Ba LabMaster E 2518902 200040 - 355 - 06
Ba LabMaster E 2518902 200040 - 355 - 06
Ba LabMaster E 2518902 200040 - 355 - 06
& LabPartner-aw
2518902
200040.355.06
Operating Instructions
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1.
Introduction
2.
3.
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30
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6.
Calibration
7.
8.
9.
10.
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15
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8
9
5.
5
6
10
10
11
12
4.
4
4
Maintenance
7.1. Cleaning
7.2. Sensor Recalibration with Humidity Standards
7.3. Replacing Protective Filters
7.4. Replacing a CM-2 Sensor Unit
7.5. Replacing an Instrument Fuse
Technical Specifications
Troubleshooting
9.1. What is wrong, when....?
9.2. Error message screens
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INDEX
1. Introduction
1.1.
Thank you for having purchased an instrument of the Novasina LabMASTERaw system for measuring water activity. You have opted for a highly
accurate and reliable instrument representing the latest state of the art in
electronics and software design when it comes to highest precision in aw
(water activity) measuring.
To get the most out of all the possibilities of your Novasina LabMASTER-aw
or LabPARTNER-aw, and to guarantee safe, reliable operation, please read
these operating instructions before setting the unit into operation carefully.
Please keep this manual within reach of the installed instrument so that it
will be at hand whenever you need it. If you lose the manual, please contact
your Novasina representative for immediate replacement.
1.2.
Important Notes
Intended use
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2.1.
System Overview
The LabMASTER-aw system has been specially developed for determining
the fraction of free water in food, cosmetics or pharmaceutical products.
This fraction is also known as "water activity" in the foodstuffs industry.
Unfortunately, these days many people still confuse water activity with the
water content of a sample. Measuring the water content of a specimen,
however, is measuring the combined fraction of both bound and free water.
The water content can be determined indirectly, yet non - destructively,
using LabMASTER-aw (see SI Sorption Isotherm)
The fundamental requisite for determining water activity quickly and
with extreme precision is an excellent moisture sensor that reaches
an exact, reproducible measurement over a very wide range (moisture
from 0....100% rF). Novasina has been developing special electrolytic
moisture sensors that stand out for such unique properties for more
than 50 years. The intelligent, resistive electrolytic sensor integrated
into the LabMASTER or PARTNER-aw is based on the latest Novasina
Novalyte Technology, with which one can guarantee such precision
and reproducibility. Thanks this technology an aw-meter as has never
been attained before.
The complete LabMASTER-aw system comprises various modular
components. The system can thus be optimally adapted to the customer
and his requirements.
The components of such a system are essentially as follows:
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2.
LabPartner-aw 1 ... 9
LabMaster-aw
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2.2.
System Architecture
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2.3.
Instrument Overview
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USB output to a PC
RS-232 output to a PC
or external printer
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2.4.
Scope Of Delivery
Novasina LabMASTER-aw BASIC:
AW measuring instrument with precise, temperature - stabilised sample
chamber and additional preconditioning chamber, software with sample
database system, without user administration/management or graphics.
This instrument can only be operated as a stand-alone system. No analysis
programs for PC (Novalog MC) and no cable are included. A connection
to an external RS-232 printer is possible. It is as well possible to expand
the instrument to a higher software level with additional functions at any
time by a option code.
Standard accessories:
Set with 6 humidity standards: SAL-T 11, 33, 58, 75, 84, 97%
50 sample cups
Operating instructions
Novasina LabMASTER-aw STANDARD: (single-channel control)
AW measuring instrument with precise, temperature-stabilised sample
chamber and additional preconditioning chamber, standard software with
sample database functions, user administration/management and graphics.
This instrument can only be operated as a stand-alone system. It can
communicate with a PC-based computer system (required PC-based
software included) over a USB/RS232 interface. An connection to an external
RS-232 printer is possible. It is as well possible to expand the instrument
to a higher software level with additional functions at any time.
English
Standard accessories:
Set with 6 humidity standards: SAL-T 11, 33, 58, 75, 84, 97%
50 sample cups
Operating instructions
Interface RS232 - PC cable 1.8m/D-Sub 9M/9F and USB cable
PC software NOVALOG MC for Win9X/2000/XP/VISTA/ 7
Novasina LabMASTER-aw ADVANCED (multi-channel control)
AW measuring instrument with precise, temperature-stabilised sample
chamber and additional preconditioning chamber, standard software with
sample database functions, user administration/management and graphics.
System extension via bus line to a LabPARTNER-aw possible.
The software for this instrument allows a multi-unit measurement system
with up to 9 LabPARTNER units. But can also be operated as a stand-alone
unit. The instrument communicates with a PC-based computer system over
a USB / RS232 interface and with the LabPARTNER units with a Field
Bus system (required software is included).An connection to an external
RS-232 printer is possible.
Standard accessories:
Set with 6 humidity standards: SAL-T 11, 33, 58, 75, 84, 97%
50 sample cups
Operating instructions
Interface RS232 - PC cable 1.8m/D-Sub 9M/9F and USB cable
PC software NovaLog MC for Win9X/2000/XP/VISTA/ 7
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2.5.
Optional Accessories
Operation manual
Plastic case
for sorption-Isotherm
Special measurement
Stainless steel
substance basket
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For certain use of the equipment, the precision measuring cell of the
LabMASTER/PARTNER-aw must be protected against aggressive vapours.
Novasina offers various protective filter systems for this purpose. Please
consult the corresponding datasheets for Novasina protective filter systems
or contact your Novasina sales partner. Using filter systems can prolong
the service life of the measuring cell considerably. Should you implement
such filter systems, please see to it that they are tested and changed at
regular intervals. Chemical filters, in particular, tend to become saturated
and thus ineffective after they have been in use for a certain time.
3.
3.1.
Packaging / Installation
Novasina precision measuring instruments are supplied in sturdy, specially
lined cardboard packaging with all necessary accessories. Upon receipt, please
check first to make sure everything is present, and immediately notify your
Novasina sales partner if anything is missing or broken. Do not put damaged
or incomplete measuring instruments into operation.
The equipment must be installed in a laboratory on an even surface, avoiding
vibrations, strong heat radiation, air flow and dust.
There must be a perimeter of at least 30 cm of free space around the entire
measuring instrument, since it can momentarily give off great heat.
The temperature controller may generate excess waste heat, depending on
settings, which is dissipated through the vent holes in the housing and by the
built-in fan. The fan is thermostatically regulated. There must be unobstructed
air circulation around and especially at the back of the instrument.
Main fuse
(+ spare fuse)
Mains plug
3.2.
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3.3.
Note: The connector cable, with 1.8 m cable and corresponding plugs,
comes with every LabPARTNER-aw. Make sure the cables are plugged into
the correct place on the back of the LabMASTER-aw and LabPARTNER-aw.
LabMaster-aw
Interface
LabPartner-aw
Interface
Instrument "ID" of a
LabPartner
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Fault
OK
3.4.
Quick Start
3.4.1. System Start
While the LabMASTER-aw System is starting, a greeting text appears
on the display. After about 3 seconds, the display automatically switches
to single-chamber measuring mode. Depending on the LabMASTER-aw
version, BASIC, STANDARD or ADVANCED, the user may need to
identify himself (password) or may be able to commence the measurements
immediately.
Please fill a suitable test sample into a sample cup. Make sure the sample
cup is well filled, but not over the lip. Do not compact the sample medium
under any circumstances. The greater the overall surface of the sample is,
the quicker and more precise the aw measurement will be. Next, place a
product sample in the left chamber (the measurement chamber). Place a
second sample into the pre-conditioning chamber on the right side. Close
the cover and the equilibrium begins to develop. Momentary values of aw
and C are shown on the display.
Samples at very different temperatures from the chamber : to save time,
it is recommended to place the next sample to be measured in the preconditioning chamber in order to minimise the temperature difference.
Pre-conditioning
chamber
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Measurement
chamber
The stable- and analyse function may be started with the Start/Stop
button. The yellow LED ANALYSING flashes. When the value becomes
stable, the green LED lights up. The system send you as well an acustic
signal, if it will be finished by a "peep". If the cover is opened or was not
properly closed, the STABLE function is interrupted and the analysing
function cannot be started!
Start / Stop
View single
"Single
chamber
mode"
View All
Every LabMASTER-aw has three different display modes for the current
reading. These will be referred to below as single-chamber display mode,
summary chamber mode and "graphic mode". Single-chamber mode
only shows the current reading from the selected chamber number. This
can be changed with the software button Select chamber. In summary
chamber display (only for LabMaster-aw "Advanced"), the current readings
of the entire system are shown. At the same time, it can be checked in
this display mode which LabPARTNER-aw (device No.) a LabMASTERaw is communicating with. In the graphic mode (only for LabMaster-aw
"Standard" or "Advanced") the measurement is dispalyed graphically. This
contributes to monitor and optimise the stability parameter configuration.
"Multi / summary
chamber mode"
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View Graph
Graphic
Display
Note : When the instrument is switched on, the last set chamber No. and
the actual aw and temperature values are displayed. You can as well check
the communication status of all other LabPARTNER-aw on the system with
the "summary chamber mode"
The internal controller system will change now the new chamber temperature.
Maybe the rotation speed of the internal fan will be changed part time and
you can hear it a little bit. On the screen you can see, that the temperature
of the actual value will move the direction to the new set temperature. This
takes a little while. During this time, the chamber system must be closed! A
sample or a SAL-T can be inside but the speed of changing will be slower.
Please wait during the temperature stabilisation process.
Note : If you are using a multi-channel system (LabMASTER-aw and at
least one LabPARTNER-aw), select the chamber number before changing
the settings !
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Set the new required chamber temperature (by keyboard) and finish your
settings by pressing the OK soft key. Return to single chamber mode by
pressing ESC or many time the function key "Previous screen".
4.
Measurement analysing
Sample data base
Graphics display
Single-user
Login / Logout
4.1.
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Function keys
LCD multi-function
display
Keypad unit
for data input
Fix functions
keys
4.2.
Selected
chamber
Number
Actual
value
Functions key
and information
Stable
value
Status line : alternating
information
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The system runs a comprehensive function control of all internal modules and
important software components when starting up. After this, the LabMASTERaw tries to establish a connection to any connected LabPARTNER-aw units.
Any errors in the LabMASTER/PARTNER-aw hardware or software are
then shown in an information window on the LabMASTER-aw.
You open the main menu by pushing the Settings soft key.
Selecting a further menu point (e.g. 3) and then pressing the ENTER
(5) soft key brings you to the submenu and the corresponding display
window. Pressing the Previous screen soft key (6) brings you back
one menu level.
.. These soft keys let you move the menu selection up or down
within the current window.
The selection in this case must be confirmed with the ENTER (5)
soft key.
Instead of making a selection with the soft keys, it is also possible to use
the keypad for the navigation through the various submenus. Each menu
point has a pre-allocated number.
Numeric or alphanumeric keypad
change the function of the key
AA, aa, 123 (p, q ,r ,s ,7)
Logout
Delete the last character
Delete the full line
Escape
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In the example given on the left, the Units function has temporarily
been allocated to button 2 on the keypad. If this button 2 is pressed, the
function is the same as selecting the row Units with the soft keys (3 +
4) and then pressing the ENTER soft key (5).
4.2.3. Graphic Display
The graphic display contributes to monitor and optimise the stability parameter configuration. Further it allows to follow easily the measurement
stabilisation. The graphic display is available with the versions "Standard"
and "Advanced".
4.2.4. Saving of Stable Data
The LabMaster-aw saves automatically the stability data of the last
10 measurements. The display of these values can be activated in the
measurement mode by pushing the button [+/- / History] . Additionally the
last 10 stable values of each sample database are stored.
Following parameters are displayed:
Column 1: measurement chamber
Column 2: results of "Limits" if activated; "PASS" oder "FAIL"
Columns 3 & 4: measurement values at the time of stability
Columns 5 & 6: date, time of measurement
Note : The function [Clear] cancels the displayed values.
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4.2.5
Stable Indicator
What is a stable indicator? Well, it is not the same as a predictor which
"predicts" the residual measurement time in minutes and seconds. It is more
a tool which takes the previous measurement history of the sample into
the account and graphically outputs the progress. This can lead to the fact
that the bar is getting less filled even if the measurement is developped in
case the establishment of the equilibrium is interrupted by the evaporation
of additional free water coming from the inner part of the sample.
How is it working? In simple terms, the system observes the change of the
measurement value within a programmable time. The maximal allowed
deviation in aw is 0.001aw. The programmable time is the one which can
be set as "stability observation time" in minutes
The progress bar indicates the already reached stability. The programed
stability parameters are displayed in the status bar.
Thus, as closer the deviation comes to 0.001aw within the programmed
stability observation time frame, the more filled the bar will get.
4.2.6
Quick Mode
The quick mode offers the opportunity to get a rough idea about the sample's
water activity within a short time. By activating this mode, all stability times
will be set to the lowest possible level of 1 min.
Activation of Quick Mode:
Press the "QUICK" labeled key which is located on the main key board
-> A pop-up window appears with a warning regarding the quick mode.
Please read carefully through as the quick mode is not suitable for all
measurement purposes.
Note: Once the measurement is done with the quick mode, the "Analyzing"
LED (yellow) is blinking faster for visual indication.In addition, "Stab. obs.
time: QUICK" is displayed in the status bar.
4.3.
If measurement was done with the quick mode, it is stated in the measurement protocol as "QUICK" where "Stab. obs. time is mentioned.
System settings
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Note: This feature is only available in firmware version higher than V3.00
All settings are only ever related to the currently selected measuring
chamber with the corresponding number, which is shown at the top right
of the screen within the Select chamber soft key.
0: Power
0 = OFF for one selected LabPARTNER-aw
or 1 = ON default setting when a system is configured.
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So that not all settings need to be changed individually for each test sample,
all necessary parameters set for a test sample can be saved under a name
in a database and allocated to a measuring chamber at any time. A database
with up to 10 possible test sample data is available for this purpose (see
chapter 4.3.2. sample database). As soon as a parameter is subsequently
changed, the link to the sample database is unmade and the display shows
OFF to confirm this. If a parameter needs to be changed generally for a
sample, this should be done in the sample database (see chapter 4.3.2.).
2: Temperature
3 : Stab.observation at start
With the setting "Yes" the "Stab. observation time at start" is queried
at each measurement start. The stability parameter for aw can be set in
minutes. This is useful when various samples are measured, which require
different stability parameter settings.
If a "LabPartner-aw" is connected, this query is performed on its display.
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In this menu point alarm thresholds can be set. The permitted aw-range
can be set, in which a sample is judged as good (Pass). This monitoring is
activated under "Enabled" - "Yes". A "Lower limit" and "Upper limit" can
be set. If the thresholds of the permitted aw-range are crossed, the warning
window is displayed (RESULT FAIL).
7 : Graph
(graph settings )
In this menu point the settings for the graphic display can be made. Available
only for the versions LabMaster-aw "Standard" and "Advanced". The
function "Range" configures the aw-range of the y-axis. With the function
"Time/div" time scale (x-axis) can be set. During the recording of the graph
these two axis are shifting automatically, in order to make the actual values
visible.
The parameter "Auto stop after stable" is used to stop the recording after
a certain time after reaching the stability value. So the stability point is not
shifted out of the diagram window in case the measurement is continuing.
8: Calibration...
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9 : Info
Under this menu point, system information on the LabMASTER/PARTNERaw (depending on selected chamber) and sensor information can be called
up. Changes cannot be made.
Instrument type and serial No. of the instrument
Hardware revision level:
The Sample database is a powerful tool for a quickl and correct setting of
all necessary parameters of a measurement relating to a type of sample. Up
to 10 different samples can be defined. The name of the sample database
can be chosen freely. A Default sample is already created by default.
This can be overwritten, added to or deleted as required.
To create further sample data in the database, please select a free table
space by pressing the soft key 0-9 or the corresponding number on the
keypad. After this, the system requests you to enter a suitable name (confirm
with ENTER). Now, the appropriate parameters for the sample can be
entered and finalised by pressing the ENTER key.
Sample data is modified in the same way as it is created.
The following parameters must be entered as sample data:
Obvious name of the sample: (max. 21 characters)
Set chamber temperature for the sample: 0....50C
Set "Stab. observation time aw" for the sample: 1....30 min
Set "Stab. observation time temp" for the sample: 1....30 min
Set "Limits" for the sample: Upper and Lower limit
Set graphic settings for the sample - "Graph"
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The last 10 stable values from each database are stored. Push
[+/-] in the measurement mode and select the database you want to display.
Epson TM-U 220 (needle printer) or Seiko DPU 414 (thermo paper
printer)
--> (connection only by RS-232 interface)
Protocol printout
Epson TM-U 220
If you have connected by the RS-232 interface a printer to the LabMasteraw system and you have configured the device following chapter printer
settings the system prints out the results automatically as soon as a stable
value is reached. Actual measuring values of all connected measuring
chambers are printed by pushing the button 0....9 on the LabMaster-aw
during the standard operation mode.
In the Stable protocol values are printed out that were valid at the time
of stability. Attention: on the protocol the user name who is momentary
logged in will be printed out as well.
In the Actual protocol values are printed out that were valid at the
start of the printing process.
Note : If "Limits" are set also the "Sample limits" and the result (Pass/
Fail) are printed on the protocol.
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Introduction
From the software version V.1.05 C003 the LabMaster-aw system has
the ability to print out information about measurements and calibration on
a printer. The software supports the protocol standard ESC/P. Novasina
recommends following printer models:
(function extensions)
After the connection of the main supply and printer cable (RS-232 null modem cable), all printing functions have to be activated by the LabMaster-aw
software. This shall be done as following:
Communication:
Settings System settings Communication, activation by selecting the menu point Printer. For de-activation please select the menu
point PC (selection for a connection with the NovaLog MC software).
Printer communication:
Settings System Settings Communication
Printer-
configuration. This menu point is only visible, if the
Device is set on Printer.
The following parameters can be selected:
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Laboratory:
Set the laboratory or company name, which should be printed on the
protocol.
Auto stable printout:
If setting is On the measured values are printed out automatically
after reaching the stability (as soon as the green LED is flashing).
Line feed, form feed:
Selection of the number of empty lines after the protocol. With that
function you can define the right position of the paper tear off line. If
there is no number input (delete 0 FF), a one page feed will be
performed.
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"Actual" Protokoll
"Single cal.point"
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"Stable" Protokoll
Printer settings
ONLY VALID FOR thermo paper printer !!
- SEIKO DPU-411 or
- DPU414
Dip SW-1/1
(OFF)
Input = Serial
Dip SW-1/2
(ON)
Printing Speed = High
Dip SW 1/3
(ON)
Auto Loading = ON
Dip SW-1/4
(OFF)
Auto LF = OFF
Dip SW-1/5
(ON)
Setting Command = Enable
Dip SW-1/6 (OFF) Printing
Dip SW-1/7
(ON)
Density
Dip SW-1/8
(ON)
= 100%
Dip SW-2/1
Dip SW-2/2
Dip SW-2/3
Dip SW-2/4
Dip SW-2/5
Dip SW-2/6
Dip SW-2/7
Dip SW-2/8
(ON)
(ON)
(ON)
(ON)
(ON)
(ON)
(ON)
(OFF)
Printing Colums = 40
User Font Back-up = ON
Character Select = Normal
Zero = Normal
International
Character
Set
U.S.A.
Dip SW-3/1
Dip SW-3/2
Dip SW-3/3
Dip SW-3/4
Dip SW-3/5
Dip SW-3/6
Dip SW-3/7
Dip SW-3/8
(ON)
(ON)
(ON)
(OFF)
(OFF)
(ON)
(ON)
(ON)
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Dip SW-3/1 through Dip SW3/8 of the Seiko DPU-414 printer have to be
set following the table above. The settings of all other switches are just a
recommendation.
Each LabMASTER-aw has an internal clock and calendar function that continues
to run even while the unit is switched OFF. By default, the system is set to
GMT (Greenwich Mean Time). This parameter should be set to local time and
current date after the first starting up of the system. The easiest way to do this
is with the keypad beside the display. Please separate day, month and year or
hours, minutes and seconds with a dot [.] and conclude the input with YES.
The displayed date is in the European format with the pattern:
DD.MM.YYYY (e.g. 17 April 2010 = 17.04.2010)
The displayed time is in 24h format with the pattern: hh.mm.ss
(e.g. 16:45:50 = 04h PM, 45min, 50sec.)
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1 : Users...
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Note: Use only numerical characters for the password. This simplifies the input
and is less likely to be forgotten!
Defining a user
To define a new user in the system, select a free space in the table (e.g. No.
3) using the soft keys or the keypad.
Then, you can enter the new user name and finalise it with ENTER. Next, you
will have the option of allocating different rights (see User Rights below) for
the respective user. The status (active = YES ; inactive = NO) is shown. This
action is terminated with the key Previous screen.
User Rights
The user management system gives the administrator the option to allocate
each entered user different rights. The table below gives an overview of the
currently possible rights. These might be extended in future. Please consult
the current user management system on the display while allocating the rights.
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Deleting a User
A user can be deleted from the administration by deleting the user name. There
must be at least one Administrator User defined at any time, however,
otherwise the system will be locked completely. Only administrator rights allow
the deletion of users or passwords.
User Password
When first entering a new user, the password must be entered twice time (to
confirm). This helps to make sure the password is entered correctly.
The administrator can see a forgotten user password in the Management
system. (see User -> 1: Password)
2 : Units...
Temperature
C or F
Date format
: DD.MM.YYYY, MM.DD.YYYY
or YYYY.MM.DD
There are three different date displays to be selected.
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Examples
: DD.MM.YYYY = 03.05.2010
MM.DD.YYYY = 05.15.2010
YYYY.MM.DD = 2010.05.27
3 : Buzzer...
(3 May 2010)
(15 May 2010)
(27 May 2010)
The volume and duration of the acoustic signal upon attained stability can be
set with this.
Volume
Stable buzz duration :
4 : LCD Settings...
:
noise 0....9 : 0 = low
0...120 sec. : 0 = OFF
9 = high
The contrast and backlighting can be individually adjusted for optimum screen
readability.
Contrast
Backlight
:
:
0....9
0....9
: 0 = OFF
Since the backlighting is a LED lighting, it is always switched on. This does not
affect the service life of the instrument.
5 : Communication..
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If the Printer device is set, there is the possibility to print out a single or several
calibration points by pressing the printer function button under "Display cal.
points".
Should, for example, the measurement data from the LabPARTNER-aw with
measuring chamber No. 3 be printed out over NovaLog MC or the Printer, it
can be activated using key "3" (or selection by arrow keys).
Under menu point Data format you can either select a single channel over
Novalog32 (Chamber x) or you can select the NovaxCom format for the new
software NovaLog MC.
This function resets the entire system (LabMASTER-aw and, where applicable,
also LabPARTNER-aw) to the original status upon delivery. This function can
only be called up by the user with administrator rights. All settings of the user
management system will be irretrievably lost. Only the serial and software
licence numbers (BASIC, STANDARD or ADVANCED) and the data based
on the sensor, such as adjustments, will be retained.To prevent unintentional
deletion, it must be confirmed twice whether all settings shall really be reset
to default settings or not. The first query must be answered with Yes and the
second with NO in order to execute this function.
This menu point contains general information on the hardware and software of
the LabMASTER/PARTNER-aw.
Instrument ID
Hardware
Firmware
:
:
:
LabMaster-aw
L001
V.01.07. C003 (date : 08/05)
This information is very important for the service centre to be able find out
function errors. It also allows any system updates to be retraced. Please keep
this information at hand whenever contacting your service centre.
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7 : Info
5.
Fill the sample cup with the material to be measured. The sample cup must
be completely clean and dry (rub dry with tissue paper if necessary)! Make
sure, the sample is free from any other impurity. Ideally, always use a fresh
cup and dispose of it after use.
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Important ! Fill the sample cup to approximately 2/3 with the product to be
measured. Do not overfill the sample cups ! Bulkier material must be suitably
crushed or manually cut into small pieces. This makes the measurement faster
and more accurate. Products consisting of several layers, or an outer coating,
must also be crushed (e.g. confectionery products). Prolonged hand contact
with the product must be avoided (falsification of measured value!). A grinder,
if used, must not warm up the product.
After sample preparation always close the cover of the sample cup.
Open the instrument cover and check the chamber inside. This must be
clean an absolute dry.
Insert the open sample cup containing the sample into the measuring
chamber (left) and close the cover immediately. Press the cover completely
down, otherwise the anlaysing function does not start.
Note : To gain time for measuring the next sample while measuring the current
sample, place the next sample cup (with its plastic cover closed!) into the
preconditioning chamber (right chamber) to reach thermal equilibrium. This
accelerates the following measurement.
Selected
chamber
Number
Actual
value
Stable
value
Status
line
28
Displayed values
The Novasina LabMASTER-aw continuously measures the water activity
(aw / %RH) and the temperature (C/F) and displays the momentary values
with bigger letters on the screen. If an analysing of a probe will be finished, the
system will fix the result. This result will be presented with an inverted display
on the lower part of the screen. The upper part will show the actual value of the
measurement at any time. So you can see after a while how good the stability
parameter are adjusted for this probe.
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As soon as the measured values are considered stable, the buzzer sounds and
the green LED Stable lights up. The display now also permanently shows aw,
temperature and elapsed time at that moment of equilibrium. This information
disappears as soon as the cover is opened or the <Start/Stop/Stable> key is
pressed again.
Switch OFF
the buzzer!
If you want to measure the next sample, take it from the pre-conditioning
chamber, open the cup (remove its cover) and place it in the measuring
chamber. The following sample may be put into the pre-conditioning space
before closing the instrument cover.
Note : Leave the instrument switched on so that it is ready to measure at any
time. The power consumption is very low.
If a product sample has a greatly different temperature from that of the chamber, a
temperature gradient inside the chamber may retard the temperature equilibrium,
thus also the aw value. The instrument measures the different temperatures inside
the chamber very accurately and can detect a to big gradient of temperature. It
may then display the following text: "reaching stability is retarded because
of a too large temperature difference inside the measuring chamber".
Then you need to wait till the temperature of the sample will be the same as
the chamber temperature. After that start the analysing again.
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English
Note : If heavy concentrations of alcohol, glycol, glycerine, acetic acid etc. were
present in the sample, leave the cover open to let the cell and its protection
filter recover in the air. Thereby the instrument respectively chamber should
be powered off.
5.2.
English
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Note : If possible, always leave the instrument switched ON. The integrated
heating system protects the sensor from saturation and the instrument is
always ready for the next measurement. At the same time, the next sample
can be preconditioned to the correct temperature. Consider that the power
consumption is extremely low.
English
5.4.
5 (= 5 minutes)
1 minute....30 minutes
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Recommended stability
Examples of products
Cheese
Butter
Sunflower oil
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10
Recommendation : There are two ways to found the optimum of the stability
English
The temperature stability observation time may also be changed from the factor
5 set by Novasina to a higher factor for products with a temperature greatly
different from that of the chamber (e.g. chilled samples).
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Definitions :
The WATER or MOISTURE CONTENT is the weight in % of the total water
in a product. Test methods are e.g. Karl Fischer Titration or drying balances.
The WATER ACTIVITY, aw, is the free water the only value that gives
information on the micro-biological safety of a product and especially important
for foodstuffs and drugs.
In materials, it is also called the RELATIVE EQUILIBRIUM HUMIDITY (% rh).
The range of 0.00....1.00 aw corresponds to 0....100% rh.
The relationship between moisture content and water activity is the SI, Sorption
Isotherm curve, which is product and temperature specific. An absolutely
constant temperature during all measurements is therefore very important!
English
5.5.
Examples of SI-curves:
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33
Measure the precise weight of the special metalic sample cup including the
transprotation glass container. This is important for the net weight definition
after changing the weight following the humidification process of the probe.
Preparing a probe : Fill the special metallic sample cup to 2/3 with the crushed
probe (in order to get the maximum possible surface). Keep your probe always
inside the glass container when you are not using it for measurments inside
the chamber or for transportation.
English
Adsorption curve
In order to start, the substance must be dry, so first it must be totally desiccated
in an oven (e.g. 2 hours at 102C, depending on the material).
1. Close the glass container before taking it out from the drying oven.
2. Weigh the probe afterwards with the closed weighing glass on a precision
balance and define the net weight of the probe.
3. Put first the SAL-T 6 in the deeper measurement chamber and afterwards
the metallic sample cup containing the cooled sample over it and close the
chamber.
sample), write the actual aw value. If you wait longer, the aw value as well
as the weight become higher, moving along the SI-curve. Therefore it is not
necessary to wait for the equilibrium inside the chamber.
5. Take our the probe and put it immediately in the glass container.
6. Weigh the probe again and write the net weight in a table and calculate the
difference between the weights before and after humidification.
7. Put the next SAL-T into the measurement chamber and perform the same
operation at point 2, 3 etc. up to the SAL-T 97 humidity standard.
Based on the acquired data you can define and print the "Adsorption curve"
for a specific product on a paper or Excel program! To determine now the
moisture content of your sample, it is only necessary to measure the aw-value.
The actual moinsture content can be read out over the soprtion isotherm curve.
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Desorption Curve
This is in princple the inverse part of an adsorption curve. The substance must
be more humid when starting to weigh (to be safely on the desorption curve to
avoid SI-hysteresis mistakes), so the first salt to use is SAL-T97. Upon reaching
a value well above 0.9, SAL-T90 can be placed in. After about one hour or
more, note the aw value and weigh the substance. Upon waiting longer, the
aw value as well as the weight are lower, moving along the SI-curve, so the
waiting time is not critical.
After that, place in SAL-T75, down to SAL-T6. Then, after totally drying the
substance in the oven, the net (dry) weight is known and all points can be plotted.
How to proceed :
1. Weigh the tare (empty substance basket and weighing glass)
2. Lift up the cup with a screwdriver; push the deeper cup into place
3. Place in the first SAL-T standard
4. Place basket with substance on top
5. Now close the cover and select the desired chamber temperature
6. Wait until the chamber temperature is reached, then wait for equilibrium
English
measurement chamber
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Example
Doing a Sorption Isotherm curve (adsorption) of a biscuit:
: 25.0C.
: 0.087aw,
: 0.290aw,
: 0.523aw,
: 0.749aw,
English
Greater humidity was not of interest in this dry biscuit case. With these
5 points, a rough SI curve can be drawn.
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6. Calibration
English
Note : Define a standard quality process for your workflow and also define a
standard test procedure for your LabMASTER/PARTNER-aw system.
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37
6.3.
6.4.
Calibration Procedure
The electrolytic sensor can be verified at any time by using the Novasina SAL-T
standards which are included in the delivery or which have been bought through
the local Novasina distributor. If verification fails, a calibration can be performed
in an easy way. These reusable standards generate defined and reproducible
humidity, respectively aw-values. Please contact the local representative if you
feel unsure, how to handle the SAL-T standards correctly or feel uncertain if
the existing ones are still in good shape.
Note:
The calibration values will be stored in a small memory which is located on
the sensor board itself. It is not required that a calibration is performed at all
available calibration points. Perform a two-point calibration with one point below
and one above of the normal measurement range (bracket calibration).
English
For example: Your samples are always around 0.700aw. It is sufficient if you
use the 58%rH und die 75.%rH SAL-T standards for calibration. If verification
is requested, calibrate at 58%rH and 84% rH and use the 75%rH SAL-T standards for verification.
6.5
Shake all SAL-T standards twice a month for one minute, nevertheless if you
have used them or not. There is no need to take it out of the plastic container.
Always store the standards in the plastic container (closed cover) and not
exposed to direct sunlight.
Do not expose the salt tablet to environmental air for longer than necessary;
thus, put it back if calibration has been finished at the particular point.
Please always double-check, if the SAL-T standards below 33%rH contain no
or just few water and all the others are present as slurries (salt/water mixture).
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Chem.
symbols
20C
25C
30C
SAL-T / 4
SC-4
white
CsF (>25%)
4.3
3.8
3.4
3.0
SAL-T / 6
SC-6
Xn
white
LiBr
6.9
6.6
6.4
6.2
SAL-T / 11
SC-11
Xn
white
LiCl
11.3
11.3
11.3
11.3
SAL-T / 33
SC-33
--
blue
MgCl2-6H2O
33.3
33.1
32.8
32.4
SAL-T / 53
SC-53
green
Mg(NO3)2-6H2O
55.9
54.4
52.9
51.4
SAL-T / 58
SC-758
--
white
NaBr
60.7
59.1
57.6
56.0
SAL-T / 75
SC-75
--
purple
NaCl
75.6
75.5
75.3
75.1
A/B
SAL-T / 84
SC-84
--
white
KCl
85.9
85.1
84.3
83.6
SAL-T / 90
SC-90
white
Ba(Cl)2-2H2O
90.9
90.5
90.1
89.9
SAL-T / 97
SC-97
--
yellow
K2SO4 (>20%)
97.9
97.6
97.3
97.0
Lit :
6.7
6.8
Menu calibration
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English
Type of
Hum.check
If the sensor is password protected, enter it with the help of the displayed
keyboard (see chapter 8.7).
Important:
There is a default password (8808) installed from factory.
6.9
English
6.10
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LabPartner
interface
6.11.
USB interface
RS-232 interface
The information comes over the line in a continuous data string from the
LabMASTER-aw system to the Novasina DLL (software part inside your
operating system) to the Novalog32 software. The data string can be as
well used for other software implementations. For example for a connection
to a production planning system (called PPS). Any string has a structure
of 23 characters.
1
2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21
22 23
Parameter T T
Example
2 5 . 0 C 8 3 . 5
%
D
6
D
1
T:
Temperature in C
F:
D:
C:
L:
D C
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English
Position
7. Maintenance
7.1. Cleaning
Caution ! Before cleaning switch OFF the Novasina LabMASTER-aw
anddisconnect it from the mains.
Use a dry smooth cloth to clean the housing of the Novasina LabMASTERaw or a LabPARTNER-aw. Use a mild cleaning agent, if required. Make sure
no water is entering the housing or the connectors. Make sure the cleaning
agents contains no alcohol and that it is not aggressive. Air the measuring
chamber after the cleaning during several hours as otherwise the sensor might
be damaged. For the outer housing area you can use damp smooth cloth with
non aggressive, water based solvents. In any case the device shall be dried
with a dry and clean cloth. Assure that no liquids can penetrate the instrument
housing and also that the back sockets are clean from any liquids and humidity.
Caution ! Please do NEVER clean the sensor CM-2! The sensor is a very
sensitive element with a chemical filter protection on the top. If you blow
or touch the filter with a mechanical part or if you try to clean it with any
cleaning products, the sensor might be damaged!
7.2.
English
At the beginning check the instrument monthly. Increase then the interval
period step by step depending on the results of the precedent inspection
measurements.
Check the nearest measurement points before and after the measurement
of critical products using the SAL-T standards.
Check the usual measurement range if the instrument utilisation has been
interrupted for several day using the SAL-T standards.
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7.3.
->
->
->
->
2ppm
2ppm
3 ppm
300 ppm
eVC-21 filter :
Chemical filter: protects against short-chained organic acids as acetic and
formic acid and other carboxylic acids (butyric acid etc) and oxidizing agents
as hydrogen peroxide and chlorine and as well againts diluted sulfur dioxide
eVC-26 filter :
Chemical filter : protects against various substances as nitrogen oxides,
amines, aldehyde solvents, aromatic hydrocarbons, oil vapours, fine dust
particles.
Redox filter :
Chemical filter : protects against volatiles containing primary and secondary
alcohols (attention, ethanol is an exception, eVALC filter or special alcohol
cell has then be used), gylcerin, glycols, aroma, perfumes, flavours etc.
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English
Attention !
Defective or wrong mounted filters do not fullfil their function and provide the
risk of instrument or sensor damage. Such filters must be replaced immediately.
English
Certain aggressive vapours may also influence the measurement result. Exactly
for that reason, the use of an appropriate protection filter is highly recommended.
A combination of 2 filters may also be used for overall protection (e.g. eVC-21
and eVALC-1).
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7.4.
Switch off the instrument and disconnect the mains from the system.
Open the instrument lid, where you have access to the measurement head
inside the lid.
Remove the 3 screws (tool is inside the SAL-T set), carefully pull out the
measuring block (NEVER let drop this unit on the instrument table).
Remove the two sensor unit screws on the backside of the measuring
block.
Push the new CM-2 unit in its position and assemble in the opposite manner.
Set the measuring block back into the instrument lid in the right place (there
is only one position possible to click in).
Screw in the last 3 screws of the measuring block (don't fix the screws too
tight).
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45
English
7.5.
Pull out the mains cable to have access to the fuse compartment.
Replace a defective fuse by one of the same type (1 spare fuse included)!
Attention ! Normally a fuse does not blow without any reason. Determine
absolutely the possible cause of the fuse blow before you operate the instrument
again.
English
fuse holder
20 x 5mm
230V / 6.3 A
incl. 1 pc spare fuse
main cable
115/ 230 V AC
46
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FUSE 20x5mm
1 x 6.3 AT
Technical Specifications
General
Mains supply
:
90260V, 50/60Hz
LabMASTER-aw
:
Fuse: 6.3 A FST (slow blow), 1 spare fuse
LabPARTNER-aw
:
Fuse: 6.3 A FST (slow blow), 1 spare fuse
Power consumption
:
max. 65 W per instrument
(after temperature equilibrium 15 W)
Permissible ambient
Temperature range
Humidity range
Surface area (W x D)
Weight
Protection class
Temperature controller
Temperature setting range
Accuracy of control
Max. cooling in respect of
ambient temperature
Max. deviation
:
:
:
:
:
545C
5...95%rH not saturated !
26 x 44 cm (LabMASTER and PARTNER-aw)
10 kg
(depends on the additional accessories)
IP 21
:
:
050 C
> +/- 0.1C
:
:
English
8.
Resolution
Repeatability
Temperature sensor accuracy
Temperature sensor resolution
:
:
:
:
0.001 aw
0.002 aw
0.3 C
0.1 C
Interface
USB / RS-232
:
USB 1.1
RS232, Baud rate 9600, 19200 ASCII
signs
LCD illuminated display
:
115mm x 86mm, 320 x 240 dot matrix LCD
LabMASTER-aw with LED backlight
LCD illuminated display
:
60mm x 17mm, 2 x 30 character orientated
LCD
LabPARNER-aw with LED backlight
Level of sound
Noice level is lower then
< 68 dBA
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9. Troubleshooting
English
Cooling power of the instrument is at 1. The abient temperature around the instrument is too high.
limit and nevertheless, temperature
2. Chemical reaction occured within the sample (producing heat)
of chamber is not stable
3. The internal cooling unit is not perfoming correctly
Visibility of Readings in the LCD
screen is very low
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If any error message appears on the LabMaster-aw screen, please proceed as follows:
Hardware-Errors
error report
error description
needed action
"PELTIER Driver!"
"Fan!"
"Temp control (temp gauge)!"
"Humidity sensor
file system!"
"Humidity Sensor
capability!"
"Capability Firmware!"
"CRC U-Settings!"
EEPROM destroyed !
"Humidity Gauge
(analog)!"
"Humidity system!"
"BUS!"
"CRC F-Settings!"
content
user
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settings
English
*
*, Check the cabling of the
LabPartner-aw
49
error report
error description
needed action
1) press "OK"
2) enter the licence-code under
"System settings" ...->"Set options code". The code is stated
on the licence-certificate or on
the sticker on the bottom of the
instrument.
This point does not apply for the
LabMaster-aw "BASIC"-version.
3) set all settings new (date, timet,
"user" account, ...)
error report
error description
needed action
"Fatal Error"
Fatal Error
English
Several errors
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English
0 off
0 Date
1 on
1 Time
1 Load from database
1 Users 0 to 9 user accounts
1 Sample database
0 Name
0 to 9 data base 1 Password
_ Dont load from file (off)
0 to 9 Sample Database
2 Administrator
0 ....(e.g. Bread white)
3 Permit Calibration
2 Temperature
4 Permit edit sample database
(0 to 50C) / (32 to 132F)
0 Name
5 Permit chamber settings
3 Stab. obs. time at start
1 Temperature 2 Units
(Yes / No) 2 Stab. Observation time aw
4 Stability parameter aw
3 Stab. Observation time C
0 Humidity (aw/%RH)
(1 to 30 min)
4 Limits
1 Temperature (C/F)
5 Stability parameter temp
5 Graph
2 Data format (D/M/Y; Y/M/D; M/D/Y)
(1 to 30 min)
3 Buzzer
6 Limits
0 Volume (0 to 9)
0 Enabled (Yes/No) 1 Stable buzz duration (0 to 120 seconds)
1 Lower limit
2 Upper limit
4 LCD settings
7 Graph
Graph settings 0 Contrast (0 to 9)
8 Calibration 1 Backlight (0 to 9)
0 Display calibration points
5 Communication
0 to 10 calibration points
1 Clear calibration points PC
1 Data format(PC) ... NovaxCom
2 Calibrate
0 Device
0 to 9 Novalog 32 (Chamber x)
3 Warning next cal.
Printer
1 Printer configuration ...
4 Set sensor password
0 Laboratory (name)
1 Auto stable printout (on/off)
9 System info 2 Line feed, form feed (0 to 99)
6 Reset to factory settings
0 System info chamber
7 Info
1 System info sensor
8_Set option code
0 Chamber settings
2 System settings
0 Power
0 Set date, time
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English
Notizen/Notes/Notes
52
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The Novasina team would like to thank you for your confidence and hope you will enjoy
and obtain successful measurements with the world leader instrument LabMaster-aw
for high performance quality measurement of water activity and its manifold options.
You have now the powerfullest water activity meter with outstanding options, simple
handling and best reproducability for your special application in quality measurements.
In case of any further questions, Novasina and its agencies will be happy to advise you
at any time.
your Novasina team
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