Laboratory 2 MRPF

A P T I 4 3 5 : A T M O S P H E R I C S A M P L I N G C O U R S E
2-1
Laboratory 2: Flow Measuring
Instrumentation
2.1 Introduction
Flow measurement is basic in any sampling scheme. Flow measuring instruments
are classified as primary, intermediate, or secondary standards, depending on
their accuracy and physical characteristics. In this laboratory exercise, you will use
each of the three types of flow measuring instruments. From these exercises you
will be able to use these flow measuring instruments and be better prepared to
select the proper flow measuring instrument when sampling for atmospheric
pollutants.
This laboratory session will consist of four experiments:

Experiment 1: The calibration of a wet test meter using the water
displacement technique and the determination of the meter correction factor.
Experiment 2: The calibration of a mass flowmeter (or mass flow
controller) using a bubble flow meter.
Experiment 3: The calibration of a rotameter at reduced pressure using a
calibrated mass flowmeter. This experiment is designed to show the need to
calibrate a rotameter under the conditions in which it is to be used.
Experiment 4: The limiting orifice experiment consists of three parts. Part
1 is the experimental determination of vacuum needed to obtain a constant
volumetric flow rate. Part 2 is designed to show that, while this is a constant
rate meter, an upstream pressure drop will affect the mass flow rate and,
therefore, the orifice has to be calibrated in the system. Part 3 demonstrates
that orifices have a directional difference and, therefore, these devices have
to be calibrated in the same direction in which they are used. This laboratory
procedure also makes use of a bubble flow meter as the calibration device.

Laboratory
2
2-2
Objectives
At the conclusion of this laboratory session, you will be able to:
1. calibrate a wet test meter using a water displacement technique;
2. calibrate a mass flowmeter (or mass flow controller);
3. calibrate a rotameter in a bubbler train using a mass flowmeter (you will
be able to describe the effects that variation in upstream pressure will
produce on flow measurements); and
4. describe how various factors affect orifice flow. These factors include:
a. vacuum,
b. effects of upstream resistance, and
c. effects of directional placement of a common orifice.
2.2 Experiment 1: Calibration of a Wet Test Meter
Introduction
Wet test meters are used as a laboratory standard. However, the time required for
the equilibration of water temperature and dissolved gases in the water, and the
meters bulk and weight, are disadvantages in using the wet test meter in the
field. Wet test meters are very accurate, yet are classified as an intermediate
standard because they cannot be calibrated by physical dimensional
measurement. Therefore, wet test meters must be calibrated against a primary
standard. An easy-to-use, inexpensive method to calibrate the wet test meter is
the displacement bottle technique. A Class A volumetric flask is used to measure
the displaced water and is considered the primary standard.

Calibration Equipment and Procedure

Equipment
To calibrate a 1-liter per revolution wet test meter, you need:
- a Class A, 2-liter volumetric flask;
- a 4-liter aspirator bottle (minimum size);
- a 2-hole rubber stopper, to fit into the top of the aspirator bottle;
- a piece of glass (or plastic) tubing, about three inches long, to fit the
rubber stopper;
- a needle valve;
- rubber tubing: one piece of vacuum tubing two feet long, one end of
which will be attached to the wet test meter, the other end to a needle
valve; one piece of vacuum tubing long enough to reach from the needle
valve to a vacuum source; two pieces of gum rubber tubing about two
feet long;
1

1
The diameter of the tubing used should fit tightly over the wet test meter and needle valve
fittings, aspirator bottle tabulation, and the tubing for the rubber stopper.
2-3
- one tubing pinch clamp;
- a vacuum source;
- an impinger saturator;
- a manometer capable of measuring six inches of water pressure drop; and
- a thermometer.

Procedure
Understand the procedure thoroughly before proceeding. Be sure to read all
footnotes.

1. Assemble the aspirator bottle.
a. Attach one end of a piece of gum rubber tubing to the drain of the
aspirator bottle (Lab 2, Figure 1a) and close off the other end of the
tubing with a pinch clamp (Lab 2, Figure 1b).
b. Insert the 3-inch piece of glass or plastic tubing and a thermometer into
the rubber stopper (Lab 2, Figure 1c). Set aside for use in step 12.
2. Fill the aspirator bottle with water and allow the water to equilibrate to room
temperature.
3. Level the wet test meter. Adjust the meter until the bubble is exactly centered
in the level (Lab 2, Figure 2a).
4. Fill the wet test meter through its funnel with distilled water until the water
just covers the pointer (Lab 2, Figure 2b).
5. Attach one end of the 2-ft length of vacuum tubing to the wet test meter
outlet. (The outlet and inlet will generally be identified on the meter.) Attach
tubing of the necessary length to the vacuum source and affix the other end
to the needle valve. The tubing should fit tightly over all fittings.
6. With the needle valve closed, turn on the vacuum source.
7. Open the needle valve to obtain a flow rate of 5 to 10 liters per minute of air.
Allow the air to flow through the wet test meter for one hour. The purpose
of this step is to saturate the water with air to prevent any of the measured
air from becoming dissolved and lost during the calibration run.

IF YOU HAVE NOT READ THROUGH THE COMPLETE PROCEDURE,
INCLUDING THE FOOTNOTES, DO SO NOW BEFORE
CONTINUING.

8. Cut off the vacuum source.
9. Disconnect the needle valve and vacuum tubing so that both the inlet and
outlet of the wet test meter are at atmospheric pressure.
10. Check the wet test meter level and adjust if necessary.
2

11. If necessary, draw off water through the small petcock (Lab 2, Figure 2) or
add water as in step 4, adjusting the water level so the center of the concave

2
The wet test meter should be leveled and adjusted, if necessary, each time the meter is moved.
Usually two or more of the wet test meter feet are screw adjustments. The meter can be leveled
by turning these.
2-4
meniscus seen in the sight glass (Lab 2, Figure 2b) just touches the tip of the
pointer.
3

12. Attach the gum rubber tubing to the glass or plastic piping which was
inserted into the rubber stopper in step 1 (Lab 2, Figure 3a). Attach the other
end to the meter outlet. Half-fill the impinger saturator with water and
assemble the equipment as shown in Lab 2, Figure 3.
4
Make certain that the
rubber stopper is tight and there are no leaks in the wet test meter by
checking the tightness of all fittings.
13. Open the pinch clamp (Lab 2, Figure 3b) and allow the aspirator bottle drain
hose to fill with water. Record the volume per revolution of the wet test
meter (liters).
14. Read the initial volume (V
i
) from the wet test meter dial (Lab 2, Figure 3)
and record on the wet test meter calibration data sheet.
15. Place a clean, dry 2-liter volumetric flask (Class A) under the siphon tube,
open the pinch clamp, and fill the volumetric flask to the 2-liter mark.
16. While the water is flowing, record the saturators manometer reading (
3
)
and the wet test meters manometer reading (
m
).
5
Record the following
additional data:
a. meter water temperature, C,
b. aspirator bottle temperature, C, and
c. barometric pressure, mm Hg.
17. At the point at which the volumetric flask reaches its calibrated capacity, stop
the flow of water by quickly closing the pinch clamp, read the final volume
(V
f
) from the wet test meter dial, and record this value on the calibration data
sheet. Pour the water back into the aspirator bottle.
18. Repeat steps 14 through 17 twice.
19. Calculate and record the corrected volume (V
c
) using the following equation
for each test:
m
r
m
s b
m b
c
V
T

V
|
|
.
|
\
|
|
|
.
|
\
|
=
Where: P
b
= barometric pressure, mm Hg

m
= wet test meter manometer reading, mm Hg
T
r
= temperature of aspirator bottle, K (K = C + 273)

s
= saturator manometer reading, mm Hg
T
m
= temperature at wet test meter, K (K = C + 273)
V
m
= volume measured by wet test meter,

An example of this calculation is presented below:

3
Whenever the water is checked or adjusted, the inlet and outlet should be open to the
atmosphere, i.e., at atmospheric pressure, and the meter should be level.
4
The mouth of the 2-liter flask must be below the final water level of the aspirator bottle. The
lower the flask and hose combination, the faster the water flow.
5
See Lab 1 for the proper reading of a manometer.
2-5
Barometric pressure, P
b
= 742.2 mm Hg
Aspirator bottle temperature, T
r
= 23.0C + 273 = 296.0 K
Saturator manometer reading = 30.0 mm H
2
O
Hg mm 21 . 2 O H mm Hg mm 0.0738 O H mm 0 . 30
2 2
= =
s

Meter temperature, T
m
= 22.5C + 273 = 295.5 K
Meter manometer reading = 35.0 mm H
2
O
Hg mm 58 . 2 O H mm Hg mm 0.0738 O H mm 0 . 35
2 2
= =
m

V
m
= 2.000

9457 . 1 95 . 1
0 . 296
5 . 295
21 . 2 2 . 742
58 . 2 2 . 742
=
|
.
|
\
|
|
.
|
\
|
= c V

20. Calculate and record the average corrected volume at meter conditions by:

3
3 2 1 c c c
c
V V V
V
+ +
= .
21. Calculate and record the error using the following equation:

st
st c
V
V V
Error

=

Where: V
st
= the volume of the standard flask.

An example computation is presented below:

0062 . 0
0000 . 2
0000 . 2 9877 . 1
=
= Error

Determining the Correction Factor
The wet test meter error can be used to determine the correction factor (C.F.), as
shown in the following equation:
6

Error
F C
+
=
1
1
. .

Using the Correction Factor
When using the wet test meter, the actual air volume can be determined by the
equation:
. .F C V V
m a
=

Where: V
a
= volume of air that passed through the wet test meter
V
m
= volume of air indicated by the wet test meter dials
C.F. = correction factor

6
Error, as determined above, may be positive or negative, and the sign should be carried in the
determination of the correction factor (C.F.).
2-6

Lab 2, Figure 1. Aspirator bottle.

Lab 2, Figure 2. Wet test meter.
2-7

Lab 2, Figure 3. Calibration of the wet test meter using an aspirator bottle and Class A
volumetric flask.
2-8
Lab 2, Table 1. Example Wet Test Meter Calibration Data Sheet.

Wet test meter serial no. _________123-A B________ Name _________SMS_________
Wet test meter revolution ________2 L__________ Date ________3/21/07________
Test flask volume, Vst _________2.000 L_________

Test
number
Barometric
pressure Pb
(mm Hg)
Aspirator
bottle data
Saturator
data
Wet test meter data
Corrected
volume
Vc
(L) Error
Correction
Factor
(C.F.)
Temperature
Tr
Manometer
reading,
s

Temperature
Tm
Manometer
reading,
m

Meter reading
(C) (K)
(mm
H2O)
(mm
Hg)
(C) (K)
(mm
H2O)
(mm
Hg)
Final,
Vf
(L)
Initial,
Vf
(L)
Vm
(L)
1 742.2 23.0 296.0 30.0 2.21 22.5 295.5 35.0 2.58 2.020 0.005 2.015 2.0106 - -
2 740.8 23.5 296.3 29.0 2.14 23.0 296.0 36.0 5399 2.041 0.015 2.026 2.0215 - -
3 735.3 22.5 295.5 31.0 2.29 22.0 295.0 35.5 2.62 2.056 0.021 2.035 2.0305 - -
Average - - - - - - - - - - - - 2.0209 -0.01045 0.9896

Calculations:
T
r
= 23.0 C + 273 = 296.0 K 0106 . 2 015 . 2
296
5 . 295
21 . 2 2 . 742
58 . 2 2 . 742
=
|
.
|
\
|
|
.
|
\
|
=
c
V
3
= 30.0 mm H
2
O 0.0738 = 2.21 mm Hg 0209 . 2
3
0305 . 2 0215 . 2 0106 . 2
3
3 2 1
=
+ +
=
+ +
=
c c c
c
V V V
V
T
m
= 22.5 C + 273 = 295.5 K
m
= 35.0 mm H
2
O 0.0738 = 2.58 mm Hg
015 . 2 005 . 0 020 . 2 = = =
i f m
V V V 01045 . 0
000 . 2
000 . 2 0209 . 2
=
=
st
st c
V
V V
Error
m
r
m
b
b
c
V
T

V
|
|
.
|
\
|
|
|
.
|
\
|
=
3

( )
9896 . 0
01045 . 0 1
1
1
1
. . =
+
=
+
=
Error
F C

Note: If air is pushed through calibration system,
s
and
m
are to be added to
b
.
2-9
Laboratory 2, Experiment 1: Wet Test Meter Calibration Data Sheet

Wet test meter serial no. ________________________ Name _______________________
Wet test meter revolution L _____________________ Date _______________________
Test flask volume, Vst ________________________

Test
number
Barometric
pressure Pb
(mm Hg)
Aspirator
bottle data
Saturator
data
Wet test meter data
Corrected
volume
Vc
(L) Error
Correction
Factor
(C.F.)
Temperature
Tr
Manometer
reading,
s

Temperature
Tm
Manometer
reading,
m

Meter reading
(C) (K)
(mm
H2O)
(mm
Hg)
(C) (K)
(mm
H2O)
(mm
Hg)
Final,
Vf
(L)
Initial,
Vf
(L)
Vm
(L)
1
2
3
Average

Calculations:

T
r
= __________ C + 273 = __________ K
i f c
V V V =
3
= __________ mm H
2
O 0.0738 = __________ mm Hg
3
3 2 1 c c c
c
V V V
V
+ +
=
T
m
= __________ C + 273 = __________ K
m
= __________ mm H
2
O 0.0738 = __________ mm Hg
m
r
m
b
b
c
V
T

V
|
|
.
|
\
|
|
|
.
|
\
|
=
3
__________L
st
st c
V
V V
Error

=

Error
F C
+
=
1
1
. .

s
and
m
are to be added to
b
.
Page 1 of Lab Report
2-10
Laboratory 2, Experiment 1: Wet Test Meter Calibration Data Sheet

Wet test meter serial no. ________________________ Name _______________________
Wet test meter, revolution L _____________________ Date _______________________
Test flask volume, Vst ________________________

Test
number
Barometric
pressure Pb
(mm Hg)
Aspirator
bottle data
Saturator
data
Wet test meter data
Corrected
volume
Vc
(L) Error
Correction
Factor
(C.F.)
Temperature
Tr
Manometer
reading,
s

Temperature
Tm
Manometer
reading,
m

Meter reading
(C) (K)
(mm
H2O)
(mm
Hg)
(C) (K)
(mm
H2O)
(mm
Hg)
Final,
Vf
(L)
Initial,
Vf
(L)
Vm
(L)
1
2
3
Average

Calculations:

T
r
= __________ C + 273 = __________ K
i f c
V V V =
3
= __________ mm H
2
O 0.0738 = __________ mm Hg
3
3 2 1 c c c
c
V V V
V
+ +
=
T
m
= __________ C + 273 = __________ K
m
= __________ mm H
2
O 0.0738 = __________ mm Hg
m
r
m
b
b
c
V
T

V
|
|
.
|
\
|
|
|
.
|
\
|
=
3
__________L
st
st c
V
V V
Error

=

Error
F C
+
=
1
1
. .

s
and
m
are to be added to
b
.

2-11
2.3 Experiment 2: Calibration of a Mass Flow
Meter
Introduction
Mass flow meters (MFM) operate on the principle that when a gas passes over a
heated surface, heat is transferred from the surface to the gas. The amount of
electric current required to keep the surface at a constant temperature is a
measure of the velocity of the gas. Since the amount of heat transferred depends
only on the mass and velocity of the gas, these meters measure the true mass
flow and have the advantage of measuring flow races without requiring
corrections for changes of temperature and barometric pressure. Flow values
from these meters are usually given in standard cubic centimeters per minute,
which is the volume occupied by a given mass of a gas at standard temperature
and pressure as specified by the manufacturer. Since mass flowmeters are not
volume displacement devices, they require periodic calibration against a primary
flow measuring device, such as a bubble flow meter.
Mass flow controllers (MFC), like MFM, measure flow rate; however, MFC
have the added capability of controlling flow at a prescribed rate. This feature
makes MFC particularly well-suited as flow controlling and measuring devices in
modern dynamic gas calibrators. It is typical to employ two MFC in a dynamic
gas calibrator; one to measure and meter the dilutent gas (i.e., zero air), and the
other to measure and meter the calibration gas (e.g., NO, CO, etc.).

Calibration Procedure
Mass flow meters can be calibrated by employing a calibrated automated bubble
meter as a calibration standard as follows:
7

1. With the mass flowmeter off, adjust the meter to zero with the pointer
needle adjustment screw located below the meter face, if so equipped.
2. Turn on the meter and allow it to warm up (typically 30 minutes).
3. After the warm-up period, adjust the electronic zero as follows:
a. Plug up the inlet and outlet of the transducer.
b. Adjust the electronic zero adjustment screw until the meter reads
zero.
c. Unplug the transducer and connect it to the test apparatus as
illustrated in Lab 2, Figure 4.
4. Turn on the vacuum pump and adjust the flow rate, with the needle valve, to
approximately 80% of full scale of the mass flow meter.
5. Allow the flow meter reading to stabilize.
6. Read and record the flow rate as measured by the bubble flow meter as Q
m
.

7
Refer to the manufacturers instructions for specific procedures and flow rate capacities.


2-12
7. Record laboratory temperature, T
m
, in K and barometric pressure, P
b
, in mm
Hg.
8. Calculate Q
std
for the bubble meter from P
b
, T
m
, Q
m
, and the vapor pressure
(VP) and record on the calibration data sheet.

-VP , and mm Hg,
b m std std
= = = 298 760
8

|
|
.
|
\
|
|
|
.
|
\
|
=
m
std
std
m
m std
Q Q

9. Plot Q
std
versus mass flow meter readings on arithmetic graph paper.
10. Repeat steps 6 through 13 for approximately 60%, 40%, and 20% of the
range of the mass flowmeter.
11. Construct a best-fit curve for the points generated and use this relationship
for future work employing the mass flow meter.

A partially completed example data sheet is found in Lab 2, Table 2.

Note: When calibrating a mass flow controller (MFC) which is integrated into a
dynamic gas calibrator unit, it is best to refer to the manufacturers instructions.
As an example, the basic procedure for the calibration of a Thermo
Environmental Instruments Dynamic Calibrator (Model 146C) is as follows.

Calibration of a Thermo Environmental Instruments Dynamic Calibrator (Model 146C)
In order to calibrate the mass flow meter section of the zero or gas mass flow
controller, a NIST traceable flow meter is required. The term calibration means
determining the actual flow versus the flow setting for seven equally spaced
flows along the range of the device. The Model 146C then corrects the output
according to an internal algorithm.
The long-term stability of the flow controllers is quite good. As shipped from
the factory, the target flow and actual flow from 20 to 100 percent of full scale
agree to within 2 percent of reading or 1 percent of full-scale, whichever is less.
Calibration may be done with a properly calibrated flow meter. For the most
accurate calibration procedure, use a volumetric NIST traceable calibrator with
the following step-by-step calibration procedure.

1. Connect a source of clean, dry air to the inlet of the mass flow controller.
2. Measure barometric pressure and room temperature.
3. Connect a suitable flow meter to the mass flow controller outlet.
4. Set Model 146C to Gas Drive or Zero Air Flow Calibration as described
in Chapter 3, Operation, in the Operators Manual for the Model 146C.

8
If a flow meter that utilizes a soap bubble is used, a correction for the addition of moisture to
the gas stream must be performed as shown. The vapor pressure (VP) can be determined by
referring to the Saturation Vapor Pressure table in the limiting orifice laboratory exercise (page
77). If a flow device such as a Dry-Cal is used the P
m
is simply the barometric pressure.


2-13
5. Set flow controller to 95 percent of full scale, then wait until flow meter
reading stabilizes.
6. Enter the flow meter reading using the flow input screen.
7. Repeat steps 5 and 6 for the remaining flow settings.
8. If difficulty is encountered due to a malfunction of the flow controller,
contact Thermo Environmental Instruments.

Lab 2, Figure 4. Mass flow meter calibration setup.

2-14
Lab 2, Table 2. Example Mass Flowmeter Calibration Data Sheet
Name ___Joe Smith_____
Date _____5/18/08______
Group no. ____2_________

Laboratory Temperature, Tm ____22.0___C __295.0 _ K
Vapor Pressure (see Saturation Vapor Pressure table in
Limiting Orifice Laboratory Exercise), VP 19.827 mm Hg
Mass flowmeter no. _________1573________________
Mass flowmeter range setting _1000 cc/min (1.0 l/min)__
Barometric pressure, Pb ____750.00___ mm Hg
Transducer no. ____873_______

Approximate
mass flowmeter
(% full scale)

Bubble
Meter
Qm
(L)

Bubble
Meter
Qstd
Mass flow
reading
( min L )
80 0.820 0.796 0.800
60
40
20

( ) ( ) | |
m m std std m std
b m
std
std
Q T T Q
mHg mm Hg-VPm P P
mm Hg P
K T
=
=
=
=
760
298

Example Calculations:

Calculations based on data in table above.

( ) ( ) | |
m m std std m std
Q T T Q =
mHg mm Hg-VPm P P
b m
=
mm Hg . mm Hg . mm Hg- P
m
173 730 827 19 750 = =
( ) ( ) | | min / 796 . 0 min / 820 . 0 0 . 295 760 298 193 . 730 L L K mmHg K mmHg Q
std
= =

2-15
Laboratory 2, Experiment 2: Mass Flowmeter Calibration Data Sheet

Name ______________________
Date ______________________
Group no. ____________________

Laboratory Temperature, Tm _________C _________ K
9

Mass flowmeter no. _________________________
Mass flowmeter range setting __________________
Barometric pressure, Pb _______________________
Transducer no. ____________________

Approximate
mass flowmeter
(% full scale)

Bubble
Meter
Qm
(L)

Bubble
Meter
Qstd
Mass flow
reading
( min L )
80
60
40
20

( ) ( ) | |
m m std std m std
b m
std
std
Q T T Q
mm Hg mm Hg-Vm P P
mm Hg P
K T
=
=
=
=
760
298


9
m


2-16

Laboratory 2, Experiment 2: Mass Flowmeter Calibration Data Sheet

Name ______________________
Date ______________________
Group no. ____________________

Laboratory Temperature, Tm _________C _________ K
10

Mass flowmeter no. _________________________
Mass flowmeter range setting __________________
Barometric pressure, Pb _______________________
Transducer no. ____________________

Approximate
mass flowmeter
(% full scale)

Bubble
Meter
Qm
(L)

Bubble
Meter
Qstd
Mass flow
reading
( min )
80
60
40
20

( ) ( ) | |
m m std std m std
b m
std
std
Q T T Q
mm Hg mm Hg-Vm P P
mm Hg P
K T
=
=
=
=
760
298


10
m


2-17

2.4 Experiment 3: Calibration of a Rotameter at
Reduced Pressure
Introduction
Although rotameters remain in use as flow measuring devices, they have been
replaced by mass flow meters and controllers to a large extent. Since they require
no power to operate and are relatively rugged, they continue to be used in some
sampling trains which are designed to manually collect samples. In addition, they
are regularly used as gross indicators of gas flow. For example, they can
provide an easy means of visually determining the presence of excess gas flow in
a sampling manifold to reassure the operator the instrument under calibration is
receiving sufficient calibration gas.
A rotameter is a conical tube with an internal float. Changes in the flow rate
cause the float to move up and down the conical tube. The length of the conical
tube has a scale which corresponds to a flow rate. In most cases, the scale is not
assigned a corresponding flow rate until the device is calibrated. (See Variable
Area Meters in Chapter 3 of the Student Manual.) Corrections can be made to
the rotameter measurements; however, it is simpler and more accurate to
calibrate a rotameter at the conditions at which it will be used.
In this experiment, you will calibrate a rotameter with a mass flow meter (or
mass flow controller) at two different upstream pressures.

Calibration Procedure
The setup is shown in Lab 2, Figure 5. Record room temperature and barometric
pressure, P
b
.
1. Close valve B.
2. Fully open valve A.
3. Turn on pump.
4. Adjust valve B until the rotameter reads approximately 80% full scale. Read
the float at the point at which it is highest and widest. For example, if the
float is a sphere, it should be read at its greatest diameter (the middle of the
sphere).
5. Record the rotameter setting, mass flow meter reading, and vacuum pressure
reading, p
g
, on the data sheet.
6. Reduce the flow rate to approximately 60% full scale on the rotameter by
adjusting valve B. It is not necessary to set the rotameter at a specific
number.
7. Adjust valve A so that the pressure reading is the same as in step 5. Repeat
steps 6 and 7 for fine adjustment of the p
g
reading. You may have to repeat
steps 6 and 7 many times because of lags in your pressure drop. It is
important to set the p
g
value at exactly the same reading, but it is not
necessary to set the rotameter reading. Just read the rotameter accurately.

2-18
8. Repeat steps 6 and 7 for rotameter settings of approximately 40% and 20% of
full scale. Note: You have just calibrated the rotameter at one upstream
pressure condition. Next, you will change the upstream pressure of the
rotameter and calibrate it again.
9. Adjust valves A and B so that an 80% full scale rotameter reading is obtained
at a new p
g
value, which should be 2 to 3 times the p
g
value used for the first
curve. Repeat steps 5 through 8 to obtain a calibration curve at this new p
g
.
Since you are going to plot curves, it is not necessary to try and duplicate the
rotameter readings obtained in the first part of the experiment.
10. Convert your gauge pressure readings to absolute pressure by using

g b
+ = . Remember, P
g
is a vacuum in this case and has a negative sign.
11. Correct all mass flowmeter readings to flow by using the mass flowmeters
calibration curve as prepared in Laboratory 2, Experiment 2. If the
calibration curve is not available, assume the mass flow meter output is
accurate.
12. Plot the two resulting curves on the same graph paper. Use the x-axis for
flow ( min L ) and y-axis for rotameter reading. Be sure to note the absolute
upstream pressure (P) on each curve.

Lab 2, Figure 5. Calibration of a rotameter at reduced pressure.

2-19
Laboratory 2, Experiment 3: Rotameter Calibration Data Sheet

Room temperature ________________C Name__________________
Mass flowmeter no. _________________ Date__________________
b
______________ Group no._______________
Transducer no. ____________________
Rotameter no. ____________________

Mass
flowmeter
reading
Flow as
indicated by
mass flow
meters
calibration
curve
( min L )
Rotameter
reading
Upstream
pressure or
vacuum
Pg
Absolute
upstream
pressure
P
Pressure
setting no.

1

2

Reduced
pressure


2-20
Laboratory 2, Experiment 3: Rotameter Calibration Data Sheet

Room temperature ________________C Name__________________
Mass flowmeter no._________________ Date__________________
b
______________ Group no._______________
Transducer no. ___________________
Rotameter no. ____________________

Mass
flowmeter
reading
Flow as
indicated by
mass flow
meters
calibration
curve
( min L )
Rotameter
reading
Upstream
pressure or
vacuum
Pg
Absolute
upstream
pressure
P
Pressure
setting no.

1

2

Reduced
pressure


2-21
2.5 Experiment 4: Calibration of a Limiting Orifice
and Investigation of Factors Affecting Flow
Introduction
Limiting orifices are commonly used to control flow rate. In this experiment, you
will calibrate a limiting orifice with a soap bubble meter (or automated flow
meter) to determine:
a. at what vacuum pressure the pressure drop across the orifice causes it to
become a limiting orifice,
b. the effect of upstream pressure on flow rate, and
c. the effect on flow rate of reversing the direction of flow through the
orifice.
The description of a soap bubble meter (or automated flow meters) can be
found in Chapter 3 of the Student Manual under the topic of volume meters.

Determination of Critical Vacuum Part I
The setup is shown in Lab 2, Figure 6. Record room temperature, T, and
barometric pressure, P
b
.
1. Make sure to orient the inlet side of the orifice so it is pointed toward
vacuum gauge #1.
2. Leave needle valve #1 completely open (to open, turn counterclockwise).
3. Turn on the vacuum pump.
4. Adjust needle valve #2 until about five inches of Hg vacuum are registered
on vacuum gauge #2.
5. Using the moving bubble meter (or automated flow meters), determine and
record the time required for the specified volume to flow through the bubble
meter (see Part I of data sheet for the specified volume).
6. Repeat at other vacuum settings (see Part I of data sheet for other vacuum
settings).
7. Calculate and correct the flow rate for each vacuum setting as directed below.
8. Plot flow rate on the y-axis and vacuum pressure on the x-axis. At what
vacuum pressure does the flow become constant? What is this flow rate?
The use of the soap bubble meter for the calibration of flow rate devices
requires correction for temperature, barometric pressure, and the vapor
pressure of the soap bubble, which is considered to be that of the vapor
pressure of water. The equation below is presented to assist the user of the
soap bubble meter with these corrections.

( )
( )
( )
( )
(
+
(
m V
Q
v b
std
273
298
760 min


2-22
Where: Q
std
= flow rate corrected to standard conditions
P
b
= barometric pressure, mm Hg
P
v
= vapor pressure of water, mm Hg (see Lab 2, Table 3)
T = temperature of gas, C (room temperature)
V = volume measured by bubble meter
= time for measured volume to flow through bubble meter

Example: Assume temperature to be 20C and barometric pressure to be
710 mm Hg.

( )
( )
( )
( )
( )
( )
927 0
min
20 273
298
760
54 17 710
min
flow rate Standard
.
m V
.
m V
|
|
.
|
\
|
=
(
+
(

If an automated flow meter (e.g., Gilibrator, Dry-Cal) which provides
an output reading as a flow rate (ml/min) is used in place of a simple bubble
meter, then make the following substitute in the equation above:

Where: Q
m
= flow rate as measured by the automated flow meter

If an automated flow meter is used that does not utilize a liquid soap
bubble (e.g., Dry-Cal ) then, in addition to the substitution mentioned
previously, also remove the term P
v
from the original equation. The term P
v
is
removed since this type of flow meter does not introduce water vapor while
measuring the volumetric flow rate.
( )
( )
m Q
min
m V
=
(


2-23

Lab 2, Figure 6. Calibration of a limiting orifice using a bubble meter.

2-24
Lab 2, Table 2. Saturation vapor pressure over water (C, mm Hg).
11

Values for fractional degree between 50 and 89 were obtained by interpolation
Temp.
C
0.0 0.2 0.4 0.6 0.8 Temp.
C
0.0 0.2 0.4 0.6 0.8
-15 1.436 1.414 1.390 1.368 1.345 42 61.50 62.14 62.80 63.46 64.12
-14 1.560 1.534 1.511 1.485 1.460 43 64.80 65.48 66.16 66.86 67.56
-13 1.691 1.665 1.637 1.611 1.585 44 68.26 68.97 69.69 70.41 71.14
-12 1.834 1.804 1.776 1.748 1.720
-11 1.987 1.955 1.924 1.893 1.863 45 71.88 72.62 73.36 74.12 74.88
46 75.65 76.43 77.21 78.00 78.80
-10 2.149 2.116 2.084 2.050 2.018 47 79.60 80.41 81.23 82.05 82.87
-9 2.326 2.289 2.254 2.219 2.184 48 83.71 84.56 85.42 86.28 87.14
-8 2.514 2.475 2.437 2.399 2.362 49 88.02 88.90 89.79 90.69 91.59
-7 2.715 2.674 2.635 2.593 2.553
-6 2.931 2.887 2.843 2.800 2.757 50 92.51 93.5 94.4 95.3 96.3
51 97.20 98.2 99.1 100.1 101.1
-5 3.163 3.115 3.069 3.022 2.976 52 102.09 103.1 104.1 105.1 106.2
-4 3.410 3.359 3.309 3.259 3.211 53 107.20 108.2 109.3 110.4 111.4
-3 3.673 3.620 3.567 3.514 3.461 54 112.51 113.6 114.7 115.8 116.9
-2 3.956 3.898 3.841 3.785 3.730
-1 4.258 4.196 4.135 4.075 4.016 55 118.04 119.1 120.3 121.5 122.6
56 123.90 125.0 126.2 127.4 128.6
-0 4.579 4.513 4.448 4.385 4.320 57 129.82 131.0 132.3 133.5 134.7
58 136.08 137.3 138.5 139.9 141.2
0 4.579 4.647 4.715 4.785 4.855 59 142.60 143.9 145.2 146.6 148.0
1 4.926 4.998 5.070 5.144 5.219
2 5.294 5.370 5.447 5.525 5.605 60 149.38 150.7 152.1 153.5 155.0
3 5.685 5.766 5.848 5.931 6.015 61 156.43 157.8 159.3 160.8 162.3
4 6.101 6.187 6.274 6.363 6.453 62 163.77 165.2 166.8 168.3 169.8
63 171.38 172.9 174.5 176.1 177.7
5 6.543 6.635 6.728 6.822 6.917 64 179.31 180.9 182.5 184.2 185.8
6 7.013 7.111 7.209 7.309 7.411
7 7.513 7.617 7.722 7.828 7.936 65 187.54 189.2 190.9 192.6 194.3
8 8.045 8.155 8.267 8.380 8.484 66 196.09 197.8 199.5 201.3 203.1
9 8.609 8.727 8.845 8.965 9.086 67 204.96 206.8 208.6 210.5 212.3
68 214.17 216.0 218.0 219.9 221.8
10 9.209 9.333 9.458 9.585 9.714 69 223.78 225.7 227.7 229.7 231.7
11 9.844 9.976 10.109 10.244 10.380
12 10.518 10.658 10.799 10.941 11.085 70 233.7 235.7 237.7 239.7 241.8
13 11.231 11.379 11.528 11.680 11.833 71 243.9 246.0 248.2 250.3 252.7
14 11.987 12.144 12.302 12.462 12.624 72 254.6 256.8 259.0 261.2 263.4
73 265.7 268.0 270.2 272.6 274.8
15 12.788 12.953 13.121 13.290 13.461 74 277.2 279.4 281.8 284.2 286.6
16 13.634 13.809 13.987 14.166 14.347 75 289.1 291.5 294.0 296.4 298.8
17 14.530 14.715 14.903 15.092 15.284 76 301.4 303.8 306.4 308.9 311.4
18 15.477 15.673 15.871 16.071 16.272 77 314.1 316.6 319.2 322.0 324.6
19 16.477 16.685 16.894 17.105 17.319 78 327.3 330.0 332.8 335.6 338.2
79 341.0 343.8 346.6 349.4 352.2
20 17.535 17.853 17.974 18.197 18.422
21 18.650 18.880 19.113 19.349 19.587 80 355.1 358.0 361.0 363.8 366.8
22 19.827 20.070 20.312 20.565 20.815 81 369.7 372.6 375.6 378.8 381.8
23 21.068 21.324 21.583 21.845 22.110 82 384.9 388.0 391.2 394.4 397.4
24 22.377 22.648 22.922 23.198 23.476 83 400.6 403.8 407.0 410.2 413.6
84 416.8 420.2 423.6 426.8 430.2
25 23.756 24.039 24.326 24.617 24.912
26 25.209 25.509 25.812 26.117 26.426 85 433.6 437.0 440.4 444.0 447.5
27 26.739 27.055 27.374 27.696 28.021 86 450.9 454.4 458.0 461.6 465.2
28 28.349 28.680 29.015 29.354 29.697 87 468.7 472.4 476.0 479.8 483.4
29 30.043 30.392 30.745 31.102 31.461 88 487.1 491.0 494.7 498.5 502.2
89 506.1 510.0 513.9 517.8 521.8
30 31.824 32.191 32.561 32.934 33.312
31 33.695 34.082 34.471 34.864 35.261 90 525.76 529.77 533.90 537.86 541.95
32 35.663 36.068 36.477 36.891 37.308 91 546.05 550.18 554.35 558.53 562.75
33 37.729 38.155 38.584 39.018 39.457 92 566.99 571.26 575.55 579.87 584.22

11
Book of Chemistry and Physics, 45
th
edition. 1965. Chemical Rubber Publishing Company.

2-25
34 39.898 40.344 40.796 41.251 41.710 93 588.60 593.00 597.43 601.89 606.38
94 610.90 615.44 620.01 624.61 629.24
35 42.175 42.644 43.117 43.595 44.078 95 633.90 638.59 643.30 648.05 652.82
36 44.563 45.054 45.549 46.050 46.556 96 657.62 662.45 667.31 672.20 677.12
37 47.067 47.582 48.102 48.627 49.157 97 682.07 687.04 692.05 697.10 702.17
38 49.692 50.231 50.774 51.323 57.879 98 707.27 712.40 717.56 722.75 727.98
39 52.442 53.009 53.580 54.156 54.737 99 733.24 738.53 743.85 749.20 754.58

40 55.324 55.91 56.51 57.11 57.72 100 760.00 765.45 770.93 776.55 782.00
41 58.34 58.96 59.58 60.22 60.86 101 787.57 793.18 798.82 804.50 810.21

Effect of Upstream Resistance Part II
1. Adjust needle valve #2 to maintain 25 in. Hg vacuum.
2. Place resistance in front of the orifice by adjusting needle valve #1 until
vacuum gauge #1 shows 10 in. Hg vacuum.
3. Determine the flow rate under these conditions using the bubble flowmeter
or automated flow meter. Determine and record the time required to pass
400 mL through the bubble flowmeter. Calculate the flow as in Part I and
record on the data sheet, Part II.
4. Calculate the percentage of change in flow rate using the following formula:

( ) 100
I Part in Hg vacuum in. 25 at flow rate
I Part in Hg vacuum in. 25 at flow rate - II Part in flow rate
Change % =

The difference between this flow rate and that determined in Part I
demonstrates the need to calibrate the orifice in the system in which it is
going to be used.

Effect of Reversing Orifice Part III

1. Shut off the vacuum pump.
2. Reverse the orifice. The orifice should be oriented with the inlet side of the
orifice pointed toward vacuum gauge #2.
3. Turn on the vacuum pump.
4. Completely open needle valve #1.
5. Obtain a vacuum of 25 in. Hg on gauge #2 and determine the flow rate as in
Part I.
6. Record the information on the data sheet, Part III.
7. Calculate the % change using the following formula:

( ) 100 %
I Part in Hg vacuum in. 25 at flow rate
I Part in Hg vacuum in. 25 at flow rate - II Part in flow rate
Change =

This demonstrates the error that would result if you calibrated the orifice in
one direction and used it in the other direction.

2-26
Laboratory 2, Experiment 4: Limiting Orifice Calibration Data Sheet

P
b
_______________________ mm Hg Name__________________
T ___________________________ C Date__________________
Needle gauge____________________ Group no._______________

Part I Data
Vacuum
(in. Hg)
Volume
(mL)
Time
(min)
Flow rate, Qstd
(mL/min)
5 200
10 200
13 400
15 400
17 400
19 400
21 400
23 400
25 400
Maximum
vacuum
400

Part II Data
Condition Vacuum
gauge #1
Vacuum
gauge #2
Volume
(mL)
Time
(min)
Flow rate,
Qstd
(mL/min)

Data from
Part I
0 25 400
Resistance
in system
10 25 400

% Change = _________

Part III Data
Condition Vacuum
(in. Hg)
Volume
(mL)
Time
(min)
Flow rate,
Qstd
(mL/min)

Data from
Part I
25 400
Orifice
reversed
25 400

% Change = _________


2-27
Laboratory 2, Experiment 4: Limiting Orifice Calibration Data Sheet

P
b
_______________________ mm Hg Name __________________
T ___________________________ C Date __________________
Needle gauge____________________ Group no._______________

Part I Data
Vacuum
(in. Hg)
Volume
(mL)
Time
(min)
Flow rate, Qstd
(mL/min)
5 200
10 200
13 400
15 400
17 400
19 400
21 400
23 400
25 400
Maximum
vacuum
400

Part II Data
Condition Vacuum
gauge #1
Vacuum
gauge #2
Volume
(mL)
Time
(min)
Flow rate,
Qstd
(mL/min)

Data from
Part I
0 25 400
Resistance
in system
10 25 400

% Change = _________

Part III Data
Condition Vacuum
(in. Hg)
Volume
(mL)
Time
(min)
Flow rate,
Qstd
(mL/min)

Data from
Part I
25 400
Orifice
reversed
25 400

% Change = _________


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