M 140-03 Emulsified Asphalt PDF

Standard Specification for
Emulsified Asphalt
AASHTO Designation: M 140-03
ASTM Designation: D 977-98
AASHTO M 140-03 is identical to ASTM D 977-98 except for the following provisions:
1. All references to the ASTM standards contained in ASTM D 977-98, listed in the following
table, shall be replaced with the corresponding AASHTO standard.
Referenced Standards
ASTM
D 140
AASHTO
T 40
2 . Replace Section 3.1 of ASTM D 977-98 with the following:

3.1 The emulsified asphalt shall be homogeneous. Within 30 days after delivery and provided
separation has not been caused by freezing, the emulsified asphalt shall be homogeneous after
thorough mixing.
3. Add the following footnotes to the end of Table 1 of ASTM D 977-98 as follows:
h
Demulsibili9-The demulsibility test shall be made within 30 days from date of shipment.
' Sieve Test-A percentage of 0.30 is acceptable for samples taken at point of use.
Refer to AASHTO R 5 for typical applications.
TS-2a
M 140-1
AASHTO
Designation: D 977 - 98
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Specification for
Emulsified ~sphalt'
This standard is issued under the fixed designation D 977; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (E) indicates an editorial change since the last revision or reapproval.
This srandard has been approved f i ) r use by a~enciesof the Deparrmenr r?f Defense
1. Scope
1.1 This specification covers thirteen grades of emulsified
asohalt for use in Davement construction in the manner
designated.
2. Referenced Documents
2.1 ASTM Standards:
D 140 Practice for Sampling Bituminous ~aterials'
D 244 Test Methods for Emulsified Asphalts2
3. Requirements
3.1 The emulsified asphalt shall be tested within 14 days of
I This s~cificationis under the jurisdiction of ASTM Committee D-4 on Road

and Paving Materials and is the direct responsibility of Subcommittee D04.41 on
Emulsified Asphalt Specifications.
Current edition approved Dec. 10, 1998. Published March 1999. Originally
published as D 977 - 48 T. Last previous edition D 977 - 97.
Annual Book of ASTM Standards. Val 0403.
TS-2a
delivery. The emulsified asphalt shall be homogeneous after

thorough mixing provided separation has not been caused by
freezing. Emulsified asphalts separated by freezing shall not be
tested.
3.2 Emulsified asphalt shall conform to the requirements
prescribed in Table 1.
4. Sampling
4.1 Samples of emulsified asphalt shall be taken in accordance with Practice D 140.
4.2 Samples shall be stored in clean, airtight sealed containers as specified in Practice D 140 at a remperature of not less
than 4C) until tested.
5. Test ~ e t h o d s
5.1 The properties of the emulsified asphalts given in Table
1 shall be determined in accordance 'with Test Methods D 244.
6. Keywords
6.1 anionic; emulsion; emulsified asphalt; high float; medium setting; rapid setting; slow setting
M 140-2
AASHTO
TABLE I Requirements for Emulsified Asphalt
N a r ~1-S-1H
NWE 2 4 S l
emulsions shall meet the requirements outlined i n D 3910 Standard Practices

h is used for Quick Set Slurry Seal systems.
for Dssign, Testing and Construction o f Slnny Seal..
Rapid-Setting
TYPe
Grade
Tests on emulu'ons:
Viscosity, Sayboil Furol at 77F
(25C). s
Viscosity, Saybon Furol at 122F
(50"C), s
Storage stability test. 24-h, %A
Demulsibility. 35 ml, 0.02 N CaCI,. 96
Coating ability and water resistance:
Coating, dry aggregate
Coating. after spraying
Coating, wet aggregate
Coating, after spraying
Cement mixing test, %
Sieve test, %A
Residue by distilblwn. %
Oil diitillate by volume of emulsion. %
Tests on residue from distillation test:
Penetration, 77F (25C). 1009, 5 s
Dudilty, 77"F, (25C). 5 cmlmin, cm
Solubility in trichbroethylene. %
Float test, 140F (60C). s
RS-1
HFRS-2
rnin
rnax
min
20
100
...
...
...
75
400
...
...
60
...
60
...
...
max
...
55
...
100
40
97.5
MS-1
min
max
...
...
75
400
.
...
...
rnin
rnax
min
20
100
100
...
100
...
...
...
...
...
...
0.10
...
...
...
63
...
...
...
200
100
40
97.5
200
100
40
97.5
1200
...
good
f?r
fair
fair
:
...
0.10
63
...
...
0.10
...
...
...
55
200
100
40
97.5
...
...
...
...
...
Medium-Setting
HFMS-1
Type
Grade
Tests on emulsions:
Viscosty, Saybolt Furol at 77F
(25C). s
Viscosty. Saybolt Furol at 122F
(50C). s
Storage stability test, 24-h, %A
Demulsibilty, 35 ml, 0.02 N CaCI,, %
Coating ability and water resistance:
Coating, dry aggregate
Coating, wet aggregate
Cement mixing test. %
Sieve test. %"
Residue by distillation, %
Oil distillate by volume of emulsion. %
Tests on residue from distillation test:
Penetration, 77F (25C). 100 g, 5 s
Dudility. 77F. (25C). 5 cmlmin. cm
Solubility in trichbroethylene, %
Float test. 140F (6OeC),s
max
min
20
100
...
...
...
HFMS-2h
...
100
40
97.5
1200
200
...
...
...
...
...
100
40
97.5
200
40
40
97.5
90
...
HFMS-2s
100
...
50
...
20
...
...
...
1
...
...
Quick Setting
SS-1
100
SS-1h
rnax
rnin
good
fair
fair
fair
...
0.10
65
100
40
97.5
1200
200
...
40
40
97.5
1200
...
...
...
...
0.10
65
1
...
...
...
200
40
97.5
1200
rnin
rnax
20
100
20
100
...
...
1
...
...
...
0.10
90
rnax
100
good
fair
fair
fair
65
QS-1H
...
...
...
...
65
rnin
0.10
...
...
...
rnax
good
fair
fair
fair
55
65
rnin
good
fair
fair
fair
...
...
0.10
max
...
...
rnin
...
...
max
good
fair
fair
fair
SlowSetting
HFMS-2
min
...
...
...
...
...
...
0.10
0.10
200
...
max
...
good
fair
fair
fair
-.
...
...
MS-2h
max
...
...
...
...
MS-2
rnin
60
...
...
...
...
...
Medium-Setting
RS-2
...
2.0
0.10
57
...
57
...
...
100
40
97.5
...
...
AThis test requirement on representative samples is waived if successful application of the material has been achieved in the field.
2.0
0.10
200
...
NIA
0.10
57
...
40
40
97.5
90
40
40
97.5
90
...
...
-l
-l
The American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connection
with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your
views known to the ASTM Committee on Standards, 100 Barr Harbor Drive, West Conshohocken, PA 19428.
TS-2a
M 140-4
AASHTO

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Standard Specification for

2 . Replace Section 3.1 of ASTM D 977-98 with the following:

Standard Specification for

I This s~cificationis under the jurisdiction of ASTM Committee D-4 on Road

delivery. The emulsified asphalt shall be homogeneous after

TABLE I Requirements for Emulsified Asphalt

emulsions shall meet the requirements outlined i n D 3910 Standard Practices

for Dssign, Testing and Construction o f Slnny Seal..

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