SS-G-659 TT-I-735 VV-C-846
Viscosity @ 100 C
Viscosity @ 54 C
Viscosity @ 40 C
Viscosity @ 20 C
Viscosity @ -40 C
Viscosity @ -54 C
Relative density X X
Distillation
Flash point X
Fire point
Pour point X
Freezing point
Penetration (worked) X
Melting point
Protection
Corrosion X
Neutralization Number (acid/base)
Acidity X X
Lead corrosion
pH X
Stability
Residue on evaporation X
Ash
Foaming
Emulsification properties X
Water content X
3

Film appearance
Drying Rate
Particle size (fineness) X
Visual check frequency (months) 12 12 12 12 12
Military Symbol(s) None None None None OS
NATO Code Numbers S-736 S-747 S-732 S-737 O-214
NOTES:
1 Also, color.
4 Check container for damage.
5 Bulk products should be tested annually prior to the winter season. Packaged products, such as 55-gal drums, have an initial 24-month
6. 18 months
7 One month after receipt
MIL-STD-3004C

123
TABLE XXVI. Conversion chart for truck (TT), tank cars, truck(tank wagons(TW),tank & trailer(TRR))
1, 2

LAST
PRODUCT
CARRIED
PRODUCT TO BE LOADED
Gasolines:
MOGAS,
E85,
AVGAS,
JP-4
Jet Fuels:
Jet A/A-1,
JP-8, JP-5,
TS-1, DFW
Jet Fuel
3
:
JPTS
RP1 /RP2 JP-10/PF-1 Diesel Fuels:
F-76, DL1,
DL2, DF1,
DF2, 1-D, 2-
D, FS1, FS2,
Biodiesel
blends >B-5
FSII
4
Lubricating
Oils
Gasolines:
MOGAS, E85,
AVGAS, JP-4
Drain/Empty Steam Dry
5
Steam Dry Steam Dry Steam Dry Steam Dry Steam Dry Steam Dry
Jet Fuels:
Jet A/A-1, JP-8,
JP-5, TS-1, DFW
Drain/Empty Drain/Empty
6, 7

Steam Dry
6, 7

Steam Dry Steam Dry Drain/Empty
6, 7

Steam Dry
6, 7

Steam Dry
6, 7

Jet Fuel: JPTS Drain/Empty Drain/Empty Drain/Empty Drain/Empty Steam Dry Drain/Empty Steam Dry Steam Dry
RP1/RP2 Steam Dry Steam Dry Steam Dry Drain/Empty Steam Dry Steam Dry Steam Dry Steam Dry
JP-10/PF-1 Steam Dry Steam Dry Steam Dry Steam Dry Drain/Empty Steam Dry Steam Dry Steam Dry
Petroleum Solvent
or Paint Thinner
Steam Dry Steam Empty Steam Dry Hot Water
Rinse & Dry
Steam Dry Steam Dry Steam Dry Steam Dry
Diesel Fuels:
F-76,DL1,DL2,
DF1,DF2,1-D,
2-D,FS1, FS2,
<B6

Steam Dry
6, 7

Steam Dry
6,
7

Steam Dry
6, 7

Steam Dry

Steam Dry

Drain/Empty

6, 7

Steam Dry
6, 7

Steam Dry
6, 7

Lubricating Oils NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD Steam Dry NO LOAD Drain/
Empty
8

ASTM D975 No.
4D, FS4,FS5,FS6,
IFOs
NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD
Naphtha Drain/Empty Steam Dry Steam Dry Steam Dry Steam Dry Steam Dry Steam Dry Steam Dry`
NOTES:
1 General Instructions for Tank Cars and Trucks :
a. Equipment carrying lubricating oil will be dry and free from loose rust, scale, and dirt. Equipment carrying other products will be substantially
free from loose rust, scale and dirt.
b. Saran lined equipment should not be steam cleaned; water wash should suffice.
c. Petroleum products will not be loaded into the transportation equipment whose previous cargo was caustic, acid, or chlorinated solvents.
d. Trucks in liquid fertilizer service shall not load aviation turbine fuels directly, but shall carry out at least two loads of commercial gasoline prior
to the aviation turbine fuel load.
e. Conversion of Government-owned tank cars from liquid fertilizer service to aviation turbine fuel service will only be done when no other
alternative exists. Tank cars being converted from liquid fertilizer service to a petroleum product shall be adequately cleaned to remove all traces of liquid
fertilizer. At a minimum the equipment must be steam cleaned; dried and will be free from loose rust, scale, and dirt. After cleaning, equipment with
unlined compartments should have its compartments lined with an approved coating at this time. Conveyances shall not be released from origin loading
point until loaded conveyance is sampled after a minimum wait of 24 hours after loading. The sample shall be tested to Type B-2 tests plus Thermal
Stability Test (if required by the product specification). After type B-2 tests indicate compliance with specification requirements, the conveyance can be
released pending results of Thermal Stability tests. The conveyance will not be unloaded until origin car notifies the destination that the Thermal Stability
test (when required) has passed. When the above condition applies, the DD-250 shall be so noted.
2. Individual Services will provide specific guidance for conversion of refueling equipment which exclusively handles Service petroleum products, e.g.:
Air Force guidance is contained in T.O. 42B-1-1, Table 3-1.
3. To be loaded only in aluminum, stainless steel equipment or equipment lined with an approved epoxy coating. If equipment is coated, clean with hot
fresh water not exceeding 58 C (136 F) and dry thoroughly.
4. For previous cargoes not listed, contact DLA-ENERGY-QA for acceptability/cleaning procedures.
5. For an additional policy on steam cleaning for JP-8 see 5.3.1.2.
6. If previous cargo contained dye marker, all traces of color must be removed.
7. If product to be loaded does not contain dye, then the vehicle shall not contain any traces of dye prior to loading.
8. Applicable only when loading compatible oils; otherwise, steam and dry.
MIL-STD-3004C

124
TABLE XXVII. Minimum requirements for the preparation of tanker cargo tanks.
1, 2

LAST PRODUCT
CARRIED
Jet fuels:
JP-4, JET B
Gasolines,
Mogas, Avgas
5

Jet fuels:
Jet A, Jet A-
1,
JP-8, DFW
Jet Fuel:
JP-5
Jet Fuel:
JPTS
Diesel Fuels:
F-76, DF1, DF2, D L1,
DL2, DS1, DS2, ASTM
D975 (No. 1, 2) (B20)
ASTM D975
(No. 4D),
FS 4, FS 5, FS
6, IFOs
Jet fuels:
JP-4, JET B
Gasolines,
Mogas, Avgas
A A,B A,B Note
3
A,B A
Jet fuels:
Jet A, Jet A-1,
JP-8, DFW
A A A,B Note
3
A A
Jet Fuel:
JP-5
A A A Note
3
A A
Jet Fuel:
JPTS
A A A,B Note
3
A A
Diesel Fuels:
F-76, DF1, DF2,
DL1, DL2, DS1,
DS2, ASTM D975
(No. 1, 2) (B20)
A,C, A,C A,C NO LOAD A,C A,C
FAME (Fatty Acid
Methyl Esters or
Diesel Blended 5
vol % FAME or
Less (B5 or less)
6

A, C A, C A, C NO LOAD A, C A, C
FAME (Fatty Acid
Methyl Esters or
Diesel Blended 15
vol % FAME or
Less (B15 or less)
6

A,C A,C A,C NO LOAD A,C A,C
FAME (Fatty Acid
Methyl Esters or
Diesel blended
15 vol % FAME
(B15 or higher)
6

E E E NO LOAD A,C A,C
ASTM D975 (No.
4D), FS4, FS5,
FS6, IFOs
NO LOAD NO LOAD NO LOAD NO LOAD D, A A
Crude
4
NO LOAD NO LOAD NO LOAD NO LOAD D, A A
Lube Oils NO LOAD NO LOAD NO LOAD NO LOAD D, A A
NOTES: 1 Legend for vessel cleaning requirements broken out into different Types are as follows:
Type
Cleaning Requirement
A All cargo lines will be dropped, tanks stripped, ballast residue removed.
B All cargo and vent lines will be drained of previous product and flushed with cold water. Cargo tanks will be thoroughly
machine washed using cold water. Cargo tanks must be free of water, loose rust, sludge, mud, silt, etc.
C The same as for B, except that hot water will be used instead of cold. If tank interiors are coated, water temperature should
not exceed 58 C (136 F).

D Cargo tanks and systems will be processed in accordance with the instructions contained in MIL-HDBK-291, Cargo Tank
Cleaning.

E Not to be loaded without special cleaning instructions. Three clean product/zero biological content intermediate cargoes
required. (See Note 6 below)

MIL-STD-3004C

125

TABLE XXVII. Minimum requirements for the preparation of tanker cargo tanks.
1, 2
Continued

2 This table is included as a guide only. Requirements for tanker cleaning are determined by MSC vessel cleaning policy (See 5.1.1.4).
Contact MSC for tank cleaning requirements for any product not listed in Table XXIV.
3 Special tank preparations and cargo handling is required for JPTS, to prevent contamination. Tanks used for loading must be coated with
an approved epoxy. Coating must be adherent: no flaking, peeling, or blistering. It is mandatory that JPTS be loaded in tanks in which the last
product carried was JP-5, JP-4, kerosene-based fuels (JP-8, Jet A, etc.), non-aromatic solvent, unleaded gasoline, or arctic diesel. Prior to
loading JPTS, tank cleaning requirements are: tanks must be machine washed with hot water, if cleaning chemical and/or salt water is used, the
final wash must be with fresh water. Tank bottoms, interior bulk heads, and internals must be completely free of sediment, scale, and other
contaminants. Tanks must be dry and all liquids completely removed from the tanks lines after cleaning, must be flushed with fresh water,
drained and free all water. Loading and unloading system must be completely isolated. This will be accomplished by completely separate
piping systems or by use of blinds. Valves will not be depended on to effect isolation. No common lines will be used. Steam smothering lines
should have at least two valves that can be sealed from the main line to the tanks, or a blind installed that can be readily removed. Each tank
will have its own individual vent. If ship has a common vent system, tanks used for JPTS must be isolated from balance of the vent system.
4 There are no circumstances were a crude carrier is capable of cleaning tanks, pumps and lines sufficiently to load an aviation fuel
immediately after a crude cargo. Crude carriers converted to a distillate diesel, aviation fuel or naphtha based fuel must carrier five cargoes of a
commercial like product without a quality incident.
5. Motor Gasoline containing Ethanol or MTBE cleaning is to be done by washing with cold sea water and drain well, purge to below 2%
hydrocarbon on by volume. Gas free, lift scale and mop. Motor Gasoline unleaded and ultra low sulfur motor gasoline (unleaded) are to be
cleaned washing with cold sea water and drain well.
6. Contamination of aviation kerosene with FAME current specifications permits only 5 ppm by mass FAME in aviation kerosene.
Intermediate cargoes and strict washing regime is therefore recommended when the following these cargoes with aviation kerosene. Special
note- Specifications for sensitive grades will require extreme care during sampling, to avoid contamination from previous cargoes or build up of
residues. To reduce the possibility of drawing unrepresentative samples, the cleaning of sampling equipment, vapor locks, stand pipes and
stilling wells is recommended as part of tank cleaning when tanks have previously held cargoes containing FAME.
Aviation Gasoline-
- To avoid contamination from FAME it is recommended to have three intermediate cargoes with NO FAME between (B100) or any cargo with
FAME content greater than 15 vol % (B15) and an aviation gasoline cargo.
- Cargoes with a FAME content of 5 vol % or less (B5 or below) a hot water wash, including flushing of the pumps and lines followed by
draining is recommended as a minimum for aviation gasoline cargoes.
- Cargoes with FAME content of 15 vol % (B15) or less, but above B5, a hot water wash, including flushing of pumps and lines, followed by
draining is recommended as a minimum. Tanks must be in good condition and washing needs to particularly stringent. A single intermediate
cargo with no FAME content is suggested as an alternative, followed by a hot water wash, including flushing of pumps and lines, and by
draining for aviation gasoline cargos.
Aviation Kerosene-
Due to strict limitations on biological contamination (FAME content maximum 5 ppm by volume) three intermediate cargoes with no FAME
between FAME (B100) or any cargo with FAME content greater than 15 vol % (B15) and a subsequent aviation kerosene cargo.
- When following cargoes with a FAME content of 5 vol % or less (B5 or below) a hot water wash, including flushing of the pumps and lines
followed by draining is recommended as a minimum for aviation kerosene cargoes.
- Cargoes with FAME content of 15 vol % (B15) or less, but above B5, a hot water wash, including flushing of pumps and lines, followed by
draining is recommended as a minimum. Tanks must be in good condition and washing needs to particularly stringent. A single intermediate
cargo with no FAME content is suggested as an alternative, followed by a hot water wash, including flushing of pumps and lines, and by
draining for aviation gasoline cargos. This is per EI (energy institute) HM50.
MIL-STD-3004C

126
TABLE XXVIII. Minimum requirements for the preparation of barge cargo tanks
1, 2

LAST PRODUCT
CARRIED
Leaded gasoline,
aviation
Gasoline,
automotive
Turbine fuel, aviation,
kerosene type F-34,
F-35, F-44
Diesel fuel
oil - distillate
Diesel fuel
oil - residual
Lube oil
Leaded Gasoline,
Aviation
A A B B B B
Gasoline,
Automotive
A A B B B B
Turbine fuel,
aviation, kerosene
TYPE, F-34, F-35,
F-44
A A A A A E
Diesel fuel oil -
distillate
C C A A A E
Diesel fuel oil -
residual
NO LOAD NO LOAD NO LOAD D A E
FAME (Fatty Acid
Methyl Esters or
Diesel blended
5 vol % FAME (B5
or less)

C

C

A,C,F

C,F

C,F

C,F
FAME (Fatty Acid
Methyl Esters or
Diesel blended
15 vol % FAME
(B15 or less)

C

C

A,C,F

F

F

F
FAME (Fatty Acid
Methyl Esters or
Diesel blended
15 vol %FAME
(B15 or higher)

C

C

A,C,F

F

F

F
Lube oils NO LOAD NO LOAD NO LOAD D A E
NOTES:
1 Legend for vessel cleaning requirements broken out into different Types are as follows:
Type Cleaning Requirement
A Drop lines and strip tanks.

B All cargo and vent lines will be drained of previous product and flushed with cold water. Cargo tanks
will be thoroughly machine washed using cold water. Tanks will be gas freed.
C The same as for Type B., except that hot water will be used instead of cold water.
D The same as for Type C above. In addition tanks and lines will be flushed with product to be loaded
and examined to confirm meeting product specification. Process will be repeated as necessary until
passing results are obtained.
E Cargo tanks and systems must be cleaned in such a manner as will remove all rust, scale, sediment,
and all traces of previous cargo and water.
F Contamination of aviation kerosene with FAME: current specifications permit on up to 5 ppm by
volume FAME in aviation kerosene. Intermediate cargoes and strict washing regime is therefore
recommended when the following these cargoes with aviation kerosene. Special note- Specifications
for sensitive grades will require extreme care during sampling, to avoid contamination from previous
cargoes or build up of residues. To reduce the possibility of drawing unrepresentative samples, the
cleaning of sampling equipment, vapor locks, stand pipes and stilling wells is recommended as part of
tank cleaning when tanks have previously held cargoes containing FAME.
Aviation Gasoline-
MIL-STD-3004C

127
-To avoid contamination from FAME it is recommended to have three intermediate cargoes with NO
FAME between aviation gasoline and any cargo with B100 or any cargo with FAME content greater
than 15 vol % B15.
- Cargoes with a FAME content of 5 volume % or less (B5 or below) a hot water wash, including
flushing of the pumps and lines followed by draining is recommended as a minimum for aviation
gasoline cargoes.
- Cargoes with FAME content of 15 vol % (B15) or less, but above B5, a hot water wash, including
flushing of pumps and lines, followed by draining is recommended as a minimum. Tanks must be in
good condition and washing needs to particularly stringent. A single intermediate cargo with no
FAME content is suggested as an alternative, followed by a hot water wash, including flushing of
pumps and lines, and by draining for aviation gasoline cargos.
Aviation Kerosene-
- Due to strict limitations on biological contamination (FAME content maximum 5 ppm by volume)
three intermediate cargoes with no FAME between FAME (B100) or any cargo with FAME content
greater than 15 vol % (B15) and a subsequent aviation kerosene cargo.
When following cargoes with a FAME content of 5 vol % or less (B5 or below) a hot water wash,
including flushing of the pumps and lines followed by draining is recommended as a minimum for
aviation kerosene cargoes.
- Cargoes with FAME content of 15 vol % (B15) or less, but above B5, a hot water wash, including
flushing of pumps and lines, followed by draining is recommended as a minimum. Tanks must be in
good condition and washing needs to particularly stringent. A single intermediate cargo with no
FAME content is suggested as an alternative, followed by a hot water wash, including flushing of
pumps and lines, and by draining for aviation gasoline cargos. This is per EI (energy institute) HM50.
2 In all cases, cargo tanks must be free of water, loose rust, sludge, mud, silt, ballast residue, etc.

TABLE XXIX. Segregation of product movements via multiproduct pipelines, head product.
1
GOVERNMENT
PRODUCT
BEING MOVED
HEAD/TAIL PRODUCT
GASOLINE DIESEL
2
DYED DIESEL JP-5 JP-8
GASOLINE MID-POINT CUT HEART-CUT MID-POINT CUT MID-POINT CUT
DIESEL HEART-CUT HEART-CUT MID-POINT CUT MID-POINT CUT
DYED DIESEL N/A N/A N/A N/A N/A
JP-5 HEART-CUT MID-POINT CUT HEART-CUT MID-POINT CUT MID-POINT CUT
JP-8 MID-POINT CUT HEART-CUT MID-POINT CUT MID-POINT CUT
1 The following pertains to segregated product as it is moved in the bulk commercial pipeline system. As a rule, Government-owned
products are moved via commercial multi-product pipelines from refineries to DFSPs or from DFSP to DFSP. Contract or tariff agreements
with the commercial pipeline company outline the type of interface cut (heart-cut or mid-point cut) that will be used on Government product.
When Government product is delivered to a customer by pipeline, it is usually through a dedicated system from the DFSP. In those situations
where product is delivered directly off of a commercial multi-product pipeline to a using customer, heart-cuts should be used.
2 Ultra Low Sulfur Diesel (ULSD) may require a little more ULSD be cut into military aviation fuels in order to protect the sulfur content
of the ULSD. The procedures will be agreed ahead of time with the carrier/contractor and be agreeable to all. Information on the total sulfur
content of the typical military aviation fuel will be used as the basis for the formation of the cutting procedures agreed.
Note-
Heart Cut- portions of pure product taken from the line before and after the interface at intermediate terminals.
Mid-point Cut- divided between the two adjacent products, usually at the mid gravity point.
MIL-STD-3004C

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TABLE XXX. Contamination tables
TYPE CONTAMINANTS APPEARANCE CHARACTERISTICS EFFECTS ON
AIRCRAFT
A. WATER
(1) Dissolved Water Not Visible. Freshwater only. Precipitates out as cloud
when fuel is cooled.
None unless precipitated out by
cooling of fuel. Can then cause
ice to form on low-pressure
fuel filters.
(2) Free Water Light cloud. Heavy
cloud. Droplets
adhering to sides of
bottle. Gross amounts
settled in bottom.
Free water may be saltwater or fresh
water. Cloudy usually indicates water-in-
fuel emulsion.
Icing of fuel systems, usually
low-pressure fuel filters; erratic
fuel gage readings; gross
amounts of water can cause
flameouts; saltwater will cause
corrosion of fuel system
components.
B. SEDIMENT
(1) Rust Red or black powder,
rouge or grains. May
appear as dye-like
material in fuel.
Red rust (Fe
2
O
3
) nonmagnetic. Black rust
(Fe
3
O
4
) magnetic. Rust generally
comprises the major constituent of total
sediment.
Will cause sticking, sluggish or
general malfunction of fuel
controls, flow dividers, pumps,
nozzles, etc.
(2) Sand or dust Crystalline, granular
or glasslike.
Usually present and occasionally
constitutes major constituent of total
sediment.
nozzles, etc.
(3) Aluminum or
magnesium
White or gray powder
or paste.
Sometimes very sticky or gelatinous when
wet with water. Normally present and can
constitute the major constituent of total
sediment.
nozzles, etc.
(4) Fibers A fiber is defined as a particle having a
length to diameter ratio of 20 to 1 or more
and having a length of 100 microns or
more.
nozzles, etc.
C. EMULSIONS
(1) Water in fuel emulsions Light cloud. Heavy
Cloud.
Finely divided drops of water in fuel.
Same as free water cloud. Will settle to
bottom in minutes, hours, or weeks,
depending on nature of emulsion.
Same as free water.
(2) Fuel in water or
inverse emulsions
Reddish, grayish, or
blackish. Sticky
material variously
described as
gelatinous, gummy,
or mayonnaise-
like.
Fine divided drops of fuel in water.
Contains rust which stabilizes or firms
the emulsion. Will adhere to most
materials normally in contact with fuels.
Usually present in globules or stringy,
fibrous-like material in clear or cloudy
fuel. Will stand from days to months
without separating. This material contains
50-70% water, a small amount of fine rust,
and 30-50% fuel.
Same as free water and
sediment, only more drastic.
Will quickly cause filter
plugging or erratic readings in
fuel quantity probes.
D. MICROBIOLOGICAL GROWTH
Brown, gray, or
black. Stringy or
fibrous
Usually found with other contaminants in
the fuel. Typically found at the fuel water
interface but can also form films on the
tanks surfaces. Develops only when free
water is present.
Fouls fuel quantity probes,
sticks flow dividers, and makes
fuel controls sluggish.
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TABLE XXX. Contamination tables. - Continued
TYPE
CONTAMINANTS
APPEARANCE CHARACTERISTICS EFFECTS ON AIRCRAFT
E. MISCELLANEOUS
(1) Interface material Lacy bubbles at
interface between fuel
and water. Sometimes
resembles jellyfish.
Extremely complicated chemically. Occurs
only when free water is present.
Effects due to presence of free
water.
(2) Air Bubbles Cloud in fuel. Disperses upward within a few seconds None.
(3) Media Migration Thin to Thickened, light
to dark brown, molasses
type material
Found in filter-separators utilizing water
absorbing (super absorbent polymer based),
filter monitor fuse filters. Polymer may
migrate downstream of the filter-separator all
the way to the aircraft fuel tank.
Capable of blocking the engine
fuel filters. May promote
microbial growth within the
wing tank.
TABLE XXXI. Minimum standards of filtration and water separation for petroleum products
PRODUCT INTO TANK
CARS AND
TRUCKS
INTO
DISPENSING
UNITS
INTO
CONTAINERS
(PACKAGE)
INTO AIRCRAFT
1
INTO USING
UNIT
Aviation Gasoline
Bulk
2

150 microns
3

(max) No
Visible Water
Filter-Separator
2
10 ppm by volume
water, max.
Filter-Separator 10
ppm by volume
water, max.
Filter or Filter-Separator
10 ppm by volume Water,
max.

Aviation Gasoline,
Packaged
Filter-Separator
2

10 ppm by volume
Water, max.
Filter or Filter-Separator
2

max.

Aviation Turbine
Fuels, Bulk
2

150 microns
3

(max.)
Filter-Separator
2

10 ppm by volume
Water, max.
Filter-Separator
2
10
ppm by volume
water, max.
Filter-Separator
max.

Aviation Turbine
Fuels, Packaged
4
Filter-Separator
2

10 ppm by volume
Water, max.

Filter-Separator
2
max.

Aircraft Piston
Engine Lube Oil, -
Bulk
240 microns
3

(max.) No
Visible Water
240 microns
3

(max) No Visible
Water
240 microns
3
(max.)
No Visible Water
240 microns
3
(max) No
Visible Water

Aircraft Piston
Engine Lube Oil,
Packaged
240 microns
3

(max.) No Visible
Water
240 microns
3
(max.)
No Visible Water
240 microns
3
(max) No
Visible Water

Aircraft jet Engine
Lube Oils, -
Packaged
25 microns,
absolute (max.)
No Visible Water
25 microns, absolute
(max.)
No Visible Water
10 microns (max) (No
Filtration necessary for
Hermetically sealed
containers)

Aircraft Hydraulic
Fluids - Packaged
(Filtered at time of
manufacture), 5
microns, absolute
(max)
5 microns, absolute (max)
(No filtration necessary
for hermetically sealed
containers)

Diesel Fuel/
MOGAS
(applicable for
Army only)
Filter-Separator
2
10
ppm by volume
Water
Filter-Separator
10 ppm by
volume Water
NOTES:
1 For Navy aircraft fuels, the ppm by volume by volume free water limit is 5, max.
2 Filter-separator in accordance with EI 1581 or MIL-PRF-52308, or other approved filter-separator equipment.
3 150 microns equal 100 mesh; 240 microns equal 60 mesh.
4 All visible water to be stripped or drained from fuel prior to issue.
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.METHOD 1000
TEST FOR EFFECTIVENESS OF PIPELINE RUST INHIBITORS
1. SCOPE
1.1 This method outlines the procedures for determining the effectiveness of rust inhibitors in
product moving through pipeline by a steel rod (coupon).
2. APPARATUS
2.1 One SAE-1020 steel rod. Rods sold as SAE-1020 may vary in rusting tendency. The rods
used in this test should produce a rating of R-7 in aviation gasoline which does not contain a rust
inhibitor.
2.2 Same apparatus as used in ASTM D665, except the oil bath and related heating equipment
are not required.
3. PROCEDURE
3.1 Polish the steel rod in accordance with ASTM D665.
3.2 Pour 350 mL of the product into a beaker. Cover the beaker and insert stirrer and polished
steel rod. Stir for 10 minutes to ensure wetting the rod.
3.3 Remove 50 mL of the product with a pipette and add 30 mL of synthetic sea water prepared
in accordance with ASTM D665. Continue stirring for one hour at room temperature.
3.4 Stop stirring, remove steel rod and examine.
4. REPORT
4.1 Inspect the steel rod for rust and rate using the following chart:
APPEARANCE OF ROD RATING DESIGNATION
Free of Rust Passes R-1
Trace of Rust, few spots Passes R-2
Less than 5% surface rusted Barely Passes R-3
5-50% surface rusted Does not Pass R-4
50-90% surface rusted Does not Pass R-5
Surface covered with light Rust Does not Pass R-6
Surface covered with heavy Rust Does not Pass R-7

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THIS PAGE INTENTIONALLY BLANK
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132
METHOD 1010
VISUAL QUALITY SURVEILLANCE TEST (Clean/Clear and Bright Test)
1. SCOPE
1.1 This method outlines the procedures for conducting the visual quality surveillance test.
2. CONTAINER
2.1 A round, transparent bottle or laboratory beaker from one L (one quart) to 4 L (one gallon) in
size. Container should be as clean as possible.
3. PROCEDURES
3.1 Be sure the sampling valve is free of solid contaminants. Flush sampling valve prior to
taking of actual sample.
3.2 Draw the sample as rapidly as possible (full flush) rather than permitting the sample to
trickle out. Avoid contaminating the sample from outside sources.
3.3 Check for proper color and all forms of visual contamination by swirling the sample so a
vortex is formed. All sediment or water that has settled will accumulate on the bottom of the bottle
directly beneath the vortex. Experience will dictate what can be considered excessive sediment.
Very fine suspended solids or water will render the product hazy. If the examination is questionable,
a laboratory analysis will be made to verify the quantity of contaminant.

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133

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134
METHOD 1020
TEST FOR SULFIDES IN WATER
1. SCOPE
1.1 This method describes a procedure for determining the presence of hydrogen sulfide that
sometimes forms as a result of bacterial action of the sulfates contained in water bottoms in fuel
storage tanks.
2. APPARATUS
2.1 250 mL conical flask.
3. Materials
3.1 Dilute (10%) ACS grade, sulfuric or hydrochloric acid.
3.2 Lead acetate paper.
4. SAMPLES
4.1 Representative water samples from storage tank bottoms must be taken in a glass bottle. In
some cases it will be necessary to take the water sample in a Bacon bomb sampler. Samples so
taken will always be transferred to a glass bottle. To preclude oxidation by air, the filled bottle must
be capped immediately. The sample should be tested as soon as possible after sampling to minimize
possible changes in the composition of materials in the water.
5. PROCEDURE
5.1 The sample must be shaken thoroughly just prior to performing the test to make certain any
sediment present is included in the portion of the sample to be tested.
5.2 Transfer 100 mL of the shaken sample into a 250 mL conical flask. Add 20 mL of dilute
(10%) ACS grade, sulfuric or hydrochloric acid to the flask. Immediately place a piece of lead
acetate paper folded into a V shape in the neck of the flask. Bring the water to a boil and continue to
gently boil for three or four minutes. Observe the color change of the paper.
6. REPORT
6.1 Report negative for sulfides if there is no color change in the lead acetate paper. Report
positive for sulfides if the color of the lead acetate paper changes. The color may vary from a light
brown to a black.

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136
METHOD 1030
DETERMINATION OF SMALL AMOUNTS OF LEAD IN FUELS
1. SCOPE
1.1 This method covers the determination of lead alkyls content of fuel in the range of 0.001g
to 0.020 g of lead per L. Note: This method is not applicable to fuels containing metal salts other
than lead that are capable of producing colored sulfides.
2. SUMMARY
2.1 The lead alkyl is extracted by refluxing the unconverted to lead chloride that is then
measured by a colorimetric method, using sodium sulfide. The brown color is compared to the color
obtained by adding a known quantity of lead nitrate to a sodium sulfide solution.
3. APPARATUS
9
3.1 Extraction apparatus.
3.2 Beakers - in Pyrex glass, 250 mL.
3.3 Burette - 5 mL, graduated in 0.05 mL.
4. REAGENTS
4.1 Hydrochloric acid (relative density = 1.19)
4.2 Sodium sulfide solution, 20g in one L of distilled water.
4.3 Lead nitrate. Solution-dry lead nitrate crystals for one hour in an oven at 110 C. Dissolve
0.8g of the dry lead nitrate in distilled water and make up to one L with distilled water. Discard the
solution if it is more than two months old.
4.4 Ammonium hydroxide solution. Prepared by mixing 30 parts of ammonium hydroxide
(relative density = 0.925) with 70 parts of distilled water.
5. PROCEDURE
5.1 Thoroughly clean all glassware.
5.2 Transfer 50 mL of the filtered sample to the flask, add 15 mL of HCl and heat until boiling.
When reflux commences, regulate the heat to stop bumping in the flask and to avoid flooding the
condenser. After 10 minutes of refluxing, stop heating to allow the sample to cool for a few minutes
and then drain the acid layer into a 250 mL beaker. Add 15 mL of distilled water to the flask and
reflux the mixture for 5 minutes, using full heat. Cool for a few minutes and drain the water layer
into the beaker already containing the acid layer.
5.3 Add 30 mL of water to the beaker. Neutralize with the ammonium hydroxide solution to
change the color of indicator paper (pH 7). Make up to 100mL with distilled water.
5.4 Fill the burette with the lead nitrate solution.
5.5 Place 100 mL of distilled water in a second beaker; the volume must be identical to that in
the first beaker.

9
Note: All glass must have a low lead content.
MIL-STD-3004C

137
METHOD 1030 - Continued
5.6 Add 10 mL of sodium sulfide solution to each beaker. Swirl gently. A brown color will
develop in the test solution. Match this color by addition of lead nitrate solution to the second
beaker (blank solution).
5.7 The preceding operations must be carried out rapidly to avoid color changes. If less than
0.2 mL or more than 2 mL of lead nitrate solution has been used, the test should be repeated using a
suitable volume of sample. Note: Avoid contact between the lead nitrate solution and vapor from
the ammonium sulfide.
6. CALCULATION
6.1 Calculate the total lead content, as follows:
X = (0.5) * (n) / V
X = Lead content in g/L
n = mL of lead nitrate solution used
V = volume of the sample in mL
7. PRECISION
7.1 The reproducibility of the method is 0.001 g/L for lead contents under
0.020 g/L.
8. REFEREE
8.1 IP-224 Test Method will be used as a referee method.
MIL-STD-3004C

138
METHOD 1040

DETECTION OF HEAVY HYDROCARBON CONTAMINATION IN AVIATION GASOLINE
1. SCOPE
1.1 This method of test covers the determination of trace amounts of turbine engine fuel or
other heavy hydrocarbon contaminant (JP-4 or heavier) in aviation gasoline. It is intended as a field
evaluation method and is not to be used in place of the distillation or other specification test.
2. DEFINITIONS
2.1 Capillary attraction: The attraction of a liquid to a solid, and the accompanying movement
of the liquid over the solid as in the movement through a wick.
2.2 Chromatography: The separation of mixtures into their constituents by preferential
absorption by a solid such as a strip of filter paper.
2.3 Aviation gasoline: Fuels conforming to ASTM D910 having a final boiling point of 170 C
or less.
2.4 Turbine engine fuel: Fuels conforming to MIL-DTL-5624, MIL-DTL-83133 or ASTM
D1655 and other fuels having a final boiling point above 238 C.
3. OUTLINE OF METHOD
3.1 Twenty five (25) ml each of a known quality aviation gasoline of the same grade being
tested and the fuel of questionable quality is dyed with approximately 0.01 mg of powdered fuel
soluble dye in addition to that already contained in the fuel. (Note: liquid dye is not to be used since
the solvent will show up as contaminant in this test). Nine (9) mL of each of the dyed fuels are
placed in separate 10 ml test tubes. The test tubes are mounted in a suitable holder and 0.6 cm (1/4")
strips of the #10 filter paper or other absorbent paper 20 cm (8 inches) long are extended to the
bottom of the test tubes. After five minutes, the height of the fuel on the paper is noted. If the
height of the fuel of questionable quality is 0.6 cm (") higher than the fuel of known quality, then
contamination should be suspected.
4. APPARATUS
4.1 10 ml test tubes 15 mm x 85 mm.
4.2 20 cm (8-inch) ruler.
4.3 Holder (fabricated in accordance with figure 1).
4.4 #40 Whatman filter paper.
4.5 50 ml beakers.
5. REAGENTS
5.1 Reference fuel (aviation gasoline that has been tested for complete specification tests and is
maintained in a sealed container).

MIL-STD-3004C

139

METHOD 1040 Continued
6. PROCEDURE
6.1 Measure 25 mL each of reference fuel and sample to be tested into separate 50 mL beakers.
Add approximately 0.01 g of blue dye to each beaker and mix thoroughly by swirling.
6.2 Transfer the dyed fuel to separate 10 mL test tubes. Fill the test tube to the top lip. Insert
the filled test tubes into the holder.
6.3 Lower a 0.6 cm wide by 20 cm long (or " by 8") long strip of Whatman filter paper into
the test tube until it touches the bottom of the tube. Affix the top of the filter paper to the holder in
an extended position.
6.4 After 5 minutes and 15 minutes, record the heights of the fuels on the two filter papers.
6.5 Contamination is indicated by the height of the fuel on the chromatography strip of the
unknown sample versus the height of the referenced fuel on the chromatography strip. A height of
0.6 cm (or ") above the referenced fuel would indicate possible contamination.
7. REPORT
7.1 Report the difference in centimeters or inches between the sample and the referenced fuel
heights on the chromatographic strip.
8. PRECISION
8.1 Results should not differ by more than 0.3 cm (or 1/8").
MIL-STD-3004C

140
METHOD 1040 Continued

FIGURE 1. Chromatography strip holder.

| 5/8|
3 1/2
3
3/4 1
1
| 1/4 |
1/2
2 1/2
8
12
3 3/4
1/4
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141

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142
METHOD 1050
DETECTION OF NITRATE IGNITION-TYPE IMPROVERS IN DIESEL FUEL
1. SCOPE
1.1 This method of test covers the determination of organic nitrate ester type cetane improver
additives used in diesel fuel. It is intended as a screening test for those diesel fuel inspection test
procedures that are affected by the presence of cetane improvers, namely ASTM D524 and ASTM
D976.
2. SUMMARY
2.1 A diesel fuel sample is saponified in a potassium hydroxide-butanol mixture and then
filtered through a glass fiber filter disc. The material remaining on the disc is treated with
diphenylamine reagent after drying. The presence of a nitrate ester cetane improver is revealed by
the formation of a blue ring and blue/black spot due to oxidation of diphenylamine to intense blue
quinoidal compounds by the nitrate salt. No color change confirms the absence of a cetane
improver.
3. APPARATUS
3.1 Reaction bottle, screw cap bottle, 29.6 mL (1 ounce) capacity, wide-mouth, flint glass, with
a tin or Teflon-lined screw cap.
3.2 Glass fiber filter paper, 3.7 cm diameter, grade 93AH (H. Reeve Angel, Inc., Clifton, NJ, or
equivalent).
3.3 Pipette, 10 mL capacity.
3.4 Graduated cylinders, 10 mL and 25 mL capacity.
3.5 Suction flask, a holder to accommodate a 60 mL glass-fritted crucible.
3.6 Crucible, 60mL capacity, glass-fritted, crucible, medium porosity.
3.7 Oven, suitable for drying filter discs at 110
o
C (230
o
F).
4. REAGENTS
4.1 Saponification mixture (IN). Prepared by mixing 6.5g potassium hydroxide (ACS grade)
with 100 mL absolute butanol and heating to dissolve the KOH. After solution cools, the mixture is
filtered through the glass fiber filter paper.
4.2 Diphenylamine (1% solution). Prepared by dissolving 0.250g diphenylamine (ACS
indicator grade) in 25 mL sulfuric acid (relative density 1.834).
4.3 Toluene (ACS reagent grade).
4.4 Benzene (ACS reagent grade).

MIL-STD-3004C

143
5. PROCEDURE
5.1 Pipette 10 mL of sample into reaction bottle and add 5 mL of toluene followed by 10 mL of
the saponification mixture.
5.2 Affix cap to reaction bottle tightly and, after mixing contents, place in an oven maintained
at 38 C for four hours.
5.3 Remove reaction bottle from oven and allow to cool to room temperature.
5.4 Filter contents of reaction bottle through the 60 mL glass-fritted crucible fitted with the
glass fiber filter disc.
5.5 Wash reaction bottle with a 25 mL aliquot of benzene and transfer to the glass-fritted
crucible.
5.6 Carefully remove the glass fiber filter disc and dry in the oven at 110
o
C for 15 minutes.
5.7 Remove filter disc and cool to room temperature.
5.8 Add three (3) drops of diphenylamine solution to center of disc and observe whether blue
or blue/black color forms.
6. REPORT
6.1 The presence of organic nitrate ester type cetane improvers will be reported if the
formation of a blue color occurs. Reference samples of diesel fuels containing 0.5 vol % of any one
of the approved cetane improvers (amyl nitrate, cyclohexyl nitrate, hexyl nitrate, and isopropyl
nitrate) given an intense blue to blue/black color throughout the reagent spot, whereas those samples
only containing 0.1 vol % produce a blue ring at the outer boundary of the reagent.

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144
METHOD 1060
DETERMINATION OF FREE WATER IN AVIATION AND TURBINE FUELS USING THE
AEL MK I OR MK II FUEL DETECTOR (NSN 6640-00-999-2786)
1. SCOPE
1.1 This method covers the determination of the level of free water in aviation and turbine fuels
by a portable field instrument, the Free Water Detector (FWD). Not all paragraphs contained in this
method apply to all FWD models. The procedure, as outlined in the manual accompanying the
specific FWD unit, supersedes the Procedures section of this Appendix. (Not used by the U. S.
Army / U.S. Air Force uses the procedures outlined in T.O. 42B-1-1, Section V.): ASTM D3240,
Undissolved Water in Aviation turbine Fuels. Aqua-Glo is used by the Army and Air Force and is a
backup for the Navy.
2. SUMMARY
2.1 A sample of fuel is passed through a chemically treated filter pad and placed in the filter
holder of the AEL MK I or MK II detector. The chemical on the pad is sensitive to any free water in
the fuel, producing a fluorescent pattern readily visible under ultraviolet light. After filtration, the
pad is examined under the ultraviolet light contained in the viewer kit. The amount of free water in
the fuel sample is determined by the intensity of fluorescence on the test pad. Visual comparison is
made with a series of standards representing known quantities of water.
3. APPARATUS
3.1 Combined Contaminated Fuel Detector (CCFD), or the MKIII Contaminated Fuel Detector
(CFD) and either the MKII Free Water Detector (FWD) or earlier MKI FWD.
3.2 Viewer kit
3.3 Detector test pads and standards
3.4 Slide plate
3.5 Sample pads
3.6 Polyethylene bottle
3.7 Filter holder
3.8 Forceps
4. PROCEDURES
4.1 Mark the polyethylene bottle used with the AEL MK III contaminated fuel detector 8.25
cm (3 ") from the bottom. When the bottom is filled to this mark, a 500 mL sample will be
obtained.
4.2 Fill the polyethylene sample bottle to the 500 mL mark with fuel to be tested.
4.3 Open a free water detector envelope and place the detector pad, orange-side up, on the
contaminated fuel detector filter base. Attach the bottle receiver to the filter base and plug in the
ground wire jack. Handle the detector pad with forceps only and use each pad only one time.

MIL-STD-3004C

145
4.4 Check to make certain the fuel flask is empty and the drain valve closed.
4.5 Shake the sample bottle containing the 500mL fuel sample vigorously for approximately 30
seconds.
4.6 Immediately after shaking, turn on the vacuum pump, unscrew bottle cap and place the
bottle receiver and pad assembly firmly over the end of the bottle. All of the threaded portion of the
bottle top should be inserted into the bottle receiver. The entire assembly (pad holder, bottle receive,
and fuel sample bottle) is then picked up as a unit, inverted, and then inserted (pad holder end) into
the fuel flask of the MK III contaminated fuel detector. This step should be accomplished in as short
a time as possible in order to keep any free water present in suspension.
4.7 After the 500 mL sample has passed through the detector pad, turn off the vacuum pump
immediately, and remove the bottle and the bottle receiver. Note: Under no circumstances continue
to draw air through the detector pad.
4.8 Remove the detector pad from the filter base using forceps and place it (orange-side up) in
the free water detector slide depression.
4.9 Light the ultraviolet bulb in the free water detector by holding the light switch in the ON
position. Insert the slide containing the test pad.
4.10 Look through the view port of the box and compare the brightness of the fluorescence of
the test pad with that of the set of standards to determine the amount of free water. Free water
content is indicated in parts per million by the numbers located directly above the standards.
4.11 Drain the fuel from the flask of the AEL MK III contaminated fuel detector through the
tygon tubing.
5. REPORT
5.1 Results should be reported as no free water or as actual free water or as actual free water
content (estimated to the nearest parts per million).

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146
METHOD 1070
TEST FOR WATER REACTION OF AVIATION FUELS
1. SCOPE
1.1 This method covers the determination of the presence of water-miscible components in
aviation gasoline and turbine fuels, and the effect of these components on volume change and on the
fuel-water interface. This test is NOT performed on JP-5.
2. PROCEDURE
2.1 Use ASTM D1094 with the following exceptions:
a. Interface conditions. Use the following chart to rate the condition of the interface.
INTERFACE CONDITIONS
RATING APPEARANCE
1 Clear and Clean
1b Small, clear bubbles covering not more than an estimated
50% of the interface and no shreds, lace, or film at
interface.
2 Shreds, lace, or film at the interface
3 Loose lace or slight scum or both.
4 Tight lace or heavy scum or both.
b. Degree of separation. Use the following chart to rate the degree of separation.
SEPARATION
RATING APPEARANCE
(1) Complete absence of all emulsions and/or precipitates
within either layer or upon the fuel layer.
(2) Same as (1), except small air bubbles or small water
droplets in the fuel layer.
(3) Emulsions and or precipitates within either layer or upon
the fuel layer, and/or droplets in the water layer or
adhering to the cylinder walls, excluding the walls above
the fuel layer.

MIL-STD-3004C

147

MIL-STD-3004C
APPENDIX A
148

MILITARY SERVICES PETROLEUM LABORATORIES AND FUEL TESTING
CAPABILITIES
A.1 SCOPE
A.1.1 Scope: This Appendix is not a mandatory part of this Standard. The information
contained herein is intended for guidance only. Unless otherwise directed, all samples
should be forwarded to the laboratory designated in the appropriate service regulations. It is
recommended to contact the laboratories listed below prior to submission of samples to
ensure capabilities exist to perform/accomplish sample testing requirements.
A.2 LIST OF LABORATORIES
AIR FORCE LABORATORIES TYPE PRODUCTS TYPE TEST
Aerospace Fuels Laboratory (FP2070)
AFPA/PTPLA
2430 C Street, Bldg 70, Area B
Wright Patterson AFB OH 45433-7632
COMM: (937) 255-2106 DSN: 785-2106

Jet Fuel
Packaged POL
Chemical
Diesel
B20 Biodiesel Blend

Burner Fuel
MOGAS

AVGAS
A
B-2
B-2
A
B-2 (Except Cetane
Number)
A
A (Except Knock
Rating)
A (Except Knock
Rating)
Aerospace Fuels Laboratory (FP 2075)
AFPA/PTPLE
1747 Utah Avenue, Bldg. 6670
Vandenberg AFB, CA 93437-5220
COMM: (805) 606-5873 DSN: 276-5873
Jet Fuel
Diesel
Burner Fuel
A
A
A
AFPA/PTPLF
Bldg 725, West Row Gate #6
RAF Mildenhall, Suffolk UK IP28 8NF
COMM: 011-44-1-638-54-2043
DSN: 314-238-2043
Jet Fuel
Diesel
Burner Fuel
A
A
A
AFPA/PTPLG
Unit 5161, Bldg 854
Kadena Air Base Okinawa JA
APO AP 96368-5161
COMM: 011-81-611-734-1602
DSN: 315-634-1602
Jet Fuel
Diesel
Burner Fuel
A
A
A

MIL-STD-3004C
APPENDIX A
149
ARMY LABORATORIES TYPE PRODUCTS TYPE TEST
USAPC Petroleum Laboratory
ATTN: RDTA-DP
U Avenue, Bldg. 85-3
New Cumberland, PA 17070-5005
Jet Fuel
Package POL
Chemicals
Coal
B-1, B-2, B-3
B-2
B-2
B-2
HHD, 260
th
QM Bn
Bldg. 120
ATTN: AFZP-SQG
Hunter Army Airfield, GA 31409-5130
All B-1, B-2, B-3
US Army Aviation Center & Ft. Rucker
Bldg. 800, N Ave
ATTN: ATZB-DOL-M-POL-BR
Fort Rucker, AL 36362-2018
Aviation Fuel B-1, B-2, B-3
CDR 101
st
AVN DIV and Ft. Campbell
Bldg. 7137, 4
th
Ave
ATTN: AFZB-RB-M
Ft. Campbell, KY 42223-5000
Jet Fuels and
Ground Mobility
Fuels

B-1, B-2, B-3
CDR Combat System Test Activity
Bldg. 362
ATTN: STECS-TS-PC
APG MD 21005-5059
All B-1, B-2, B-3
HHD, 505
th
QM Bn.
Rt 74 Chibana, Bldg. 53140
ATTN: APAJ-GOQ-L
Unit 35130
APO AP 96376-5130
All B-1, B-2, B-3

DLA-ENERGY LABORATORIES TYPE PRODUCTS TYPE TEST
Mail Address:
DFR Europe Petroleum Laboratory
Unit 23135, Box 28
APO AE 09227
Sample Address:
DFR Europe Petroleum Laboratory
Bldg. 320, Rhine Ordnance Barracks
Am Opelkriesel
D-67663 Kaiserslautern, Germany
Phone: 49-631-536-6812
FAX: 49-631-536-7084
JP-8/ JP-5
JPTS
Jet A/A-1
Diesel (EN 590)

Diesel (F76)
Gasoline (EN 228)

AVGAS (D910)
Hydraulics
A
A (exc. JFA-5, add.)
A
A (exc. Cetane # &
Polycyc. Aromatics
A (exc. D613)
A (exc. Benzene
Content, Oxygen Cont.,
Oxygenates)
A
B-2
Defense Energy Support Center
Petroleum Laboratory - Pyongtaek
APO AP 96218-02666
DSN 315-753-7291
Comm. (82)(031)-691-0963
Aviation Turbine
JPTS
Ground Mobility
Packaged Products
A, except naphthalenes
A
B-1, B-2, B-3
B-1 plus
MIL-STD-3004C
APPENDIX A
150
DLA-ENERGY LABORATORIES TYPE PRODUCTS TYPE TEST
Defense Energy Support Center
Petroleum Laboratory - Anchorage
Ft. Richardson, AK 99505-5700
Aviation Turbine
DFA, DF1, DF2
Aviation Gasoline
Motor Gasoline
B-1, B-2, B-3
B-1, B-2, B-3
B-1, B-2, B-3
B-1, B-2, B-3

NAVY LABORATORIES TYPE PRODUCTS TYPE TEST
Naval Air Systems Command
Fuels and Lubricants Division, AIR 4.4.5
22229 Elmer Road, Bldg 2360
Patuxent River, MD 20670

Ship samples to:
Naval Air Systems Command
HAZMART Bldg 2385
22680 Hammond Road
Sample (AIR 4.4.5)
Patuxent River, MD 20670
Aviation & Ship
Fuels; Turbine
Engine Oils (Special
samples only as
defined in NAVAIR
00-80T-109)

All
Mid-Atlantic Regional Fuels Laboratory
9673 Virginia Avenue, Bldg. W-388
Norfolk, VA 23511-3323
JP-5
F-76
2190 (LTL)
9250 (LO6)
JP8
Jet A
MUR (ASTM
D4814)
Fuel Oil
B-2
B-1
B-2
B-2
B-2
B-1

B-1
B-1
FISC Jacksonville FL
Code 700, Fuel Dept.
8808 Somers Road, Bldg. 56
Jacksonville, FL 32226-2600
JP-5
F-76
B-1
B-1
U. S. Naval Station
Rota Spain
Attn: Fuels Officer
PSC 819, Box 21
FPO AE 09645-21
JP-5
F-76
B-2
B-1
FISC San Diego
Petroleum Laboratory
Bldg 70A
Point Loma Annex
San Diego, CA 92106
JP-5
F-76
2190 (LTL)
B-2
B-2
B-2
MIL-STD-3004C
APPENDIX A
151
NAVY LABORATORIES TYPE PRODUCTS TYPE TEST
FISC Puget Sound
Manchester Fuel Department
Attn: Q.A. Laboratory
7501 Beach Drive East
Port Orchard, WA 98366
JP-5
F-76
2190 (LTL)
B-2
B-2
B-1
FISC Pearl Harbor POL Laboratory
300 Neches Ave
Bldg 1685, Code 704
Pearl Harbor, HI 96860-4549
JP-5
F-76
2190 (LTL)
B-2
B-2
B-2
Commanding Officer
U.S. Naval Base Guam Fuel Division
Laboratory
PSC 455, BOX 190
FPO AP 96540-1082
JP-5
F-76
2190 (LTL)
C
C
C
Commanding Officer
FISC Yokosuka Code 700
PSC 473, Box 11
FPO AP 96349-0011
JP-5
F-76, Diesel
2190 (LTL)
Gasoline
A
A
B-2
B-2 + Engine
Officer-in-Charge
FISC Yokosuka Det.
Sasebo
PSC 476, Box 6
FPO AP 96322-0001
JP-5
F-76
2190 (LTL)
B-2
B-2
B-2
U. S. Navy Support Facility Diego Garcia
Attn: Petroleum Testing Lab
PSC 466, Box 24
FPO AP 96595-0004

JP-5
F-76
2190 (LTL)

B-2
B-2
B-2

Commanding Officer
FISC Hachinohe, Code 703.1
Unit 5260
APO AP 96319-5000
JP-5 B-1

MIL-STD-3004C
APPENDIX B
152

SIGNIFICANCE OF TESTS
B.1 SCOPE
B.1.1 Scope This appendix discusses the significance and purpose of some of the tests used
in the quality surveillance of fuels and lubricants. This Appendix is not a mandatory part of this
Standard. The information contained herein is intended for guidance only.
B.2 GENERAL
B.2.1 General. Each of the various tests of fuels and lubricants indicated in the product
specification has a certain significance in relation to the quality of the product tested. Certain
ones can give a quick, easy and positive identification of the product and at the same time, aid in
detecting the presence of contaminants. Although descriptions of the testing equipment and test
methods are not to be included in this publication, it is considered worthwhile to include a brief
statement on the significance and purpose of certain tests. These statements may assist by
providing a better understanding and appreciation of the scope and importance of the Quality
Surveillance Program. For a more detailed coverage of this subject, see the ASTM Manual 1,
Manual on Significance of Tests of Petroleum Products.
B.3 Ash. The ash content of an oil is determined by burning off the organic matter and
weighing the remaining inorganic materials. Straight mineral oils normally contain only a trace
of ash. Oils containing metallic salts as additives will have larger amounts of ash than straight
mineral oils. Increase of ash content is indicative of contamination with inorganic matter such as
sand, dust and rust. In the case of straight mineral oil this must be very low as any abrasive
substance such as sand, clay, or rust may damage the internal metal surfaces of engines, fuel
injectors, plug injection nozzles, or form deposits in the engine. Residual fuels should have low
amounts of ash since some constituents of ash may cause corrosion or embitterment of boiler fire
boxes and boiler tubes.
B.4 Bottom sediment and water. The bottom sediment and water test (BS&W) is conducted
on fuel to determine the amount of water and other foreign materials that may be present.
Excessive sediment will plug the burner tips and may prevent proper atomization. Clogging of
the strainers, accumulation of sediment in fuel tanks and formation of carbon deposits may be a
result of a high percentage of BS&W. Water in the fuel may freeze and also clog the lines
resulting in improper flow of the fuel.
B.5 Carbon residue. The results of the carbon residue test are an estimation of the
carbonizing properties of a lubricating oil or fuel. The carbon residue on a lubricating oil is not
directly related to carbon formation in an engine, but gives an indication of the type of carbon
formation (loose and flaky, or hard and flinty) and is useful primarily as an identity and control
test in conjunction with other specification tests. In diesel fuels, after distilling off 90%, the
carbon residue on the last 10% must be low enough to avoid large carbon deposits that could
cause coking in the fuel injectors and affect the fuel spray pattern. High carbon residual fuels
should be carefully checked for sediment. The Ramsbottom test is the required test for both fuel
and lubricants as it has better repeatability and correlates better to carbon formation.
MIL-STD-3004C
APPENDIX B
153
B.6 Cetane index. An approximation of the cetane number (the ignition performance) of
distillate diesel fuels, which does not contain a cetane improver additive, calculated from the API
gravity and mid-boiling point or from density and recovery temperature measurements.
B.7 Cetane number. The cetane number is a measure of the ignition performance of a
diesel fuel obtained by comparing it to reference fuels in a standardized engine test and is based
on a scale resembling that of octane numbers. This value is determined by a test method which
measures the length of time (ignition lag) between injection and starting of combustion within
the combustion chamber of an engine. The cetane number requirement varies with the type of
diesel engine. Large, slow-speed units of stationary installations do not require high cetane
numbers (below 40). Smaller, high-speed engines having 1,000 rpm or more require fuels of
high Cetane number (above 40). The cetane number is related to operating and starting
characteristics at low temperatures. The higher the cetane value, the better or easier the starting
capability. Cetane number is not to be confused with cetane index. The cetane number is
determined by ASTM D613; the cetane index is a calculated value and may not always equate
with the cetane number.
B.8 Cloud and pour points. The cloud point is the temperature at which wax crystals or
water in an oil or fuel appear, causing the oil or fuel to appear cloudy or hazy. In wick feed
systems, the waxy crystals may clog the wick and either wax or water crystals may block filter
passages in fuel systems. The cloud point is the limiting factor for controlling low-temperature
operability of diesel and burner fuels. Vehicles and equipment will experience low temperature
fluidity problems (filter plugging, fuel line restrictions, and waxing) if operated with diesel fuels
having cloud points above ambient temperature. The pour point is the lowest temperature at
which flow is observed under controlled conditions. The pour point as determined by laboratory
test procedures is only indicative of its behavior at low temperatures. The fact that an oil or a
fuel has a specific pour point is not indication that it can be handled satisfactorily at that
temperature. Because of the low temperatures encountered by aviation fuels in high altitudes
and cold weather flying, the low temperature characteristics are determined by freezing point
test.
B.9 Color. Various types of petroleum products such as aviation and automotive gasolines
are dyed to permit a rapid visual determination of product type and grade. Visually detectable
changes in color intensity or hue may be an indication of product contamination or deterioration.
Aviation turbine fuels have no color limitations on procurement or use. This is not to be
construed to mean visual color determination is without significance. Unexpected color changes
will require additional testing to ensure product quality. Progressive darkening of jet and
distillate type fuels during storage is a good indication that oxidation is occurring with the
formation of insoluble gums. Naphthas and solvents intended for use as fabric cleaners should
be water white to prevent discoloration of the fabric.
B.10 Conductivity. This measures the electrical conductance of the fuel in pS/m.
Conductivity additive reduces the amount of time necessary for static charges to dissipate.
Conductivity readings can be affected by temperature readings. Figure B-1 shows the effect of
temperature on a sample of JP-8 with Stadis 450. The US Navy does not use conductivity
additive. Conductivity additive is only added to JP-5 when the product is used for issue or
purging of Air Force tactical aircraft.
MIL-STD-3004C
APPENDIX B
154

-10 0 10 20 30 40 50 60 70 80 90 100 110 120
TEMPERATURE (F)

FIGURE B-1. Conductivity

500

400

300

200

150

100
90

70

60

50

40

30

C
O
N
D
U
C
T
I
V
I
T
Y
p
S/
m
MIL-STD-3004C
APPENDIX B
155
B.11 Copper Strip Corrosion. This test indicates whether a petroleum product is free of
corrosive compounds.
B.12 Distillation. The distillation test is a measure of the volatility of a product. The lower
boiling fractions of a gasoline indicate the starting ability of an engine at the given temperature,
and the engines ability to warm up quickly when using that gasoline. An excessive amount of
highly volatile constituents in gasoline may cause vapor lock; conversely, an excessive amount
of heavy-ends may not completely burn in the combustion chamber and consequently may cause
damage through excessive crankcase dilution. Specifications designate minimum and maximum
percentages to be evaporated at specified temperatures as well as initial and final boiling points
of the product. A high end point and high percentage of residue may be indicative of
contamination of gasoline with fuel or oil. Fuel with considerable lower initial boiling point or
flash point may be indicative of contamination with gasoline.
B.13 Existent gum. Existent gum is the amount of nonvolatile residue present in the gasoline
or aviation turbine fuel at the time of test. The results indicate the quantity of gum deposition
which may occur if the product is consumed immediately, but do not indicate the stability of the
product toward gum formation on storage. As the name implies, the gum is a sticky, tacky,
varnish-like material that is objectionable in fuel systems. When present in excess, it tends to
clog fuel line filters, pump screens, aircraft engine fuel systems, carburetor jets, and cause
manifold deposit and sticky intake valves.
B.14 Filtration time. The filtration time test determines the filterability of aviation turbine
fuels. It is designed to identify those fuels which can cause rapid differential pressure build up in
filtration equipment.
B.15 Flash point. The flash point of a product is an indication of its fire hazard during
handling and storage. The flash point is primarily applicable to lower temperature boiling range
products such as diesel fuel, JP-5, kerosene and solvents. It is also used to determine whether a
product is contaminated. As an example, very small quantities of gasoline will lower the flash
point of diesel fuel considerably below the minimum safe operating level. On new lubricating
oils, the flash point is used primarily for the purpose of identification and classification, and must
be above the operating temperature of the equipment.
B.16 Foam stability. This paragraph addresses Government-owned lubricating oil. All
lubricating oils will foam to some extent when agitated. The foam that is formed in additive oils
is often very stable and instead of breaking quickly tends to build in the oil system with
subsequent oil loss through the breather outlets and other openings in the engine crankcase.
Consequently, additive type motor oils are frequently treated with antifoam agents to eliminate
potential foaming difficulties. The foam test requires agitating the oil sufficiently so a large
quantity of foam is formed, then noting the time required for this foam to collapse. Some
lubricants containing antifoam additive may fail initial foam tests. If they meet the foam
requirements after agitation as described in Option A of ASTM D892, Foaming Characteristics
of Lubricating Oils, they are satisfactory for use.
B.17 Fuel system icing inhibitor. This is a quantitative test to determine the concentration
of diethylene glycol monomethyl ether in aviation turbine fuel. The FSII additive prevents ice
formation in aircraft fuel systems. ASTM D5006 (using the B2 AIA Kit) is the preferred
method.
MIL-STD-3004C
APPENDIX B
156
B. 18 API Gravity or density. Density, relative density (specific gravity is a factor that
governs the quality and pricing of crude petroleum. Accuracy of these tests, whichever is
applicable for petroleum and its products is necessary for the conversion of measured volumes to
volumes or masses, or both, at the standard reference temperatures during transfer. The storage,
handling and combustion of automotive, aviation and marine fuels are affected by density, which
makes it a significant quality indicator. The API gravity of a petroleum oil is based on an
arbitrary hydrometer scale which is to a specific formula:
Degrees API at 60
o
F = (141.5 / (Relative Density 60/60
o
F)) - 131.5
(Source: API MPMS Chapter 1, Vocabulary, API Gravity)
B.18.1 Relative Density. The relative density of a petroleum oil or a mixture of petroleum
products with other substances is the ratio of the weight of a given volume of the material at a
temperature of 60 F to the weight of an equal volume of distilled water at the same temperature.
If the relative density is determined at a temperature other than 60 F, the result is corrected to
that temperature by the use of the appropriate correction tables. The higher the relative density,
the lower the API gravity. The API scale is now used almost exclusively by the petroleum
industry to designate the gravities of petroleum liquids. Correct gravity is important in the
gauging of the liquid content of storage tanks, tankers and barges. A change of gravity may
indicate a change of composition caused by mixing of grades of product.
B.19 Knock value. The knock value is normally expressed as an octane number for
automotive gasoline and as octane or performance number for aviation gasoline. These values
are determined by actually comparing the knocking tendency of a fuel to laboratory standard test
fuels of known knock value in a standard test engine. The significance of knock value is to
indicate whether the fuel will tend to burn uniformly and evenly in a cylinder without pre-
ignition or detonation. Fuels of inadequate knock value will reduce power output in all types of
engines and, if used for more than brief periods, can cause overheating of the engine unit, burned
pistons and cylinders, lubrication failure, and even piston and cylinder melting.
B.19.1 Octane number-motor method. Octane number of automotive gasoline is determined
by a method of test that is indicative of fuel antiknock performance in engines operating at high
engine speeds and wide open throttle.
B.19.2 Octane number-research method. Octane number of automotive gasoline is
determined by a method of test that is indicative of fuel antiknock performance in engines
operating at relatively low engine speeds, low engine temperatures and wide open throttle.
B.19.3 Antiknock index ((R+M)/2). The antiknock index is the average of the motor and
research octane numbers. This value indicates the knocking tendency of the fuel under average
driving conditions.
B.19.4 Octane/performance number-aviation method. Antiknock rating is determined by a
method of test that indicates the knock characteristics at lean fuel-to-air ratio in engines
operating under lean or cruise conditions.
B.19.5 Octane/performance number-supercharge method. Antiknock ratings are determined
by a method of test that indicates the knock characteristics under supercharge rich mixture
condition, corresponding to the mixture ratio used in an aircraft engine under takeoff and
climbing conditions. The antiknock characteristics of a fuel above 100 octane are expressed in
terms of a tetraethyl lead or performance number.
MIL-STD-3004C
APPENDIX B
157
B.20 Lubricity. In lubricants it is proportional to film strength. In fuels it refers to a value
that is measured either by the scuffing load wear test, the high frequency reciprocating rig test, or
the BOCLE test. The tests were developed to determine the ability of the fuel to properly
lubricate fuel-wetted components/surfaces.
B.21 Potential gum or oxidation stability. Stability of a fuel is its ability to retain its
original properties, except for evaporation losses, after prolonged storage. When added to fuel
chemical inhibitors tend to retard gum formation, but they will not reduce gum that has already
been formed. The stability value is determined by a test that indicates the presence of gum
materials and the relative tendency of gasoline and aviation turbine fuel to form gums after a
specified period of accelerated aging. In addition, the formation of gum may reduce the knock
values of gasoline.
B.21.1 Oxidation stability. For automotive gasolines, the oxidation stability may be
expressed as the induction period (sometimes called the breakdown time), which is measured as
the time in minutes elapsed during the accelerated test until the fuel absorbs oxygen rapidly.
B.21.2 Accelerated gum. For aviation gasoline and aviation turbine fuels the oxidation
stability may be expressed as the potential or accelerated gum. It is the gum plus lead deposits
(from leaded fuels) measured at the end of a specified accelerated aging (oxidation) period.
B.22 Sulfur. Grade 1K kerosene, intended for use in non-flue connected burner appliances
and in wicked illuminating lamps, must not contain appreciable levels of sulfur in order to
prevent the formulation of sulfur compounds in combustion gases. The presence of sulfur
compounds may present a health and toxicological hazard.
B.23 Thermal oxidation stability for turbine fuels. The thermal oxidation stability for
turbine fuels (ASTM D3241) measures the high temperature stability of gas turbine fuels, which
subjects the test fuel to conditions that can be related to those occurring in gas turbine engine
systems. Test results are indicative of fuel performance during gas turbine operations and can be
used to assess the level of deposits that form when liquid contacts a heated surface that is at a
specified temperature.
B.24 Vapor pressure. The vapor pressure of a fuel is determined by the RVP test and
indicates the tendency of the fuel to vaporize. Vapor Pressure increases with temperature for any
given gasoline. Gasoline must have a certain vapor pressure to ensure adequate starting and
accelerating qualities.
B.24.1 Vapor lock. Too high a vapor pressure for the particular operating condition may
cause what is commonly known as vapor lock, which prevents the fuel from reaching the engine.
B.24.2 Vaporization. The tendency of gasoline to vaporize in an automobile fuel system is
indicated by the vapor-to-liquid ratio of that gasoline at conditions approximating those in
critical parts of the fuel system. This test is currently used at procurement levels in conjunction
with Vapor Pressure test to determine vaporizing properties of automobile gasoline.
B.25 Viscosity. Viscosity is the measure of a liquids resistance to flow. The significance
of viscosity depends on the intended use of the product. From the point of view of application
and performance, proper viscosity is highly important since specified minimum and maximum
rates of flow are required for all fuels and lubricating oils. In fuel, viscosity determination serves
MIL-STD-3004C
APPENDIX B
158
as an index of how it will flow to the burners, the extent to which it will be atomized and the
temperature at which the fuel must be maintained in order for heavy residual fuel to be properly
atomized.
B.26 Water and sediment.
B.26.1 Aviation fuels. Significance of contamination of aviation fuels with water and
sediment is covered in Section 5.9.
B.26.2 Automotive fuels. Significance of contamination of automotive fuels with water and
sediment is covered in Section 5.10.
B.26.3 Diesel and burner fuels. Diesel fuels must be clean and should not contain more
than a trace of foreign substances, otherwise fuel pump and injector difficulties may occur.
Excessive sediment and rust will plug the burner tip and the fuel will not atomize properly.
Water can cause rough operation and may corrode the fuel handling system, causing the
formation of rust in the system and can also create significant microbiological deterioration
problems. The type of equipment and type of burner fuels will determine the amount of
sediment that is permissible in the fuel.
B.26.4 Lubricating oils. Care should be exercised to avoid contaminating lubricating oils
with water, as it will hasten the decomposition of many oils, wash out additives, emulsify, and
lead to engine malfunctioning. In used lubricating oils, water sediment may indicate poor
maintenance or malfunctioning of screens, or its formation may have been caused by
condensation of combustion products.
B.27 Water reaction. A measure of the presence of water-miscible compounds in aviation
gasoline and turbine fuels (See Test Method 1070 in this Standard). An interfacial emulsion may
indicate a carryover of treating compounds or contamination with surfactants (surface active
agents). A change in fuel volume indicates a contamination with alcohol or other components
which absorb appreciable amounts of water. An interface emulsion may also indicate
contamination with microbiological growth. Not preformed on JP-5.
B.28 Water separation index modified (WSIM). The WSIM (also referred to as
microseparometer or MSEP method) test measures the water separation characteristics of fuels.
The test reflects the ease with which a fuel releasing dispersed or emulsified water surfactants
has an adverse effect on the WSIM rating. Fuels having low WSIM rating will poison filter-
separators and prevent them from functioning properly.
B.29 Water tolerance. The ability of fuel and alcohol blends to resist separation into two
phases when a known quantity of water is added.
MIL-STD-3004C

159

MIL-STD-3004C
APPENDIX C

160

RECEIPT AND QUALITY SURVEILLANCE OF COAL
C.1 SCOPE
C.1.1 Scope. This appendix provides general instruction and procedures to be used by the
Military Services and the Defense Logistics Agency in receipt and quality surveillance of coal.
C.2 APPLICABLE DOCUMENTS
C.2.1 General. The documents listed in this section are specified in C.3, C.4, and C.5 of
this appendix.
C.2.2 Non-Government publications. The following documents form a part of this
appendix to the extent specified herein. Unless otherwise specified, the issues of this appendix
are those cited in the solicitation or contract.
ASTM INTERNATIONAL
Annual Book of ASTM Standards, Section 5, Petroleum Products, Lubricants, and
Fossil Fuels, Volume 05.05, Gaseous Fuels, Coal and Coke
ASTM D2013 Standard Practice for Preparing Coal Samples for Analysis
(DoD adopted)
ASTM D2234 Standard Practice for Collection of a Gross Sample of Coal
ASTM D4749 Standard Test Method for Performing the Sieve Analysis of
Coal and Designating Coal Size (DoD adopted)
(Copies of these documents are available online at http://www.astm.org or from ASTM
International, 100 Barr Harbor Drive, West Conshohocken PA 19428-2959)
C.3 DEFINITIONS
C.3.1 Definitions. The definitions in Section 3 of this Standard apply to this appendix.
C.4 GENERAL INFORMATION
C.4.1 Coal Rank. A classification designation that indicates the degree of coalification or
metamorphism, that is expressed in successive stages according to percentages of fixed carbon,
moisture, and ash. The degree of coalification is classified into four general categories, or
ranks; lignite, sub bituminous, bituminous, and anthracite.
C.4.1.1. Lignite. Also referred to as brown coal, is the lowest rank of coal. Lignite has the
lowest carbon content, 25 35 percent and a heating value less than 8,300 BTUs per pound.
Typically, lignite has high moisture, greater than 30 percent, and volatile content of ~27 percent.
C.4.1.2 Sub bituminous. A coal whose properties range from those of lignite to those of
bituminous coal. Typically, sub bituminous coal has a carbon content of 35 45 percent, and a
heating value of 8,300 11,500 BTUs per pound. Sub bituminous coal has an inherent moisture
content of 20 30 percent, and a volatile content of 35 47 percent. Sub bituminous coal
generally has a much lower sulfur content than other types, making it an attractive, cleaner-
burning fuel.
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C.4.1.3 Bituminous. A dense, firm black coal, representing about fifty (50) percent of the
steam-electric power generation in the United States. It is also used as a raw material in the steel
and coke industries. Bituminous coal has a carbon content of 45 85 percent, and a heating
value of 10,500 15,500 BTUs per pound. Bituminous coal has a moisture content of 7 20
percent, and a volatile content of 14 36 percent. The only drawback to bituminous coal-fired
power plants is the sulfur content. The sulfur content ranges from 0.5 3.0 mass percent (5,000
30,000 ppm by mass).
C.4.1.4 Anthracite. The highest rank of coal, anthracite is a hard, brittle, lustrous coal. It
represents only a very small segment of the U.S. coal market. Currently, it is only found in 11
northeastern counties of Pennsylvania. Anthracite has a carbon content of 85 98 percent and a
heating value of 13,500 15,000 BTUs per pound. Anthracite coal has very low moisture
content, less than 7 percent and a volatile content of 5 15 percent.
C.4.2 Specifications. Coal specifications are based on the boiler requirements outlined by
the coal-burning facility. Reduced efficiencies plus increased maintenance and handling costs
are associated with the use of non-specification coal. Table C-I outlines the significant coal
combustion characteristics and sensitivities for six (6) different coal combustion technologies.
TABLE C-I. Significant Coal Characteristics Combustion Performance.
1

Properties Single
Retort
Multiple
Retort
Traveling
Grate
Spreader
Stoker
Pulverized
Firing
Cyclone
Size Consist V V V V V V
Moisture M M I M V M
Caking Index I I V M N N
Ash Fusibility I I M M I V
Grind ability N N N N V N
Friability M M M M N N
Volatile Matter M M M I I M
Fixed Carbon N N N N M N
Ash Content I I I I M M
Calorific Value I I I N N N
Ash Viscosity M M M N I V
Ash Composition + + + + + +
Sulfur + + + + + + + + + + + +
Notes
1. Legend for Table is as follows:
V Very important, I Important, M Minor importance, N Little/No importance
+ Very important Ior Iouling reIractory, but little importance to combustion,
++ Important Irom a corrosive standpoint, but little importance to combustion
C.4.2.1 Size requirement. The size requirement (size-consist) is also part of a coal
specification. Double-screened coal is coal that has been screened for both top and bottom size.
Size is defined by the percentage of the coal sample retained on top of the largest-sized screen
and the percentage passing through the smallest-sized screen. An example of double-screened
coal requirement is: 5%, weight, maximum for coal greater than 1 inch, and 15%, weight,
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maximum for coal less than inch. Single-screened coal is only screened for bottom size. Size
is defined by the percentage of sample passing through the smallest-sized screen. An example of
single-screened coal requirement is: 15%, weight, maximum for coal less than inch.
C.4.2.2 Specification revision. A facilitys coal specifications may require revision based on
equipment changes, operational problems or Environmental Protection Agency (EPA)
compliances. The revision of the coal specification will be accomplished by the submission of
DD Form 416, Purchase Request for Coal, Coke or Briquettes. The request will specify the new
requirement or specification and must include justification for the revision or change. Changes
needed during the contract performance will require formal contract modification by the
contracting officer. Contractor agreement and equitable price adjustment will be obtained by the
contracting officer to establish the new coal specification requirement. Until the contract is
modified, coal ordered will continue to comply with the original specification requirements.
C.4.3 Significance of Testing. Many large consumers of coal, as well as most of the large
coal mining companies, have laboratories that sample and analyze coal. This work is done by
the consumer to verify the quality of the coal purchased and to measure the efficiency of their
coal burning equipment. The coal producer performs periodic analyses to monitor coal
preparation methods and variations within a coal seam.
a. Standards used for analytical testing of coal, along with coal specifications and
definitions have been subjected to continuous study and refinement for more than 60 years by the
American Society for Testing and Materials (ASTM). Adhering to these procedures is critical to
the veracity of the sample results.
b. Before any analysis is conducted, Care should be taken to insure that the sample
represents the material being produced. A coal sample usually contains some ratio of coal
particles and extraneous material such slate, pyrite, etc. The analysis is only as good as the
sample it represents.
C.4.3.1 Proximate Analysis. The proximate analysis is an evaluation of four items:
moisture, volatile matter, fixed carbon, and ash. The sum of the percentages of each must equal
100 percent. This analysis is roughly designed to separate the combustible matter from non-
combustible matter, and is used in some instances to determine rank.
C.4.3.2 Calorific Value. The calorific value of coal, or heat content, is express in BTUs per
pound. A BTU (British Thermal Unit) is the amount of heat required to raise one pound of water
from 60F to 61F. The metric system expresses the heat content in calories. One BTU equals
252 calories. To compare the heating value of two or more coals, the calorific value must be
expressed on a dry basis.
C.4.3.3 Sulfur. Is a naturally occurring element in fossil fuels that originated during the
coalification process. Sulfur combined with moisture creates a highly corrosive liquid that is
detrimental to all carbon steel combustion equipment components. In recent years, the
Environmental Protection Agency (EPA) along with state regulatory agencies has been
scrutinizing the sulfur content of coal and other fossil fuels. When fuels containing sulfur are
burned, sulfur dioxide (SO2) is formed in the combustion process and is discharge into the
atmosphere along with other combustible byproducts such as hydrogen sulfide (H2S) and
nitrogen oxides (NOx). If these emissions are combined with a sufficient quantity of water vapor
then sulfuric acid is emitted into the atmosphere. This is commonly referred to as acid rain. For
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these reasons, the federal government has implemented stringent sulfur regulations in an attempt
to drastically reduce the quantity of combustible byproducts emitted into the atmosphere.
C.4.3.4 Ultimate Analysis. The composition of coal is better represented by the ultimate
analysis. This analysis reports the percentage of carbon, hydrogen, sulfur, oxygen, nitrogen, and
ash in a coal sample. It also provides the data needed to calculate combustion factors for steam
generation plants. However the data provides little assistance in predicting the burning
characteristics of coal in a fuel bed.
C.4.3.5 Moisture. All coal has some form of moisture which acts as a diluents during the
combustion process. As a rule, a one percent increase in moisture will reduce the calorific value
by 80-120 BTUs. Moisture may be considered as surface moisture that comes from external
sources such as snow, rain, and mechanical cleaning processes, or inherent moisture (not
external) which is proportional to the coals rank. The moisture reported in proximate analysis is
both surface and inherent. High moisture can affect the handling characteristics of coal.
Freezing temperatures cause wet coal to amass, which directly effects offloading, pulverize
capacity, and flow from storage bunkers.
C.4.3.6 Ash. The chemical composition of the ash is important in determining the fouling
characteristics in a boiler. The quantity of ash generated will help determine the cost and type of
ash handling equipment that is required for a given steam generation plant. There are four (4)
fundamental measurements of coal ash with respect to clinkering tendency and slagging. They
are the softening or fusion temperature of the ash, ash chemical composition, and the total
percent ash in the coal.
a. Initial Deformation Temperature (IDT) - the temperature at which the first rounding of
the apex of the ash cone occurs.
b. As Softening Temperature (AST) the temperature at which the cone has fused down to
a spherical lump in which the height is equal to the width at the base.
c. Hemispherical Temperature (HT) the temperature at which the cone has fused down to
a hemispherical lump at which point the height is one half the width at the base.
d. Fluid Temperature (FT) the temperature at which the fused mass has is almost flat with
a maximum height of 1/16 in.
C.4.3.7 Volatile Matter. Volatile matter in coal is given off as volatile gases, such as
hydrogen, carbon monoxide, methane, and sulfur dioxides. Volatile matter reflects the coals
ability to ignite and burn. Coal having a low volatile content will be more difficult to ignite and
burn than coal having a high volatile content. Volatile content is a very important chemical
characteristic during suspension burning.
C.4.3.8 Free Swelling Index (FSI). Among the numerous test methods used to determine
the expansion and swelling, or caking characteristics of coal, the free swelling index (FSI) is the
most widely accepted. All bituminous coals coke in the sense that when the volatile matter is
driven off by heat in the absence of air, the fixed carbon and ash remaining is coke. The caking
characteristic of coal, however, is the tendency of coal to melt together into a solid mass. Caking
characteristics have little or no effect on the performance of spreader stokers or pulverized coal
fired boilers.
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C4.3.9 Petrographic Analysis. This type of analysis is typically conducted during a mine
evaluation or pre-award survey. The Petrographic analysis of coal was originally used to study
the lithography of coal as a sedimentary rock and to identify the various coal laminae. Two
methods were used: the thin section method and the polished surface method. By studying the
various lithotypes and microlithotypes present, a determination could be made with regards to
the quantity of homogeneous constituents. These constituents are called macerals. Macerals can
be distinguished into the following types: Macerals whose origin is definitely due to woody and
cortical tissues are vitrinite, fusinite, and semi-fusinite. Macerals whose origin is definitely due
to plant material other than woody tissues are resinite, sporinite, alginate, cutinite, and
sclerotinite. Macerals whose origin has not yet been traced to a specific vegetable tissue is called
micrinite. Micrinite is completely structureless and was probably derived from humic mud and
therefore from strongly decaying plant material. Since each of the various macerals has definite
characteristics, a petrographer can determine the characteristics of a particular coal. By knowing
the amount of the various macerals present, a petrographer can also predict a coals behavior
under certain conditions.
C.4.4 DLA-Energy contracts. Under DLA-Energy contracts coal is usually inspected at
source, with acceptance at destination. The contractor samples and tests coal prior to delivery.
Commercial analytical test reports are prepared and accompany the DD Form 250 before or
along with the shipment. If the accompanying documentation, visual examination of the coal
being delivered, or the sampling/testing of the coal being delivered shows failure to meet the
contractual requirements, then it should be rejected as non-conforming (see C.5.10). The activity
shall immediately provide notification to DLA-Energy with all pertinent information regarding
off-specification coal. The contractor may request a waiver through the contracting officer for
Government acceptance of the nonconforming coal.
C.4.5 Quality control plan/procedures. The facility should establish a written quality
control plan for each coal-burning facility (see C.5.1).
C.4.6 Government Representative. In the event work is contracted out a Government
Representative should be assigned to the contract. The representative will serve as point of
contact when coal is received, sampled, tested, or when problems arise.
C.4.7 Personnel training. The receiving facility is responsible for acceptance and receipt
sampling. Only personnel who have been trained and are experienced to receive, sample, and
test coal should be assigned these functions. Guidelines or policy should require individual
training programs and should document completed training. DLA-Energy teaches the Coal
Samplers Certification Course to installation personnel on a cost-reimbursable basis. Contact
DLA-Energy-QA (Phone 703-767-8736 or email DLA-Energy.bqoffice@dla.mil) to request the
DLA-Energy Coal Samplers Certification Course training. Installations may provide this
training through alternate means provided the same level of instruction is provided. Personnel
assigned the responsibility of coal receipt should also be familiar with applicable coal contact
requirements. Personnel not experienced in performing visual examination should receive on the
job training from experienced personnel.
C.4.8 Acceptance. When all contract requirements are satisfied, acceptance is
accomplished by designated facility personnel on behalf of the Government. The DD Form 250
is completed by the responsible official by signing in block 21b, Acceptance. Block 22 is signed
to acknowledge receipt quantity and may be signed by a Government or Government contract
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employee. The DD Form 250 is then forwarded to the proper office within 24 hours of
acceptance to exact payment.
C.5 DETAILED GUIDANCE
C.5.1 Quality control plan.
C.5.1.1 Organization. The quality control plan should contain the name of a person
responsible for coordination on changes and updates to the quality control plan. The quality
control plan should also contain the name of personnel who are points of contact in receiving,
storing, issuing and consumption.
C.5.1.2 Schematic diagram. The quality control plan should contain a detailed schematic of
the facility identifying the coal offloading locations, conveyor systems, sampling points, testing
locations and storage locations. Information on the type of storage, handling equipment, additive
treatment for dust reduction or freeze prevention, and movements of coal within the facility
should be included.
C.5.1.3 Government Representative. The quality control plan should include name of the
Government Representative (see C.4.4), their telephone, cell phone, pager, and facsimile
numbers. The quality control plan should include a sufficient notification time that allows the
Government Representative to be present when coal is received, sampled or tested.
C.5.1.4 Documentation. Identify in the quality control plan who will assure receipt of
copies of solicitations, contract awards and modifications. Identify how product receipt
documents such as DD Form 250s, test reports and weigh bills will be received and distributed.
Identify who will prepare or receive supplemental documentation such as: blending records (if
performed), corrective action requests, quality/quantity investigations, certificates of calibration
(e.g. scales for determination of weight and any other testing equipment), and manufacturers
certificates of conformance (additives for dust control, freeze proofing, etc.). State where (the
office) and how long this documentation will be kept. Note: Contract specified sampling and
testing methods can be found in the Annual Book of ASTM Standards, Section 5, Petroleum
Products, Lubricants and Fossil Fuels, Volume 05.05, Gaseous Fuels, Coal and Coke.
C.5.1.5 Blending. If performed, the quality control plan should include detail procedures
on how coal blending is accomplished.
C.5.1.6 Sampling. The quality control plan should define and include minimum procedures
for the following in the sampling plan: coal sampling for chemical analysis, size-consist, and
additives (receipt and storage sampling). Include requirements for labeling and retaining
samples (specify retention time for each sample). A size consist sample must be retained for a
full seven days.
C.5.1.7 Testing. The quality control plan shall identify or contain the test procedures to be
used for conducting each test. Table C-II outlines by coal rank, the tests typically performed. If
testing is contracted to a commercial laboratory, the testing requirements and methods shall be
outlined in the QCP.

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TABLE C-II. Coal Analysis
Analyses Properties Sub-bituminous Bituminous Anthracite
Proximate Analysis (H20, VM, FC,
ash)
Chemical
Ultimate Analysis (C, H, O, N, S, ash) Chemical
Calorific Value (Btus) Chemical
Fixed Carbon Chemical
Ash Content Chemical
Moisture Content Chemical
Volatile Matter Chemical
Sulfur Content Chemical
Grindability (Hardgrove Index) Physical
Ash Fusibility Physical
Caking Index Physical
Friability Physical
Free-swelling Index Physical
Size Consist Physical
C.5.1.8 Calibration of testing and measuring equipment. Include procedures in the quality
control plan for the calibration of testing and measuring equipment, if used at the facility.
C.5.1.9 Credits and debits. The quality control plan should identify who will monitor the
credits and debits for coal contracts.
C.5.1.10 Off-specification product/operational problems. The quality control plan should
outline procedures for notification of nonconforming coal or operational problems related to
using nonconforming coal. Include notification of DLA-Energy and SCPs when any problem
arises, both remedial and preventative type of corrective action. Examples of areas to be
included are: off-specification product during and after receipt and loss/gain investigations.
C.5.1.11 Product rejection. Include in the QCP procedures on identifying conditions for
rejection and notification of DLA-Energy. DLA-Energy Contracting Officer shall be notified of
0ff-specification coal and approve the rejection before it is returned to the contractor.
C.5.2 Ordering and receiving procedures. All coal orders are issued and funded by the
installation. All coal shipments should be inspected when received, before final acceptance.
Clear and proper inspection procedures are essential, as they show compliance to contract
requirements and are the basis for accurate analytical results. Proper inspection, sampling and
testing procedures support coal being rejected and provide supporting evidence for a price
adjustment claim. These procedures should also be timely because prolonged or delayed
inspection could cause demurrage costs to accrue against railcars or contractors trucks.
C.5.2.1 Documentation. Examine all documentation before offloading (e.g.; weigh bills,
DD Form 250s, analytical test reports).
a. Rail shipment identification. Documentation for rail shipments shall be faxed by the
contractor directly to the receiving facility, SCP and DLA-Energy Offices specified in the
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contract prior to shipment arrival. Rail cars may be separated in transit by the rail company in
the course of normal business practices; therefore, it is necessary to check each car number
against the DD 250 for each shipment. Contractor documentation provided to destination should
include sufficient information to identify the loaded cars by railcar number, quantity loaded,
loading source, and consignee on the DD Form 250.
b. Truck shipment identification. Commercial analytical test results for new stockpiles shall
be faxed to the receiving facility before or concurrent with the first truck delivery from that
stockpile. Material Inspection and Receiving Reports, DD 250s, identifying truck tickets and
weights for each days delivery are to be provided to the receiving activity within 48 hours after
delivery.
c. Source of coal. Receipt documents should identify the required source listed in the
contract. Coal from another mine may not be substituted except as authorized by contract
modification. Before an alternate mine is added to the contract, a mine analysis sample should
be performed to determine the mines capability to deliver spec coal. Report the use of
unauthorized mines to the contracting officer immediately.
C.5.2.2 Quantity determination. When quantity is determined by a facilitys weigh scale,
and not by railroad weigh bill or truck scale weight, then the scales used shall be calibrated as
required by state or local requirements, whichever is more stringent.
C.5.2.3 Credits and debits. Credit and debits are determined based on the analytical test
report data issued by the Army Petroleum lab. Coal may be regularly and continuously sampled
by the using facility in accordance with ASTM D2234. The Army Petroleum lab shall analyze
each sample with respect to the actual tonnage sampled. If the Army analysis report determines
that any coal delivered does not meet the contractors guaranteed specification, the installation
may apply its rights for credits and debits under contract clauses to include Sampling and
Evaluation and Consideration for Excess Sulfur and Ash. If the final determination is a debit,
then the contractor shall be debited before the closing of the contract. Credits shall not be issued.
This data should be reported to the contracting officer prior to end of the contract (penalties for
low ash or high sulfur shall be taken by the contracting officer directly for each delivery
affected).
C.5.2.4 Shipments after end of contract. The installation shall not order any coal after the
contract expiration date. Deliveries of properly placed orders may be accepted up to the last day
of the month following contract expiration. Note: The Contracting Officer may authorize a
contractors request for acceptance of end-of-contract shipments, provided the installation is in
agreement.
C.5.2.5 Acceptance/rejection log. An acceptance/rejection log is recommended, recording
all coal shipments accepted or rejected. This will prevent the off loading of over shipments after
contract completion. The following should be considered when developing a tracking system:
a. A method to assure that shipments and shipping notices are being made according to the
delivery schedule.
b. A schedule that indicates the type of coal and number of rail cars or trucks that are in
transit.
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c. A record of delays in delivery and demurrage charges. Delays in offloading should be
documented in detail to support payment of demurrage. Identify actions being taken (e.g. receipt
sampling, testing), or other actions involved in the demurrage charges.
C.5.3 Inspection procedures. All coal received is to be inspected and sampled for chemical
analysis. Sampling techniques should comply with the standards cited in the contract for coal
sampling methods.
C.5.3.1 Visual examination. Visual inspections should be simple and thorough. They are
mostly subjective, for example, examining coal by comparing to previous shipments. Each coal
shipment should be visually inspected before unloading to assure that:
a. The shipment is free from slate, bone, rocks, sulfur balls, dirt and other foreign material.
b. The coal is properly prepared, is reasonably free from fines (coal smaller than the bottom
screen size), oversize coal (coal larger than the top screen size), and is not weathered. If the coal
does not appear to meet the minimum size requirements, as determined by visual examination
and the facility wishes to reject the coal, a size-consist sample should be collected. The facility
may elect to sample for size-consist on a regular or periodic basis for verification purposes. The
size-consist analysis should be performed in accordance with C.5.8 below.
c. There is no evidence of loss or theft in transit. During the visual examination assure
railroad cars were loaded to full capacity. Loss in transit can occur when hopper doors are not
completely closed during loading, doors are forced ajar during transit, a hole in a car is not
patched properly, or a hole patch worked loose. Ordinarily loss in transit can be determined by a
depression in the contour of the coal above or near the holes or openings in the car. Theft
usually occurs when cars stand for extended periods of time and can be detected by irregular
appearances in the coal on the top of the car. A record should be kept with all information on
discrepant shipments received, including car numbers and discrepancy observed. If losses
appear to be something other than random theft, e.g.: losses occur regularly or from consistent
locations, then fraud should be considered and reported to the proper authorities for
investigation.
C.5.4 Sampling general.
C.5.4.1 Personnel. Only personnel who are qualified by obtaining certification in
accordance with the requirements of section C.4.7 shall collect and prepare the coal samples for
official analysis.
C.5.4.2 Sample preparation. Prepare samples in accordance with ASTM D2013.
C.5.4.3 Sample containers.
10
C.5.4.4 Sample tags. Make complete and correct entries on samples tags regarding each
sample to assure proper analysis and reporting of the sample submitted. The information listed
in C.5.4.6 should appear on the sample identification tag.
Sample containers should be thoroughly clean, dry and
inspected for foreign matter. Care should be taken to protect the gross sample when storing.
C.5.4.5 Sample retention time. When size consist is in dispute, the screened sample should
be retained in a protected area for one week from the date the sample test was completed, or for a

10
Note: The use of glass containers for mailing is not permitted.
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longer time, as determined by the QAR (the sample shall be available to the Contractor and the
QAR for inspection).
C.5.4.6 Sample identification for testing. Proper identification of coal shipments and timely
submission of coal samples is essential. Inaccurate entries may result in preventing the receiving
facility from recovering liquidated damages in claim actions for product substitution. The
following information should be provided:
a. Name and complete mailing address of the facility submitting the sample.
b. Name of the contractor supplying the coal.
c. Contract number.
d. Contract line item number.
e. Size and kind of coal.
f. Tons represented by the sample.
g. Railroad car, truck, or barge number/s.
h. Name of mine and state where the mine is located.
i. Sample number.
j. Sample can number.
k. Sampling point and ASTM condition used in obtaining sample.
l. Date the coal was delivered.
m. Provide mailing addresses of those who shall receive a copy of the analysis.
n. Special test requested, i.e. hardgrove grindability index.
o. Identification of coal sampler.
p. Signature and date signed.
C.5.4.7 Mailing coal samples for chemical analysis. Package the sample in accordance with
ASTM D2013. Send samples to the following Army testing facilityor designated commercial
laboratory for analysis:
US ARMY PETROLEUM CENTER (USAPC)
PETROLEUM TESTING FACILITY
ATTN: AMSTA-LCEJPT, BLDG 85-3
U AVENUE
NEW CUMBERLAND PA 17070-5005
C.5.4.7.1 Special Sample. When packaging and mailing special coal samples to be
tested for dry ash or free swelling index include the following:
a. Mark Special Sample for dry ash or free swelling index analysis.
b. Include in Remarks: Coal represented by this sample is subject to rejection.
c. Mark the mailing wrapper, Special Sample.
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d. Forward by air mail.
e. Inform the DLA-Energy contracting officer, coordinating with the service control point,
by telephone or facsimile that the sample was mailed, and provide the sample container number.
This shall enable the Contracting Officer to expedite the testing of the coal sample.
C.5.5 Sampling for chemical analysis. The collection of the gross sample for chemical
analysis is the single most important function in the process of testing for coal quality and
payment. Sampling for chemical analysis should occur at time of receipt. Automatic samplers
in accordance with ASTM D4702 are best for obtaining coal samples due to consistency of
timing and type of cuts. Coal may also be sampled manually in accordance with ASTM D2234
with the preferred sampling conditions being either condition A (Stopped-Belt Cut) or condition
B (Full-Stream Cut). Condition C (Part-Stream Cut) and condition D (Stationary Coal
Sampling) of ASTM D2234 are considered to be the least reliable methods of sampling coal. If
condition C or D are called for in the contract, extreme care is needed to assure proper sampling.
Table 2 of ASTM D2234 should be used when determining increment weight. It is recognized
that in some cases it is not feasible to use either ASTM D4702 or ASTM D2234 conditions A, B,
or C. Therefore, the following is provided as a guide in obtaining the samples for chemical
analysis.
C.5.5.1 Sampling equipment. All sampling devices should have an opening of at least two
and one half times larger than the top size of the coal being sampled. The device should be
capable of retaining the required increment weight and not spill material when the increment is
withdrawn. Equipment such as a square shovel with built-up metal plates 4 inches (10 mm)
high, a hand-operated auger, or a powered auger may be used in obtaining coal samples from
stationary conveyances. The sample device should be capable of collecting the entire increment.
Post-hole diggers may not provide a representative sample because small particles may escape.
C.5.5.2 Procedures. For obtaining stationary samples, use diagrams and tables in ASTM
D4915, for rail or trucks shipments (9-Point, Car top Sampling). The sampling guide in ASTM
D4915 is to be used only when the preferred methods in ASTM D2234, condition A condition
B or condition C are not feasible. Condition D is the least desirable method for the
collection of a gross sample. The use of this method should only be used when it is required by
the contract or when sampling conditions A, B, or C is not feasible.
C.5.6 Sampling for dry ash and free swelling index. The gross sample for determination of
ash and FSI should be obtained by using the methods outlined in ASTM D2234, Condition D,
and ASTM D4915. Samples should be prepared in accordance with ASTM D2013.
C.5.7 Sampling for size consist. The facility is responsible for performing the sizes consist
sampling and testing when required at destination for railcars and trucks. Stationary sampling of
trucks may be performed by activity personnel, provided training and safety requirements are
met. Sampling for size consist is performed when a visual inspection indicates coal exceeds the
size requirement in the specification. If the facility does not have properly trained personnel or
necessary equipment to perform the sampling or testing, the facility may contract for this
function to an approved coal inspection company. When determining the size consists on coal
received, use the contract specification requirement.
C.5.7.1 Collection of the size consist sample (9-Point, car-top sampling method). Sample
should be taken in accordance with figure C-1 below and ASTM D4915. A size consist sample
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should be no less than 453.59 kg (1000 pounds) taken in equal increments, from the nine points
of each conveyance, representing one shipment of no more than five (5) conveyances, received
in one day. The sample should be collected, weighed, and then screened without mixing or other
preparation. The following minimum weights and increments are required for the number of
cars and/or trucks to be represented by the sample.

Numbers of
Conveyances
Minimum Weight from
Each Point/Conveyance
Total Increment Weight from
Each Car
1 50.80 kg (112 lbs) 453.59 kg (1000 lbs)
2 25.40 kg (56 lbs) 226.80 kg (500 lbs)
3 17.24 kg (38 lbs) 151.50 kg (334 lbs)
4 12.70 kg (28 lbs) 113.40 kg (250 lbs)
5 10.42 kg (22 lbs) 90.72 kg (200 lbs)
FIGURE C-1. Weights and Increments
a. Lay out three diagonals across the top of each conveyance to be sampled (see figure C-2).
Remove the top 450 mm (18 inches) of the coal from each of the diagonals to form trenches the
width of the coal sampling device. Begin at the front corner of the conveyance extending
diagonally across. Begin the second trench near the center and the third at the rear corner.
Distribute the spoil over the top of the undisturbed coal where it shall not intrude into the sample.
b. Collect equal increments from each of the nine sampling points. As can be seen from
figure C.2., the sampling points 1, 3, 4, 6, 7, and 9 are located near the edge of the conveyance.
c. The required minimum weight of each increment is found in the chart above.
d. A shovel meeting ASTM D4915 requirements shall be used. Build up standard flat
square shovel with two sides and back plates. Build up should be at least 4 inches (100 mm),
constructed from metal. Exercise care in taking each increment to keep to a minimum the
quantity of coal falling from the sides into the bottom of the trench. Each shovel full taken
without loss of coal is considered an increment.
e. At each point (figure C.2.) proceed as follows:
(1) Trench 1, first sampling point. Retain the first increment for the sample and spoil the
second. Then alternately retain one increment and spoil one until the predetermined weight of
coal is collected at point number 1.
(2) Trench 1, second sampling point. Spoil the first increment then retain the second and
third increment. Then alternately spoil two increments and retain one increment, until the
predetermined weight is obtained.
(3) Trench 1, third sampling point. Spoil the first two increments, retain the third and
spoil the next three. Then alternately retain one and spoil three until the predetermined weight is
collected.
(4) Trench 2, fourth sampling point. Collect as trench 1, third sampling point (see
above).
(5) Trench 2, fifth sampling point. Collect as trench 1, first sampling point (see above).
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(6) Trench 2, sixth sampling point. Collect as trench 1, second sampling point (see
above).
(7) Trench 3, sampling points 7, 8, and 9. These sample points shall be handled the same
as trench number 1, sampling points 1, 2, and 3, respectively.

FIGURE C-2. Car Top Sampling
C.5.8 Size-consist test procedures. The sieve analysis should be performed in accordance
with ASTM D4749.
C.5.8.1 Record of analysis. For each sieve analysis performed the following information
should be recorded:
a. Contractor providing the coal.
b. Contract number and contract line item number.
c. Conveyance identification and number/s.
d. Mine name and seam the coal originated from.
e. Method used in obtaining the sample (ASTM D2234).
f. Date the sample was obtained.
g. Date the sieve analysis was performed.
h. Type, kind (round hole or square) and size of screen(s) used, and whether automatic or
manual method was used.
i. Percent of coal remaining on the screen (single-screen coal).
j. Percent of coal remaining on the top screen, percentage of coal passing through the
bottom screen and the total percent between the screens (double-screened coal).
k. Percentage gained or lost.
l. Name of the person performing the sieve analysis.
C.5.8.2 Example of calculation. A sample of one thousand pounds was used to perform the
sieve analysis. A double-screen analysis was required with a top size of 2 and a bottom size oI
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. One hundred pounds oI coal remained on the top screen, and fifty pounds passed through
the bottom screen after completion of the test. Eight hundred and fifty pounds remained between
the two screens.
a. Top size percent (weight of coal remaining on top screen) (100 lbs, top screen/1000 lbs,
total sample) x 100 = 10%.
b. Bottom size percent (Weight of Coal Passing through the Bottom Screen) (50 lbs pass
thru, bottom screen / 1000 lbs, total sample) x 100 = 5%.
C.5.8.3 Testing accuracy. To ensure the accuracy of the size testing, a gain or loss
percentage should also be calculated. A gain or loss percentage is the total weight remaining on
the top screen, plus the total weight remaining on the bottom screen, plus the total weight passing
through the bottom screen, and divided by the total weight of the sample used to perform the test
times 100.
a. Gain (Loss) = (total weight of sample (1000 lbs)) minus (100 lbs top + 50 lbs pass
bottom + 840 lbs remaining on bottom screen) / (total weight of sample (1000 lbs)) x 100 = 1%.
b. If the gain or loss is greater than two percent (2%), the testing tolerance has been
exceeded and the results are invalid. The test should be repeated after validation of proper
testing technique.
C.5.9 Rejection of unidentified or non-conforming shipments. Shipments should be
rejected for any of the following:
a. A discrepancy exists in or between the shipping notices, weigh bills, and contract
requirements or the DD Form 250 is not received. For example: coal is sent to wrong facility;
coal is received from the wrong mine or contractor; receipt of an unauthorized over shipment; or
coal test reports showing non-conforming coal.
b. When visual examination shows non-conforming coal (inherent or foreign matter).
(1) When rejection of coal is based on excessive inherent material (e.g.; slate, bone, dirt,
rock or other contaminating material that through experience would fail the ash requirement), the
Contractor may request the facility to obtain a sample and have the sample analyzed for ash
content. The Contractor should make the request through the Contracting Officer within 48
hours after the notice of rejection.
(2) When a shipment is rejected based on excessive foreign matter (e.g.; magnetite,
wood, large sulfur balls, lumps of rock, slate), the facility should immediately advise the
contracting officer through channels of the rejection. The contracting officer notifies the
contractor of the rejection. No sample for ash analysis is required for rejections based on foreign
matter.
(3) When the basis for rejection is excessive oxidized or weathered coal, the Contractor
may request a sample be obtained and analyzed for FSI, if FSI is required or guaranteed by the
contract (use the sampling procedures in C.5.6).
(4) When visual examination indicates that a shipment will be rejected for size consist, a
sample should be obtained and a sieve analysis performed. Guidance for obtaining a sample for
sieve analysis is found in C.5.7.1 (nine-point method). The nine-point method outlined, along
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with ASTM D4749 should be used as a standard for obtaining the 1,000 pound sample for testing
for size consist.
c. Coal shipment should be rejected when visual examination shows there is evidence of
loss or theft in transit that exceeds the tolerances established by the railroad tariff. The facility
should take action to have the shipment weighed as near to the point of acceptance as possible.
If railroad scales are not available and the shipment cannot be weighed without delay, any
excessive back haul or additional freight adjustments should be established by the railroad claim
agent or other designated individual. All parties involved in the dispute may, by visual
examination, determine an agreed revised estimated weight to be accepted. As stated earlier, if
losses appear to be something other than random theft, e.g., losses occur regularly or from
consistent locations, then fraud should be considered and reported to the proper authorities for
investigation.
C.5.10 Product rejection procedures. When chemical samples taken during offloading are
tested and reported as nonconforming, the Contracting Officer shall be notified, identifying the
failing characteristic, quantity of coal, and location.
C.5.10.1 Notification to Contracting Officer. The facility shall notify the Contracting
Officer, DLA-Energy-APC (Phone: 703-767-8527; FAX: 703-767-8757), DLA-Energy-BPE
(Phone: 703-767-8362; FAX: 703-767-8366), and DLA-Energy-QA (Phone: 703-767-8744; Fac:
703-767-8747). DLA-Energy-BPE monitors coal Product Quality Deficiency Reports (PQDRs).
Include the following information:
a. Name of the Contractor
b. Contract number
c. Quantity of coal in tons awaiting disposition
d. Date of shipment
e. Status of the shipment
f. Nature of the discrepancy or problem
g. Point of origin
h. Railroad car or truck numbers
i. Status of any ongoing or planned testing pertaining to the coal shipment, Chemical
Analysis.
C.5.10.2 Notification of contractor. The contractor is formally notified of the rejection by
the contracting officer. The contractor has the right to confirm coal quality or provide missing
information. The contractor may request acceptance by the Government of nonconforming coal,
referred to as a contract waiver request. The contracting officer shall provide the facility with
disposition instructions on the rejected coal through required channels in a timely manner.
C.5.10.3 Withdrawal of rejection. If testing shows the coal meets contract specification
requirements, the facility shall notify the contracting officer, coordinating with the service
control point, of the results. The contracting officer shall then withdraw the rejection notice,
notifying the contractor. The receiving facility is responsible for paying any charges associated
with the delay of off loading the conveyances due to the unsubstantiated rejection. The facility
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should not discuss with the contractor matters regarding nonconforming coal. Negotiations, as
appropriate, are conducted through the contracting officer.
C.5.11 Evaluation of the Coal. Upon receipt, the U.S. Army Petroleum Center or contract-
designated laboratory shall test and issue an analytical test report of the coal sample. These
reports are used to evaluate contractor performance. These reports can also be used by the
facility to compare results received at origin to those received at destination. The price paid to
the supplier may be adjusted either up or down based upon the test results of the sample taken at
the destination (see C.5.2.3).
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176

GOVERNMENT QUALITY SURVEILLANCE OF FUEL
D.1 SCOPE
D.1.1 Scope. This appendix provides general information on the Governments quality
surveillance program for fuels, lubricants and related products. This appendix is not a mandatory
part of this Standard. The information contained herein is intended for guidance only.
D.2 APPLICABLE DOCUMENTS
D.2.1 This section is not applicable to this appendix.
D.3 DEFINITIONS
D.3.1 The definitions in Section 3 of this Standard apply to this appendix.
D.4 RESPONSIBILITIES
D.4.1 Joint Petroleum Office (JPO). The JPO is responsible in overseas areas for ensuring
an adequate quality surveillance program is maintained within the unified command. Direct
communication between DLA-Energy and the JPO on all petroleum matters has been authorized.
D.4.2 Military Services. The Service having physical possession of the petroleum products
is responsible for establishing and maintaining a quality surveillance program. The Services also
establish or furnish minimum usability limits for petroleum products.
D.4.2.1 Non-conforming product. All Service-owned petroleum products exceeding
allowable specification limits should be reported to the owning military Service Control Point for
disposition instructions. For nonconforming Defense Working Capital Fund products, the
Services retain the right of acceptance (see 5.13 for disposition procedures with non-conforming,
Defense Working Capital Fund product).
D.4.2.2 Service laboratory testing. See Appendix A for a breakdown of Service
laboratories, their locations, and testing capabilities. For overseas locations, laboratory facilities
are provided and maintained for the testing of fuels and lubricants in accordance with DLA
4155.29. The Military Service(s) should identify when laboratory support cannot be provided as
cited above.
D.4.2.3 Specification development. The Military Services, as engineering support
activities, develop specifications, or accept specifications developed by other organizations.
D.4.3 Headquarters DLA-Energy, its regions and offices. DLA-Energy maintains and
oversees quality control programs to assure product quality is maintained from purchase to
customer receipt. DLA-ENERGY maintains this Standard in coordination with the technical
services.
D.4.3.1 Nonconforming Defense Working Capital Fund product. In addressing
nonconforming, Defense Working Capital Fund product, the requirements of this Standard
should be followed. When Defense Working Capital Fund products show deterioration beyond
specification requirements, DLA-Energy-QA or DLA Aviation should be notified, as stated in
5.13 and 5.14.4. Customers should be notified prior to receiving product when only meeting
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intra-Governmental receipt limits. Service control points determine the acceptability of material
not meeting intra-Governmental receipt limits.
D.4.3.2 Commercial laboratory facilities for bulk petroleum products. DLA-Energy
contracts for commercial laboratory testing of petroleum products worldwide in accordance with
the needs of DLA-Energy and the Military Service(s).
D.4.3.3 (DLA AVIATION). For packaged products, DLA Aviation maintains and
oversees quality control programs to assure product quality is maintained from purchase to
customer receipt.
D.4.3.4 Commercial laboratory facilities for packaged petroleum product. DLA Aviation
identifies and contracts for commercial laboratory testing of packaged products. The Military
Service(s) identify to DLA Aviation required testing coverage.
D.4.4 Conflict with service publications. Anyone who has knowledge of a conflict between
what is in this Standard and any Service technical publication is requested to bring it to the
attention of DLA-Energy-QA/BP. Resolution of these conflicts will be addressed individually.
D.4.5 Quality surveillance representative (Government Representative) responsibilities.
The Government Representative responsibilities include the following:
a. Assure that the contractor establishes and maintains an acceptable program for the control
of quality of petroleum products furnished to or handled for the Government. The contract may
require a written quality control plan or procedures.
b. Report to the region and the ordering officer at the activity placing the order, any
information on delays in shipping the product caused by labor strikes, fires, or other conditions
that result in non-availability of cargo or the inability of the contractor to perform. The reports
should be made as soon as possible, but no later than the next working day, via telephone, fax, or
e-mail.
c. Perform the following, when requested:
(1) Investigate petroleum product reported to be contaminated or causing unsatisfactory
operation of equipment. The results of any findings given to a using activity are in an advisory
capacity only.
(2) Participate in pre-award surveys and post-award conferences.
(3) Monitor/witness the analysis of special samples of products submitted to commercial
laboratories under contract.
(4) Maintain surveillance over the special blending and compounding of products.
(5) Assist the military supply and transportation offices on pertinent matters.
(6) For issues effecting termination settlement at the facility, ascertain the quality and
quantity of products on hand, volume of tank bottoms, and numbers of drums.
d. Advise the contracting officer, through appropriate channels, of contractor
noncompliance with contract provisions in those cases where adequate local correction is not
possible or failure to report might jeopardize the rights of the Government under the contract.
e. In contracts relating to receipt and storage of products procured for Government use, if
the contractor does not provide technical personnel to perform laboratory testing, the
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178
Government Representative may be responsible for performing those tests necessary to assure
the quality of products received, stored, and shipped at that location. Instructions contained in
this Standard and DoDM4140.25M should be used.
f. Maintain vigilance over quality and quantity of Government-owned petroleum products,
containers, and equipment in the possession of contractors.
g. Advise the contracting officer of the date and time a commercial storage tank used to
store Government-owned product is put into or out of service. Such reports apply to the removal
of tanks from service for cleaning or repairs as well as initial use of termination of use under a
contract.
h. Verify inventory process for Government-owned petroleum product. The certifies the
accuracy of the inventory data and agrees or disagrees in writing with the contractors stated
cause(s) of losses/gains. In the event that the Government Representatives opinion as to loss
data is at variance with the statements of the contractor, the Government Representative submits
his reasons for nonoccurrence by letter to the office receiving the report. The Government
Representative assures, to the extent practicable, that all factual data pertaining to losses are
included in the stock report or in a separate letter. Certain contracts provide for periodic
evaluations of contractor performance by the Government Representative. These reports are
valuable tools in the correction of deficiencies and selection of contractors. Accordingly, such
reports should factually report any and all significant areas and incidents of poor performance.
Details relating to losses and accounting of Defense Working Capital Fund products are
contained in the DoDM4140.25M. There is no Government Representative certification on the
DD Form 1788, Bulk Petroleum Terminal Report. The results of the periodic Government
Representative inventory verification is documented with wording from the appropriate contract
clause and filed with the individual transaction document. These documents are kept at the
DFSP with a copy forwarded to the cognizant property administrator or accountable activity.
The Government Representative witnesses the contractor inventories within the time intervals
listed below. The Government Representative witnesses the contractors end-of-month
inventories whenever the adequacy of the contractors inventory reporting system is questionable
and continues until the contractors system is considered acceptable. The witnessing of the
inventory and verification of the contractors system should be scheduled at different times
within the intervals provided below with the contractors coordination. The following time
intervals are the minimum, in determining the frequency of inventory verification:
(1) Active DFSP (three or more issues/receipts in six months): witness inventory and
verify against receipts/issues monthly.
(2) Semi-active DFSP (less than three issues/receipts in six month): witness inventory
and verify against issues/receipts once each calendar quarter.
(3) Commingled storage (Government-owned product stored with contractor-owned
product): verify that sufficient inventory is on hand each calendar quarter.
(4) Foreign Government and NATO held storage under memorandums of agreement
(MOAs) or country-to-country agreements: inventory should be witnessed and verified by the
Government Representative according to the terms of the agreement.
i. Losses of Government-owned product in the custody of contractors, which are caused by
accident or mishap, including line breaks, tank overflows, spillage, product contamination, and
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179
fire, are investigated by the Government Representative, and a detailed factual report is provided
to the accountable activity and the contracting officer.
j. Government property is subject to loss, damage, or destruction and may be found, upon
receipt, to differ from the property indicated to have been shipped. In order to assist in the
preparation of reports of survey, the Government Representative responsible for inspection of
shipments received submits all pertinent information to the designated accountable activity and
the contracting officer.
k. Certain contracts require the Government Representative to certify the contractor invoice
for specified services delineated in the contract, e.g.: guard service, laboratory testing services,
overtime, etc. Since the Government Representative normally is not physically present at the
facility during the entire period covered by the invoice, a certification as follows should be used.
Based on recorded checks made during surveillance of the contractors quality program and a
review of the contractors time and attendance records, I certify the contractors invoice to be
true and correct. Specified service invoices shall comply with contractual requirements which
are covered under Bulk Services Contract clause G148.05, paragraph b, subparagraph 3.
l. The Government Representative is responsible for developing their own checklists and
tailoring them to the particular facility.
m. SF 361, Transportation Discrepancy Report, is prepared by the designated accountable
activity when Government-owned petroleum and related products, shipped on Government bills
of lading, are received at a contractors facility in an improper condition, and such damage, loss,
or destruction is attributable to causes incident to shipping. In order to facilitate the preparation
of this report, the Government Representative responsible for inspection at contractors facilities
receiving shipments submits all pertinent information to the designated accountable activity.
The Government Representative checks shipments to determine the extent of the damage,
shortage, and the cause, if possible. Information and documents submitted include:
(1) Two true copies of Government bill of lading, including discrepancy notation on the
reverse side.
(2) Certified true copies of the freight bill or delivery receipt showing any discrepancy
notation and signature thereon.
(3) A signed statement of the carriers local agent (carriers inspection report) admitting
existence of the shortage or damage. It should be noted that this is not an admission of liability.
(4) The receiving Government Representative checks signed statement containing the bill
of lading number, the number of packages received, the condition of the packages, a record of
seals on the car or vehicles at origin and destination, and whether applied by shipper or carrier,
and a statements as to the cause of damage, if known or otherwise a reliable opinion based on
circumstantial evidence shall be furnished.
n. The Government Representative assists in the development of operating agreements,
between the Government and the carrier that establish procedures for transportation,
accountability, and quality control of Government fuel. The instructions applicable to petroleum
movements via Government-owned multi-product pipeline systems are contained in this
Standard and departmental instructions.
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180
o. The Government Representative assures that samples of Government-owned petroleum
products in bulk storage at Government or contractor-operated terminals in CONUS are
submitted in accordance with this Standard.
p. When Government-owned stock in the custody of a contractor is indicated to be off-
specification or projected to deteriorate below specification requirements in the near future, the
Government Representative forwards copies of the test reports to DLA-Energy, ATTN: DLA-
Energy-QA; and to the appropriate DLA-Energy Region. The reports should clearly indicate the
product deficiency by appropriate comment on the reports and its relation to any recommended
disposition action.
q. Implemented in 1992, process control (formerly in-plant quality evaluation) is used in the
quality surveillance program to assess the adequacy of contractors processes to consistently
meet contractual requirements in storage and laboratory testing contracts. (Note: This does not
apply to mandatory inspection requirements performed on vessel loadings/discharges, pipeline
shipments/receipts.) For those contractor facilities whose processes are in control and where no
customer complaints have been received, the cognizant Government Representative may reduce
physical oversight at that facility.
r. The Government Representative assists in the reporting and investigation of customer
complaints or product quality deficiency reports (PQDRs) in a timely manner to DLA-Energy-
QA. Basic PQDR information is input into the DLA-Energy-QA database (CDC); supplemental
information is forwarded to DLA-Energy-QA. PQDRs are used to evaluate contractor
performance under best value.
D.5 QUALITY CONTROL PLAN/PROCEDURES.
D.5.1 Quality control plan/procedures. Each fuel handling activity is usually required to
establish a written quality control plan. Service technical orders, field manuals, and instructions
fulfill this requirement. For contractors, the contractor usually has the option to provide and
maintain an inspection system that, as a minimum, incorporates the requirements such as those in
Q91 (ISO 9001) Quality Systems - Model for Quality Assurance in Design/Development,
Production Installation, and Servicing. However, the exact requirements for contractor quality
control plans/procedures appear in the contract and those requirements rather than this appendix
are what must be followed. If the owning service/contractor chooses to comply with Q91 quality
system format, then all the specific quality provisions listed below would normally be included
in the Q91 written quality plan:
D.5.2 Typical contents of a quality control plan/procedures.
a. The existing organization of the service or storage facility is defined, identifying points of
contact responsible for coordinating all quality control functions within the facility. In each key
position a person should be appointed, such as laboratory, tank farm, docks, etc., to act as point
of contact for operations.
b. A quality control plan contains a detailed schematic of the facility. All areas covered by
the inspection system are marked, such as blending, pipelines, tanks, docks, loading racks,
laboratories, and all other areas concerning key processes.
c. In the event responsibility for petroleum products has been contracted out, a quality
control plan assigns a Government Representative to the contractor and includes the
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181
representatives name, their telephone, pager, and facsimile numbers, to allow contact.
Notification is made for such operations as: testing, sampling, loading, discharges, or when an
unscheduled situation arises that might cause a problem in product or service. Notification will
be in sufficient time, as identified in the quality control plan, to allow the representative to be
present.
d. Only competent and properly trained personnel are to be assigned responsibility of
receiving/storing/releasing, sampling, and testing of Defense Working Capital Fund fuel.
Established service guidelines or company policy should include an individual training program
and the training completed should be documented.
e. A quality control plan states how documents will be controlled: A quality control plan
outlines document distribution time for reporting, document retention time, and projected date
for the next review and obsolete documents will be removed from the area. Required documents
include the quality control plan, specifications, test procedures, SOPs, and any other material
directly affecting the inspection system.
f. A quality control plan describes the procedures used for receiving both product and
additives. This includes: item specification, quality procedures (receipt and storage), and a
description of the location and overall receiving operation.
g. A quality control plan describes the procedures used for blending. This includes all
products and additive injection at all locations.
h. A quality control plan describes the sampling plan. The plan includes as a minimum
procedures for the following: additives (receipt and storage); tank samples; line samples;
conveyance samples; and samples to be taken prior, during, and after loading. The plan contains
the method by which all samples will be labeled and retained. The time of retention is also
specified for each sample. Sampling is in accordance with the MPMS, Chapter 8, and retention
times in accordance with this Standard.
i. A quality control plan describes the tests to be conducted on each sample submitted. It
contains the test procedures for each test. The requirements of Tables VIII and IX are
incorporated into the plan. The plan specifies where the tests will be conducted. When samples
are to be shipped for testing, the plan states the quantity, type of container, identification,
packaging, packing, and mode of shipment to be used.
j. A quality control plan describes the method by which all laboratory and field testing and
measuring equipment is calibrated in accordance with ISO 10012-1. For items not covered by
that publication, the applicable manufacturers recommended calibration method(s) are used.
k. A quality control plan includes detailed information on the type of storage and handling
equipment and procedures to be used. All tanks, lines, valves, manifolds should be designed to
handle the specified product and be in good repair. The plan includes a description of: the use of
segregated/common product systems; controls to assure the capability for proper gauging,
sampling, and draining of water; filtration; circulation; and other process/system used in
maintaining product integrity during storage and handling.
l. A quality control plan describes the manner by which products will be moved from
acceptance tanks to the conveyance. Examples of information needed are size of lines, type of
product in lines, valves to be operated/blocked/blinded, how lines will be packed, etc. The plan
includes details on how product integrity will be assured immediately before, during, and after
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182
loading and shipping operations. The plan gives detailed information on the procedures to be
used to assure line fills meet specification requirements; conveyance inspection criteria prior,
during, and after loading; completion and distribution of required documentation; and any other
information deemed necessary.
m. A quality control plan describes how all required records and reports will be prepared and
maintained. The plan states where, how, when, who, and for how long retained. The documents
to be covered include, but not limited to, test reports (both additive and product), blending
records, gauging records, movement records, dock logs, corrective action requests,
quality/quantity investigations, ullage reports, DD Forms 250 and 250-1, bills of lading,
certificates of calibration, manufacturers certificates of conformance, and any other documents
affecting product.
n. A quality control plan describes how the contractor will determine the quantity of product
and additives received, stored, injected, and shipped. All measurements are made in accordance
with the MPMS, Chapters: 2 (Tank Gauging), 5 (Metering), 7 (Temperature Determination), 10
(Sediment and Water), 11 (Physical Properties Data), 12 (Calculation of Petroleum Quantities),
and 17 (Marine Measurement). Procedures should cover shore facilities and conveyances
(vessels, trucks, pipelines, etc.) All quantities are determined by use of calibrated bobs and
tapes, calibrated scales, or calibrated meters.
o. A quality control plan outlines the complete plan of corrective action. This includes
notification of DLA-Energy and DLA-Energy Regions when any unscheduled event arises that
may affect product or service quality or quantity. It includes both remedial and preventative type
of corrective action. Examples of items to be included (but not limited to) are: off-specification
product (prior to, during, and after loading / discharge); conveyance rejection; leaks; loss/gain
investigations, etc.
D.6 NOTES
D.6.1 This section is not applicable to this appendix.

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APPENDIX E
183

PRODUCT CHANGE RECORD
E.1 SCOPE
E.1.1 Scope. This appendix provides general guidance on preparing a product change record.
This appendix is not a mandatory part of this Standard. The information contained herein is intended
for guidance only.
E.2 APPLICABLE DOCUMENTS
E.2.1 This section is not applicable to this appendix.
E.3 DEFINITIONS
E.3.1 The definitions in Section 3 of this Standard apply to this appendix.
E.4 SUGGESTED FORMAT FOR A PRODUCT CHANGE RECORD
E.4.1 Product Change Record. The following information should be included in a product
change record.
a. Location: Enter the name of terminal or location on line where data is being generated.
b. Date: Indicate day, month, and year data was accumulated.
c. From: Indicate name, density (API gravity), and flash (if applicable) of head product.
d. To: Indicate name, density (API gravity), and flash (if applicable) of material displacing head
product.
e. Pumping rate: Indicate barrels per hour and barrels per minute.
f. Change arrived: Indicate dispatchers estimated time of product arrival and actual time of first
gravity break.
g. Time: Indicate the hour and minute each line sample is taken.
h. API gravity/density: Enter the API gravity/density of each line sample.
i. Tank Number: Enter the number of the tank or tanks receiving the interface (if applicable).
j. Flash: Indicate flash point in degrees Celsius (Fahrenheit) (if applicable).
k. BBLS Mix: Indicate increment volume receiving from time of one sample to the next.
l. Average API Gravity/density: Indicate average API gravity.
m. Average relative density. Indicate the average API Gravity/density converted to relative
density.
. Percent displacing product in mix: Enter in this column the results from the following formula:
(Average relative density of BBLS mix)-(relative density of head product
X 100

(relative density of displacing product)- (relative density of head product)
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184
n. BBLS Displacing product in mix: Enter in this column the results of the following formula:
(Percent displacing product in BBLS mix) (BBLS mix)
o. BBLS head product in mix: Enter in this column the result of the following formula:
(BBLS Mix) - (BBLS Displacing product in mix)
p. Gravity change: Enter in this column the result of the following formula:
(Average relative density of BBLS MIX) - (Relative density of head product)
E.4.2 Example of product change record. The product change record illustrates typical
entries. An example of a minute increment calculation is as follows:
a. Head product is gasoline with 66.1 API gravity and 0.7161 relative density.
b. Displacing product is fuel oil with 41.4 API Gravity and 0.8184 relative density.
c. Flow rate is 2025 barrels per hour or 33.74 BBLS per minute.
d. Calculation:
(1) Sample at 0809 (14 minutes): API: 45.9, SpGr: 0.7976
(2) Barrels mix at 0809 (14 minutes) is 33.8.
(3) Average gravity of volume increments at 0808 (13 minutes) at 0809 (14 minutes) is an
API gravity of 47.2 API, or density of 0.7918.
(4) Example: Percent displacing product in mix would be:
((0.7918(average relative density of BBLS Mix)-0.7161(relative density of head product)) 100 =73.99% of mix
((0.8184(Relative density of displacing product)-0.7161(relative density of head pProduct))
(5) Example: BBLS Displacing product in mix would be:
(73.99% (displacing product of fuel oil mix)) (33.8 (BBLS mix))=8.8 head product (gasoline) in mix
(6) Example: BBLS head product in mix would be:
(33.8 (BBLSs mix))-(25.0 BBLS displacing product (fuel oil))= 8.8 BBLS head product (gasoline) in mix
(7) Similar data should be calculated for each increment of change. The cumulative totals of
each product are then added and inserted at bottom of applicable columns of the work sheet (see
figure E-1.).
E.5 NOTES
E.5.1 This section is not applicable to this appendix.
MIL-STD-3004C
APPENDIX E
185

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LOCATION: 7:55 66.1
PRODUCT: MOGAS 7:57 65.9 67.5 66.0 0.7165 0.39 0.27 67.2 0.0004
API GRAVITY: 66.1 7:58 65.8 33.8 65.9 0.7158 0.68 0.23 33.6 0.0007
RELATIVE DENSITY:
0.7161
7:59 65.7 33.8 65.8 0.7172 1.07 0.36 33.4 0.0011
FLASH: N/A 8:00 65.2 33.8 65.5 0.7183 2.15 0.73 33.1 0.0022
8:01 64.7 33.8 65.0 0.7201 3.91 1.3 32.5 0.0040
8:02 63.8 33.8 64.3 0.7227 6.45 2.2 31.4 0.0066
TO 8:04 61.7 67.5 62.8 0.7283 11.93 8.1 59.4 0.0122
PRODUCT: FUEL OIL 8:05 58.2 33.8 60.0 0.7389 22.29 7.5 26.3 0.0228
API GRAVITY: 41.4 8:06 54.1 33.8 56.2 0.7539 36.95 12.5 21.3 0.0378
RELATIVE DENSITY:
0.8184
8:07 50.3 33.8 52.2 0.7703 52.98 17.9 15.9 0.0542
FLASH: N/A 8:08 48.5 33.8 49.4 0.7822 64.61 21.8 12.0 0.0661
8:09 45.9 33.8 47.2 0.7918 74.0 25.0 8.8 0.0757
8:10 44.2 33.8 45.1 0.8012 83.19 28.2 5.6 0.0851
8:11 43.4 33.8 43.8 0.8072 89.05 30.1 3.7 0.0911
8:12 43.2 33.8 43.3 0.8095 91.30 30.9 2.9 0.0934
PUMPING RATE: 8:13 42.3 33.8 42.8 0.8118 93.55 31.6 2.2 0.0957
BARRELS PER HOUR: 2025 8:14 42.2 33.8 42.3 0.8142 95.89 32.4 1.4 0.0981
BARRELS/MINUTE: 33.75 8:15 42.0 33.8 42.1 0.8151 96.77 32.7 1.1 0.0990
8:16 41.4 33.6 41.7 0.8170 98.63 33.3 0.5 0.1009
8:18 41.4 67.5
CHANGE ARRIVED: 8:20 41.4 67.5
DISPATCHER EST: 0750
HRS

FIRST BREAK: 7:57 a.m.

FIGURE E-1. Sample calculation product change record

MIL-STD-3004C

APPENDIX F
186

PETROLEUM SAMPLE CHAIN OF CUSTODY DOCUMENT
F.1 SCOPE
F.1.1 Scope. This appendix provides the examples of page 1 and page 2 of the Chain of
Custody Document recommended for tracking sample history and transfer of custody. See figures F-
1. and F-2. This appendix is not a mandatory part of this Standard. The information contained herein
is intended for guidance only.

MIL-STD-3004C

APPENDIX F
187

FIGURE F-1. Chain of Custody Document Page 1
COC DOCUMENT NUMBER
RECEIVING ACTIVITY LOCATION
NAME, GRADE AND TITLE OF PERSON FROM WHOM RECEIVED ADDRESS (Include Zip Code)
OWNER
OTHER
LOCATION FROM WHERE OBTAINED REASON OBTAINED TIME/DATE OBTAINED
SIGNATURE SIGNATURE
NAME, GRADE OR TITLE NAME, GRADE OR TITLE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
Page 1
RELEASED BY RECEIVED BY
NO. QUANTITY
NO.
(Include product, seal numbers, final destination, condition and unusual marks or scratches)
OF CUSTODY
PURPOSE OF CHANGE
CHAIN OF CUSTODY
ITEM DATE
PETROLEUM SAMPLE CHAIN OF CUSTODY DOCUMENT
DESCRIPTION OF ARTICLES ITEM
MIL-STD-3004C

APPENDIX F
188
FIGURE F-2. Chain of Custody Document Page 2
CHAIN OF CUSTODY
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
SIGNATURE SIGNATURE
RELEASED TO OWNER OR OTHER (Name/Unit)
DESTROY
OTHER (Specify)
ITEM(S) ON THIS DOCUMENT, PETAINING TO THE INVESTIGATION INVOLVING
(IS) (ARE) NO LONGER
(Grade)
(Name) (Organization)
RE QUIRED AS EVIDENCE AND MAY BE DISPOSED OF AS INDICATED ABOVE. (If article(s) must be retained, do not sign, but explain in separate
correspondence.)
(Typed/Printed Name, Grade, Title) (Signature) (Date)
THE ARTICLE(S) LISTED AT ITEM NUMBER(S) (WAS) (WERE) DESTORYED BY THE EVIDENCE
CUSTODIAN, IN MY PRESENCE, ON THE DATE INDICATED ABOVE.
(Typed/Printed Name, Organization) (Signature)
Petroleum Sample Chain of Custody Document - Page 2
FINIAL DISPOSITION ACTION
FINIAL DISPOSITION AUTHORIY
WITNESS TO DESTRUCTION OF EVIDENCE
OF CUSTODY
PURPOSE OF CHANGE
NO.
ITEM DATE
RELEASED BY RECEIVED BY
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

189
Acceptable fuel ..................................................................................5.11.4................................63
Acceptance (definition list) ................................................................3.1.....................................12
Acronyms and abbreviations used in this Standard ...........................3.2.....................................20
ACS (acronym list) ............................................................................3.2 ....................................20
Additional references .........................................................................6.5.....................................81
Additive concentration .......................................................................5.2.1.10.3..........................40
Additive injection/mixing .................................................................5.13.7.3.............................71
Additives (definition list) ...................................................................3.1.....................................12
Additives, receipt and injection .........................................................5.8.....................................48
After delivery / before departure (tank cars/trucks) ..........................5.4.1.1...............................45
After discharge ...................................................................................5.3.2.4...............................44
AIR card .............................................................................................5.6.1..................................47
Alcohol content (automotive gasoline) ..............................................5.10.4.6.............................58
All level sample .................................................................................4.2.1.4.1............................23
Alternate test methods........................................................................4.2.2.5.3............................28
5.14.3.7.............................74
Appearance (definition list) ...............................................................3.1.....................................13
Applicability ......................................................................................1.2.....................................1
ASSIST (definition list) ....................................................................3.1.....................................13
ASSIST (acronym list) .......................................................................3.2.....................................23
Automatic sample ..............................................................................4.2.1.4.13..........................24
Automotive gasoline ..........................................................................5.12.1.1.............................64
Automotive spark ignition engine fuel (commercial gasoline)..........5.10.4................................57
Aviation fuel contamination and quality standards ...........................5.11...................................61
Aviation turbine fuel, NATO F-18 (ASTM D910/100LL)
and Unleaded Aviation Gasoline D7547 ..........................................5.10.1................................54
Ballast (definition list) ......................................................................3.1.....................................13
Barge cargo tanks, minimum preparation requirements ....................Table XXVIII ...................126
Barge delivery ....................................................................................5.4.2..................................45
Barrel (definition list) ........................................................................3.1.....................................13
Batch cuts and segregation.................................................................5.2.1.7.2............................39
Batch/lot samples ...............................................................................4.2.1.4.17..........................24
BDN (acronym list)............................................................................3.2.....................................23
Before receipt (tank cars/trucks) ........................................................5.3.2.1...............................43
Biodiesel (definition list) ...................................................................3.1.....................................13
Blending (definition list) ....................................................................3.1.....................................13
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

190
Blending, reclamation ........................................................................5.13.7.2.............................71
Bottom Water Sample ........................................................................4.2.1.4.9............................23
Bottom sample ...................................................................................4.2.1.4.8............................23
Bulk additives, receipt .......................................................................5.8.1..................................48
Bulk products (definition list) ............................................................3.1.....................................13
Bulk storage .......................................................................................5.9.....................................49
Bulk tanks, protective treatment ........................................................5.9.3.6...............................51
Bulk tank water restriction .................................................................5.9.2..................................50
Bunkering, after .................................................................................5.5.3..................................46
Bunkering, before ..............................................................................5.5.1..................................46
Bunkering, during ..............................................................................5.5.2..................................46
Bunkers (definition list) .....................................................................3.1.....................................13
Burner Fuel (definition list) ...............................................................3.1.....................................13
CCAI (acronym list) ..........................................................................3.2 ....................................23
Calibrating test equipment .................................................................4.2.2.7...............................28
5.14.3.8.............................75
Calibration (definition list) ................................................................3.1.....................................14
Capitalization (definition list) ............................................................3.1.....................................14
Carbon residue on 10% bottoms ........................................................5.10.6.5.............................59
5.10.7.8.............................61
Cargo cleaning, required, MSC vessels .............................................5.1.1.4.2............................30
Car top sampling (coal) ......................................................................Figure C-2. .......................172
Cargo Fuel (definition list).................................................................3.1.....................................14
Certificate of Conformance (definition list) ......................................3.1.....................................14
Certifying statements .........................................................................5.1.1.3...............................29
Cetane index.......................................................................................B.6 ....................................153
Cetane number ...................................................................................5.10.6.1.............................59
B.7 ....................................153
Cetane number (ignition quality) (F-76) ............................................5.10.7.4.............................60
Chain of Custody ...............................................................................5.13.4................................70
Chain of Custody (Document) ...........................................................Appendix F.......................186
Chain of Custody (Shipping samples) ...............................................4.2.1.9...............................26
Changing product in a storage tank ...................................................5.9.3.2...............................50
Chromatography strip holder (Method 1040) ....................................Figure 1 ............................140
Clean (clear) and bright (definition list) ............................................3.1.....................................14
Cleaning of pipelines .........................................................................5.2.1.6.2............................38
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

191
Cloud point.........................................................................................5.10.7.7............................. 61
B.8 ....................................153
Cloudy or hazy fuel ............................................................................5.11.4.3.............................64
Coal, receipt and quality surveillance of ............................................Appendix C ......................160
Coal sampling, weights and increments.............................................Figure C-1. .......................171
Coalesce (definition list) ....................................................................3.1.....................................14
Color (gasoline, aviation)...................................................................5.10.1.2.............................54
Color (gasoline, automotive F-67) .....................................................5.10.3.2.............................57
Color (F-76) .......................................................................................5.10.6.2.............................59
Color (Kerosene) ................................................................................5.10.8.1.............................61
Color ..................................................................................................B.9 ....................................153
Commingling (definition list) ............................................................3.1.....................................14
Commingling with other petroleum products ....................................5.11.3.1.............................62
Communication copies.......................................................................5.13.3.1.............................70
Composite sample ..............................................................................4.2.1.4.6............................23
Conductivity (definition list)..............................................................3.1.....................................14
Conductivity .......................................................................................5.10.2.8.............................56
B.10 ..................................153
Conductivity, chart .............................................................................Figure B-1. .......................154
Container inspection ..........................................................................5.14.6.2.............................76
Container sealant ................................................................................5.9.9.4...............................54
Container suitability ...........................................................................5.14.6.3.............................76
Contaminant (definition list) ..............................................................3.1.....................................14
Contaminated fuel detector ................................................................Method 1060 ....................144
Contaminated pipeline shipment........................................................5.2.1.7.3............................39
Contaminated product (definition list) ...............................................3.1.....................................14
Contaminated product ........................................................................5.1.3.3...............................36
Contamination ....................................................................................5.14.6.9.............................77
Contamination, ground fuel ...............................................................5.12.2................................65
Contamination, fuel quality ...............................................................5.11.3................................62
Contamination, leaking valve ............................................................5.9.3.5...............................51
Contamination, microbial ..................................................................5.9.2.3...............................50
Contamination prevention. .................................................................5.12.2.4.............................66
Contamination problems ....................................................................4.2.1.10.1..........................27
Contamination, sources of .................................................................5.9.9 .................................53
Contamination tables .........................................................................Table XXX .......................128
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

192
Contamination tests ............................................................................4.2.2.1...............................27
Contamination tests ............................................................................5.14.3.1.............................74
Contamination with other fuels (commingling) .................................5.12.2.1.............................65
Contamination with sediment ............................................................5.12.2.3.............................66
Contamination with water ..................................................................5.12.2.2.............................65
Contamination with water, solids, and microbiological growth ........5.11.3.2.............................62
Continuous sample (definition list) ....................................................3.1.....................................14
Conversion chart for tank cars and trucks..........................................Table XXVI .....................123
Conveyance composite sample ..........................................................4.2.1.4.11..........................24
Corrosion (aviation turbine fuel) .......................................................5.10.2.3.............................55
Corrosion (gasoline, aviation) ............................................................5.10.1.4.............................54
Corrosion (gasoline, automotive, F-67) .............................................5.10.3.5.............................57
Corrosion (gasoline, automotive, D 4814/A-A-52530) .....................5.10.4.4.............................58
Corrosion control (pipelines) .............................................................5.2.1.10.............................40
Corrosion, copper strip.......................................................................B.11 ..................................155
Corrosion inhibitors (pipelines) .........................................................5.2.1.10.2..........................40
Corrosives in tanks .............................................................................5.9.2.1...............................50
Cracked stock (definition list) ............................................................3.1.....................................14
Cross Country System (pipeline) .......................................................5.2.1.7...............................39
Dedicated system (definition list) ......................................................3.1.....................................14
Dehydration (definition list) ..............................................................3.1.....................................14
Density (definition list) ......................................................................3.1.....................................14
Deteriorated product (definition list) .................................................3.1.....................................15
Deterioration of a product ..................................................................5.9.8..................................53
Deterioration of products ...................................................................5.14.7................................78
Determination of sediment (solids - pipeline) ...................................5.2.1.10.1..........................39
Determination of quantity ..................................................................5.1.4.2...............................37
Determining factors in Reclamation ..................................................5.13.6.1.............................71
Diesel fuel ..........................................................................................5.12.1.2.............................64
Diesel fuel, biodiesel blend, B20 (ASTM D7467) ............................5.10.9................................61
Diesel, fuel oil (ASTM D 975) ..........................................................5.10.7................................60
Discharge (tanker or barge receipts) ..................................................5.1.3.4...............................36
Dispensing from curbside pumps.......................................................5.9.7..................................53
Dispensing fuel, references (pipeline) ...............................................5.2.1.8.3............................39
Disposition request procedures (non-conforming product) ...............5.13.2................................67
Disposition procedures.......................................................................5.14.4................................75
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

193
Dissolved water (definition list).........................................................3.1.....................................15
Distillation (diesel, ASTM D 975).....................................................5.10.7.6.............................60
Distillation (F-76) ..............................................................................5.10.6.4.............................59
Distillation..........................................................................................B.12 ..................................155
Documentation (packaged products) .................................................5.14.6.1.............................76
Documentation ...................................................................................C.5.1.4 ..............................165
Documentation, offloading ................................................................C.5.2.1 ..............................166
Downgrading (definition list) ............................................................3.1.....................................15
Downgrading (non-conforming product) ...........................................5.13.7.1.............................71
Drag Reducer Additives (DRA).........................................................5.2.1.10.5..........................40
Drain sample ......................................................................................4.2.1.4.7............................23
Drum storage (packaged products) ....................................................5.14.6.4.............................76
DWCF (acronym list) ........................................................................3.2.....................................21
Dyed fuel (diesel) ...............................................................................5.10.7.5.............................60
Dye, red turbine fuel (contamination) ................................................5.11.4.2.............................63
Entrained water (definition list) .........................................................3.1.....................................15
E85 (definition list) ............................................................................3.1.....................................15
Exception/quality data (truck shipment) ............................................5.3.1.2.1............................42
Existent gum (aviation turbine fuel) ..................................................5.10.2.1.............................55
5.10.3.3.............................57
5.10.4.2.............................58
B.13 ..................................155
FAEE (definition list)..........3.1 ...................................15
FAME (definition list) ... 3.1 ...................................15
Filtering (definition list) .....................................................................3.1.....................................15
Filtering requirements ........................................................................5.1.1.2...............................29
Filter-separator (definition list) ..........................................................3.1.....................................15
Filtration .............................................................................................5.9.5..................................53
Filtration and water separation, minimum standards .........................Table XXXI .....................129
Filtration time (aviation turbine fuel) ................................................5.10.2.6.............................56
B.14 ..................................155
Flash point (F-76) ..............................................................................5.10.6.3.............................59
B.15 ..................................155
Flash point (kerosene) ........................................................................5.10.8.2.............................61
Flash point specification (aviation turbine fuel) ................................5.10.2.5.............................56
FOB (acronym list) ...........................................................................3.2 ....................................21
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

194
Free water...........................................................................................5.11.4.1.............................63
Free water (definition list) .................................................................3.1.....................................15
Free water, AEL MK I or MK II fuel detector ..................................Test Method 1060 ............147
Fuel, naval distillate (NATO F-76 MIL-DTL-16884) .......................5.10.6................................59
Fuel oil, diesel (ASTM D 975). .........................................................5.10.7................................60
Fuel quality and fuel contamination ..................................................5.11.3................................62
Fuel system icing inhibitor (FSII) (aviation turbine fuel) ..................5.10.2.4.............................55
Fuel Standardization Policy ...............................................................5.10.2.10...........................56
Galvanized containers ........................................................................5.14.6.7.............................77
Gaskets and hose connections (truck loading) ...................................5.3.1.3.5............................43
Gasohol (definition list) .....................................................................3.1.....................................15
Gasoline and turbine fuel differences ................................................5.11.1................................61
Gasoline, automotive, unleaded (F-67). .............................................5.10.3................................57
Gasoline, automotive .........................................................................5.12.1.1.............................64
Gasoline, automotive tests required ...................................................Table XIV ........................98
Gasoline, aviation, NATO F-18 (ASTM D910/100LL and
Unleaded Aviation Gasoline ASTM D7547 ......................................5.10.1................................54
Gasoline, aviation tests required ........................................................Table X.............................96
Gasoline, receipt limits(NATO F-67, and STANAG 7090) ..............Table VI ...........................87
Gauging and sampling JPTS cargo ranks or vessels ..........................4.2.1.10.............................26
Gauging for water (definition list) .....................................................3.1.....................................15
Gauging or gaging (definition list) ....................................................3.1.....................................15
Government documents .....................................................................2.2.....................................2
Government-owned property (change in grade of fuel) ....................4.5.....................................28
Greases ...............................................................................................5.14.7.3.............................79
Ground mobility fuel contamination ..................................................5.12...................................64
Ground Mobility Fuels .......................................................................5.12.1................................64
Gum (definition) ................................................................................3.1.....................................15
Gum, existent .....................................................................................5.10.2.1.............................55
5.10.3.3.............................57
5.10.4.2.............................58
B.13 ..................................155
Handling personnel (bulk storage) .....................................................5.9.9.2...............................53
Homogeneity (definition list) .............................................................3.1.....................................15
Hydraulic fluids .................................................................................5.14.7.2.............................79
Hydrocarbon contamination, in aviation gasoline .............................Test Method 1040 ............138
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

195
Identification of piping system ..........................................................5.9.3.7...............................51
Identification of transfers ...................................................................5.9.10................................54
Identification tests (definition list) .....................................................3.1.....................................16
Inadvertent mixtures (bulk storage) ...................................................5.9.9.1...............................53
Inert-gas system (definition list) ........................................................3.1.....................................16
Injection, after (additives) ..................................................................5.8.3..................................49
Injection, during (additives) ...............................................................5.8.2..................................49
Innage (definition list)........................................................................3.1.....................................15
Inspect (definition list) .......................................................................3.1.....................................15
Inspection documents covering tanker and barge loading .................5.1.4.3...............................37
Inspection policy, MSC vessels .........................................................5.1.1.4...............................29
Inspection procedures cargoes ...........................................................5.1.2.3...............................34
Inspection, vessel inspection ..............................................................5.1.1.5.2............................31
Insulating oils .....................................................................................5.14.7.4.............................80
Intended use .......................................................................................6.1.....................................80
Interface (definition list) ....................................................................3.1.....................................16
Internal tank inspection requirements ................................................5.1.1.4.3............................30
Internal preservation ..........................................................................5.9.6..................................53
International standard agreements .....................................................6.2.....................................80
ISO (acronym list)..............................................................................3.2.....................................21
Intra-Governmental receipt limit (definition list) ..............................3.1.....................................16
Intra-Governmental receipt limit, (Tables I-VII) ...............................5.10...................................54
Intra-Governmental receipt limits for automotive gasoline ...............Table VII ..........................88
Intra-Governmental receipt limits for aviation turbine fuels .............Table I. .............................84
Intra-Governmental receipt limits for fuel, naval distillate (F-76) ....Table III ...........................85
Intra-Governmental receipt limits for fuel oil, diesel ........................Table IV ...........................86
Intra-Governmental receipt limits for fuel oil, diesel (F-54) .............Table V.............................86
Intra-Governmental receipt limits for fuel system icing inhibitor .....Table II .............................85
Intra-Governmental receipt limits for gasoline, F-67 Unleaded ........Table VI ...........................87
Invoice/Acquisition procedures .........................................................5.7.3..................................48
Kerosene, F-58 (ASTM D 3699) .......................................................5.10.8................................61
Kerosene, tests required .....................................................................Table XV ..........................99
Knock rating.......................................................................................5.10.1.1.............................54
Laboratories, military services ...........................................................Appendix A ......................148
Laboratory reports ..............................................................................5.13.5................................70
Laws, compliance with ......................................................................4.8.....................................29
MIL-STD-3004C

INDEX
PARAGRAPH PAGE

196
Lead content (gasoline, automotive, F-67) ........................................5.10.3.4.............................57
Lead content (gasoline, automotive, ASTM D 4814/A-A-52530) ....5.10.4.3.............................58
Lead in fuels, determination of small amounts of..............................Test Method 1030 ............136
Leaking valve contamination (bulk storage)......................................5.9.3.5...............................51
Light-ends (definition list) .................................................................3.1.....................................16
Lines (vessel loading inspection) .......................................................5.1.1.7.1............................34
Loading procedures for tankers .........................................................5.1.1.7...............................33
Loading line (truck shipment) ............................................................5.3.1.3.2............................42
Loading plans, vessel .........................................................................5.1.1.5.4............................32
Loading rates .....................................................................................5.1.1.7.2............................34
Long-term storage (bulk) ...................................................................5.9.1..................................49
Long-term storage (definition lists) ..................................................3.1.....................................16
Loss or gain, unaccountable product ...............................................4.2.1.10.2..........................27
Lower sample .....................................................................................4.2.1.4.4............................23
Lubricating oils and gear oils .............................................................5.14.7.1.............................78
Lubricity (definition list)....................................................................3.1.....................................15
Marine Gas Oil (definition list)..........................................................3.1.....................................16
Marking of boxes and cartons ...........................................................5.14.6.12...........................78
Marking of contractor supplied product ...........................................5.14.6.13...........................78
Marking of used drums .....................................................................5.14.6.14...........................78
Markings (pipelines),pumps, and valves ...........................................5.2.1.3...............................38
Markings ...........................................................................................4.2.1.8.1............................26
Markings, field-filled container ........................................................5.14.6.11...........................77
Markings, minimum container ..........................................................5.14.6.10...........................77
Material Inspection and Receiving Report
(DD Form 250/250-1) (definition list) ...............................................3.1.....................................16
Measurement and sampling and calibration ......................................4.7.....................................29
Micron (definition list) .......................................................................3.1.....................................16
Middle sample ....................................................................................4.2.1.4.3............................24
Mineral oil (definition list).................................................................3.1.....................................16
Minimum frequency for testing long term storage ............................Table VIII.........................88
Mixed sample. ....................................................................................4.2.1.4.14..........................24
MPMS Guidelines ..............................................................................5.1.1.1...............................29
Multi-port inspection .........................................................................5.1.1.5.5............................32
Multi-product pipelines ......................................................................5.2.1.5...............................38
NATO codes (truck shipment) ...........................................................5.3.1.3.4............................43
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197
Nitrate ignition-type improvers in diesel fuel ....................................Test Method 1050 ............142
Non-conforming product ...................................................................5.13...................................67
Non-conforming product (communication copies) ............................5.13.3.1.............................70
Non-conforming product (disposition request) ..................................5.13.2................................67
Non-conforming product (custody requirements) .............................5.13.4................................70
Non-Government publications ...........................................................2.3.....................................6
Octane (gasoline, automotive, unleaded, F-67...................................5.10.3.1.............................57
Octane (gasoline, automotive, ASTM D 4814/A-A-52530) ..............5.10.4.1.............................58
Off-specification product (definition list) ..........................................3.1.....................................16
Order of precedence ...........................................................................2.4.....................................12
Other Government Documents, Drawings, and Publications ............2.2.2..................................2
Outage, or ullage (definition list) .......................................................3.1.....................................16
Outlet (suction) sample ......................................................................4.2.1.4.12..........................24
Oxygenated fuel (definition list) ........................................................3.1.....................................17
Packaged products .............................................................................5.14...................................71
Packaged product (definition list) ......................................................3.1.....................................16
Packaging and storage of packaged petroleum products ...................5.14.6................................76
Personnel competency. ......................................................................4.1.....................................22
Personnel conducting sampling .........................................................4.2.1.2...............................23
Personnel to conduct sampling (packaged products) .........................5.14.2.2.............................72
Pipeline batch (definition list) ............................................................3.1.....................................17
Pipeline receipts, before receipt .........................................................5.2.2.1...............................41
Pipeline receipts, completion .............................................................5.2.2.3...............................41
Pipeline receipts, during receipt .........................................................5.2.2.2...............................41
Pipeline tender (definition list) ..........................................................3.1.....................................17
Pipeline transfer velocity ...................................................................5.2.1.5.3............................38
Placarding (truck)...............................................................................5.3.1.3.10..........................43
Post loading tankers and barges ......................................................5.1.4..................................37
Precautions (packaged products) .......................................................5.14.2.1.............................72
Pre-loading and loading inspection ....................................................5.1.2.1...............................34
Pre-loading inspection of tankers.......................................................5.1.1.5...............................31
Pre-loading procedures Shore Tanks .................................................5.1.1.6...............................33
Pressure drop ......................................................................................5.2.1.10.4..........................40
Procedures at the loading rack ...........................................................5.3.1.3.3............................42
Product change record........................................................................Appendix E ......................183

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198
Product change, sample calculation ..................................................E.4.2 .................................184
Figure E.1 .........................185
Product compatibility (pipelines) .......................................................5.2.1.6.1............................38
Product conversion.............................................................................5.1.2.2...............................34
Product equilibrium (definition list) ..................................................3.1.....................................17
Product free fall (truck shipment) ......................................................5.3.1.3.7............................43
Production identification (multiproduct pipelines) ............................5.2.1.5.1............................38
Product tankage cargo check for quality ............................................5.9.3.3...............................51
Product receipt (packaged products) ..................................................5.14.1................................71
Pumping time (pipelines) ...................................................................5.2.1.5.2............................38
Purification .........................................................................................5.13.7.4.............................71
Qualified Product List (QPL) (definition list) ...................................3.1.....................................17
Quality (definition list) ......................................................................3.1.....................................17
Quality and contamination, aviation fuel ...........................................5.11.3................................62
Quality and quantity determination (vessel movements)...................5.1.1.5.6............................32
Quality assurance (QA) (definition list) ............................................3.1.....................................17
Quality assurance representative (definition list) ..............................3.1.....................................17
Quality fuel deliveries, .......................................................................5.11.2................................62
Quality Product Database (QPD) (definition list) .............................. 3.1 ...................................17
Quality status list (QSL) (definition list) ...........................................3.1.....................................17
Quality surveillance of fuel, government...........................................Appendix D ......................176
Quality surveillance pipeline procedures ...........................................5.2.1.11.............................40
Quality surveillance program (definition list) ....................................3.1.....................................17
Quantity, determination of (tankers and barges) ................................5.1.4.2...............................37
Quantity variation (tankers) ...............................................................5.1.1.4.5............................30
Receipt limits .....................................................................................5.14.3.3.............................74
Receipts of aviation secured fuel and support aircraft .......................5.7.....................................47
Receipt of approved additives and injection ......................................5.8.....................................48
Receipt of turbine fuel approved packaged additives ........................5.8.1.1...............................49
Receipts by pipeline ...........................................................................5.2.2..................................41
Receipts from the bunkering program ...............................................5.5.....................................45
Receipts from the into-plane program ...............................................5.6.....................................47
Receipts, tanker or barge, completion................................................5.1.3.5...............................36
Receipts, tanker or barge, shore side .................................................5.1.3.1...............................35
Receipts, truck/car..............................................................................5.3.2..................................43
Receipts under the post, camps & station (PC&S) ............................5.4.....................................44
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199
Reclamation (definition list) ..............................................................3.1.....................................18
Reclamation techniques .....................................................................5.13.7................................71
Refueling units (into-plane) ...............................................................5.6.2..................................47
Regulations and laws, compliance with .............................................4.8.....................................29
Relative density (definition list).........................................................3.1.....................................18
Repeatability (definition list) .............................................................3.1.....................................18
Reproducibility (definition list) .........................................................3.1.....................................18
Required cargo cleaning ....................................................................5.1.1.4.2............................30
Requiring installation (definition list) ................................................3.1.....................................18
Responsibility (packaged products) ...................................................5.14.2.3.............................72
Responsibility (tanker inspection) .....................................................5.1.1.4.1............................30
Responsibility for off-specification cargo (tanker inspection) ..........5.1.1.4.6............................31
Retained samples ...............................................................................4.2.1.8.3............................26
Rubber surface to fuel (bulk storage).................................................5.9.9.3...............................53
Rust inhibitors effectiveness (pipeline) ............................................Test Method 1000 ............130
Safety (truck shipment) ......................................................................5.3.1.3.1............................42
Safety precautions ..............................................................................4.6.....................................29
Sample (definition list) ......................................................................3.1.....................................18
Sample serial numbers .......................................................................4.2.1.8.2............................27
Sample, single tank composite ...........................................................4.2.1.4.10..........................24
Sample size, B20 ................................................................................4.2.1.7.5............................26
Sample size, E85 ................................................................................4.2.1.7.4............................26
Sample size, jet fuel ...........................................................................4.2.1.7.3............................26
Sample size, normal ...........................................................................4.2.1.7.1............................26
Samples, size of (packaged products) ................................................5.14.2.6.............................72
Sample size, special ...........................................................................4.2.1.7.2............................26
Sample tag ..........................................................................................3.1.....................................18
Samples, identification of ..................................................................4.2.1.8...............................26
Samples, identification of (packaged products) .................................5.14.2.7.............................73
Samples, size of .................................................................................4.2.1.7...............................26
Samples, taking of ..............................................................................4.2.1.5...............................25
Samples, types of ...............................................................................4.2.1.4...............................24
Samples, types of (packaged products) ..............................................5.14.2.4.............................72
Sampling (general requirements). ......................................................4.2.1..................................23
Sampling (packaged products) ...........................................................5.14.2................................71
Sampling and testing, for petroleum products(minimum) .................Table IX ...........................89
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200
Sampling apparatus, containers, and procedures ...............................4.2.1.5.1............................24
Sampling apparatus, containers and procedures
(packaged products) ...........................................................................5.14.2.5.............................72
Sampling, precautions ........................................................................4.2.1.6...............................25
Sampling, precautions (general). .......................................................4.2.1.1...............................23
Sampling, responsibility ....................................................................4.2.1.3...............................23
Scope ..................................................................................................1.1.....................................1
Sealing (tank truck and tank cars) ......................................................5.3.1.3.9............................43
Sediment in fuel (aviation fuel) .........................................................5.11.4.4.............................64
Segregation (pipeline) ........................................................................5.2.1.9...............................39
Segregation during transfer (pipelines) ..............................................5.2.1.5.4............................38
Segregation of product (bulk storage tanks) ......................................5.9.3.4...............................51
Segregation of product movements via multi-product pipelines .......Table XXIX .....................127
Service and DLA responsibilities, (packaged products) ....................5.13.3................................69
Service/contractor responsibilities .....................................................4.2.....................................22
Settling time (definition list) ..............................................................3.1.....................................18
Settling time in tank (bulk storage). ...................................................5.9.3.8...............................51
Shelf life (definition list) ....................................................................3.1.....................................18
Shipments by barges and refueling craft ............................................5.1.2..................................34
Shipments by pipelines. .....................................................................5.2.1..................................37
Shipments by(tank cars/trucks/tank wagons/tank & trailer) ..............5.3.1..................................41
Shipments by tanker ...........................................................................5.1.1..................................29
Significance of tests ...........................................................................Appendix B ......................152
Specification (definition list) .............................................................3.1.....................................18
Specification limits (definition list) ...................................................3.1.....................................19
Specifications (general requirements)................................................4.3.....................................28
Specifications, Standards, and Handbooks ........................................2.2.1..................................2
Specific gravity (definition list) .........................................................3.1.....................................19
Static electricity, control of (aviation turbine fuels) ..........................5.9.4..................................52
Stock rotation (packaged products) ...................................................5.14.6.6.............................77
Storage of similar products (bulk storage) .........................................5.9.3.1...............................50
Storage, separate (packaged products) ...............................................5.14.6.5.............................76
Storage, small container (packaged products) ...................................5.14.6.8.............................77
Storage Stability .................................................................................5.10.6.6.............................59
Storage tank (definition list) ..............................................................3.1.....................................19
Storage tanks and piping (bulk storage).............................................5.9.3..................................50
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201
Subject term (key word list) ...............................................................6.4.....................................80
Suitability to load (tankers) ................................................................5.1.1.4.4............................30
Sulfides in water, test for ..................................................................Test Method 1020 ............134
Sulfur (kerosene) ................................................................................5.10.8.3.............................61
Super-clean fluid (definition list) .......................................................3.1.....................................19
Surfactant (definition list) ..................................................................3.1.....................................19
Synthetic oil (definition list) ..............................................................3.1.....................................19
System isolation (pipeline) ................................................................5.2.1.7.4............................39
Tailoring guidance .............................................................................6.3.....................................80
Tank car (TC or RTC) (definition list) ..............................................3.1.....................................19
Tanker cargo tanks preparation of .....................................................Table XXVII ....................124
Tanker inspection policy for MSC vessels ........................................5.1.1.4...............................29
Tanker, receipts ..................................................................................5.1.3..................................35
Tank protective treatment (bulk storage) ...........................................5.9.3.6...............................51
Tariffs and agreements (pipeline) ......................................................5.2.1.1...............................37
Terminal, depot and base system (pipelines) .....................................5.2.1.6...............................38
Test, equivalent ..................................................................................4.2.2.5.1............................28
Testing (definition list) ......................................................................3.1.....................................19
Testing (general requirements) ..........................................................4.2.2..................................27
Testing capabilities (general) .............................................................4.2.2.6...............................28
Testing frequency (general) ...............................................................4.2.2.3...............................27
Testing frequency long term storage of petroleum products .............5.14.3.4.............................74
Testing, laboratory (pipeline shipments) ...........................................5.2.1.2...............................38
Testing, minimum (general) ...............................................................4.2.2.4...............................27
Testing minimum, (packaged products) ............................................5.14.3.5.............................74
Testing (packaged products) ..............................................................5.14.3................................74
Testing, predictive..............................................................................4.2.2.5.2............................28
Test methods (general) .......................................................................4.2.2.2...............................27
Test methods (packaged products).....................................................5.14.3.2.............................74
Test required (packaged products) .....................................................5.14.3.6.............................74
Test results, recording (truck shipment) ............................................5.3.1.3.8............................43
Tests, identification (pipelines) ..........................................................5.2.1.4...............................38
Tests required, Support for Secured Fuels .........................................Table XIII.........................97
Tests required, automotive gasoline ..................................................Table XIV ........................98
Tests required, aviation gasoline ........................................................Table X.............................96
Tests required, aviation turbine fuels .................................................Table XII ..........................97
MIL-STD-3004C

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202

Upper sample .....................................................................................4.2.1.4.2............................23
Vapor Pressure (VP) (acronym list) ..................................................3.1.....................................20
Valve and pipeline control .................................................................5.2.1.6.3............................39
Vapor pressure (definition list) ..........................................................3.1.....................................20
Vehicle tank cleanliness (tank car and truck shipment) .....................5.3.1.3.6............................43
Verification Test (definition list) .......................................................3.1.....................................20
Vessel inspection, pre-loading ...........................................................5.1.1.5.1............................31
Vessel pre-discharge inspection (tanker or barge receipts). ..............5.1.3.2...............................35
Vessel pre-loading plans ....................................................................5.1.1.5.4............................32
Vessel rejection/delay (tankers) .........................................................5.1.1.5.7............................32
Vessel samples (post-loading tankers and barges) .............................5.1.4.1...............................37
Vessel tank inspection........................................................................5.1.1.5.2............................31
Visual quality surveillance test ..........................................................Test Method 1010 ............132
Volatile alkyl lead antiknock (definition list) ....................................3.1.....................................20
Vapor Pressure (VP) (aviation turbine fuel) ......................................5.10.2.2.............................55
VP (gasoline, automotive, automotive, unleaded (F-67)) ..................5.10.3.6.............................57
VP (gasoline, automotive, ASTMD4814/A-A-52530) ......................5.10.4.5.............................58
VP (gasoline, aviation, F-18) .............................................................5.10.1.3.............................54
Water and sediment (aviation turbine fuel) .......................................5.10.2.7.............................56
Water and sediment (F-76) ................................................................5.10.6.7.............................60
Water and sediment (gasoline, aviation, F-18) ..................................5.10.1.5.............................55
Water and sediment control (diesel, D975) .......................................5.10.7.3.............................60
Waterborne operations .......................................................................5.1.....................................29
Water reaction, test for, of aviation fuels ...........................................Method 1070 ....................146
Water removal (non-conforming product) .........................................5.13.7.5.............................71
Water, tank, check frequency.............................................................5.9.2.2...............................50
Water tolerance (gasoline, automotive, and gasohol
ASTM D4814/A-A-52530) ................................................................5.10.4.7.............................58

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203
CONCLUDING MATERIAL

Custodians: Preparing activity:
Army AT DLA PS
Navy - SA (Project 91GP-2009-002)
Air Force - 68
Review activities:
Navy - AS, SH, OS
Air Force - 11
DLA GS

NOTE: The activities listed above were interested in this document as of the date of this
document. Since organizations and responsibilities can change, you should verify the currency
of the information above using the ASSIST Online database at https://assist.daps.dla.mil.

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