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Orbisphere 3610

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3610 OM E0310

3610

Operator's manual
CO 2 - N 2 - H 2

3610
Analyzer for precise
measurement & control
s/n 32893 and up

3610 Analyzer - Table of contents

Table of contents
1

Introduction

Safety note and Warnings


2.1
2.2
2.3

Operating information
3.1
3.2
3.3
3.4
3.5
3.6
3.7
3.8
3.9

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Calibrate menu.......................................................................................27
Barometric pressure sensor calibration..................................................28
External pressure sensor calibration......................................................28
TC sensor calibration .............................................................................29
Calibration tables ...................................................................................33

Accessories and attachments


6.1
6.2
6.3

Operators Manual

Options menu.........................................................................................17
Display units...........................................................................................18
Thermal cutoff ........................................................................................20
Alarm and analog outputs ......................................................................20
Serial output ...........................................................................................21
Continuous purge mode.........................................................................21
Rolling average ......................................................................................22
Language ...............................................................................................22
Hold recovery (CO2 and N2 systems only)............................................22
Offset......................................................................................................22
Corrections.............................................................................................23
Liquid/Gas coefficient.............................................................................24
Membrane selection...............................................................................25

Calibrations
5.1
5.2
5.3
5.4
5.5

Instrument controls...................................................................................9
Program menus......................................................................................10
Entering numerical values......................................................................10
Additional information.............................................................................10
Measure menu .......................................................................................11
Measurement displays ...........................................................................11
Measurement hold switch (CO2 and N2 systems only) .........................12
Accessing measurements from the PC..................................................12
Shutting down the system ......................................................................15

Options set up
4.1
4.2
4.3
4.4
4.5
4.6
4.7
4.8
4.9
4.10
4.11
4.12
4.13

Signs used in this manual ........................................................................7


Precautionary labels on instrument..........................................................7
Safety recommendations .........................................................................7

Model 32605 purge backup unit.............................................................39


Model 32557/32559 external temperature sensor .................................39
Data acquisition software .......................................................................39

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Table of contents - 3610 Analyzer

Maintenance and troubleshooting


7.1
7.2
7.3

General maintenance .............................................................................41


Instrument and sensor maintenance ......................................................43
Troubleshooting......................................................................................44

Installation
8.1
8.2
8.3
8.4
8.5
8.6
8.7
8.8
8.9
8.10
8.11
8.12

Mounting.................................................................................................50
Connections ...........................................................................................53
Wiring identification ................................................................................57
User-supplied cabling requirements .......................................................60
LEMO connector assembly instructions .................................................60
Cable gland wiring instructions...............................................................61
Sensor and sensor purge gas installation ..............................................62
Model 28117 pressure sensor installation ..............................................62
Analog outputs .......................................................................................62
Serial outputs .........................................................................................65
Alarm outputs .........................................................................................66
Installation completion check list ............................................................68

Specifications
9.1

10

System specifications .............................................................................71

Part lists

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10.1 Instrument ..............................................................................................73


10.2 Accessories ............................................................................................74
10.3 Spare parts .............................................................................................74

Operators Manual

3610 Analyzer - Introduction

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Introduction
About this manual
The information in this manual has been carefully checked and is believed to be
accurate. However, Hach Ultra Analytics assumes no responsibility for any inaccuracies
that may be contained in this manual. In no event will Hach Ultra Analytics be liable for
direct, indirect, special, incidental, or consequential damages resulting from any defect
or omission in this manual, even if advised of the possibility of such damages. In the
interest of continued product development, Hach Ultra Analytics reserves the right to
make improvements in this manual and the products it describes at any time, without
notice or obligation.

Equipment serial numbers covered by this manual


This manual is intended for the following piece of equipment:
Orbisphere 3610 Analyzer; Serial number 32893 and up

Scope of supply
Equipment included

3610 analyzer

TC sensor

Part number

Notes

3610/xxx

See Table 30, Indicating


Instrument Configurations, on
page 73 for possible configurations

3125x or 3126x or
3145x or 3146x or
3155x or 3156x

Flow chamber

For measuring hydrogen


For measuring carbon dioxide
For measuring nitrogen

32001/2
For sensor service and maintenance

Recharge kit
Certificate of conformity
Operators manual

3610 OM E0310.fm

English language

Your 3610 system for Carbon Dioxide (CO 2 ), Hydrogen (H 2 ) or Nitrogen (N 2 )


measurements, includes two basic components:

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A series 3610 Indicating Instrument available as a portable, panel mount or wall


mount unit.
A model 3125x (or 3126x) H2, a model 3145x (or 3146x) CO2, or a model 3155x
(or 3156x) N2 Thermal Conductivity (TC) Sensor.

Intended use of this equipment


In conjunction with the Orbisphere TC (Thermal Conductivity) sensor, the 3610 provides
precise, selective measurement of Carbon Dioxide (CO2), Nitrogen (N2) or Hydrogen
(H2).

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Introduction - 3610 Analyzer

The instrument is designed for durability, ruggedness and harsh environments providing
accurate process monitoring in a wide range of applications, whether in a liquid or
gaseous phase, from in-line beverage production to corrosion control in power
generation.
There are three models, all with IP65, NEMA 4X protection that ensures the optimum
monitoring solution. The portable version offers a handle and wrap-around bumpers for
added protection. The panel and rack mounted versions fit through a cutout from the
front for easier access in tight spaces. The wall mount version is housed in a stainless
steel outer enclosure.
The instrument is simple to use with only four front panel keys operating through menu
driven software with a large backlit display. The instrument can be used and installed
throughout the plant. A key switch provides added protection, to prevent accidental or
unauthorized use. The instrument can also be connected to a serial printer, monitor or
computer for additional data display and collection facilities.

Common units
Unit

meaning

ppm

parts per million, by weight

ppb

parts per billion, by weight

g/kg

grams per kilogram

mg/l

milligrams per liter

%
cc/kg

percentage, by weight
cubic centimeters per kilogram

ml/l

milliliters per liter

v/v

volume per volume (ratio)

% vbar

percentage per volume, barometric pressure referenced

% vext

percentage per volume, sample pressure compensated

Terms and definitions


meaning

Relative pressure

Relative pressure is absolute pressure, less atmospheric pressure


(this is the customary gauge reading).

Absolute pressure

Absolute pressure is relative pressure, plus atmospheric pressure

Headspace

The empty volume above a liquid or solid in a closed container.

Conductivity

The reciprocal of electrical resistivity.

Resistivity

The opposition offered by a body or substance to the passage


through it of a steady electric current.

Concentration

The relative content of a component in a gaseous or liquid media.

Operators Manual

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Terms

3610 Analyzer - Introduction

Acknowledgements

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Operators Manual

Dacron, Delrin, Tedlar, Tefzel, and Viton are registered trademarks of DuPont.
Halar is a registered trademark of Ausimont U.S.A., Inc.
Hastelloy is a registered trademark of Haynes International.
Kynar is a registered trademark of The Pennwalt Corporation.
Monel is a registered trademark of IMCO Alloys International, Inc.
Saran is a registered trademark of Dow Chemical Co.
Swagelok is a registered trademark of Swagelok Co.
Microsoft and Windows are registered trademarks of Microsoft Corporation.

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Introduction - 3610 Analyzer

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Operators Manual

3610 Analyzer - Safety note and Warnings

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Safety note and Warnings


2.1 Signs used in this manual
Where needed, this manual uses the following signs and paragraph:

WARNING
Whenever a potentially hazardous situation to people or equipment is present.

CAUTION :
Things to know (to do or to avoid) to get the equipment to operate as intended.

Note :
Particularly important fact to know for correct operation.

2.2 Precautionary labels on instrument


Read all labels and tags attached to the instrument. Personal injury or damage to this
instrument could occur if not observed.
This label is present wherever a potentially hazardous situation to
people or equipment is present. Refer to Operators Manual for
details.

This label indicates the need for protective eye wear.

This label indicates a connection point for shield earth or/and ground.

2.3 Safety recommendations


For safe operation, it is imperative that these service instructions be read and that the
safety recommendations mentioned herein be scrupulously respected.
If repairs or adjustments are necessary, the instrument should be returned to an
authorized Orbisphere service center.
If danger warnings are not heeded to, serious material or bodily injury could occur.

WARNING
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In accordance with safety standard, it must be possible to disconnect the power supply
of the instrument in its immediate vicinity.

WARNING
The installation of the instrument should be performed exclusively by personnel
specialized and authorized to work on electrical installations, in accordance with
relevant local regulations.
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Safety note and Warnings - 3610 Analyzer

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Operators Manual

3610 Analyzer - Operating information

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Operating information
3.1 Instrument controls
The front panel of the 3610 series instruments (as illustrated in Fig 1) has several
displays and controls associated with it.

Fig 1 : Instrument Controls

The Key Switch should be turned to the horizontal unlocked position to start the
instrument in measurement mode. The function keys (see Fig 2) are only active if
the key switch is in the unlocked position. Use the vertical locked position to avoid
accidental modifications.
The Display has a two-line liquid crystal display (LCD) with 16 characters per line.
A Light Button, when pressed, provides illumination to the LCD for three minutes
(when connected to an external power supply).
Four Function Keys provide simple operator control over the instrument functions:

Fig 2 : Function Keys

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ESC jumps back a step within a program menu.


The UP/DOWN ARROW keys are used to scroll through screen displays.
ENTER selects a highlighted item from the menu.

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Operating information - 3610 Analyzer

3.2 Program menus


The operator controls the instrument by menu-selectable commands using the four
function keys.
The main menu has three choices:
MEASURE to start the measurement sequence (for
full instructions refer to Measure menu on
page 11)
OPTIONS to enable the instrument to be
customized (for full instructions refer to Options
menu on page 17)
CALIBRATE to provide a choice of sensor
calibration procedures (for full instructions refer to
Calibrate menu on page 27)
To select one of these commands, first press ESC until the main menu is displayed, next
press the UP/DOWN ARROWS until your choice is flashing, and then press ENTER.

3.3 Entering numerical values


When entering numbers in any of the instrument menus, the current numerical value is
displayed with one digit highlighted by the ^ symbol below it.
Use the UP/DOWN ARROWS to increase/decrease the
value of the digit (0-9 plus a decimal point) until you reach
your required target value. Then press ENTER to shift the
highlight symbol one digit to the right and repeat the
process. Pressing ENTER after the last digit saves the
value.

3.4 Additional information

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The CO2, H2 and N2 instrument procedures are, for the most part, operationally identical.
In general, this manual describes CO2 measurement procedures. When an operational
difference arises, the manual also describes the appropriate H2 or N2 measurement
procedure.

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3610 Analyzer - Operating information

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3.5 Measure menu


The flow chart (Fig 3 below) depicts the instrument measurement options available. The
flow lines are keyed to specific instrument actions.

Fig 3 : Instrument Measurement Menu Flow Diagram

Your instrument is pre-set with certain default values to anticipate your measurement
conditions, such as measurement display units, thermal cutoff temperature, etc. You
may, however, change these using the Instrument Modify Options Menus described in
Options set up on page 17.

3.6 Measurement displays


Switching on the indicating instrument first shows the software version and date on the
LCD, and then switches to a Configuration Display showing the gas being measured,
the purge gas required for the sensor, and the membrane model number for this sensor.
In the example shown in Fig 4 the display shows the gas being measured (g) as CO2, the
purge gas (p) as being N2 and the sensor membrane (m) as being model number 29561.
The configuration screen appears for the duration of the measurement cycle (usually 15
to 25 seconds), before switching to a continuous gas and temperature Measurement
Display.

Fig 4 : Configuration and Measurement Displays

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There will be a delay between successive display updates depending on the length of the
purge/measurement cycle. Depending on the Number of Ranges configured for the
instrument (see Display units on page 18), the display resolution changes automatically
to reflect gas and temperature measurement value changes. To make changes to the
displayed units of measurement and display resolution, refer to Display units on
page 18.
Press the ESC key to exit from the measurement display and move to the Main Menu to
access additional menus (Measure, Options and Calibrate).

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Operating information - 3610 Analyzer

3.7 Measurement hold switch (CO2 and N2 systems only)


Interruptions in the sample flow can cause temporary variations in measurements of CO2
or N2 gas concentrations. For this reason, the instrument provides a Hold capability to
exclude these measurements from the statistics. To use this capability, you must provide
an external switch (for example, on a filling machine) that is open while the sample is
flowing and closed during the flow interruption. Wire this switch as described in Hold
switch wiring identification on page 59.
When the switch is closed, indicating a Hold condition, the instrument holds the last gas
measurement values on all outputs, though temperature changes continue to occur,
flashes a HOLD message between LCD updates, and shows a Hld code in the LCD
bottom line at the right of the temperature measurement
Once the switch is reopened (typically, with the restart of sample flow) the instrument will
start to display the new measurement values. However, these values should not be
considered accurate until after one to four additional measurement cycles have been
performed (15-60 seconds). You can specify the number of additional cycles using the
Hold Recovery option in the Options menu, see Hold recovery (CO2 and N2 systems
only) on page 22.

3.8 Accessing measurements from the PC


If you have installed the Data Acquisition Software (as described in Data acquisition
software on page 39), you can use this program to download measurement data to your
PC.

a ) Menu overview
The program's main menus appear as follows:

Fig 5 : Data Acquisition Main Menu

b ) Acquiring data
With the instrument connected to your PC, and the sensor placed in a sample, you
should be able to conduct an initial data acquisition test.
First, make sure the program knows which COM port is used by your PC by choosing
Communications from the Configuration menu. Ensure the correct COM port is
checked (see Fig 6).

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File includes typical Windows file management and printing functions.


Terminal commences and ends the data acquisition process.
Export sends the information to the Windows Clipboard, for inclusion in other
Windows programs.
Configuration lets you customize the program for your application's
requirements.
About gives information about the current acquisition software version number.

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Fig 6 : Serial Port Configuration

Next, check that you have set the acquisition rate to a convenient interval. Do this by
choosing Data Acquisition from the Configuration menu, and selecting the required rate
(see Fig 7).

Fig 7 : Data Acquisition Interval

The All data choice enables the program to accept measurements from every
measurement cycle. The longest interval is one hour. Select OK when you have the rate
you require.

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Finally, make sure you have chosen the proper gas to measure from the Gas Selection
menu under Configuration (see Fig 8).

Fig 8 : Gas Selection

To commence data acquisition, choose Go from the Terminal menu. You can expect to
see a running display like the following:

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Operating information - 3610 Analyzer

Fig 9 : Data Acquisition Display

The number of samples in the buffer continues to rise until you choose End from the
Terminal menu, or when the limit of 2000 samples is reached.

c ) Printing, copying and saving data


The File, Print command places your list of values into a pre-formatted tabular template,
and sends it to your printer. The program asks you to enter Title and Author information
as illustrated in Fig 10. The operating system automatically sets the Date.

Fig 10 : Print Data Option

The resulting printed list includes the Title, Author and Date information on each page.
To save this list as a text (.txt) file, capable of being recalled by the MOCA3610 program
or imported as a file into other Windows programs, choose File, Save as. A dialog box
appears, with a space to fill in with an eight-letter name. (The program automatically
attaches a .txt suffix to these files.)

To copy this list to the Windows Clipboard, so that this information can be pasted into a
spreadsheet, word processor or any other kind of Windows program that accepts tabular
text information, choose Export, To Clipboard.

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If you have saved previous files, a grayed-out list of these names appears as well.
Typical to Windows programs, Directories and Drives boxes can be used to locate
other places to save the file. You may also type the drive and directory yourself when
saving the file.

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3.9 Shutting down the system


Since the indicating instrument has a non-volatile memory, important parameters remain
memorized even when the instrument power is off.
During a short shutdown period (such as weekends), the sensor can be left in line, with
the instrument operating and the purge gas supplied.

Note :
If the model 32605 Purge Backup Unit is installed as described in Model 32605 purge
backup unit on page 39, the instrument can also be turned off.

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If the inactive period is likely to last for a period of longer than 2 days, then to avoid any
damage to the sensor, remove it from the line and dry it off before storing. Refer to the
associated TC Sensors - Maintenance & Installation Manual, provided with your
instrument, for full instructions on this process.

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Operating information - 3610 Analyzer

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3610 Analyzer - Options set up

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Options set up
4.1 Options menu
Your instrument includes a full set of programmable outputs, and the ability to specify
different units of measurement, sample media and sample conditions. The flow charts
illustrated in Fig 11 and Fig 12 outline these routines.

Fig 11 : Modify Options Menu - Part 1

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With your system in Measurement Mode, press the ESC key to display the main menu.
Using the UP/DOWN ARROW keys, highlight OPTIONS and press ENTER to bring up
the MODIFY OPTIONS menu.

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Options set up - 3610 Analyzer

Fig 12 : Modify Options Menu - Part 2

4.2 Display units


This option allows you to specify your type of measurement (dissolved, fraction or partial
pressure), the units of measurement to be displayed, the display resolution (i.e. decimal
point placement), the number of display ranges desired and the temperature units to be
displayed.
The initial menu provides a choice of DISSOLVED, FRACTION or PARTIAL
PRESSURE gas measurement. Highlight your choice and press ENTER.

a ) Dissolved gas measurement


Dissolved CO2 measurements start with a special set of menus. First, you have a choice
of sampling media in the DISSOLVED INTO menu. The choices are WATER, BEER,
COLA and WINE. Highlight your sampling media, then press ENTER.

If your sampling media is WINE, then you must specify its sugar and alcohol
concentrations.

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Choosing BEER or COLA applies a calculated density factor for this beverage.

3610 Analyzer - Options set up

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Enter the sugar concentration of the wine in grams per


liter.

Next enter the alcohol concentration in percent, of the


wine.

On completion of the above, or if the gas being measured is not N2, then the menu for
display units comes up. Table 1 shows the available choices of display units (certain
specialized applications may have additional units available as well).
Table 1 : Dissolved Gas Units
ppm

Gas concentration in parts per million, by weight

Gas concentration in percentage, by weight

cc/kg Gas concentration in cubic centimeters per kilogram


ml/l

Gas concentration in milliliters per liter

V/V

Gas concentration in volume per volume (ratio)

g/kg

Gas concentration in grams per kilogram

Then choose one of the formats to set the decimal point placement of the LOWEST
RANGE to display.
Next, choose the NUMBER OF RANGES. This menu limits the number of measurement
ranges that can be displayed (see Measurement displays on page 11). For example, if
your measurement values displayed are only from XX.XX to XXX.X with the XX.XX value
as the lowest, select 2 as the number of ranges.
Finally, choose the TEMPERATURE units (C, F, or K) from the temperature menu.

b ) Partial pressure gas measurement


The menu for display units comes up. Table 2 shows the available choices of display
units (certain specialized applications may have additional units available as well).
Table 2 : Partial Pressure Gas Units
bar

Gas pressure in bar

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mbar Gas pressure in millibars


kPa

Gas pressure in kilopascals

psia

Gas pressure in pounds per square inch, absolute

Atm

Gas pressure in atmosphere

bar20 Gas pressure in bar, calculated at 20C

Then choose the LOWEST RANGE, NUMBER OF RANGES and TEMPERATURE


units as described above.

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Options set up - 3610 Analyzer

c ) Fraction gas measurement


The menu for display units comes up. Table 3 shows the available choices of display
units.
Table 3 : Fraction Gas Units
%vbar

Percentage of gas volume, calculated at barometric pressure using the instrument's internal pressure sensor ([partial pressure / internal pressure] * 100)

%vext

Percentage of gas volume, calculated at external pressure using the external


pressure sensor ([partial pressure / external pressure] * 100)

Then choose the LOWEST RANGE, NUMBER OF RANGES and TEMPERATURE


units as described above.

4.3 Thermal cutoff


If the sample temperature is liable to exceed the compensated temperature range of the
TC sensor, you can set an upper temperature limit to automatically cut off the electrical
signal to the sensor to extend the sensor's life.
Under the MODIFY OPTIONS menu, highlight THERMAL CUTOFF and press ENTER.
The sensor can be ENABLED or DISABLED. Select ENABLED to move to the data
entry screen, or DISABLED to disable this option for the TC sensor.

If ENABLED, enter the thermal cutoff value in the data


entry screen.

Once enabled, if the sample temperature exceeds this limit, then alarms are set and a
Hot message appears on the bottom right of the measurement display.

4.4 Alarm and analog outputs


While HIGH and LOW LIMIT alarms serve different purposes than ANALOG CURRENT
outputs, their modification procedures are the same in the menu. Thus, this section
explains only how to set the LOW LIMIT ALARM.
The flow chart in Fig 11 shows all available options. In addition, Analog outputs on
page 62 and Alarm outputs on page 66 describe these outputs in more detail.
Connector and wiring identification for these outputs are in Wiring identification on
page 57.

If you choose LowHigh, the first menu allows you to enter


the low limit. Enter the value and press ENTER to move
on the next screen.

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Under the MODIFY OPTIONS menu, highlight ALARM and press ENTER. Choose
DISABLED if you want to disable alarms, or choose between the standard LowHigh or
High-HighHigh alarm. For ANALOG OUTPUT, the menu choice is either DISABLED or
ENABLED.

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On this screen, LL stands for LOW LIMIT. Use the UP/


DOWN ARROWS to move the decimal place to the
correct position in the displayed value, and press ENTER
to confirm and save this limit, and move to the next screen
where you can enter the HIGH LIMIT.
The HIGH LIMIT (HL), HIGHHIGH LIMIT (HH), ANALOG LOW LEVEL (AL), and
ANALOG HIGH LEVEL (AH) values, are all entered in the same way.

a ) Alarm and recorder output test


When you set each limit in the menus, the associated instrument alarm or analog output
provides a test signal. The Alarm Limit menus provide test relay outputs at the Alarm
Relay pins (see Table 25, Low/High Alarm Relay Responses, on page 67 and
Table 26, High/High-High Alarm Relay Responses, on page 67). The Analog Level
menus apply a test current (or voltage) at the recorder output Gas Concentration pins.
For example, when Analog Output, High Level is selected, after you press ENTER to
save the new limit in the UP/DOWN MODIFIES screen, the instrument provides a 20 mA
(or 5 V) test signal at the Gas Concentration pins of the Recorder connector.
The test analog signal or alarm output remains on the associated output pins until you
press ESC to return to the main menu. Refer to Alarm and recorder output testing on
page 69, for further description and use of these diagnostic outputs.

4.5 Serial output


The instrument serial output provides formatted text for an RS-232 compatible printer,
monitor, or computer interface.
Choose SERIAL OUTPUT from the MODIFY OPTIONS menu, to give you a choice of
DISABLED, ENABLED, DIAGNOSTICS and UPLOAD.
When ENABLED, the output provides a running log of gas concentration and sample
temperature measurement information. See Alarm outputs on page 66 for a more
detailed description of the outputs.
The DIAGNOSTICS output provides lines of hexadecimal code indicating how your
instrument is performing. In addition, the RS-232 output provides a running log of
diagnostic results for every measurement cycle.
The UPLOAD option is currently unavailable.

4.6 Continuous purge mode


Use this option to view the sensor voltages, particularly when seeing the Prg message
on your instrument LCD.
Choose CONTINUOUS PURGE from the MODIFY OPTIONS menu.

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The sensor voltage (V) and temperature (T) details are


displayed. The voltage should be in the range of -2.5V to
+4.5V (depending on the sensor being used - contact
your local Orbisphere Service Representative for more
details).
Press ESC to exit this option.

Note :
The sensor is continually purged whenever you exit the measurement mode.

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Options set up - 3610 Analyzer

4.7 Rolling average


The rolling average feature causes the instrument to average measurements over
successive measurement cycles. It suppresses sharp peaks and troughs, while retaining
reasonably fast response to real concentration changes.
Choose ROLLING AVERAGE from the MODIFY OPTIONS menu. Then select
DISABLED if rolling averages are not required, or select the number of successive
measurement cycles (each being approximately 22 seconds), over which the average
will be taken (3,5,7 or 9).

4.8 Language
The instrument can display its menus in English, French, Japanese, Spanish, German,
or Italian although the units of measurement remain the same (i.e. parts per million is still
expressed as ppm regardless of language).
Choose LANGUAGE from the MODIFY OPTIONS menu and select your preference.

4.9 Hold recovery (CO2 and N2 systems only)


This option allows you to choose a longer or shorter recovery time after a Hold condition
has ended.
Choose HOLD RECOVERY from the MODIFY OPTIONS menu. You are given a choice
of 1, 2, 3 or 4 cycles before normal measurement resumes, each cycle being
approximately 15 seconds in length. Highlight the desired recovery period, and then
press ENTER.

4.10 Offset
While Orbisphere analyzers are accurate to within 0.006 V/V of CO2, 0.01 cc/kg of H2, or
0.3 ppm of N 2, you may wish to apply a specific offset value to the displayed gas
measurement.
If, for example, 0.1 V/V should be subtracted from CO2 measurements, choose OFFSET
from the MODIFY OPTIONS menu to bring up the data entry screen.

For this example, you would want a negative offset so


highlight NEG. and press ENTER.

Enter the value to be subtracted and press ENTER.

The measurement display, recorder analog output, and RS-232 output of gas
concentration reflect this offset value. The RS-232 output also lists the offset value in a
separate column.

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Use the UP/DOWN ARROWS to move the decimal place to


the correct position in the displayed value, and press
ENTER to confirm and save.

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4.11 Corrections
Note :
This option is reserved for qualified Orbisphere Service Representatives only. As such,
if you feel that corrections are required, please contact your local Orbisphere Service
Representative to perform this operation for you.

a ) Temperature correction
If the sample temperature varies during the measurement cycle, the temperature change
is translated as an interference signal on the sensor measurements. This option reduces
the influence of temperature variation on the sensor.
When the process temperature is steady or changes very slowly, this correction is not
necessary, thus it should be disabled.
Choose CORRECTIONS in the MODIFY OPTIONS menu followed by TEMP
CORRECTION. Select ENABLED to apply a temperature correction to gas
measurements, or DISABLED if no correction is required.

b ) Humidity correction
This routine only concerns measurements made in 100% humid gases or in traces of
dissolved gas in water.
Choose CORRECTIONS from the MODIFY OPTIONS menu and HUMIDITY. This menu
provides a choice of DISABLED, ENABLED and CALIBRATE.
If you are making trace measurements in dry, or less than 100% saturated gases, then
the built-in humidity correction would be inappropriate, and should be DISABLED.
If you are measuring gases in the presence of humidity, however, the contribution from
humidity to the measured thermal conductivity is calculated from built-in formulae, and
subtracted from the net measured result.
Choose ENABLED to apply the correction, using previously stored humidity parameters,
for the amplitude and temperature coefficient of the correction. When you enable
humidity correction, this correction is applied to each sensor reading. The amount of
correction is listed in the RS-232 diagnostic output (see Serial output on page 21).
Choose CALIBRATE from the menu to begin calibration of the humidity effect and
perform a recalculation of the amplitude parameter. The temperature coefficient is set by
default, and cannot be changed.
The next screen then directs you to expose the sensor to a humid gas sample. You must
expose the sensor to a sample having a known humidity, and no measured or interfering
gas. Either the sensor can be exposed to a sample of humid purge gas or it can be
directly immersed in water and purge gas.
In the case of measurements in humid air, using a dry air purge, the water can be simply
aerated, and it suffices to immerse the sensor in water from a tap.
KB - 30/07/04 - 3610OptionsSetup.fm

It is permitted, however, to have the purge gas present in the sample since this gas does
not interfere. You can either use purge gas saturated with water, or water saturated with
the purge gas.
The act of saturating water with the purge gas (see Fig 13) eliminates all other potentially
interfering gases, given enough time. If the water volume is restricted to a few tens of
milliliters, about 15 minutes is adequate time to ensure complete purging of interfering
gases and temperature equilibration.

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Options set up - 3610 Analyzer

Fig 13 : Purge Gas Saturated with Water

Watch the signal (Slope value displayed on screen) change until it becomes stable.
When the signal is stable, press ENTER to store the new humidity correction.
As an alternative to exposing the sensor to humid gas, expose the sensor to a water
sample that is saturated with the purge gas. In this calibration, the purge gas passes
through water-saturated material (a porous piece of paper) that is in the flow chamber
(see Fig 14).

Fig 14 : Water Saturated with Purge Gas

To perform this calibration, wet a piece of paper until it is saturated with water, but not
dripping. Use a porous and durable type of paper, such as a piece of coffee filter paper
cut to fit into the flow chamber. Then, disconnect the flow chamber from the sensor, place
this paper into the flow chamber (as illustrated in Fig 14) and reconnect the sensor.

Run the gas through the saturated paper, for about 5 minutes, until the signal becomes
stable. When the signal is stable, stop the flow of gas to the Flow Chamber. Watch the
signal change again until it is stable at a new level. When no further change occurs,
press ENTER to store the new humidity correction.

4.12 Liquid/Gas coefficient


If the liquid sample flow rate is below the minimum required, then the measurement will
be lower than the actual value. If the actual measurement value is known by some other
measurement system, then a value can be entered here which will be used to compute
the correct actual value.

Operators Manual

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Next, start the purge gas into the flow chamber, running the gas at a flow rate of about
one bubble per second into a beaker of water.

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25 of 78

Enter the value of the liquid/gas coefficient.

The measured value will be multiplied by the coefficient value entered here to give the
correct measured value. By default, this value is set to 1.

4.13 Membrane selection


The H2 sensor can be fitted with different membranes, each having individual sensitivity
and flow requirements. To select the correct membrane, choose MEMBRANE from the
MODIFY OPTIONS menu then choose the membrane model number from the list
displayed.
Once you select any membrane (even if you reselect the same membrane and press
ENTER), you must re-calibrate the sensor, as described in Calibrations on page 27. In
addition, you must re-calibrate any corrections you may be using, as described in
Corrections on page 23.

Note :

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For detailed specifications regarding sensors and membranes, please refer to the
accompanying TC Sensors - Maintenance & Installation Manual.

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Options set up - 3610 Analyzer

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3610 Analyzer - Calibrations

27 of 78

Calibrations
5.1 Calibrate menu
Note :
Dependant on your instrument configuration, some of the options described in this
section may not be available on your system.
As delivered, 3610 systems are pre-calibrated. Check your sensor in measurement
mode (see Operating information on page 9) before attempting to calibrate.
The flow chart in Fig 15 illustrates the sensor calibration menus.

KB - 30/07/04 - 3610Calibrations.fm

Fig 15 : Instrument Calibration Menu Flow Diagram

Note :
When you select the Calibration menu, the instrument discontinues all measurement
operations.
All of the menus require user input of one form or another. This is carried out using the
four function keys on the Instrument Panel (see Instrument controls on page 9). You

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28 of 78

Calibrations - 3610 Analyzer

should ensure you are familiar with the use of these keys in entering and modifying
numeric fields (see Entering numerical values on page 10), before accessing these
menus.

Note :
When using non-Orbisphere instruments during calibration processes (e.g. pressure
gauges), their accuracy should be 10 times more precise than Orbisphere instruments.

5.2 Barometric pressure sensor calibration


You can verify or calibrate the instrument's internal barometric pressure sensor against
your local atmospheric pressure.
Select CALIBRATE from the main menu followed by BAROM PRESSURE.
The instrument first displays the current barometric
pressure reading. Press ESC if this agrees with your
current atmospheric pressure, or ENTER to modify and
bring up the next screen.
Enter the new value and press ENTER to return to the
previous BAROM. PRESSURE display, followed by ESC
to accept the value.

5.3 External pressure sensor calibration


The instrument can be fitted with a model 28117 external pressure sensor, capable of
measuring up to 3.5 bar (50 psi). An accurate pressure gauge is required to calibrate this
sensor.
Select CALIBRATE from the main menu followed by EXTERN. PRESSURE.
The instrument first displays its current external pressure
sensor measurement. If this agrees with the pressure
currently applied to the external pressure sensor, then
press ESC. If this measurement does not agree, and you
wish to re-calibrate, press ENTER to display the menu for
selection of pressure measurement units. Choose the
desired units to bring up the calibration Method menu.
There are two methods of calibrating this sensor:

Choosing ONE POINT allows you to enter the absolute


(gauge plus atmospheric) pressure currently applied to
the external pressure sensor. Press ENTER when the
value has been entered.
Use the UP/DOWN ARROWS to move the decimal place
to the correct position in the displayed value, and press
ENTER to confirm. The instrument then calibrates the
sensor and returns to the external pressure display.

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KB - 30/07/04 - 3610Calibrations.fm

ONE POINT permits you to calibrate at one pressure value


TWO POINT requires that you calibrate against high and low pressure values
(generally required only for high-pressure applications)

3610 Analyzer - Calibrations

29 of 78

The TWO POINT calibration requires that you apply and enter a LOW POINT and a
HIGH POINT pressure value. The menus are similar to the ONE POINT menu described
above.
Enter the atmospheric pressure as the low point value. Then, adjust the forcing gas
pressure to between 2.5 and 3 bar (absolute) for the high point. Enter the absolute
pressure (gauge plus atmospheric pressure) of the forcing gas for the high point.
After you enter the second value, the instrument calibrates the sensor and returns to the
external pressure display.

5.4 TC sensor calibration


When calibrating, the TC sensor is exposed to either:
1) A source of 100% pure CO2, H2, or N2 gas at a known elevated pressure (Partial
Pressure)
2) A known concentration of CO2, H2, or N2 gas at a known pressure (Fraction)
3) A known concentration of dissolved CO2, H2, or N2 (Dissolved)
The Partial Pressure method is generally recommended only when measuring at higher
line pressures, and requires a precise in-line pressure gauge to perform.
For calibration in a gaseous sample, the advantage of the Fraction method is that it is
independent of the precision of other devices, and is fairly easy and quick to perform.

WARNING
Handle H2 gas with great care ! It is extremely flammable and explosive.
TC sensor calibration may be performed either in-line, with the sensor left in its mounting
(such as a sensor socket or flow chamber), or off-line with the sensor removed, using a
separate flow chamber.

a ) In-Line calibration
Performing an in-line sensor calibration with a gaseous or liquid sample of known gas
concentration can be convenient, since you can leave the sensor in its mounting. You
simply introduce the reference gas or liquid to the sensor, and enter the expected values
via the menus.
For in-line calibration, first you must shut off the sample flow. Then, connect a source of
the gaseous or liquid reference sample to the sensor in its mounting (sensor socket or
flow chamber), and purge all existing gas or liquid out of the system. If you are calibrating
in-line, using a gaseous sample, in a model 32001 flow chamber, connect the calibration
gas source to the flow chamber's outer port (as illustrated in Fig 16).

KB - 30/07/04 - 3610Calibrations.fm

Fig 16 shows how to introduce both calibration gas and normal sample media to the flow
chamber, if required. A and B represent 3-way valves. Calibration gas is sent in through
the sample out port and waste gas is sent out through the sample in port, as shown (left).
In normal measurement operation (right), the calibration gas inlets and outlets are shut
off

Note :
When your system returns to measurement immediately after a successful in-line
calibration, the displayed value may appear slightly lower than expected until two or
three measurement cycles have elapsed. This is the sensor's normal response to
switching from Calibration to Measurement mode.

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Calibrations - 3610 Analyzer

Fig 16 : Flow Chamber - Calibrate & Measure Flows

b ) Off-line calibration
First shut off the sample flow. Then, extract the sensor from its socket or mounting and
close off the socket with the stainless steel plug provided. (If you are using a model
32003 ProAcc insertion/extraction valve, the sample is sealed off automatically as the
sensor is withdrawn.) If you are using a flow chamber, shut off the sample flow and then
extract the sensor from the flow chamber. Also, if you are using an external temperature
sensor, disconnect it from the sensor.
Make sure that the grill in the front of the sensor is clean and dry. Insert the sensor in the
model 32001 flow chamber, and tighten with its collar. Connect the gaseous or liquid
reference sample to the flow chamber's central sample entry port and purge all air and
water out of the system.
The exit from the flow chamber should be unobstructed, thus making the pressure in
contact with the sensor equilibrated with that of the atmosphere. If the exit from the flow
chamber is completely free, the gas pressure in contact with the sensor will be that of the
atmosphere.
Alternatively, adjust a needle valve on the exit from the calibration unit to raise the
applied pressure to any other desired calibration pressure. This has the advantage that
you can simulate more closely the actual gas pressure in the sample, so raising the
precision of later measurements - but it has the disadvantage that an accurate pressure
gauge must be available.

c ) Partial pressure calibration

The procedure requires a source of pure gas (regulated by a pressure valve) connected
to the central entry port of the flow chamber, an accurate pressure gauge at the exit of
the flow chamber, a needle valve to control the gas flow on exit, and a beaker of water to
monitor the gas flow (as illustrated in Fig 17).
To carry out the calibration, open the valve on the gas cylinder. Adjust the needle valve
until gas is flowing through the chamber at a rate of about 1 bubble per second indicated
by the beaker of water. Adjust both the valve on the gas cylinder and the needle valve

Operators Manual

KB - 30/07/04 - 3610Calibrations.fm

With this procedure, you must expose the sensor to a known pressure of pure CO2, H2
or N2 gas, in the range of 1 to 5 bar absolute.

3610 Analyzer - Calibrations

31 of 78

Fig 17 : Partial Pressure Calibration Diagram

until your desired calibration pressure is indicated on the accurate pressure gauge at the
exit to the flow chamber and the flow rate is approximately 1 bubble per second.
To expose the sensor to the gas and to stabilize the reading, operate in Measurement
Mode for about 30 minutes. After this time, press ESC and select CALIBRATE from the
main menu, followed by SENSOR TC and PARTIAL PRESSURE. Select your preferred
unit of measurement from the PART PRESS CAL menu, to bring up the menu for
specifying the gas pressure.
Enter the absolute gas pressure, taken from the pressure
gauge at the exit of the flow chamber. Press ENTER
when the value has been entered.
Use the UP/DOWN ARROWS to move the decimal place
to the correct position in the displayed value, and press
ENTER to confirm and start the calibration process.
The calibrating... please wait message appears for a
few seconds, and then the instrument starts three
calibration cycles.
The partial pressure and temperature measurements are
displayed. On this display, the current calibration cycle
number (cal:n) is also displayed in the bottom right-hand
corner.
KB - 30/07/04 - 3610Calibrations.fm

On completion of the three cycles, the instrument then


shows the sensitivity of the sensor as a percentage of the
sensitivity determined when calibration was last
performed.

Note :
If this is the first calibration then the message indicates a percentage of the expected
value, rather than the last calibration.
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Calibrations - 3610 Analyzer

This percentage must be between 30% and 170% in order to calibrate. If the percentage
is outside the limits, you will see the CALIBRATION OUT OF BOUNDS message. You
will need to press ESC to continue. Check that the membrane does not need to be
replaced and that no leaks are evident.
If the percentage is within the limits press ENTER to accept and complete the calibration
process (the message CALIBRATION COMPLETE will appears briefly) or ESC to abort.

d ) Fraction calibration
This method uses a known purity of CO2, H2 or N2 gas at a known pressure, and requires
either the instrument internal barometric pressure sensor or an external pressure sensor
as a reference. The pressure sensor is pre-calibrated at the factory. However, to check
or re-calibrate either pressure sensor, see Barometric pressure sensor calibration on
page 28 or External pressure sensor calibration on page 28.
To expose the sensor to the gas and to stabilize the reading, operate in Measurement
Mode for about 30 minutes. After this time, press ESC and select CALIBRATE from the
main menu, followed by SENSOR TC and FRACTION. Select your preferred unit of
measurement from the FRACTION CAL menu (either %vbar if using the barometric
pressure sensor, or %vext if using the external pressure sensor), to bring up the menu
for specifying the gas pressure.

Note :
If you choose %vbar, the exit port of the flow chamber or sensor mounting must be
open to the atmosphere.
Enter the concentration of the calibration gas in volume percent and proceed as
described above for Partial Pressure Calibration.

Note :
If the sensor voltage slope shifts more than 1%, calibration restarts and the message
Recal Err XXX% will appear. Three continuous calibrations with a shift of less than 1%
must be performed, before the calibration can be completed.

e ) Dissolved calibration
This method requires a known concentration of CO2, H, or N2 dissolved in liquid as a
reference sample.
Select CALIBRATE from the main menu, followed by SENSOR TC and DISSOLVED.
Select your preferred unit of measurement from the DISSOLVED CAL menu.

KB - 30/07/04 - 3610Calibrations.fm

Enter the dissolved CO2 concentration of the sample and proceed as described above
for Partial Pressure Calibration.

Operators Manual

3610 Analyzer - Calibrations

33 of 78

5.5 Calibration tables

a ) CO2 concentration table in V/V


Table 4 : CO2 Concentrations in V/V in Distilled Water

KB - 30/07/04 - 3610Calibrations.fm

CO2 Partial Pressure (bar)

Operators Manual

1.5

2.5

3.5

4.5

1.695

2.544

3.394

4.246

5.099

5.952

6.807

7.663

8.521

1.631

2.448

3.266

4.085

4.905

5.726

6.548

7.372

8.196

1.570

2.356

3.143

3.932

4.721

5.511

6.303

7.095

7.888

1.512

2.269

3.027

3.786

4.546

5.307

6.069

6.832

7.596

1.457

2.187

2.917

3.649

4.381

5.114

5.848

6.583

7.319

1.405

2.108

2.812

3.518

4.223

4.930

5.638

6.346

7.055

1.355

2.034

2.713

3.393

4.074

4.755

5.438

6.121

6.805

1.308

1.963

2.618

3.275

3.932

4.589

5.248

5.907

6.566

1.263

1.895

2.528

3.162

3.796

4.431

5.067

5.703

6.340

1.220

1.831

2.442

3.055

3.667

4.281

4.895

5.509

6.124

10

1.179

1.770

2.361

2.952

3.545

4.137

4.731

5.325

5.919

11

1.140

1.711

2.283

2.855

3.428

4.001

4.574

5.149

5.723

12

1.103

1.656

2.209

2.762

3.316

3.871

4.426

4.981

5.537

13

1.068

1.603

2.138

2.674

3.210

3.747

4.284

4.821

5.359

14

1.034

1.552

2.071

2.589

3.109

3.628

4.148

4.669

5.189

15

1.002

1.504

2.006

2.509

3.012

3.515

4.019

4.523

5.028

16

0.972

1.458

1.945

2.432

2.919

3.407

3.895

4.384

4.873

17

0.942

1.414

1.886

2.358

2.831

3.304

3.777

4.251

4.725

18

0.914

1.372

1.830

2.288

2.746

3.205

3.665

4.124

4.584

19

0.887

1.331

1.776

2.221

2.666

3.111

3.557

4.003

4.449

20

0.862

1.293

1.725

2.156

2.589

3.021

3.454

3.887

4.320

21

0.837

1.256

1.675

2.095

2.515

2.935

3.355

3.776

4.197

22

0.814

1.221

1.628

2.036

2.444

2.852

3.261

3.670

4.079

23

0.791

1.187

1.583

1.980

2.376

2.773

3.170

3.568

3.965

24

0.769

1.155

1.540

1.926

2.311

2.697

3.084

3.470

3.857

25

0.749

1.124

1.499

1.874

2.249

2.625

3.001

3.377

3.753

26

0.729

1.094

1.459

1.824

2.190

2.555

2.921

3.287

3.654

27

0.710

1.065

1.421

1.776

2.132

2.488

2.845

3.201

3.558

28

0.692

1.038

1.384

1.731

2.077

2.424

2.772

3.119

3.466

29

0.674

1.012

1.349

1.687

2.025

2.363

2.701

3.040

3.378

30

0.657

0.986

1.315

1.645

1.974

2.304

2.634

2.964

3.294

31

0.641

0.962

1.283

1.604

1.926

2.247

2.569

2.891

3.213

32

0.626

0.939

1.252

1.566

1.879

2.193

2.507

2.821

3.135

33

0.611

0.916

1.222

1.528

1.834

2.141

2.447

2.753

3.060

34

0.596

0.895

1.194

1.492

1.791

2.090

2.389

2.689

2.988

35

0.583

0.874

1.166

1.458

1.750

2.042

2.334

2.627

2.919

36

0.569

0.854

1.139

1.425

1.710

1.995

2.281

2.567

2.853

37

0.557

0.835

1.114

1.393

1.672

1.951

2.230

2.509

2.788

38

0.544

0.817

1.089

1.362

1.635

1.908

2.181

2.454

2.727

39

0.533

0.799

1.066

1.332

1.599

1.866

2.133

2.400

2.668

40

0.521

0.782

1.043

1.304

1.565

1.826

2.087

2.349

2.610

41

0.510

0.766

1.021

1.276

1.532

1.788

2.043

2.299

2.555

42

0.500

0.750

1.000

1.250

1.500

1.751

2.001

2.252

2.502

43

0.489

0.734

0.979

1.224

1.470

1.715

1.960

2.206

2.451

44

0.480

0.720

0.960

1.200

1.440

1.680

1.921

2.161

2.402

45

0.470

0.705

0.941

1.176

1.412

1.647

1.883

2.119

2.355

46

0.461

0.692

0.922

1.153

1.384

1.615

1.846

2.077

2.309

47

0.452

0.678

0.905

1.131

1.358

1.584

1.811

2.038

2.265

48

0.444

0.666

0.888

1.110

1.332

1.554

1.777

1.999

2.222

49

0.436

0.653

0.871

1.089

1.308

1.526

1.744

1.962

2.181

34 of 78

Calibrations - 3610 Analyzer

b ) CO2 concentration table in g/kg


Table 5 : CO2 Concentrations in g/kg in Distilled Water
1

1.5

2.5

3.5

4.5

3.328

4.996

6.665

8.337

10.012

11.688

13.367

15.049

16.732

3.202

4.806

6.412

8.020

9.631

11.243

12.858

14.475

16.093

3.082

4.626

6.172

7.720

9.269

10.821

12.375

13.931

15.488

2.968

4.455

5.944

7.434

8.927

10.421

11.917

13.414

14.914

2.860

4.293

5.727

7.164

8.601

10.041

11.482

12.925

14.369

2.758

4.139

5.522

6.906

8.292

9.680

11.069

12.460

13.852

2.660

3.993

5.327

6.662

7.999

9.337

10.677

12.018

13.361

2.568

3.854

5.141

6.430

7.720

9.011

10.304

11.598

12.893

2.480

3.722

4.965

6.209

7.454

8.701

9.949

11.199

12.449

2.396

3.596

4.797

5.999

7.202

8.406

9.612

10.819

12.027

10

2.316

3.476

4.637

5.798

6.961

8.125

9.291

10.457

11.624

11

2.240

3.362

4.484

5.608

6.732

7.858

8.985

10.113

11.241

12

2.168

3.253

4.339

5.426

6.514

7.603

8.693

9.784

10.876

13

2.098

3.149

4.200

5.253

6.306

7.360

8.415

9.471

10.528

14

2.032

3.050

4.068

5.088

6.108

7.129

8.150

9.173

10.196

15

1.970

2.956

3.942

4.930

5.918

6.907

7.897

8.888

9.880

16

1.910

2.865

3.822

4.779

5.737

6.696

7.656

8.616

9.577

17

1.852

2.779

3.707

4.636

5.565

6.495

7.425

8.357

9.289

18

1.797

2.697

3.597

4.498

5.400

6.302

7.205

8.109

9.013

19

1.745

2.618

3.492

4.367

5.242

6.118

6.995

7.872

8.749

20

1.695

2.543

3.392

4.241

5.091

5.942

6.793

7.645

8.497

21

1.647

2.471

3.296

4.121

4.947

5.774

6.601

7.428

8.256

22

1.601

2.402

3.204

4.006

4.809

5.612

6.416

7.221

8.026

23

1.557

2.336

3.116

3.896

4.677

5.458

6.240

7.022

7.805

24

1.515

2.273

3.032

3.791

4.550

5.310

6.071

6.832

7.593

25

1.475

2.212

2.951

3.690

4.429

5.169

5.909

6.649

7.391

26

1.436

2.154

2.873

3.593

4.313

5.033

5.754

6.475

7.196

27

1.399

2.099

2.799

3.500

4.201

4.903

5.605

6.307

7.010

28

1.363

2.045

2.728

3.411

4.094

4.778

5.462

6.147

6.831

29

1.329

1.994

2.660

3.325

3.992

4.658

5.325

5.992

6.660

30

1.296

1.945

2.594

3.243

3.893

4.543

5.194

5.844

6.496

31

1.265

1.898

2.531

3.165

3.799

4.433

5.067

5.702

6.338

32

1.235

1.853

2.471

3.089

3.708

4.327

4.946

5.566

6.186

33

1.206

1.809

2.413

3.016

3.621

4.225

4.830

5.435

6.040

34

1.178

1.767

2.357

2.947

3.537

4.127

4.718

5.309

5.900

35

1.151

1.727

2.303

2.879

3.456

4.033

4.610

5.188

5.766

36

1.125

1.688

2.251

2.815

3.379

3.943

4.507

5.071

5.636

37

1.100

1.651

2.202

2.753

3.304

3.856

4.407

4.959

5.512

38

1.076

1.615

2.154

2.693

3.232

3.772

4.312

4.852

5.392

39

1.053

1.581

2.108

2.635

3.163

3.691

4.219

4.748

5.276

40

1.031

1.547

2.064

2.580

3.097

3.613

4.131

4.648

5.165

41

1.010

1.515

2.021

2.527

3.033

3.539

4.045

4.552

5.058

42

0.989

1.485

1.980

2.475

2.971

3.467

3.963

4.459

4.955

43

0.970

1.455

1.940

2.426

2.911

3.397

3.883

4.370

4.856

44

0.951

1.426

1.902

2.378

2.854

3.330

3.807

4.284

4.761

45

0.932

1.399

1.865

2.332

2.799

3.266

3.733

4.201

4.668

46

0.915

1.372

1.830

2.288

2.746

3.204

3.662

4.121

4.579

47

0.897

1.346

1.796

2.245

2.694

3.144

3.594

4.044

4.494

48

0.881

1.322

1.763

2.204

2.645

3.086

3.528

3.969

4.411

49

0.865

1.298

1.731

2.164

2.597

3.030

3.464

3.897

4.331

Operators Manual

KB - 30/07/04 - 3610Calibrations.fm

CO2 Partial Pressure (bar)


C

3610 Analyzer - Calibrations

35 of 78

c ) H2 concentration table in cc/kg


Table 6 : H2 Concentrations in cc/kg in Distilled Water

KB - 30/07/04 - 3610Calibrations.fm

H2 Partial Pressure (bar)

Operators Manual

1.5

2.5

3.5

4.5

21.59

32.39

43.18

53.98

64.78

75.57

86.37

97.17

107.97

21.33

31.99

42.66

53.32

63.99

74.65

85.32

95.98

106.65

21.07

31.61

42.15

52.69

63.23

73.76

84.30

94.84

105.38

20.83

31.25

41.66

52.08

62.50

72.91

83.33

93.75

104.16

20.60

30.90

41.19

51.49

61.79

72.09

82.39

92.69

102.99

20.37

30.56

40.74

50.93

61.12

71.30

81.49

91.68

101.86

20.15

30.23

40.31

50.39

60.47

70.55

80.62

90.70

100.78

19.95

29.92

39.89

49.87

59.84

69.82

79.79

89.77

99.74

19.75

29.62

39.49

49.37

59.24

69.12

78.99

88.87

98.74

19.55

29.33

39.11

48.89

58.67

68.44

78.22

88.00

97.78

10

19.37

29.05

38.74

48.43

58.11

67.80

77.48

87.17

96.86

11

19.19

28.79

38.39

47.98

57.58

67.18

76.77

86.37

95.97

12

19.02

28.53

38.04

47.56

57.07

66.58

76.09

85.60

95.12

13

18.86

28.29

37.72

47.15

56.58

66.01

75.44

84.87

94.30

14

18.70

28.05

37.40

46.75

56.11

65.46

74.81

84.16

93.51

15

18.55

27.83

37.10

46.38

55.65

64.93

74.21

83.48

92.76

16

18.41

27.61

36.81

46.02

55.22

64.42

73.63

82.83

92.04

17

18.27

27.40

36.54

45.67

54.80

63.94

73.07

82.21

91.34

18

18.13

27.20

36.27

45.34

54.40

63.47

72.54

81.61

90.68

19

18.01

27.01

36.01

45.02

54.02

63.03

72.03

81.04

90.04

20

17.89

26.83

35.77

44.71

53.66

62.60

71.54

80.49

89.43

21

17.77

26.65

35.54

44.42

53.31

62.19

71.08

79.96

88.85

22

17.66

26.49

35.31

44.14

52.97

61.80

70.63

79.46

88.29

23

17.55

26.33

35.10

43.88

52.65

61.43

70.20

78.98

87.76

24

17.45

26.17

34.90

43.62

52.35

61.07

69.80

78.52

87.25

25

17.35

26.03

34.70

43.38

52.06

60.73

69.41

78.09

86.76

26

17.26

25.89

34.52

43.15

51.78

60.41

69.04

77.67

86.30

27

17.17

25.76

34.34

42.93

51.51

60.10

68.69

77.27

85.86

28

17.09

25.63

34.17

42.72

51.26

59.81

68.35

76.89

85.44

29

17.01

25.51

34.01

42.52

51.02

59.53

68.03

76.54

85.04

30

16.93

25.40

33.86

42.33

50.80

59.26

67.73

76.20

84.66

31

16.86

25.29

33.72

42.15

50.58

59.01

67.44

75.87

84.30

32

16.79

25.19

33.58

41.98

50.38

58.77

67.17

75.57

83.97

33

16.73

25.09

33.46

41.82

50.19

58.55

66.92

75.28

83.65

34

16.67

25.00

33.34

41.67

50.01

58.34

66.67

75.01

83.34

35

16.61

24.92

33.22

41.53

49.84

58.14

66.45

74.75

83.06

36

16.56

24.84

33.12

41.40

49.68

57.96

66.23

74.51

82.79

37

16.51

24.76

33.02

41.27

49.53

57.78

66.04

74.29

82.55

38

16.46

24.69

32.92

41.16

49.39

57.62

65.85

74.08

82.31

39

16.42

24.63

32.84

41.05

49.26

57.47

65.68

73.89

82.10

40

16.38

24.57

32.76

40.95

49.14

57.33

65.52

73.71

81.90

41

16.34

24.51

32.69

40.86

49.03

57.20

65.37

73.54

81.72

42

16.31

24.46

32.62

40.77

48.93

57.08

65.24

73.39

81.55

43

16.28

24.42

32.56

40.70

48.84

56.98

65.12

73.26

81.40

44

16.25

24.38

32.50

40.63

48.75

56.88

65.00

73.13

81.26

45

16.23

24.34

32.45

40.57

48.68

56.79

64.91

73.02

81.13

46

16.20

24.31

32.41

40.51

48.61

56.72

64.82

72.92

81.02

47

16.19

24.28

32.37

40.46

48.56

56.65

64.74

72.84

80.93

48

16.17

24.25

32.34

40.42

48.51

56.59

64.68

72.76

80.85

49

16.16

24.23

32.31

40.39

48.47

56.55

64.62

72.70

80.78

36 of 78

Calibrations - 3610 Analyzer

d ) H2 concentration table in ppm


Table 7 : H2 Concentrations in ppm in Distilled Water
1

1.5

2.5

3.5

4.5

1.942

2.913

3.884

4.855

5.826

6.797

7.768

8.739

9.710

1.918

2.877

3.836

4.795

5.755

6.714

7.673

8.632

9.591

1.895

2.843

3.791

4.738

5.686

6.634

7.582

8.530

9.477

1.873

2.810

3.747

4.684

5.620

6.557

7.494

8.431

9.368

1.852

2.779

3.705

4.631

5.557

6.484

7.410

8.336

9.262

1.832

2.748

3.664

4.580

5.496

6.413

7.329

8.245

9.161

1.813

2.719

3.625

4.532

5.438

6.344

7.251

8.157

9.064

1.794

2.691

3.588

4.485

5.382

6.279

7.176

8.073

8.970

1.776

2.664

3.552

4.440

5.328

6.216

7.104

7.992

8.880

1.759

2.638

3.517

4.397

5.276

6.155

7.035

7.914

8.794

10

1.742

2.613

3.484

4.355

5.226

6.097

6.968

7.839

8.711

11

1.726

2.589

3.452

4.315

5.178

6.041

6.905

7.768

8.631

12

1.711

2.566

3.422

4.277

5.132

5.988

6.843

7.699

8.554

13

1.696

2.544

3.392

4.240

5.088

5.936

6.784

7.632

8.481

14

1.682

2.523

3.364

4.205

5.046

5.887

6.728

7.569

8.410

15

1.668

2.503

3.337

4.171

5.005

5.839

6.674

7.508

8.342

16

1.655

2.483

3.311

4.138

4.966

5.794

6.622

7.449

8.277

17

1.643

2.464

3.286

4.107

4.929

5.750

6.572

7.393

8.215

18

1.631

2.446

3.262

4.077

4.893

5.708

6.524

7.339

8.155

19

1.619

2.429

3.239

4.049

4.859

5.668

6.478

7.288

8.098

20

1.608

2.413

3.217

4.021

4.826

5.630

6.434

7.239

8.043

21

1.598

2.397

3.196

3.995

4.794

5.593

6.392

7.191

7.990

22

1.588

2.382

3.176

3.970

4.764

5.558

6.352

7.146

7.940

23

1.578

2.368

3.157

3.946

4.735

5.525

6.314

7.103

7.892

24

1.569

2.354

3.139

3.923

4.708

5.493

6.277

7.062

7.847

25

1.560

2.341

3.121

3.901

4.682

5.462

6.242

7.023

7.803

26

1.552

2.328

3.104

3.881

4.657

5.433

6.209

6.985

7.761

27

1.544

2.316

3.089

3.861

4.633

5.405

6.177

6.949

7.722

28

1.537

2.305

3.073

3.842

4.610

5.379

6.147

6.915

7.684

29

1.530

2.294

3.059

3.824

4.589

5.354

6.118

6.883

7.648

30

1.523

2.284

3.046

3.807

4.568

5.330

6.091

6.853

7.614

31

1.516

2.274

3.033

3.791

4.549

5.307

6.065

6.824

7.582

32

1.510

2.265

3.020

3.776

4.531

5.286

6.041

6.796

7.551

33

1.504

2.257

3.009

3.761

4.513

5.266

6.018

6.770

7.523

34

1.499

2.249

2.998

3.748

4.497

5.247

5.996

6.746

7.496

35

1.494

2.241

2.988

3.735

4.482

5.229

5.976

6.723

7.470

36

1.489

2.234

2.978

3.723

4.468

5.212

5.957

6.701

7.446

37

1.485

2.227

2.969

3.712

4.454

5.197

5.939

6.681

7.424

38

1.481

2.221

2.961

3.701

4.442

5.182

5.922

6.663

7.403

39

1.477

2.215

2.953

3.692

4.430

5.168

5.907

6.645

7.384

40

1.473

2.210

2.946

3.683

4.419

5.156

5.892

6.629

7.366

41

1.470

2.205

2.940

3.674

4.409

5.144

5.879

6.614

7.349

42

1.467

2.200

2.933

3.667

4.400

5.134

5.867

6.601

7.334

43

1.464

2.196

2.928

3.660

4.392

5.124

5.856

6.588

7.320

44

1.461

2.192

2.923

3.654

4.385

5.115

5.846

6.577

7.308

45

1.459

2.189

2.919

3.648

4.378

5.108

5.837

6.567

7.297

46

1.457

2.186

2.915

3.643

4.372

5.101

5.829

6.558

7.287

47

1.456

2.183

2.911

3.639

4.367

5.095

5.823

6.550

7.278

48

1.454

2.181

2.908

3.635

4.363

5.090

5.817

6.544

7.271

49

1.453

2.179

2.906

3.632

4.359

5.085

5.812

6.538

7.265

Operators Manual

KB - 30/07/04 - 3610Calibrations.fm

H2 Partial Pressure (bar)


C

3610 Analyzer - Calibrations

37 of 78

e ) N2 concentration table in ppm


Table 8 : N2 Concentrations in ppm in Distilled Water
N2 Partial Pressure (bar)

KB - 30/07/04 - 3610Calibrations.fm

Operators Manual

1.5

3.5

29.382

44.073

58.764

73.456

2.5

88.148

102.840

117.533

132.226 146.919

4.5

28.645

42.968

57.291

71.614

85.937

100.261

114.585

128.910 143.234

27.941

41.912

55.884

69.855

83.827

97.799

111.771

125.744 139.717

27.269

40.905

54.540

68.175

81.811

95.447

109.084

122.720 136.357

26.628

39.942

53.256

66.571

79.885

93.200

106.516

119.831 133.147

26.014

39.021

52.029

65.037

78.045

91.053

104.061

117.070 130.079

25.428

38.142

50.856

63.570

76.285

89.000

101.715

114.431 127.146

24.867

37.300

49.734

62.168

74.602

87.037

99.471

111.906 124.341

24.330

36.495

48.661

60.827

72.993

85.159

97.325

109.492 121.658

23.817

35.725

47.634

59.543

71.452

83.362

95.271

107.181 119.091

10

23.325

34.988

46.651

58.315

69.978

81.642

93.306

104.970 116.634

11

22.855

34.283

45.711

57.139

68.567

79.995

91.424

102.853 114.282

12

22.405

33.607

44.810

56.013

67.216

78.419

89.622

100.826 112.029

13

21.973

32.960

43.947

54.934

65.921

76.909

87.896

98.884

109.872

14

21.560

32.340

43.120

53.901

64.682

75.462

86.243

97.024

107.806

15

21.164

31.746

42.329

52.911

63.494

74.077

84.659

95.243

105.826

16

20.785

31.177

41.570

51.963

62.355

72.749

83.142

93.535

103.929

17

20.421

30.632

40.842

51.053

61.265

71.476

81.687

91.899

102.110

18

20.072

30.109

40.145

50.182

60.219

70.256

80.293

90.330

100.367

19

19.738

29.608

39.477

49.347

59.216

69.086

78.956

88.826

98.697

20

19.418

29.127

38.836

48.546

58.255

67.965

77.675

87.385

97.095

21

19.111

28.666

38.222

47.778

57.334

66.890

76.446

86.002

95.559

22

18.816

28.225

37.633

47.042

56.450

65.859

75.268

84.677

94.086

23

18.534

27.801

37.068

46.336

55.603

64.871

74.138

83.406

92.674

24

18.263

27.395

36.527

45.659

54.791

63.923

73.055

82.188

91.320

25

18.003

27.005

36.007

45.009

54.012

63.014

72.016

81.019

90.022

26

17.755

26.632

35.509

44.387

53.265

62.143

71.020

79.898

88.777

27

17.516

26.274

35.032

43.790

52.549

61.307

70.066

78.824

87.583

28

17.287

25.931

34.574

43.218

51.862

60.506

69.150

77.794

86.439

29

17.068

25.601

34.135

42.670

51.204

59.738

68.272

76.807

85.341

30

16.857

25.286

33.715

42.144

50.573

59.002

67.431

75.861

84.290

31

16.656

24.984

33.312

41.640

49.968

58.297

66.625

74.954

83.282

32

16.463

24.694

32.926

41.157

49.389

57.621

65.853

74.085

82.317

33

16.278

24.417

32.556

40.695

48.834

56.974

65.113

73.252

81.392

34

16.101

24.151

32.202

40.252

48.303

56.354

64.404

72.455

80.506

35

15.931

23.897

31.862

39.828

47.794

55.760

63.726

71.692

79.659

36

15.769

23.653

31.538

39.423

47.307

55.192

63.077

70.962

78.847

37

15.614

23.421

31.227

39.035

46.842

54.649

62.456

70.264

78.071

38

15.465

23.198

30.931

38.664

46.396

54.129

61.863

69.596

77.329

39

15.323

22.985

30.647

38.309

45.971

53.633

61.295

68.957

76.620

40

15.188

22.782

30.376

37.970

45.565

53.159

60.753

68.348

75.942

41

15.059

22.588

30.117

37.647

45.177

52.706

60.236

67.766

75.296

42

14.935

22.403

29.871

37.339

44.806

52.274

59.743

67.211

74.679

43

14.818

22.227

29.636

37.045

44.454

51.863

59.272

66.682

74.091

44

14.706

22.059

29.412

36.765

44.118

51.471

58.824

66.178

73.531

45

14.599

21.899

29.198

36.498

43.798

51.098

58.398

65.698

72.998

46

14.498

21.747

28.996

36.245

43.494

50.744

57.993

65.242

72.492

47

14.402

21.603

28.804

36.005

43.206

50.407

57.608

64.810

72.011

48

14.311

21.466

28.621

35.777

42.932

50.088

57.244

64.400

71.555

49

14.224

21.336

28.449

35.561

42.674

49.786

56.899

64.011

71.124

38 of 78

Calibrations - 3610 Analyzer

f ) N2 concentration table in ml/l


Table 9 : N2 Concentrations in ml/l in Distilled Water
1

1.5

4.5

23.507

35.260

47.014

58.768

2.5

70.523

82.277

3.5

94.032

105.787

117.542

22.918

34.378

45.838

57.298

68.758

80.218

91.679

103.140

114.601

22.357

33.535

44.714

55.893

67.072

78.251

89.431

100.611

111.791

21.819

32.730

43.640

54.550

65.461

76.372

87.283

98.194

109.105

21.306

31.959

42.613

53.266

63.920

74.574

85.229

95.883

106.538

20.815

31.223

41.631

52.039

62.447

72.856

83.264

93.673

104.082

20.345

30.518

40.691

50.864

61.038

71.211

81.385

91.559

101.733

19.896

29.844

39.792

49.740

59.689

69.638

79.587

89.536

99.485

19.465

29.198

38.931

48.665

58.398

68.132

77.865

87.599

97.333

19.053

28.580

38.107

47.635

57.162

66.690

76.217

85.745

95.273

10

18.659

27.988

37.318

46.648

55.978

65.308

74.639

83.969

93.300

11

18.281

27.422

36.562

45.703

54.844

63.985

73.127

82.268

91.410

12

17.919

26.878

35.838

44.798

53.758

62.718

71.678

80.638

89.599

13

17.572

26.358

35.144

43.930

52.716

61.503

70.289

79.076

87.863

14

17.239

25.858

34.478

43.098

51.718

60.338

68.958

77.579

86.199

15

16.920

25.380

33.840

42.300

50.761

59.221

67.682

76.143

84.604

16

16.614

24.921

33.228

41.536

49.843

58.151

66.458

74.766

83.074

17

16.321

24.481

32.641

40.802

48.963

57.124

65.285

73.446

81.607

18

16.039

24.059

32.079

40.098

48.118

56.139

64.159

72.179

80.200

19

15.769

23.654

31.539

39.423

47.308

55.194

63.079

70.964

78.849

20

15.510

23.265

31.020

38.776

46.531

54.287

62.042

69.798

77.554

21

15.261

22.892

30.523

38.154

45.785

53.417

61.048

68.679

76.311

22

15.023

22.535

30.046

37.558

45.070

52.582

60.094

67.606

75.118

23

14.794

22.191

29.588

36.986

44.383

51.780

59.178

66.576

73.973

24

14.574

21.862

29.149

36.436

43.724

51.011

58.299

65.587

72.875

25

14.363

21.545

28.727

35.909

43.091

50.273

57.456

64.638

71.820

26

14.161

21.242

28.322

35.403

42.484

49.565

56.646

63.727

70.808

27

13.967

20.950

27.934

34.918

41.901

48.885

55.869

62.853

69.837

28

13.780

20.671

27.561

34.452

41.342

48.233

55.124

62.014

68.905

29

13.602

20.402

27.203

34.005

40.806

47.607

54.408

61.209

68.011

30

13.430

20.145

26.860

33.575

40.291

47.006

53.722

60.437

67.153

31

13.265

19.898

26.531

33.164

39.797

46.430

53.063

59.696

66.329

32

13.107

19.661

26.215

32.769

39.323

45.877

52.431

58.985

65.540

33

12.956

19.434

25.912

32.390

38.869

45.347

51.825

58.304

64.782

34

12.811

19.216

25.622

32.027

38.433

44.838

51.244

57.650

64.056

35

12.671

19.007

25.343

31.679

38.015

44.351

50.687

57.023

63.360

36

12.538

18.807

25.076

31.345

37.615

43.884

50.153

56.423

62.692

37

12.410

18.615

24.820

31.026

37.231

43.436

49.642

55.847

62.053

38

12.288

18.432

24.576

30.720

36.864

43.008

49.152

55.296

61.441

39

12.170

18.256

24.341

30.427

36.512

42.598

48.683

54.769

60.855

40

12.058

18.087

24.117

30.146

36.175

42.205

48.234

54.264

60.294

41

11.951

17.927

23.902

29.878

35.854

41.829

47.805

53.781

59.757

42

11.848

17.773

23.697

29.621

35.546

41.470

47.395

53.320

59.244

43

11.750

17.626

23.501

29.376

35.252

41.127

47.003

52.879

58.754

44

11.657

17.485

23.314

29.143

34.971

40.800

46.629

52.458

58.287

45

11.568

17.352

23.136

28.920

34.704

40.488

46.272

52.056

57.841

46

11.483

17.224

22.965

28.707

34.448

40.190

45.932

51.673

57.415

47

11.402

17.103

22.803

28.504

34.206

39.907

45.608

51.309

57.010

48

11.325

16.987

22.649

28.312

33.974

39.637

45.300

50.962

56.625

49

11.251

16.877

22.503

28.129

33.755

39.381

45.007

50.633

56.259

Operators Manual

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N2 Partial Pressure (bar)


C

3610 Analyzer - Accessories and attachments

39 of 78

Accessories and attachments


Certain applications may require the use of one or more of the items described below.

6.1 Model 32605 purge backup unit


Since it is necessary to continuously purge the sensor to prevent the ingress of moisture,
normally you would want to leave the instrument switched on at all times even when gas
analysis is not required. If it is more practical to be able to switch off an analyzer for
several days at a time (without removing the sensor), a purge backup unit is
recommended.
Install the model 32605 Purge Backup Unit directly between the instrument and sensor
using the sensor cable. It is powered by internal batteries which batteries recharge
automatically (using the sensor cable) when the instrument is switched on. When the
instrument is switched off, the purge backup unit continues to leave the sensor's solenoid
in the open position (enabling purge gas entry) for up to four days. A green LED
illuminates when the battery is adequately charged; a red LED illuminates when
recharging is necessary.

6.2 Model 32557/32559 external temperature sensor


This temperature sensor is ideal for applications where the sampling line or room
temperatures undergo frequent change. It provides an independent temperature signal
to the instrument that is not affected by room temperature. The temperature sensor
connects to an adapter that is factory-mounted to the rear of the model 31260, 31460, or
31560 sensor (and available as a retrofit for model 31250, 31450, or 31550 sensors).
The temperature sensor connects to this adapter using a 4-pin LEMO connector.
The model 32557 temperature sensor is mounted in-line in a pipe, using a model 29501
sensor socket. The on-line temperature sensor, model 32559, is designed for mounting
in 6-mm or -inch stainless steel tubing.

6.3 Data acquisition software


The 3610 instrument can be used as an acquisition device through the Windowscompatible MOCA3610 PC program, available as model number 32681.E from
Orbisphere.
The program uses the instrument's RS-232 connection (ENABLED in the Options
Menu, as described in Serial output on page 21) to set up a table of measurement
information including gas, temperature, and time.
The program interfaces to any available RS-232 serial port on your computer. It may be
necessary to run an independent utility on your PC in order to designate such a COM
port.

a ) Program setup
KB - 30/07/04 - 3610Accessories.fm

This installation procedure will copy the contents of the MOCA3610 source floppy disk
(designated here as drive A) onto your hard drive (designated here as drive C). About 80
kilobytes of hard disk space will be required.
To setup the program using Windows, first place the floppy disk in its drive. Now, open
Windows Explorer and copy the program, as follows:
1) In the Explorer's Folders list, click on the plus sign of the My Computer icon
2) Click on the (C:) drive icon.

Operators Manual

Accessories and attachments - 3610 Analyzer

3) In the Explorer File menu, point to New, and then click on Folder.
4) Type MOCA3610 for the folder name, and press ENTER.
You can change the folder name at any time by clicking the folder icon with the
right mouse button, selecting the Rename command, and then retyping the name.
5) In the Folders list, click on the Floppy (A:) drive icon.
6) Using the left mouse button, click on the MOCA3610.exe icon, drag it to the
MOCA3610 folder just created above, and then release the button. The
MOCA3610 program is now copied onto your hard drive.
Next, set up the program for conventional Windows access (i.e. where you can click on
a desktop icon to start the program), as follows:
1) In the Explorer's Folders list, locate and click on the new MOCA3610 folder icon.
2) Using the right mouse button, click on the MOCA3610.exe icon.
3) Click the Send To command on the menu displayed and select Desktop from
the list. An icon will then be created on your Desktop.
4) To change the name of the icon (e.g. to remove the name "Shortcut to..."), use
the right mouse button to click on the Shortcut icon, then click on the Rename
command. Type in MOCA3610 Program over the program name, and press
ENTER.
To start the MOCA3610 program, simply double click on the desktop icon.
When it starts, the MOCA3610 program creates a MOCA3610.INI file, in the
C:\Windows directory, to save any user changes to default program settings.

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40 of 78

Operators Manual

3610 Analyzer - Maintenance and troubleshooting

41 of 78

Maintenance and troubleshooting


7.1 General maintenance
While unauthorized opening of the instrument normally voids the Orbisphere warranty, it
is necessary to open the process instrument for output wiring connections.
Fuse replacement, AC voltage changes, and conversion from current to voltage output
also can be performed by the user.

WARNING
Disconnect power before opening the instrument.
To open a panel/rack mount or portable instrument, remove the front panel key
and place the instrument face down. Remove the four 3-mm Allen head screws on
the rear, and carefully pull off the rear panel, taking care not to disconnect any
wires.
To open a wall mount instrument, unlock the front panel of the unit with the key
provided to expose the electronics inside.

a ) Internal fuse replacement


For panel/rack mount and portable instruments, the power supply is attached to the
inside of the rear panel. For wall mount instruments, the power supply is located on the
rear panel of the instrument housing.
At position F1 on the power supply is a black plastic fuse holder. Remove the fuse cover
using a thin coin or a small flat-bladed screwdriver to push down and turn.
The 230 VAC power supply uses a T 100 mA fuse.
The 115 VAC power supply uses a T 250 mA fuse.
The 10-30 VDC power supply uses a T 1.25 A fuse.

b ) AC voltage switch
A rotary 115/230 VAC switch is located next to the fuse holder (see Internal fuse
replacement above). You can change this with a turn from a small flat-bladed
screwdriver. Check to see that the correct fuse for your voltage is installed before
connecting the instrument to a power supply.

c ) Alarm output jumper settings

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The default factory setting is for Normally Open operation. You can change this to
Normally Closed (or vice versa) by changing the J14 jumper settings.

Fig 18 : Jumper J14 Pin Number Identification

Operators Manual

42 of 78

Maintenance and troubleshooting - 3610 Analyzer

The pin number identification is illustrated in Fig 18, and Table 10 shows the pin settings.
Table 10 : Alarm Output Jumper Settings
Normally Open (NO) Normally Closed (NC)
Jumper

Pins

Pins

J14

5-6 and 8-9

4-5 and 7-8

Note :
This is valid for all configurations except the 3610/x10 and 3610/x40 instruments which
have no alarm outputs.

d ) Analog current/voltage output jumper settings


To reach the output card of a panel/rack mount or portable instrument, you must pull off
the outer case. Carefully turn the rear panel so that you can slip the outer case over it.
Remove the isolating shield to expose the electronics inside.
The printed circuit board number 1121B, contains the jumpers you must set. To remove
this board, remove the screws on either side that hold the board in place and carefully lift
it out. The pin identification is illustrated in Fig 19.

Fig 19 : Jumper Pin Number Identification

Replace the board by placing it back into position and gently pushing it a final 2 mm to
make the electrical connection. Then reattach the two holding screws.
The following tables, listed by instrument configuration, indicate the jumper settings
required for the current or voltage output.

Configurations 3610/x10-x40
Table 11 : Current/Voltage Jumper Settings - Table 1

Jumper

Pins

J2

1-2

J8

1-2

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Voltage 0-5V

Operators Manual

3610 Analyzer - Maintenance and troubleshooting

43 of 78

Configurations 3610/x11-x20-x30-x41-x50-x60
Table 12 : Current/Voltage Jumper Settings - Table 2
Current 4-20mA Current 0-20mA Voltage 0-5V
Jumper

Pins

Pins

Pins

J2

2-3

2-3

1-2

J3

1-2

2-3

J8

2-3

2-3

J9

1-2

2-3

1-2

Configurations 3610/x21-x31-x51-x61
Table 13 : Current/Voltage Jumper Settings - Table 3
Current 4-20mA Current 0-20mA Voltage 0-5V
Jumper

Pins

Pins

Pins

J2

2-3

2-3

1-2

J3

1-2

2-3

J6

2-3

2-3

J7

1-2

2-3

J8

2-3

2-3

J9

1-2

2-3

1-2

1-2

Note :
You can alternate between a Current and Voltage output simply by re-setting the
appropriate jumpers as outlined in the tables above. However, If you need to change the
Current output from 0-20 mA to 4-20 mA (or vice versa), contact your Orbisphere
Service Representative first.

7.2 Instrument and sensor maintenance


Under normal operating conditions, your 3610 analyzer requires no maintenance. If the
indicating instrument is properly connected, handled with reasonable care and kept
clean, it should give you no mechanical or electrical problems.

KB - 30/07/04 - 3610MaintTroubleshoot.fm

Periodically, check the TC sensor calibration using a known standard. As long as the
reading is 1% of the expected value, no action needs to be taken. If the calibration has
changed 1-10%, perform a new calibration. If the deviation is more than 10% of the
original values, a change of membrane may be required.
A visual inspection of the sensor face may also reveal any problem like dust deposits or
accumulation of dirt onto the protection grill.
The TC sensor will require regular servicing. For sensor servicing and membrane
replacement details, please refer to the associated TC Sensors - Maintenance and
Installation Manual, which should have been delivered with your instrument.

Operators Manual

44 of 78

Maintenance and troubleshooting - 3610 Analyzer

7.3 Troubleshooting

a ) Measurement troubleshooting
Table 14 lists all possible measurement errors, which could be caused by poor handling
of the instrument and/or identifiable installation conditions.
Table 14 : Measurement Troubleshooting
Probable Cause
Sensor not connected
Message Out
Wrong sensor
connected

Purge pressure too low


or wrong purge gas

Message Prg

Corrective Action

Check sensor cable


connection (at sensor and Measurement
should return after
instrument end)
approximately 20
Connect correct CO2, H2 seconds
or N2 sensor
Restore correct purge
pressure and gas (refer to
the accompanying TC
Sensors - Maintenance
& Installation Manual for
details). Push the small
plastic tube firmly into the
purge exit and check
purge flow rate (over 3
bubbles per
second.) Check
voltage in continuous
purge mode.

For experienced
service personnel only:
Damaged sensing
Remove membrane and
element caused by
support. Check for
mishandling during
broken wires of the
membrane replacement
thermal conductivity chip
under microscope
Too much sample
pressure
Message Lmt

Leak in the membrane


Wrong membrane

Calibration out of
bounds

Expected Result

In continuous
purge mode,
voltage should be
in the range
-2.5V to +4.5V. If
purge flow rate is
too small, or if
voltage remains
above 4.5V,
contact your
Orbisphere agent

Contact your
Orbisphere agent

Check sample pressure


Stabilized reading
Replace membrane and
recalibrate

Wrong membrane
model; pierced/torn
membrane; or two
membranes
superimposed

Replace membrane

Wet protection cap

Blow grill with


compressed air and let
dry, carefully, in dry gas
flow for one hour

Wrong calibration
values entered against
actual
calibration fluid or
pressure

Check that gas


concentration or
pressure fit the entered
numerical data and units

Calibration
constant should be
50% of default
value

Operators Manual

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Symptom

3610 Analyzer - Maintenance and troubleshooting

45 of 78

Table 14 : Measurement Troubleshooting


Symptom

Probable Cause

Improper line voltage

Blown fuse

Unplug instrument and


replace blown fuse.
See Internal fuse
replacement on page 41
for instructions.

Voltage drift
during
measurement

Purge gas pressure too


low

Set correct pressure or


Measurement will
adjust pressure in order to
return to expected
get over 3 bubbles per
value
second from exit tube

Low reading

Leak in purge inlet line

Check line for leaks with


soapy water

Expected reading

High reading

Erroneous calibration in
gas with a wet
membrane protection
grill

Recalibrate in liquid. Or,


carefully dry out the
membrane and calibrate
in gas

Expected reading

Noisy reading
during gas
calibration

Calibrating gas flow


restricted generating
pressure pulses

Make sure calibration gas Stabilized


flows freely
reading

Improperly mounted
protection cap or membrane

Turn off purge gas and


check membrane and
protection cap
mounting procedure.
Restart purge

Stabilized
reading

Leaking solenoid valve

Check purge outlet. No


gas bubble should evolve
during the
measurement ramp

If solenoid leaks
(more than 1
bubble in 15
seconds), return
sensor to
Orbisphere

Grounding mismatch
between Orbisphere
instrument and
electronic
accessories (plotter,
terminal)

Plug all accessories and


instrument into same
mains terminal

Stabilized
reading

Mains power supply


unstable

Install a UPS unit as close


Stabilized
as possible to the
reading
instrument

Noisy readings
during
measurement

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Expected Result

Select proper
Check rear panel label for voltage (115V or
instrument voltage
230V) on power
supply card

System does not


start: No display
or backlight

Operators Manual

Corrective Action

Instrument should
start up. If not, or if
fuse blows again,
contact your
Orbisphere agent

In most cases,
sensor operates
properly. But
condensation may
result in
serious damage,
requiring service

Totally erratic
readings

Water condensation into


the thermal
conductivity element
due to purge failure or
humid purge gas

No bubble at
purge outlet

Purge gas block caused Replace outlet tubing and


Check for bubble. It
by faulty fitting, or
check in continuous purge
should reappear
mode
damaged tubing

Blow dry purge gas in


"continuous purge mode"
overnight. Resume
measurement mode.

46 of 78

Maintenance and troubleshooting - 3610 Analyzer

Table 14 : Measurement Troubleshooting


Symptom
Large
temperature
changes

Probable Cause
Slow TC sensor
temperature response

Corrective Action
Install external
temperature sensor

Expected Result
Stabilized reading

b ) Warning messages
During measurement, the instrument performs various diagnostic checks, and warns of
abnormal conditions with various messages and outputs as outlined below:
The instrument flashes a warning message on the LCD for one second, between
measurement display updates
The bottom line of the display includes a warning condition as a three-letter code
on the right-hand side
The alarm relays respond accordingly
For example, if your sensor was disconnected for any reason, you would see the Check
the Sensor message displayed for one second, followed by the measurement display
with the Out message code, as illustrated in Fig 20. This cycle would then be repeated
until the problem was solved.

Fig 20 : Example Warning Message Display

The following table lists possible sensor warning messages.


Table 15 : Sensor Warning Messages
LCD
Code

Analog
Output

High Low
Relay Relay

Reason

Action

#n CHECK
THE SENSOR

Out

20mA

On

On

Sensor
disconnected

Connect
sensor

#n WARNING
THERMAL
CUTOFF

Hot

20mA

On

On

Sensor Thermal cutoff

Check
process

On

At the beginning of a
measurement cycle if
V3beg< -2500mV or
V3beg> +4450mV

Restore
purge gas

On

At the end of a measurement cycle if


V3end< -2500mV or
V3end> +4450mV

Check
membrane

#n SENSOR
PURGE
FAILURE

#n RAMP LIMIT
VIOLATED

Prg

Lmt

Measure

Measure

On

On

Operators Manual

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Message on
Instrument LCD

3610 Analyzer - Maintenance and troubleshooting

47 of 78

Table 15 : Sensor Warning Messages


Message on
Instrument LCD

LCD
Code

Analog
Output

High Low
Relay Relay

#n PURGE
VOLTAGE
DRIFTING

Chk

Measure

Off

Off

#n HOLD

Hld

Last

Last

Last

Hold switch closed

None

#n ATTENTION
LOW LIMIT

LoL

Measure

Off

On

Gas Low limit alarm

Check
process

#n ATTENTION
HIGH LIMIT

HiL

Measure

On

Off

Gas High limit alarm

Check
process

#n ATTENTION
HIGHHIGH LIMIT

HHL

Measure

On

On

Gas HighHigh limit


alarm

Check
process

#0 indicates the TC sensor


#2 indicates the barometric pressure sensor
#3 indicates the external pressure sensor

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Action

At the beginning of a
measurement cycle if
V3beg< -2000mV or
V3beg> +3950mV OR
at the end of a measurement cycle if
V3end< -2000mV or
V3end> +3950mV

In Table 15, #n is defined as follows:

Operators Manual

Reason

Check purge
gas

Maintenance and troubleshooting - 3610 Analyzer

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Operators Manual

3610 Analyzer - Installation

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Installation
This section provides necessary information to install and connect the instrument. If you
have any questions or experience any difficulties, do not hesitate to contact your
Orbisphere representative regarding this installation procedure.
The instrument is available in a variety of configurations, as identified in Table 30,
Indicating Instrument Configurations, on page 73.
The instrument front panel has a key-lock to switch on the instrument, a two-line liquid
crystal display (LCD) displaying 16 characters per line, a light switch to illuminate the
LCD for three minutes when connected to an external power source and four control
keys.
Check to see that any required mounting and sampling hardware has been included.
This varies with each application, but in general:
A model 29501 sensor socket or a model 32003 ProAcc insertion/extraction valve
is used to mount the sensor directly in a pipe.
A model 32001 or model 32002 flow chamber is used to introduce an on-line
sample with 6-mm or -inch tubing, or to introduce a gas for calibrating.
A model 28117 pressure sensor may be used when calibrating or measuring in
gaseous samples.
Special mounting hardware is included for panel and rack mount instruments.

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Finally, certain accessories, such as a purge backup unit, external temperature sensor,
or data acquisition software for Windows may have been ordered. Refer to Accessories
and attachments on page 39 for a description of these items.

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Installation - 3610 Analyzer

8.1 Mounting
Note :
For all mountings, include at least 100mm additional rear clearance for cable protrusion.

a ) Panel instrument installation


The standard panel mount instrument configuration is illustrated in Fig 21.

Fig 21 : Panel Mount Configuration

Use the model 32200 panel mount template as a guide for the necessary panel cutting
and drilling. To use, place the template where you wish to mount the instrument, and
mark the drill holes and cut lines. Your mounting hardware includes a drill bit. Use this to
drill the 5.4 mm holes required, then cut the 214.5 mm wide by 125.5 mm high panel
holes.
Four self-clinching bolts secure the instrument to the panel. It is easiest to attach the
bottom two bolts first, guide the instrument into place, and then fix the top two bolts to
finish the procedure. Once tightened, the self-clinching bolts ensure that only one person
is required to remove the instrument.

The instrument can also be mounted in a 19" rack, either one across (model 32202
illustrated in Fig 23) or two across (model 32203 illustrated in Fig 24).
As with the panel mount configuration, four self-clinching bolts secure the instrument to
the rack panel.

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A retrofit panel mount (model 32201) is also available. This enables users of existing
Orbisphere analyzers to replace their instruments with the 3610 series, without additional
drilling or panel cutting, as shown in Fig 22.

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Fig 22 : Retrofit Panel Mount Configuration

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Fig 23 : 19 Rack Mount - One Across (Model 32202)

Fig 24 : 19 Rack Mount - Two Across (Model 32203)

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Installation - 3610 Analyzer

b ) Wall mount instrument installation


The instrument is available as a wall mount configuration as indicated in Fig 25.

Fig 25 : Wall Mount Configuration

Note :
Include at least 400 mm additional frontal clearance for front panel access, and at least
100 mm bottom clearance for cable protrusion.

Series 3610 portable instruments require no permanent mounting. Locate the instrument
near the power source and the sensors.

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c ) Portable instrument installation

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8.2 Connections

a ) Power input
WARNING
The installation of a 3610 instrument should only be performed by personnel specialized
and authorized to work on electrical installations, in accordance with relevant European
and/or national regulations. In accordance with safety standard EN 61010-1, it must be
possible to disconnect the power supply of a 3610 instrument in its immediate vicinity.
While the instrument electronics are well shielded, it is still advisable to locate the
instrument as far as possible from any source of electromagnetic perturbation.

AC power input
CAUTION :
Use a power supply cable type H05VV-F 3 X 0.75 mm2 (supplied with the instrument).
The length of the cable should be three meters maximum and it should have a
separable plug (with three connectors, L+N+PE), without a locking device, to mate with
a socket outlet in the building. The cable and the plug must conform to an appropriate
European or national standard.
For wall mount instruments, AC power connections use the right most waterproof
cable gland (see illustration in Fig 25). The power cable must be wired according to the
label inside the housing. Three FAST ON 6.3-mm spade-type connectors are supplied
with the wall mount instrument for wires measuring from 0.5 - 1 mm2.
1)
2)
3)
4)
5)

Remove the exterior insulation of the cable for a length of about 50 mm.
Insert the cable through the right most cable gland.
Strip the wires for a length of about 8 mm.
Put a FAST ON (spade-type) connector on each of the three wires.
Put the live, neutral, and earth wires on the corresponding spade plugs of the
mains filter, as indicated on the label affixed to the bottom of the wall mount box,
opposite the filter.
6) Slide the cable farther through its cable gland until its external insulation
penetrates about 6 mm inside the housing, blocking the cable gland.
For panel and portable instruments, AC power connections use a standard detachable
power cable on the rear panel of the instrument (as illustrated in Fig 27 and Fig 31).

10-30 VDC power input


Note :
This is only applicable to the 3610/450 and 3610/550 panel mount instruments and the
3610/540 portable instrument.

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DC powered instruments have a Male Binder connector on their rear


panel. It accepts 10-30 VDC power as follows:

Operators Manual

Pin 1: DC Return
Pin 2: Earth (Chassis)
Pin 3: Not connected
Pin 4: 10-30 Volts DC

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The necessary DC power wiring connections must be made using the Female Binder
connector supplied. User-supplied power cable can have an outer diameter of between
5mm and 8mm.

Fig 26 : Female Binder Connector - Exploded View

Disassemble the plug by squeezing the two clips located in the middle of the plug
(position C in Fig 26). This reveals numbered wiring connections inside, to be matched
one-to-one with the Male Binder connector diagram above.

b ) Electrical signal connections


Connections to the gas sensor and (optional) external pressure sensor use pre-wired
LEMO receptacles on the rear of the panel mount and portable instruments, and on the
bottom of the wall mount instrument housing. Fig 27 shows the rear of the panel mount
instrument with AC power input and optional external pressure sensor input. Fig 31
shows the rear of the portable instrument and Fig 25 shows the wall mount instrument.
The supplied sensor cables have mating LEMO connectors. The LEMO connector pin
assignments are identified in Wiring identification on page 57.

Note :
Disconnect power to the instrument before removing any panels, and ground each cable
shield securely to ensure proper operation.

Panel mount instrument

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Connections for RS-232, recorder (analog) output, hold input, and alarm relays use
watertight cable glands on the instrument rear panel. These cables must be wired to a
terminal strip inside the instrument. To make any of these connections, remove the rear
instrument panel.

Fig 27 : Instrument Rear View - Panel Mount Model

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First remove the front-panel key. Then place the instrument facedown and remove the
four 3 mm Allen-head screws. Carefully pull off the rear panel (taking care not to
disconnect any wires) to expose the terminal block (illustrated in Fig 28) and wiring
diagram label (illustrated in Fig 29).

Fig 28 : Instrument Terminal Block

Terminal block pin assignments can be found in Wiring identification on page 57. Refer
also to User-supplied cabling requirements on page 60 for the user-supplied cables,
and to Cable gland wiring instructions on page 61 for wiring connections through the
cable glands.

Fig 29 : Wiring Labels

The illustration in Fig 29 shows the wiring labels for the 3610 instruments with and
without the external pressure inputs. The label on the left is without the pressure sensor
and the label on the right includes the pressure sensor.

Wall mount instrument


Connections for RS-232, recorder (analog) output, hold input, and alarm relays use
watertight cable glands on the bottom of the instrument housing. These cables must be
wired to the terminal block on a printed circuit board, located inside the instrument
housing. A wiring diagram label inside identifies each unit's terminal strip connections.
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To access this board, unlock the front panel of the wall mount unit with the key provided
to expose the instrument electronics inside.
The connection board, number 1127.002 (this part number is on the lower edge of the
card), contains the terminal block connections and a terminal block pin label.

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Fig 30 : 1127.002 Connection Board

Terminal block pin assignments can be found in Wiring identification on page 57. Refer
also to User-supplied cabling requirements on page 60 for the user-supplied cables,
and to Cable gland wiring instructions on page 61 for wiring connections through the
cable glands.

Portable instrument
Connections for RS-232, recorder (analog) output, hold input, and alarm relays, cables
must be wired to LEMO connectors. LEMO connector pin assignments can be found in
Wiring identification on page 57. Refer also to User-supplied cabling requirements on
page 60 for the user-supplied cables. Instructions for wiring the supplied LEMO
connectors are described in LEMO connector assembly instructions on page 60.

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Fig 31 : Instrument Rear View - Portable Model

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8.3 Wiring identification

a ) CO2, H2 or N2 sensor wiring identification


Fig 32 : CO2, H2 or N2 Sensor Wiring
Sensor Signal

LEMO-10
Pin

GND for Power

Pin 1

V2 Signal

Pin 2

Solenoid

Pin 3

Relay Coil

Pin 4

+12V Power

Pin 5

+24V Power

Pin 6

V3 Signal

Pin 7

GND for Signal

Pin 8

-5V Power

Pin 9

Temperature

Pin 10

b ) External pressure sensor input wiring identification


Fig 33 : External Pressure Sensor Wiring

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Sensor Signal

Operators Manual

LEMO-4
Pin

Voltage (+)

Pin 1

Ground

Pin 2

Input (+)

Pin 3

Input (-)

Pin 4

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c ) Serial (RS-232) wiring identification


Fig 34 : Serial (RS232) Output Wiring

RS232
Signal

Portable
LEMO-6
Pin

Panel/Rack
Mount
Terminal
Strip
Position

Wall Mount
Terminal
Block
Position

TXD

Pin 1

J13.8

J5.1

->

RXD

RXD

Pin 2

J13.7

J5.2

<-

TXD

Pins 3-5

N/A

N/A

N/A N/A

Pin 6

J14.9

J5.3

<-> GND

Not Used
GND

User
Recorder
Signal

d ) Analog (recorder) output wiring identification


Fig 35 : Analog (Recorder) Output Wiring

Portable
LEMO-8
Pin

Panel/Rack
Mount
Terminal
Strip
Position

Wall Mount
Terminal
Block
Position

User
Recorder
Signal

Gas Out

Pin 1

J13.3

J6.1

->

Gas In

Temp. Out

Pin 2

J13.2

J6.3

->

Temp. In

Press. Out

Pin 3

J13.1

J6.5

->

Press. In

Press. Gnd

Pin 4

J14.1

J6.6

<-

Press. Gnd

Temp. Gnd

Pin 5

J14.2

J6.4

<-

Temp. Gnd

Gas Gnd

Pin 6

J14.3

J6.2

<-

Gas Gnd

Not Used

Pins 7/8

N/A

N/A

N/A N/A

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Analog
Output

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e ) Alarm output wiring identification


Fig 36 : Alarm Output Wiring

Alarm
Relay *

Portable
LEMO-5
Pin

Panel/Rack
Mount
Terminal
Strip
Position

Wall Mount
Terminal
Block
Position

User
Alarm
Device
Signal

Low Relay

Pin 1

J13.6

J7.1

Low

High Relay

Pin 2

J13.5

J7.2

High

Not Used

Pins 3-4

N/A

N/A

N/A

Common

Pin 5

J14.7

J7.3

Common

* If you use the High/High-High alarm option, refer to Alarm outputs on


page 66 for identification of the alarm conditions and relay responses.

f ) Hold switch wiring identification


Fig 37 : Hold Switch Wiring

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Hold
Signal

Operators Manual

Portable
LEMO-2
Pin

Panel/Rack
Mount
Terminal
Strip
Position

Wall Mount
Terminal
Block
Position

User
Alarm
Device
Signal

+5V Out

Pin 1

J13.9

J8.1

->

+5V In

Return

Pin 2

J14.10

J8.2

<-

Return

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8.4 User-supplied cabling requirements


Cables for the recorder output, alarm relays, hold switch, and RS-232 should be control
cables (i.e. not power cables) with twisted copper wires and shield, meeting the
specifications in Table 16.
Table 16 : Alarm and Analog Output Cable Specifications
Description

Specification

External Diameter
Alarms, Hold, RS-232 Output:
Recorder Output:

4-6 mm
6-8 mm

Wire (core) Area

0.14 - 0.25 mm

Insulation

PVC

Nominal Voltage

250 V

Absolute Maximum Voltage

1200 V

Absolute Maximum Current

1.5 - 2.5 A

Wire Resistance

140 - 70 /km

Wire Capacitance @ 800 Hz

100 pF/m

Shield Capacitance @ 800 Hz 240 pF/m

Note :
Ground the cable shield securely to the instrument case to ensure proper operation.
The maximum cable length for the RS-232 connection is 20 meters. For installations that
require connection distances up to 1 km, use RS-232/RS-485 converters at each end of
the cable.

8.5 LEMO connector assembly instructions


Disassemble the LEMO connector, referring to Fig 38.

1) Slide the pieces over the cable in the following order: boot, back nut, collet, ring
(beveled edge down), rubber seal, and reducer (narrow edge down).
2) Strip off 8 mm of the insulation and 6 mm of the shield from the cable.
3) Fan out the remaining wires and the shield.
4) Remove the clear plastic wrap from the wires.
5) Strip off about 1 mm of insulation from the wires.

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Fig 38 : LEMO Connector - Exploded View

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6) Slide the mid piece up over the wires to the shield. Make sure the shield is
pinched between the mid piece and the reducer to ensure proper grounding.
7) Place the pin assembly in a vice and solder the wires to the numbered pins.
8) Slide all the pieces down into the shell (note: the key in the mid piece must match
the notch in the pin assembly) and secure the entire connector assembly by
tightening the back nut.

8.6 Cable gland wiring instructions


The nickel-plated, brass cable glands are EMC-types, designed so that the cable shields
attach directly to the instrument box. Typical cable wiring through one of these glands is
illustrated in Fig 39.

Fig 39 : Cable Gland Wiring - 1

1) Unscrew the cable gland nut. You will find a rubber gasket, then a metal washer
with an interior diameter of 8.3 mm, and then another metal washer with an
interior diameter of 7.5 mm.
2) Pass the cable through the nut, the gasket, and the 8.3-mm washer.
3) Strip off 110 mm of external insulation, and 85 mm of shielding (see Fig 40).

Fig 40 : Cable Gland Wiring - 2

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4) Pass the cable prepared in this fashion through the 7.5-mm washer.
5) Pinch the shield so that its entire circumference is pressed between the two
washers (as shown in Fig 39).
6) Pass the cable into the box, blocking the cable gland.
7) Reattach and tighten the cable gland nut.
8) Strip the wires about 8 mm from their ends.
9) Attach the wires to the corresponding terminal block connections, as follows:
For panel mount instrument terminal blocks, use a small-bladed flat screwdriver
to gently push back the spring-loaded plastic lever on top of the terminal strip

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connector. Insert the wire into the connector opening and release the lever to hold
the wire firmly in place.
For wall mount instrument terminal blocks, use a small-bladed flat screwdriver to
loosen the screw at the top of the terminal block connector. Insert the wire into the
connector opening and tighten the screw to hold the wire firmly in place.

8.7 Sensor and sensor purge gas installation


The TC sensor has a threaded collar and storage cap, a screw-on protection cap
covering the membrane, and a LEMO 10-pin connector for the sensor cable. The sensor
cable has a mating screw-on connector, and a snap-in LEMO plug for connecting to the
instrument. The standard sensor cable length is three meters, but extension cables of up
to 100 meters can be provided without any loss in signal sensitivity.
The TC sensor also has entry and exit ports for a purge gas supply. A LEMO 4-pin
adapter may be mounted at the rear of the sensor to connect to an external temperature
sensor. When factory-fitted with the external temperature sensor adapter, the H2 sensor
is designated model 3126x, the CO2 sensor is model 3146x, and the N2 sensor is model
3156x.
For full instructions on sensor and sensor purge gas installation, please refer to the TC
Sensors - Maintenance & Installation Manual that was provided with your instrument.

8.8 Model 28117 pressure sensor installation


The pressure sensor can be mounted in the model 32002.x flow chamber. It is held in
place by a threaded, blue-colored aluminum collar. The pressure sensor 4-pin LEMO
connector plugs into the socket labeled pressure on the instrument. The maximum cable
length is 50 meters.

8.9 Analog outputs


The 3610 instrument provides a choice of three analog output signals of 0-5 Volts, 0-20
mA, or 4-20 mA, which represent the measured CO2, H2, or N2 gas concentration,
temperature, and pressure. See Wiring identification on page 57 for output wiring
connections and Analog current/voltage output jumper settings on page 42 for current/
voltage output conversion.
The instrument generates these analog outputs using a 12-bit digital converter. Thus, the
minimum increment of any output can be determined by dividing the output range by
4096. For example: You could set the gas concentration range to 0-500 ppm for 4-20mA,
and your recorder would still pick up changes of 0.122 ppm. The accuracy of each
increment is 1%.

a ) Gas concentration output

When ANALOG OUTPUT is DISABLED in these menus, the instrument scales the gas
concentration output to vary linearly with the measured gas concentration, from 0 to 9999
(of the measurement units selected). The relation between the gas concentration
measurement M and the analog output signal V (voltage V) or I (current, mA) is as shown
in Table 17.

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You can scale the analog output signal of CO2, H2, or N2 concentration to vary between
any two custom gas concentration levels. Instructions for setting these levels are in
Alarm and analog outputs on page 20.

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Table 17 : Custom Analog Output Disabled


Analog Output Gas Concentration Measurement (M)
4-20mA (I)

M = (I-4) * 625

0-20mA (I)

M = I * 500

0-5V (V)

M = V * 2000

When ANALOG OUTPUT is ENABLED, the instrument rescales outputs for each of the
three signals (4-20mA, 0-20mA and 0-5V) between any Low (L) and High (H) limits that
are defined in the Modify Options Menu (See Alarm and analog outputs on page 20.).
The relationship between the analog output signal V (voltage V) or I (current, mA), and
the measurement M is represented in Table 18.
Table 18 : Custom Analog Output Enabled
Analog Output Gas Concentration Measurement (M)
4-20mA

M = L + ((H - L) * ((I - 4) / 16))

0-20mA

M = L + ((H - L) * (I / 20))

0-5V

M = L + ((H - L) * (V / 5))

Using Table 18, the following is an example of the measurement calculation for a 16mA
analog signal (I) (on a 4-20mA configuration) and where the low and high limits are
defined as 10 (L) and 20 (H):
M = L + ((H - L) * ((I - 4) / 16))
M = 10 + ((20 - 10) * ((16 - 4) / 16))
M = 10 + (10 * 0.75)
M = 10 + 7.5
M = 17.5

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This same calculation can also be represented graphically as illustrated in Fig 41.

Fig 41 : Analog Output - Graphical Representation

The output upper limit is fixed at 20mA or 5V whenever the displayed concentration is
equal to or exceeds the defined High limit value. Similarly, the output lower limit is fixed

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at 4mA, 0mA or 0V if the concentration is equal to or less than the defined Low limit
value.
The output also shows these extreme upper and lower limit values under other
conditions as summarized in Table 19.
Table 19 : Analog Output - Additional Upper and Lower Limit Conditions
Analog Output
4-20mA

0-20mA

0-5V

4mA

0mA

0V

Menu, sensor thermal


cutoff, negative gas
concentration value,
custom analog output low
level or display under range
Normal Operating
Condition

4mA < signal < 20mA 0mA < signal < 20mA 0V < signal < 5V

Display over range, custom


analog output high level or
sensor disconnected

20mA

20mA

5V

b ) Temperature output
The analog output representative of the sample temperature varies linearly with the
measured temperature from -20C to 100C, as illustrated in Table 20.
Table 20 : Analog Output - Temperature Calculations
Analog Output

Temperature
C = -20 + (7.5 * (I - 4))

4-20mA

F = -4 + (13.5 * (I - 4))
K = 253.15 + (7.5 * (I - 4))
C = -20 + (6 * I)

0-20mA

F = -4 + (10.8 * I)
K = 253.15 + (6 * I)
C = -20 + (24 * V)

0-5V

F = -4 + (43.2 * V)
K = 253.15 + (24 * V)

c ) Pressure output
The analog output representative of sample pressure varies linearly, from 0 to 5000
mbar, as illustrated in Table 21.

Analog
Output

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Table 21 : Analog Output - Pressure Calculations


Pressure (P)

4-20mA

P = 312.5 * (I - 4)

0-20mA

P = 250 * I

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Table 21 : Analog Output - Pressure Calculations


Analog
Output

Pressure (P)

0-5V

P = 1000 * V

8.10 Serial outputs


The instrument serial output provides formatted text for an RS-232 compatible printer,
monitor, or computer interface (see Serial (RS-232) wiring identification on page 58 for
serial output wiring connections). The pertinent RS-232 communications parameters
are:

Baud rate = 9600


Stop Bit = 1
Data Bits = 8
Parity = None
Flow Control = None

Instructions for selecting the serial output operating mode are in Serial output on
page 21.

Enabled
This output provides a running log of gas concentration plus sample temperature. It also
includes information on conditions that affect gas measurement as shown in the sample
output in Table 22.
Table 22 : Sample of RS232 Measurement Output
Concentration

CO2= 1.001
CO2= 1.002
CO2= 1.001

Temperature

bar T = 29.8 C
bar T = 29.8 C
bar T = 29.9 C

Alrm

Chk

Pext
bar

Patm
mbar

1.001
1.002
1.001

998
999
999

Offset

0.000
0.000
0.000

Status

T
T
T

The output generates a new row of headings (see line starting Concentration... in the
Table 22 example) every sixteen measurement cycles. Concentration, Temperature,
and Alrm values are as seen on the instrument's display. External pressure Pext is
displayed in bars and barometric pressure Patm is displayed in mbars. If an offset has
been entered (see Offset on page 22), the Offset column shows the value. A code
appearing in the Status column signifies the following conditions:
A = Rolling Average enabled
H = Humidity Correction enabled
T = Temperature Correction enabled

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When enabled, the serial output also generates a report when you calibrate the sensor
as shown in Table 23.
This example reveals an initial recalibration cycle of more than 1% (Recal err = 1.2%)
outside normal limits, followed by successful calibration cycles.

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Table 23 : Sample of RS232 Sensor Calibration Cycles Output


CP= 2002 mbar 3
-67 542
43.404
-67 549
43.922
-68 549
44.005
-66 548
43.761
-67 549
43.888

UP/DOWN MODIFIES
Calibration Coeff at
CO2= 2025 mbar
Calibration Coeff at
CO2= 1990 mbar
CO2= 1996 mbar

25C: 21.967 mV/s


Recal err= 1.2%
25C: 21.274 mV/s
T =24.4C cal:1
T =24.4C cal:2

Diagnostics
This output selection provides several lines of hexadecimal codes indicating how your
instrument is performing. In addition, when you return to Measurement mode after
selecting diagnostics, the serial output subsequently provides a running log of diagnostic
results for every measurement cycle, as shown in Table 24.
Table 24 : Sample of RS232 Diagnostics Output

Vi
Vf
mV mV
1998
4005
1998
4005

Slope
mV/s
332.566
332.520

Temp No PartPres StDv


C
bar
%
29.8
1
1.001
0.0
29.8
2
1.000
0.1

H2O
Tcorr
mV/s
mV/s
0.000
0.000
0.000
0.001

The first three columns of the diagnostics output indicate the sensor voltage at the
beginning and end of the purge cycle, and the calculated voltage Slope. Temp is the
sample temperature and No is the output line number (1 to 9999). PartPres and StDv
track deviations from expected conditions. H2O and Tcorr list humidity and temperature
corrections applied (see Corrections on page 23).
If you want to bring this serial output information into your personal computer, it is
advisable to use Orbisphere's Windows data acquisition software described in Data
acquisition software on page 39. Otherwise, you may use a third-party communication
software (such as Hyper Terminal).

8.11 Alarm outputs


Note :
Alarm outputs are NOT applicable to series 3610/x10 and 3610/X40 instruments.
Two alarm relay outputs are available in most instrument configurations (see also Alarm
output wiring identification on page 59 for alarm output wiring connections). Each alarm
relay can be set for Normally Open (NO) or Normally Closed (NC) operation - the factory
default setting is Normally Open. If you wish to change the setting on your instrument,
please refer to Alarm output jumper settings on page 41 for details.

You can set your own alarm limits. If the measured gas concentration is outside of these
limits, the instrument activates the appropriate alarm relay. Instructions for selecting the
alarm configuration and setting the alarm limits are in Alarm and analog outputs on
page 20.
Table 25 and Table 26 list all alarm conditions and alarm relay responses for your
options settings.

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The Alarm Outputs options menu gives you the choice of selecting the alarm
configuration (Low/High or High/High-High). This configuration determines the manner
in which the alarm relays respond to various system or measurement conditions.

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Table 25 : Low/High Alarm Relay Responses


Condition

Low Relay
Set For NO*

High Relay
Set for NO*

Low Relay
Set For NC*

High Relay
Set For NC*

No alarm:
LL < measured gas < HL
Low alarm:
measured gas < LL
Low test:
Low Alarm test **
High alarm:
measured gas > HL
High test:
High Alarm test **
System alarm:
In Calibration or Modify Options
menu, or instrument power off

* Low and High refer to the alarm relays identified in the instrument wiring labels
** See Alarm and recorder output testing on page 69
Table 26 : High/High-High Alarm Relay Responses
Condition

Low Relay
Set For NO*

High Relay
Set for NO*

Low Relay
Set For NC*

High Relay
Set For NC*

No alarm:
measured gas < HL
High alarm:
HL < measured gas < HH
High test:
High Alarm test **
High-High alarm:
measured gas > HH
High-High test:
High-High Alarm test **
Instrument Power Off
System alarm:
In Calibration or Modify
Options menu

* Low and High refer to the alarm relays identified in the instrument wiring labels
KB - 30/07/04 - 3610Installation.fm

** See Alarm and recorder output testing on page 69

Note :
The High-High alarm condition does not correspond to a single alarm relay response,
rather, it sets both alarm relays.

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Installation - 3610 Analyzer

Fig 42 shows a graphical representation of when the alarms are triggered.

Fig 42 : Alarm Conditions - Graphical Representation

The High or HighHigh alarm is initially activated, once the measurement goes above the
limits set. The Low alarm is activated when the measurement falls below the low limit.
The instrument clears the Low alarm when the gas concentration rises to 1% above the
low limit, or clears the High or High-High alarm when the gas concentration drops to 1%
below the high or high-high limit.

8.12 Installation completion check list

a ) Check voltage and line power


The indicating instrument is available in 115 VAC, 230 VAC, and 10-30 VDC versions.
Make sure that it is correct before connecting to a power supply, and make sure that the
ground of the AC supply is connected.

Note :
While the instrument case is watertight, the detachable power cable connection is not.

b ) Check purge gas supply


It is critical that the TC sensor has a supply of purge gas running before operating the
system. The TC sensor, when exposed to a liquid sample, could be damaged if the purge
gas is not running.
For full details on the correct purge gas to use for your sensor, refer to the accompanying
TC Sensors - Maintenance & Installation Manual.

The TC sensor must be purged continuously. The instrument does this automatically;
thus make certain that power is supplied constantly to the instrument. If it is desirable to
be able to shut off the instrument while leaving the sensor installed in a liquid sample,
install a model 32605 purge backup unit as described in Model 32605 purge backup
unit on page 39.

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c ) Maintain instrument power at all times

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d ) Alarm and recorder output testing


When connecting the alarm or recorder (analog) outputs to user-supplied equipment, it
may be helpful to verify the connections using a test signal from the instrument. For this
purpose, the 3610 instrument provides diagnostic signals for both the alarm output pins
and the recorder current (or voltage) gas concentration output pins.
When you set alarm and analog output limits using the Modify Options menus (see
Alarm and analog outputs on page 20), an associated alarm or analog output test
signal is provided at the connections.
The alarm limit selections of this menu set the high and low alarm relays.
The analog output selections of this menu apply a test current (or voltage) output
at the recorder output gas concentration pins.
The diagnostic outputs provided from the Modify Options menu procedures are:
Table 27 : Alarm and Recorder Diagnostic Outputs
Modify Options Selection

Output Provided

Alarm, Low Limit

Closure (*) of Low Alarm relay, Low Alarm Pin to Common

Alarm, High Limit

Closure (*) of High Alarm Relay, High Alarm Pin to Common

Alarm, High-High Limit

Closure (*) of both High Alarm Relay and Low Alarm Relay,
High Alarm Pin and Low Alarm Pin to Common

Analog, Low Level

4mA (or 0mA or 0 Volts) applied to Gas Concentration Pins

Analog, High Level

20mA (or 5 Volts) applied to Gas Concentration Pins

(*) These alarm relay outputs are for Normally Open alarm relays. If the relays are set to
Normally Closed, these relay outputs are the opposite, Opening instead of Closure (see
Alarm outputs on page 66)

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The test alarm relay closure or analog signal remains on the output pins until you return
to the Main Menu.

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3610 Analyzer - Specifications

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Specifications
9.1 System specifications

a ) General technical data


Table 28 : General Technical Data
Power Requirements 115/230 VAC 10% @ 50/60 Hz, or 10 to 30 VDC
Power Consumption Maximum 30 VA
Analog Outputs

Current outputs: 0/4 to 20 mA, R max. 500


Voltage outputs: 0 to 5 V, 10 K

Digital Output
(RS232C)

Baud rate: 9600; Data bits: 8; Stop Bits: 1; Start Bits: 0; Parity: None

Alarms

Two dry contact relays rated:


30 Watts, 150 VDC max. and 1 Amp max.
60 VA, 125 VAC max. and 1 Amp max.

Dimensions

Portable:
221.5 x 133 x 190 mm
Panel/Rack Mount: 221.5 x 132.5 x 195 mm
Wall Mount:
380 x 300 x 181.5 mm

Weight

2.6 kg (wall mount 8 kg)

Operating Limits

-20 to 60 C ambient temperature

Enclosure Protection IP 65/NEMA 4

b ) Standard sensor cable specifications


Table 29 : Standard Sensor Cable Specifications
Casing

Fire-retardant Elastolan

Maximum Temperature

80 C

Cable Diameter

6.1 mm 0.3 mm. 10 each stranded wires of 26 AWG,


individually insulated with polyethylene, 90% shielded by tinned
copper braid.

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Maximum Pulling Tension 7 kg

Operators Manual

Resistivity

138 /km

Minimum Bend Radius

15 times cable diameter

Maximum Cable Length

50 m

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3610 Analyzer - Part lists

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10 Part lists
10.1 Instrument
Table 30 : Indicating Instrument Configurations
Description
Portable battery powered, No Alarms,
Voltage outputs: 2

3610/210

3610/410

3610/510

Portable battery powered, Alarms: 2,


Current outputs: 2

3610/211

3610/411

3610/511

Portable battery powered, Alarms: 2,


Current outputs: 2, Special sensor: 31252/31262HP,
Special sensor purge: Carbon dioxide.

3610/213

N/A

N/A

N/A

N/A

3610/513

Panel, Alarms: 2, Current outputs: 2

3610/220

3610/420

3610/520

Panel, Alarms: 2, Current outputs: 2,


Special sensor: 31251/31261(H2), 31553/31563 (N2),
Special sensor purge: Argon.

3610/221

N/A

3610/523

Panel, Alarms: 2, Current outputs: 3,


External pressure input.

3610/222

3610/422

3610/522

Panel, Alarms: 2, Current outputs: 2,


Special sensor: 31252/31262HP,
Special sensor purge: Carbon dioxide

3610/223

N/A

N/A

Wall, Alarms: 2, Current outputs: 2

3610/230

3610/430

3610/530

Wall, Alarms: 2, Current outputs: 3,


External pressure input.

3610/232

N/A

N/A

Portable battery powered, No Alarms,


Voltage outputs: 2,
Instrument voltage: 10-30 VDC,
Special connector: Binder 4 power.

N/A

N/A

3610/540

Panel, Alarms: 2, Current outputs: 2,


Instrument voltage: 10-30 VDC,
Special connector: Binder 4 power.

N/A

3610/450

3610/550

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Portable battery powered, Alarms: 2,


Current outputs: 2, Special sensor: 31564,
Special sensor purge: Helium.

Operators Manual

H2
CO2
N2
Instrument Instrument Instrument

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Part lists - 3610 Analyzer

10.2 Accessories
Part N

Description

28117

Pressure sensor, 0-5 bar absolute.

29501

Stainless steel sensor socket for welding to stainless steel pipe.

32003

Sensor insertion and retraction valve for use with Tuchenhagen adapter.

32605

Purge Backup Unit for TC sensors.

32557

External temperature sensor for in-line use, supplied with 4 pin LEMO connector
for TCD sensors equipped with sensor adapter 32558. Sensor socket must be
ordered separately.

32558

Adapter for TCD sensors for attaching an external temperature sensor.

32559

External temperature sensor for off-line use, supplied with 4 pin LEMO connector
for TCD sensors equipped with sensor adapter 32558. T piece for connection
included.

32681.E

MOCA3610 Windows software for logging data from 3610 instruments.

32200

Front plate sticker template for installation of 3610 panel mount instruments.

32201

Retrofit front plate for 3610 panel mount instruments.

32202

19" Front plate for one panel mount instrument. (3610).

32203

19" Front plate for two panel mount instruments. (3610).

32204

Installation kit for panel mount instrument. (3610).

10.3 Spare parts


The Orbisphere Recharge Kit should contain sufficient material for several years of
sensor servicing. However, it must be replenished over time. What follows are
replacement items you may require in the future. Be sure to mention the model number
and item description when ordering.
For a complete listing of sensor spare parts, please refer to the TC Sensors Maintenance and Installation Manual.
Table 31 : Spare Parts Table
Part N

Description

28114

Membrane support mounting tool.

28210

Connector LEMO 8 pin, male.

29006.0

EPDM O-ring set for standard flow chambers (32001, 32002, 32007, 32009) and
29501 sensor socket. (34x2mm & 28x2 mm).

29661.MM 10 wire extension sensor cable (price per meter) .MM = specify total length.
Flow chamber

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3610 Analyzer - Annex

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Annex
Tables and illustrations

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Fig 1 :
Fig 2 :
Fig 3 :
Fig 4 :
Fig 5 :
Fig 6 :
Fig 7 :
Fig 8 :
Fig 9 :
Fig 10 :
Fig 11 :
Fig 12 :
Table 1 :
Table 2 :
Table 3 :
Fig 13 :
Fig 14 :
Fig 15 :
Fig 16 :
Fig 17 :
Table 4 :
Table 5 :
Table 6 :
Table 7 :
Table 8 :
Table 9 :
Fig 18 :
Table 10 :
Fig 19 :
Table 11 :
Table 12 :
Table 13 :
Table 14 :
Fig 20 :
Table 15 :
Fig 21 :
Fig 22 :
Fig 23 :
Fig 24 :
Fig 25 :
Fig 26 :
Fig 27 :
Fig 28 :
Fig 29 :
Fig 30 :
Fig 31 :
Fig 32 :
Fig 33 :
Operators Manual

Instrument Controls ............................................................................. 9


Function Keys......................................................................................9
Instrument Measurement Menu Flow Diagram .................................11
Configuration and Measurement Displays.........................................11
Data Acquisition Main Menu..............................................................12
Data Acquisition Interval....................................................................13
Gas Selection ....................................................................................13
Serial Port Configuration ...................................................................13
Data Acquisition Display....................................................................14
Print Data Option ...............................................................................14
Modify Options Menu - Part 1............................................................17
Modify Options Menu - Part 2............................................................18
Dissolved Gas Units ..........................................................................19
Partial Pressure Gas Units ................................................................19
Fraction Gas Units.............................................................................20
Water Saturated with Purge Gas.......................................................24
Purge Gas Saturated with Water.......................................................24
Instrument Calibration Menu Flow Diagram ......................................27
Flow Chamber - Calibrate & Measure Flows.....................................30
Partial Pressure Calibration Diagram ................................................31
CO2 Concentrations in V/V in Distilled Water ...................................33
CO2 Concentrations in g/kg in Distilled Water ..................................34
H2 Concentrations in cc/kg in Distilled Water....................................35
H2 Concentrations in ppm in Distilled Water .....................................36
N2 Concentrations in ppm in Distilled Water .....................................37
N2 Concentrations in ml/l in Distilled Water ......................................38
Jumper J14 Pin Number Identification...............................................41
Alarm Output Jumper Settings ..........................................................42
Jumper Pin Number Identification .....................................................42
Current/Voltage Jumper Settings - Table 1 .......................................42
Current/Voltage Jumper Settings - Table 2 .......................................43
Current/Voltage Jumper Settings - Table 3 .......................................43
Measurement Troubleshooting..........................................................44
Example Warning Message Display..................................................46
Sensor Warning Messages ...............................................................46
Panel Mount Configuration ................................................................50
Retrofit Panel Mount Configuration ...................................................51
19 Rack Mount - One Across (Model 32202) ...................................51
19 Rack Mount - Two Across (Model 32203) ...................................51
Wall Mount Configuration ..................................................................52
Female Binder Connector - Exploded View.......................................54
Instrument Rear View - Panel Mount Model......................................54
Instrument Terminal Block.................................................................55
Wiring Labels.....................................................................................55
Instrument Rear View - Portable Model.............................................56
1127.002 Connection Board..............................................................56
CO2, H2 or N2 Sensor Wiring ...........................................................57
External Pressure Sensor Wiring ......................................................57

Annex - 3610 Analyzer

Fig 34 :
Fig 35 :
Fig 36 :
Fig 37 :
Table 16 :
Fig 38 :
Fig 39 :
Fig 40 :
Table 17 :
Fig 41 :
Table 18 :
Table 19 :
Table 20 :
Table 21 :
Table 22 :
Table 23 :
Table 24 :
Table 25 :
Table 26 :
Fig 42 :
Table 27 :
Table 28 :
Table 29 :
Table 30 :
Table 31 :

Serial (RS232) Output Wiring ............................................................58


Analog (Recorder) Output Wiring ......................................................58
Alarm Output Wiring ..........................................................................59
Hold Switch Wiring.............................................................................59
Alarm and Analog Output Cable Specifications.................................60
LEMO Connector - Exploded View ....................................................60
Cable Gland Wiring - 1 ......................................................................61
Cable Gland Wiring - 2 ......................................................................61
Custom Analog Output Enabled ........................................................63
Analog Output - Graphical Representation........................................63
Custom Analog Output Disabled .......................................................63
Analog Output - Additional Upper and Lower Limit Conditions..........64
Analog Output - Temperature Calculations .......................................64
Analog Output - Pressure Calculations..............................................64
Sample of RS232 Measurement Output............................................65
Sample of RS232 Diagnostics Output ...............................................66
Sample of RS232 Sensor Calibration Cycles Output ........................66
Low/High Alarm Relay Responses ....................................................67
High/High-High Alarm Relay Responses ...........................................67
Alarm Conditions - Graphical Representation ...................................68
Alarm and Recorder Diagnostic Outputs ...........................................69
General Technical Data .....................................................................71
Standard Sensor Cable Specifications ..............................................71
Indicating Instrument Configurations .................................................73
Spare Parts Table..............................................................................74

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User notes - 3610 Analyzer

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User notes

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78

tel. ++41 22 / 855 91 00


fax ++41 22 / 855 91 99
6, route de Compois, C.P.212
CH-1222 Vesenaz-Geneva
Switzerland

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