PET Syllabus

ANNA UNIVERSITY, CHENNAI
UNIVERSITY DEPARTMENTS
CHOICE BASED CREDIT SYSTEM
B.TECH. PETROLEUM ENGINEERING AND TECHNOLOGY
PROGRAMME EDUCATIONAL OBJECTIVES (PEOs) :
I. To inculcate in students, a professional and ethical attitude, effective communication

skills, teamwork skills, multidisciplinary approach, and an ability to solve problems
encountered in petrochemical sector
II. To make the students conversant with oils and their properties, principles of chemical
analysis and preparation of chemicals
III. To acquaint the students with the standards for the analysis of petroleum products
IV. To give them an opportunity to gain knowledge on various reaction mechanisms
V. To help the students understand the theory, instrumentation and applications of
analytical equipments used in industries for testing the quality of petroleum,
intermediates and products
VI. To make them learn basic rock and fluid properties relevant to petroleum reservoirs
VII. To teach the students to solve chemical engineering problems using C and MATLAB
and other computational tools
VIII. To given an introduction to the students on control systems along with instrumentation
PROGRAMME OUTCOMES (POs):

On successful completion of the programme,
I. Graduates will be able to demonstrate their knowledge professionally and shoulder

ethical responsibilities
II. Graduates will be capable to design experiments, analyze and interpret data
III. Graduates will be able to meet the world's ever-increasing demand for hydrocarbon fuel,
thermal energy, and waste and pollution management
IV. Graduates will gain a knowledge of the basic principles involved in different chemical
synthesis and will be able to apply them in chemical industries
V. Graduates will have the capacity to choose a proper measuring instrument for a
parameter to be measured
VI. Graduates will have a knowledge of different analytical techniques and shall apply them
to analyze chemical and petrochemical products
VII. Graduates will understand the characteristics of source and reservoir rocks
VIII. Graduates will become familiar with environmentally sound exploration, evaluation and
recovery of oil, gas and other fluids in the earth
IX. Graduates will have the ability to solve chemical engineering problems.
X. Understand the pre requisites of control strategies and the mechanism of advance
control systems
1
Programme Programme Outcomes
Educational PO1 PO2 PO3 PO4 PO5 PO6 PO7 PO8 PO9 PO10
Objectives
I    
II  
III   
IV  
V  
VI  
VII 
VIII 
2
ANNA UNIVERSITY : : CHENNAI 600 025
UNIVERSITY DEPARTMENTS
B. TECH. PETROLEUM ENGINEERING AND TECHNOLOGY
R – 2015
CHOICE BASED CREDIT SYSTEM
CURRICULA AND SYLLABI I - VIII SEMESTERS
SEMESTER I
S.No COURSE COURSE TITLE CATE CONTACT

L T P C
CODE GORY PERIODS
THEORY
1. HS7151 Foundational English HS 4 4 0 0 4
2. MA7151 Mathematics – I BS 4 4 0 0 4
3. PH7151 Engineering Physics BS 3 3 0 0 3
4. CY7151
Engineering Chemistry BS 3 3 0 0 3
5. GE7151 Computing
ES 3 3 0 0 3
Techniques
PRACTICALS
6. BS7161 Basic Sciences
BS 4 0 0 4 2
Laboratory
7. GE7161 Computer Practices
ES 4 0 0 4 2
Laboratory
TOTAL 25 17 0 8 21
SEMESTER II

L T P C
CODE GORY PERIODS
THEORY
1. HS7251 Technical English HS 4 4 0 0 4
2. MA7251 Mathematics – II BS 4 4 0 0 4
3. PH7257 Physics of Materials BS 3 3 0 0 3
4. CY7255 Chemistry for
BS 3 3 0 0 3
Technologists
5. GE7152 Engineering Graphics ES 5 3 2 0 4
6. CY7256 Organic Chemistry BS 3 3 0 0 3
PRACTICALS
7. CH7261 Chemical Analysis
BS 4 0 0 4 2
Laboratory
8. GE7162 Engineering Practices
ES 4 0 0 4 2
Laboratory
TOTAL 30 20 2 8 25
3
SEMESTER III

L T P C
CODE GORY PERIODS
THEORY
1. AS7301 Fluids and Solid
PC 4 4 0 0 4
Operations
2. AS7302 Petroleum Chemistry PC 3 3 0 0 3
3. Spectroscopic
AS7303 Techniques for PC 3 3 0 0 3
Petroleum Engineers
4. Principles of Electrical
EE7254 and Electronics ES 3 3 0 0 3
Engineering
5. GE7153 Engineering Mechanics ES 4 4 0 0 4
6. MA7357 Probability and Statistics BS 4 4 0 0 4
PRACTICALS
7. Electrical Engineering
EE7312 Laboratory for ES 4 0 0 4 2
Technologists
8. Fluid Mechanics and
AS7313 Mechanical Operations ES 4 0 0 4 2
Laboratory
TOTAL 29 21 0 8 25
SEMESTER IV

L T P C
CODE GORY PERIODS
THEORY
Chemical Engineering
1. AS7401 PC 4 4 0 0 4
Thermodynamics
2. AS7402 Industrial Stoichiometry ES 3 3 0 0 3
3. AS7403 Reservoir Engineering PC 3 3 0 0 3
4. ME7251 Basic Mechanical
ES 3 3 0 0 3
Engineering
5. Open Elective I* OE 3 3 0 0 3
PRACTICALS
6. AS7412 Organic Chemistry
Laboratory for
BS 4 0 0 4 2
Petrochemical
Engineers
7. ME7262 Mechanical Engineering
ES 4 0 0 4 2
Laboratory
TOTAL 24 16 0 8 20
*Course from the curriculum of other UG Programmes
4
SEMESTER V

CODE GORY L T P C
PERIODS
THEORY
1. AS7501 Heat and Mass Transfer
for Petrochemical PC 4 4 0 0 4
Engineers
2. AS7502 Natural Gas Engineering PC 3 3 0 0 3
3. AS7503 Petroleum Refining I PC 3 3 0 0 3
4. GE7351 Engineering Ethics and
HS 3 3 0 0 3
Human Values
5. Professional Elective I PE 3 3 0 0 3
6. Open Elective II* OE 3 3 0 0 3
PRACTICALS
7. Petroleum Testing
PC 4 0 0 4 2
AS7511 Laboratory
8. CH7561 Heat Transfer
PC 4 0 0 4 2
Laboratory
TOTAL 27 19 0 8 23
SEMESTER VI

L T P C
CODE GORY PERIODS
THEORY
1. AS7601 Catalytic Reaction
PC 4 4 0 0 4
Engineering
2. AS7602 Petrochemicals PC 4 4 0 0 4
3. AS7603 Petroleum Refining II PC 4 4 0 0 4
4. HS7551 Employability Skills HS 3 3 0 0 3
5. Open Elective III* OE 3 3 0 0 3
6. Professional Elective II PE 3 3 0 0 3
PRACTICALS
7. AS7611 Computational
Programming in
Chemical Engineering PC 4 0 0 4 2
Laboratory for
Petrochemical Engineers
8. AS7612 Mass Transfer
Laboratory for PC 4 0 0 4 2
TOTAL 29 21 0 8 25
5
SEMESTER VII

L T P C
CODE GORY PERIODS
THEORY
1. Petroleum Equipment
PC 3 3 0 0 3
AS7701 Design
2. CH7651 Process Instrumentation
PC 3 3 0 0 3
Dynamics and Control
3. Environmental Science
GE7251 HS 3 3 0 0 3
and Engineering
4. Professional Elective III PE 3 3 0 0 3
5. Professional Elective IV PE 3 3 0 0 3
6. Professional Elective V PE 3 3 0 0 3
7. AS7711 Process Control

Laboratory for PC 4 0 0 4 2
8. AS7712 Seminar I EEC 3 3 0 0 3
9. CH7661 Chemical Reaction
PC 4 0 0 4 2
Engineering Laboratory
TOTAL 29 21 0 8 25
SEMESTER VIII

L T P C
CODE GORY PERIODS
THEORY
1. Professional Elective VI PE 3 3 0 0 3
PRACTICALS
3. AS7811 Seminar II EEC 3 3 0 0 3
2. AS7812 Project Work EEC 20 0 0 20 10
TOTAL 26 6 0 20 16
TOTAL NO. OF CREDITS : 180
PROFESSIONAL ELECTIVES (PE)
S.No COURSE COURSE TITLE CATEG CONTACT L T P C

CODE ORY PERIODS
1. AS7024 Advanced Separation PE 3
3 0 0 3
Techniques
2. AS7025 Chemical Process Modeling PE 3
3 0 0 3
and Simulation
3. AS7026 Computational Fluid PE 3
Dynamics for Petrochemical 3 0 0 3
Engineers
4. AS7027 Crude oil transportation PE 3 3 0 0 3
6
5. AS7028 Drilling operations PE 3 3 0 0 3
6. AS7029 Engineering Economics PE 3 3 0 0 3
7. AS7030 Enhanced Oil Recovery PE 3 3 0 0 3
8. AS7031 Equilibrium staged PE 3
operations 3 0 0 3
9. AS7032 Multicomponent Distillation PE 3 3 0 0 3
10. AS7033 Petroleum Geology PE 3 3 0 0 3
11. AS7011 Petroleum Production PE 3
3 0 0 3
Engineering
12. AS7012 Plant Safety and Risk PE 3
3 0 0 3
Analysis
13. AS7013 Process Engineering PE 3 3 0 0 3
14. AS7014 Process Optimization PE 3 3 0 0 3
15. AS7015 Process Plant Utilities for PE 3
3 0 0 3
16. AS7016 Product Design and PE 3
Development for 3 0 0 3
17. AS7017 Refinery process design PE 3 3 0 0 3
18. AS7018 Safety and Environmental PE 3
Health 3 0 0 3
19. AS7019 Science and Health in PE 3
3 0 0 3
resonance
20. AS7020 Supply Chain Management PE 3
3 0 0 3
for Petrochemical Engineers
21. AS7021 Technical analysis – An PE 3
3 0 0 3
Analytical Insight
22. AS7022 Transport Phenomena for PE 3
3 0 0 3
23. AS7023 Well Completion PE 3
3 0 0 3
Techniques
24. CH7071 Energy Technology PE 3 3 0 0 3
25. CY7352 Physical Chemistry PE 3 3 0 0 3
26. GE7071 Disaster Management PE 3 3 0 0 3
27. GE7074 Human Rights PE 3 3 0 0 3
28. MA7072 Statistics and Linear PE 4
4 0 0 4
Programming
29. MA7354 Numerical Methods PE 4 4 0 0 4
30. ME7074 Design of Heat Exchangers PE 3 3 0 0 3
31. ME7075 Design of Pressure Vessels PE 3
3 0 0 3
and Piping
7
HUMANITIES AND SOCIAL SCIENCES (HS)
S.No COURSE COURSE TITLE CATEGORY CONTACT L T P C

CODE PERIODS
1. HS7151 Foundational HS
4 4 0 0 4
English
2. HS7251 Technical English HS 4 4 0 0 4
3. Engineering Ethics HS
GE7351 and Human 3 3 0 0 3
Values
4. HS7551 Employability HS
3 3 0 0 3
Skills
5. Environmental HS
GE7251 science and 3 3 0 0 3
engineering
BASIC SCIENCES (BS)
S.No COURSE COURSE TITLE CATE CONTACT L T P C

CODE GORY PERIODS
1. MA7151 Mathematics – I BS 4 4 0 0 4
2. PH7151 Engineering Physics BS 3 3 0 0 3
3. CY7151 Engineering Chemistry BS 3 3 0 0 3
4. BS7161 Basic Sciences BS
4 0 0 4 2
Laboratory
5. MA7251 Mathematics – II BS 4 4 0 0 4
6. PH7257 Physics of Materials BS 3 3 0 0 3
7. CY7255 Chemistry for BS
3 3 0 0 3
Technologists
8. CY7256 Organic Chemistry BS 3 3 0 0 3
9. CH7261 Chemical analysis BS
4 0 0 4 2
Laboratory
10. MA7357 Probability and Statistics BS 4 4 0 0 4
11. AS7412 Organic Chemistry BS
Laboratory for 4 0 0 4 2
ENGINEERING SCIENCES (ES)
S.NO COURSE COURSE TITLE CATE CONTACT L T P C

CODE GORY PERIODS
1. GE7151 Computing Techniques ES 3 3 0 0 3
2. GE7161 Computer Practices ES
4 0 0 4 2
Laboratory
3. GE7152 Engineering Graphics ES 4 4 0 0 4
4. GE7162 Engineering Practices ES
4 0 0 4 2
Laboratory
5. GE7153 Engineering Mechanics ES 4 4 0 0 4
6. EE7254 Principles of Electrical ES
and Electronics 3 3 0 0 3
Engineering
8
7. EE7312 Electrical Engineering ES
Laboratory For 4 0 0 4 2
Technologists
8. AS7311 Fluids Mechanics and ES
Mechanical operations 4 0 0 4 2
Laboratory
9. AS7402 Industrial Stoichiometry ES 3 3 0 0 3
10. ME7251 Basic Mechanical ES
3 3 0 0 3
Engineering
11. ME7262 Mechanical Engineering ES
4 0 0 4 2
Laboratory
PROFESSIONAL CORE (PC)
S.No COURSE COURSE TITLE CATEG CONTACT L T P C

CODE ORY PERIODS
1. AS7302 Petroleum Chemistry PC 3 3 0 0 3
2. AS7301 Fluids and Solid PC
4 4 0 0 4
operations
3. Spectroscopic PC
AS7303 Techniques for 3 3 0 0 3
Petroleum engineers
4. Chemical engineering PC
4 4 0 0 4
AS7401 thermodynamics
5. PC
Reservoir Engineering 3 3 0 0 3
AS7403
6. PC
Petroleum Refining I 3 3 0 0 3
AS7503
7. Natural Gas PC
3 3 0 0 3
AS7502 Engineering
8. AS7501 Heat and Mass PC
Transfer for
4 4 0 0 4
Petrochemical
Engineers
9. CH7561 Heat Transfer PC
4 0 0 4 2
Laboratory
10. AS7511 Petroleum Testing PC
4 0 0 4 2
Laboratory
11. AS7603 Petroleum Refining II PC 4 4 0 0 4
12. AS7602 Petrochemicals PC 4 4 0 0 4
13. AS7601 Catalytic Reaction PC
4 4 0 0 4
engineering
14. AS7612 Mass Transfer PC
Laboratory for
4 0 0 4 2
Petrochemical
Engineers
15. AS7611 Computational PC
Programming in
Chemical Engineering
4 0 0 4 2
Laboratory for
Petrochemical
Engineers
9
16. CH7651 Process PC
Instrumentation, 3 3 0 0 3
Dynamics and Control
17. AS7701 Petroleum Equipment PC
3 3 0 0 3
Design
18. AS7711 Process Control PC
Laboratory for
4 0 0 4 2
Petrochemical
Engineers
19. CH7661 Chemical Reaction PC
4 0 0 4 2
Engineering Laboratory
EMPLOYABILITY ENHANCEMENT COURSES (EEC)
S.No COURSE COURSE TITLE CATEGORY CONTACT L T P C

CODE PERIODS
1. AS7712 Seminar I EEC 3 3 0 0 3
2. AS7812 Project Work EEC 0 0 0 20 10
3. AS7811 Seminar II EEC 3 3 0 0 3
SUMMARY
Credits per Semester

S.No Subject Area Credits Total
I II III IV V VI VII VIII
1 HS 4 4 - - 3 3 3 - 17
2 BS 12 15 4 2 - - - - 33
3 ES 5 6 11 8 - - - - 30
4 PC - - 10 7 14 16 10 - 57
5 PE - - - - 3 3 9 3 18
6 OE - - - 3 3 3 - - 9
7 EEC - - - - - - 3 13 16
Total 21 25 25 20 23 25 25 16 180
Non-Credit/
8
Mandatory
10
HS7151 FOUNDATIONAL ENGLISH LT PC
4 0 04
COURSE DESCRIPTION:
This course aims at developing the language skills necessary for the first year students of
Engineering and Technology.
OBJECTIVES:
 To develop the four language skills – Listening, Speaking, Reading and Writing.
 To improve the students’ communicative competence in English.
 To teach students the various aspects of English language usage.
CONTENTS
UNIT I GREETING AND INTRODUCING ONESELF 12

Listening- Types of listening – Listening to short talks, conversations; Speaking – Speaking
about one’s place, important festivals etc. – Introducing oneself, one’s family/ friend;Reading –
Skimming a passage– Scanning for specific information;Writing- Guided writing - Free writing
on any given topic ( My favourite place/ Hobbies/ School life, writing about one’s leisure time
activities, hometown, etc.); Grammar – Tenses (present and present continuous) -Question
types - Regular and irregular verbs; Vocabulary – Synonyms and Antonyms.
UNIT II GIVING INSTRUCTIONS AND DIRECTIONS 12

Listening – Listening and responding to instructions; Speaking – Telephone etiquette - Giving
oral instructions/ Describing a process – Asking and answering questions; Reading – Reading
and finding key information in a given text - Critical reading - Writing –Process description( non-
technical)- Grammar – Tense (simple past& past continuous) - Use of imperatives – Subject –
verb agreement – Active and passive voice; - Vocabulary – Compound words – Word formation
– Word expansion ( root words).
UNIT III READING AND UNDERSTANDING VISUAL MATERIAL 12

Listening- Listening to lectures/ talks and completing a task; Speaking –Role play/ Simulation
– Group interaction; Reading – Reading and interpreting visual material;Writing- Jumbled
sentences – Discourse markers and Cohesive devices – Essay writing (cause & effect/
narrative);Grammar – Tenses (perfect), Conditional clauses –Modal verbs; Vocabulary –Cause
and effect words; Phrasal verbs in context.
UNIT IV CRITICAL READING AND WRITING 12

Listening- Watching videos/ documentaries and responding to questions based on them;
SpeakingInformal and formal conversation;Reading –Critical reading (prediction &
inference);Writing–Essay writing ( compare & contrast/ analytical) – Interpretation of visual
materials;Grammar – Tenses (future time reference);Vocabulary – One word substitutes (with
meanings) – Use of abbreviations & acronyms – Idioms in sentences.
UNIT V LETTER WRITING AND SENDING E-MAILS 12

Listening- Listening to programmes/broadcast/ telecast/ podcast;Speaking – Giving impromptu
talks, Making presentations on given topics- Discussion on the presentation;Reading –
Extensive reading;Writing- Poster making – Letter writing (Formal and E-mail) ;Grammar –
Direct and Indirect speech – Combining sentences using connectives;Vocabulary –Collocation;
TEACHING METHODS:
Interactive sessions for the speaking module.
Use of audio – visual aids for the various listening activities.
Contextual Grammar Teaching.
11
EVALUATION PATTERN:
Internals – 50%
End Semester – 50%
TOTAL:60 PERIODS
LEARNING OUTCOMES:
 Students will improve their reading and writing skills
 Students will become fluent and proficient in communicative English
 Students will be able to improve their interpersonal communication
TEXTBOOK:
1. Richards, Jack.C with Jonathan Hull and Susan Proctor New Interchange : English for
International Communication. (level2, Student’s Book) Cambridge University
Press,New Delhi: 2010.
REFERENCES:
1. Bailey, Stephen. Academic Writing: A practical guide for students. New York:
Rutledge,2011.
2. Morgan, David and Nicholas Regan. Take-Off: Technical English for Engineering.
London: Garnet Publishing Limited, 2008.
3. Redston, Chris & Gillies Cunningham Face2Face (Pre-intermediate Student’s Book&
Workbook) Cambridge University Press, New Delhi: 2005
4. Comfort, Jeremy, et al. Speaking Effectively : Developing Speaking Skillsfor Business
English. Cambridge University Press, Cambridge: Reprint 2011.
MA7151 MATHEMATICS – I L T P C
4 0 0 4
(Common to all branches of B.E. /B.Tech. Programmes in I Semester)
COURSE OBJECTIVES
 The goal of this course is for students to gain proficiency in calculus computations.
In calculus, we use three main tools for analyzing and describing the behavior of
functions: limits, derivatives, and integrals. Students will use these tools to solve
application problems in a variety of settings ranging from physics and biology to business
and economics.
 To make the student acquire sound knowledge of techniques in solving ordinary
differential equations that model engineering problems.
 To familiarize the student with functions of several variables. This is needed in many
branches of engineering.
 To acquaint the student with mathematical tools needed in evaluating multiple integrals
and their usage.
UNIT I DIFFERENTIAL CALCULUS 12

Representation of functions - New functions from old functions - Limit of a function - Limits at
infinity - Continuity - Derivatives - Differentiation rules - Polar coordinate system -
Differentiation in polar coordinates - Maxima and Minima of functions of one variable.
UNIT II FUNCTIONS OF SEVERAL VARIABLES 12

Partial derivatives – Homogeneous functions and Euler’s theorem – Total derivative –
Differentiation of implicit functions – Change of variables – Jacobians – Partial differentiation of
12
implicit functions – Taylor’s series for functions of two variables – Errors and approximations –
Maxima and minima of functions of two variables – Lagrange’s method of undetermined
multipliers.
UNIT III INTEGRAL CALCULUS 12

Definite and Indefinite integrals - Substitution rule - Techniques of Integration - Integration by
parts, Trigonometric integrals, Trigonometric substitutions, Integration of rational functions by
partial fraction, Integration of irrational functions - Improper integrals.
UNIT IV MULTIPLE INTEGRALS 12

Double integrals – Change of order of integration – Double integrals in polar coordinates –
Area enclosed by plane curves – Triple integrals – Volume of solids – Change of variables in
double and triple integrals.
UNIT V DIFFERENTIAL EQUATIONS 12

Method of variation of parameters – Method of undetermined coefficients – Homogenous
equation of Euler’s and Legendre’s type – System of simultaneous linear differential equations
with constant coefficients.
TOTAL : 60 PERIODS
COURSE OUTCOMES
 Understanding of the ideas of limits and continuity and an ability to calculate with them and
apply them.
 Improved facility in algebraic manipulation.
 Fluency in differentiation.
 Fluency in integration using standard methods, including the ability to find an appropriate
method for a given integral.
 Understanding the ideas of differential equations and facility in solving simple standard
examples.
TEXT BOOKS
1. James Stewart, "Calculus with Early Transcendental Functions", Cengage Learning, New
Delhi, 2008.
2. Narayanan S. and Manicavachagom Pillai T. K., “Calculus" Volume I and II, S.
Viswanathan Publishers Pvt. Ltd., Chennai, 2007.
3. Erwin Kreyszig, "Advanced Engineering Mathematics", John Wiley and Sons, 9th Edition,
New Delhi, 2014.
4. Grewal B.S., “Higher Engineering Mathematics”, Khanna Publishers, New Delhi, 43rd
Edition, 2014.
REFERENCE BOOKS
1. Ramana B.V., “Higher Engineering Mathematics”, Tata McGraw Hill Co. Ltd., New Delhi,
11th Reprint, 2010.
2. Jain R.K. and Iyengar S.R.K., “Advanced Engineering Mathematics”, Narosa Publications,
New Delhi, 3rd Edition, 2007.
3. Bali N., Goyal M. and Watkins C., “Advanced Engineering Mathematics”, Firewall Media
(An imprint of Lakshmi Publications Pvt., Ltd.,), New Delhi, 7th Edition, 2009.
4. Greenberg M.D., “Advanced Engineering Mathematics”, Pearson Education, New Delhi,
2nd Edition, 5th Reprint, 2009.
5. Peter V.O’Neil, “Advanced Engineering Mathematics”, Cengage Learning India Pvt., Ltd,
New Delhi, 2007.
13
PH7151 ENGINEERING PHYSICS L T P C
3 0 0 3
(Common to all branches of B.E. /B.Tech. Programmes)
COURSE OBJECTIVES
 To introduce the basic physics concepts relevant to different branches of Engineering and
Technology.
UNIT I PROPERTIES OF MATTER 9

Elasticity – Poisson’s ratio and relationship between moduli (qualitative) - stress-strain
diagram for ductile and brittle materials, uses - factors affecting elastic modulus and tensile
strength - bending of beams - cantilever - bending moment - Young’s modulus determination
- theory and experiment - uniform and non-uniform bending - I shaped girders - twisting
couple - hollow cylinder - shaft - torsion pendulum - determination of rigidity modulus-
moment of inertia of a body (regular and irregular).
UNIT II ACOUSTICS AND ULTRASONICS 9

Classification of sound - loudness and intensity - Weber-Fechner Law - standard intensity
and intensity level - decibel - reverberation - reverberation time - calculation of reverberation
time for different types of buildings – sound absorbing materials - factors affecting acoustics
of buildings : focussing, interference, echo, echelon effect, resonance - noise and their
remedies. Ultrasonics: production - magnetostriction and piezoelectric methods - detection of
ultrasound - acoustic grating – ultrasonic interferometer - industrial applications – Non-
destructive testing - ultrasonic method: scan modes and practice.
UNIT III THERMAL AND MODERN PHYSICS 9

Thermal expansion - thermal stress - expansion joints - bimetallic strips - thermal
conductivity- heat conductions in solids – flow of heat through compound media - Forbe’s
and Lee’s disc method: theory and experiment- Black body radiation – Planck’s theory
(derivation) – Compton effect – wave model of radiation and matter – Schrödinger’s wave
equation – time dependent and independent equations – Physical significance of wave
function – particle in a one dimensional box.
UNIT IV APPLIED OPTICS 9

Interference - Michelson interferometer: construction, working, determination of wave length
and thickness - anti-reflection coating - air wedge and its applications - Lasers – principle and
applications – Einstein’s coefficients – CO2 and Nd:YAG laser - semiconductor lasers: homo
junction and hetro junction - construction and working – applications. Optical fibres -
classification (index & mode based) - principle and propagation of light in optical fibres -
acceptance angle and numerical aperture - fibre optic communication system - active and
passive sensors.
UNIT V CRYSTAL PHYSICS 9

Single crystalline, polycrystalline and amorphous materials – Single crystals: unit cell, crystal
systems, Bravais lattices, ditections and planes in a crystal, Miller indices - interplanar
distance for a cubic crystal - coordination number and packing factor for SC, BCC, FCC, HCP
and diamond structures - structure and significance of NaCl, CsCl, ZnS and graphite - crystal
imperfections: point defects, line defects – Burger vectors, dislocations and stacking faults –
Growth of single crystals: Bridgman and Czochralski methods.
TOTAL : 45 PERIODS
COURSE OUTCOMES
 The students will acquire knowledge on the basics of physics related to properties of
matter, optics, acoustics etc., and they will apply these fundamental principles to solve
practical problems related to materials used for engineering applications.
14
TEXT BOOKS
1. Palanisamy P.K., “Engineering Physics”, Scitech Publications (P) Ltd. (2006).
2. Arumugam M., “Engineering Physics”, Anuradha Publications (2000)
3. Gaur R.K. and Gupta S.L., “Engineering Physics”, Dhanpat Rai Publications (2013)
REFERENCE BOOKS
1. Serway R.A. and Jewett, J.W. “Physics for Scientists and Engineers with Modern
Physics”. Brooks/cole Publishing Co. (2010).
2. Tipler P.A. and Mosca, G.P., “Physics for Scientists and Engineers with Modern
Physics”. W.H.Freeman, (2007).
3. Markert J.T.,Ohanian, H. and Ohanian, M. “Physics for Engineers and Scientists”.
W.W.Norton & Co. (2007).
CY7151 ENGINEERING CHEMISTRY L T P C

3 0 0 3
COURSE OBJECTIVES
 To develop an understanding about fundamentals of polymer chemistry.
 Brief elucidation on surface chemistry and catalysis.
 To develop sound knowledge photochemistry and spectroscopy.
 To impart basic knowledge on chemical thermodynamics.
 To understand the basic concepts of nano chemistry.
UNIT I POLYMER CHEMISTRY 9

Introduction: Functionality-degree of polymerization. Classification of polymers- natural and
synthetic, thermoplastic and thermosetting. Types and mechanism of polymerization: addition
(free radical, cationic, anionic and living); condensation and copolymerization. Properties of
polymers: Tg, tacticity, molecular weight-weight average, number average and polydispersity
index. Techniques of polymerization: Bulk, emulsion, solution and suspension.
UNIT II SURFACE CHEMISTRYAND CATALYSIS 9

Adsorption-Types of adsorption-adsorption of gases on solids- adsorption from solutions-
Types of isotherms–Frendlich adsorption isotherm,Langmuir adsorption isotherm.Industrial
applications of adsorption. Catalysis: Characteristics and types of catalysts-homogeneous
and heterogeneous, auto catalysis. Enzyme catalysis -factors affecting enzyme catalysis,
Michaelis-Menton equation.Industrial applications of catalysts.
UNIT III PHOTOCHEMISTRY AND SPECTROSCOPY 9

Photochemistry: Laws of photochemistry-Grotthuss-Draper law, Stark-Einstein law and
Lambert-Beer Law. Photo processes-internal conversion, inter-system crossing,
fluorescence, phosphorescence, chemiluminescence and photo-sensitization. Spectroscopy:
Electromagnetic spectrum-absorption of radiation-electronic, vibrational and rotational
transitions. Width and intensities of spectral lines.Spectrophotometric estimation of iron.UV-
Vis and IR spectroscopy- principles, instrumentation (Block diagram) and applications.
UNIT IV CHEMICAL THERMODYNAMICS 9

Second law: Entropy-entropy change for an ideal gas, reversible and irreversible processes;
entropy of phase transitions; Free energy and work function: Helmholtzand Gibbs free energy
functions; Criteria of spontaneity; Gibbs-Helmholtz equation; Clausius Clapeyron equation;
15
Maxwell relations-Van’t Hoff isotherm and isochore. Chemical potential; Gibbs-Duhem
equation- variation of chemical potential with temperature and pressure.
UNIT V NANOCHEMISTRY 9
Basics-distinction between molecules, nanoparticles and bulk materials; size-dependent
properties.Preparation of nanoparticles – sol-gel and solvothermal.Preparation of carbon
nanotube by chemical vapour deposition and laser ablation.Preparation of nanowires by VLS
growth, electrochemical deposition and electro spinning.Properties and uses of
nanoparticles, nanoclusters, nanorods, nanotubes and nanowires.
TOTAL : 45 PERIODS
COURSE OUTCOMES
 Will be familiar with polymer chemistry, surface chemistry and catalysis.
 Will know the photochemistry, spectroscopy and chemical thermodynamics.
 Will know the fundamentals of nano chemistry.
TEXT BOOKS
1. Jain P. C. & Monica Jain., “Engineering Chemistry”, DhanpatRai Publishing Company
(P) Ltd, New Delhi, 2014.
2. Kannan P., Ravikrishnan A., “Engineering Chemistry”, Sri Krishna Hitech Publishing
Company Pvt. Ltd. Chennai, 2014
REFERENCE BOOKS
1. Pahari A., Chauhan B., “Engineering Chemistry”, Firewall Media, New Delhi, 2012.
2. Sivasankar B., “Engineering Chemistry”, Tata McGraw-Hill Publishing Company Ltd,
New Delhi, 2012.
3. AshimaSrivastava. Janhavi N N, Concepts of Engineering Chemistry”, ACME Learning
Private Limited., New Delhi., 2010.
4. Vairam S., Kalyani P., Suba Ramesh., “Engineering Chemistry”, Wiley India Pvt Ltd.,
New Delhi., 2011.
GE7151 COMPUTING TECHNIQUES L T P C

(Common to all branches of Engineering and Technology) 3 0 0 3
OBJECTIVES:
• To learn programming using a structured programming language.
• To provide C programming exposure.
• To introduce foundational concepts of computer programming to students of different
branches of Engineering and Technology.
UNIT I INTRODUCTION 9
Introduction to Computers – Computer Software – Computer Networks and Internet - Need for
logical thinking – Problem formulation and development of simple programs - Pseudo code -
Flow Chart and Algorithms.
UNIT II C PROGRAMMING BASICS 9

Introduction to C programming – Fundamentals – Structure of a C program – Compilation and
linking processes - Constants, Variables – Data Types – Expressions - Operators –Decision
Making and Branching – Looping statements – Solving Simple Scientific and Statistical
Problems.
16
UNIT III ARRAYS AND STRINGS 9
Arrays – Initialization – Declaration – One dimensional and two dimensional arrays - Strings-
String operations – String Arrays - simple programs- sorting- searching – matrix operations.
UNIT IV POINTERS 9
Macros - Storage classes –Basic concepts of Pointers– Pointer arithmetic - Example Problems
- Basic file operations
UNIT V FUNCTIONS AND USER DEFINED DATA TYPES 9

Function – definition of function – Declaration of function – Pass by value – Pass by reference –
Recursion –Enumerators – Structures - Unions
TOTAL : 45 PERIODS
OUTCOMES
At the end of the course, the student should be able to:
• Write C program for simple applications
• Formulate algorithm for simple problems
• Analyze different data types and arrays
• Perform simple search and sort.
• Use programming language to solve problems.
TEXTBOOKS:
1. Pradip Dey, Manas Ghosh, “Computer Fundamentals and Programming in C”, Second
Edition, Oxford University Press, 2013
2. Ashok N. Kamthane, “Computer programming”, Pearson Education, 2007.
3. Yashavant P. Kanetkar. “Let Us C”, BPB Publications, 2011.
REFERENCES:
1. Kernighan,B.W and Ritchie,D.M, “The C Programming language”, Second Edition,
Pearson Education, 2006
2. Byron S Gottfried, “Programming with C”, Schaums Outlines, Second Edition, Tata
McGraw-Hill, 2006.
3. R.G. Dromey, “How to Solve it by Computer”, Pearson Education, Fourth Reprint, 2007
BS7161 BASIC SCIENCES LABORATORY LTPC

(Common to all branches of B.E. / B.Tech Programmes) 004 2
PHYSICS LABORATORY: (Any Seven Experiments)
OBJECTIVE:
To introduce different experiments to test basic understanding of physics concepts applied in

optics, thermal physics, properties of matter and liquids.
1. Torsional pendulum - Determination of rigidity modulus of wire and moment of inertia of disc
2. Non-uniform bending - Determination of young’s modulus
3. Uniform bending – Determination of young’s modulus
17
4. Lee’s disc Determination of thermal conductivity of a bad conductor
5. Potentiometer-Determination of thermo e.m.f of a thermocouple
6. Laser- Determination of the wave length of the laser using grating
7. Air wedge - Determination of thickness of a thin sheet/wire
8. a) Optical fibre -Determination of Numerical Aperture and acceptance angle
b) Compact disc- Determination of width of the groove using laser.
9. Acoustic grating- Determination of velocity of ultrasonic waves in liquids.
10. Ultrasonic interferometer – determination of the velocity of sound and compressibility of

liquids
11. Post office box -Determination of Band gap of a semiconductor.
12. Spectrometer- Determination of wavelength using gating.
13. Viscosity of liquids - Determination of co-efficient of viscosity of a liquid by
Poiseuille s flow
OUTCOME:
The hands on exercises undergone by the students will help them to apply physics principles of
optics and thermal physics to evaluate engineering properties of materials.
CHEMISTRY LABORATORY:
(Minimum of 8 experiments to be conducted)
1. Estimation of HCl using Na2CO3 as primary standard and Determination of alkalinity in water
sample.
2. Determination of total, temporary & permanent hardness of water by EDTA method.
3. Determination of DO content of water sample by Winkler’s method.
4. Determination of chloride content of water sample by argentometric method.
5. Estimation of copper content of the given solution by Iodometry.
6. Determination of strength of given hydrochloric acid using pH meter.
7. Determination of strength of acids in a mixture of acids using conductivity meter.
8. Estimation of iron content of the given solution using potentiometer.
9. Estimation of iron content of the water sample using spectrophotometer (1, 10-
Phenanthroline/thiocyanate method).
10. Estimation of sodium and potassium present in water using flame photometer.
11. Determination of molecular weight of poly vinyl alcohol using Ostwald viscometer.
12. Pseudo first order kinetics-ester hydrolysis.
13. Corrosion experiment-weight loss method.
14. Determination of CMC.
15. Phase change in a solid.
TOTAL: 60 PERIODS
TEXT BOOKS
1. Vogel’s Textbook of Quantitative Chemical Analysis (8TH edition, 2014)
2. Laboratory Manual- Department of Chemistry, CEGC, Anna University (2014).
18
GE7161 COMPUTER PRACTICES LABORATORY L T P C
0 0 4 2
OBJECTIVES
 To understand the basic programming constructs and articulate how they are used to
develop a program with a desired runtime execution flow.
 To articulate where computer programs fit in the provision of computer-based solutions
to real world problems.
 To learn to use user defined data structures.
LIST OF EXPERIMENTS
1. Search, generate, manipulate data using MS office/ Open Office
2. Presentation and Visualization – graphs, charts, 2D, 3D
3. Problem formulation, Problem Solving and Flowcharts
4. C Programming using Simple statements and expressions
5. Scientific problem solving using decision making and looping.
6. Simple programming for one dimensional and two dimensional arrays.
7. Solving problems using String functions
8. Programs with user defined functions
9. Program using Recursive Function
10. Program using structures and unions.
TOTAL: 60 PERIODS
OUTCOMES
At the end of the course, the student should be able to:
 Write and compile programs using C programs.
 Write program with the concept of Structured Programming
 Identify suitable data structure for solving a problem
 Demonstrate the use of conditional statement.
LABORATORY REQUIREMENTS FOR BATCH OF 30 STUDENTS

30 Systems with C compiler
HS7251 TECHNICAL ENGLISH L T P C

4 0 0 4
OBJECTIVES
 To enable students acquire proficiency in technical communication.
 To enhance their reading and writing skills in a technical context.
 To teach various language learning strategies needed in aprofessional environment.
CONTENTS
UNIT I ANALYTICAL READING 12

Listening- Listening to informal and formal conversations; Speaking – Conversation
Skills(opening, turn taking, closing )-explaining how something works-describing technical
functions and applications;Reading –Analytical reading, Deductive and inductive reasoning;
Writing- vision statement–structuring paragraphs.
19
UNIT II SUMMARISING 12
Listening- Listening to lectures/ talks on Science & Technology;Speaking –Summarizing/ Oral
Reporting, Reading – Reading Scientific and Technical articles; Writing- Extended definition –
Lab Reports – Summary writing.
UNIT III DESCRIBING VISUAL MATERIAL 12

Listening- Listening to a panel discussion; Speaking – Speaking at formal situations; Reading
–Reading journal articles - Speed reading;Writing-data commentary-describing visual material-
writing problem-process- solution-the structure of problem-solution texts- writing critiques
UNIT IV WRITING/ E-MAILING THE JOB APPLICATION 12

Listening- Listening to/ Viewing model interviews; Speaking –Speaking at different types of
interviews – Role play practice ( mock interview); Reading – Reading job advertisements and
profile of the company concerned;Writing- job application – cover letter –Résumé preparation.
UNIT V REPORT WRITING 12

Listening- Viewing a model group discussion;Speaking –Participating in a discussion -
Presentation;Reading – Case study - analyse -evaluate – arrive at a solution;Writing–
Recommendations- Types of reports (feasibility report)- designing and reporting surveys- –
Report format.- writing discursive essays.
TEACHING METHODS:
Practice writing
Conduct model and mock interview and group discussion.
Use of audio – visual aids to facilitate understanding of various forms of technical
communication.
Interactive sessions.
EVALUATION PATTERN:
Internals – 50%
End Semester – 50%
TOTAL:60 PERIODS
LEARNING OUTCOMES
 Students will learn the structure and organization of various forms of technical
communication.
 Students will be able to listen and respond to technical content.
 Students will be able to use different forms of communication in their respective fields.
TEXTBOOK:
1. Craig,Thaine. Cambridge Academic English: An integrated skills course for
EAP(Student’s Book)Level: Intermediate Cambridge University Press, New Delhi: 2012
REFERENCES:
1. Laws, Anne. Presentations. Hyderabad: Orient Blackswan, 2011.
2. Ibbotson, Mark. Cambridge English for Engieering. Cambridge University Press,
Cambridge,New Delhi: 2008
3. Naterop, Jean B. and Rod Revell. Telephoning in English. Cambridge: Cambridge
University Press, 2004.
4. Rutherford, Andrea J. Basic Communication Skills for Technology. New Delhi: Pearson
Education, 2001.
5. Bailey, Stephen. Academic Writing A practical Guide for Students. Routledge, London:
2004.
6. Hewings, Martin. Cambridge Academic English: An integrated skills course for
EAP(Student’s Book)Level: Intermediate Cambridge University Press, New Delhi: 2012.
20
MA7251 MATHEMATICS – II L T P C
4 0 0 4
(Common to all branches of B.E. /B.Tech. Programmes in II Semester)
COURSE OBJECTIVES
 To develop the use of matrix algebra techniques this is needed by engineers for
practical applications.
 To acquaint the student with the concepts of vector calculus, needed for problems in
all engineering disciplines.
 To develop an understanding of the standard techniques of complex variable theory
so as to enable the student to apply them with confidence, in application areas such
as heat conduction, elasticity, fluid dynamics and flow the of electric current.
 To make the student appreciate the purpose of using transforms to create a new
domain in which it is easier to handle the problem that is being investigated.
UNIT I MATRICES 12
Eigenvalues and Eigenvectors of a real matrix – Characteristic equation – Properties of
eigenvalues and eigenvectors – Cayley-Hamilton theorem – Diagonalization of matrices –
Reduction of a quadratic form to canonical form by orthogonal transformation – Nature of
quadratic forms.
UNIT II VECTOR CALCULUS 12

Gradient and directional derivative – Divergence and Curl – Irrotational and Solenoidal
vector fields – Line integral over a plane curve – Surface integral - Area of a curved surface -
Volume integral - Green’s, Gauss divergence and Stoke’s theorems – Verification and
application in evaluating line, surface and volume integrals.
UNIT III ANALYTIC FUNCTION 12

Analytic functions – Necessary and sufficient conditions for analyticity - Properties –
Harmonic conjugates – Construction of analytic function - Conformal mapping – Mapping by
1 2
functions w  z  c, az, , z - Bilinear transformation.
z
UNIT IV COMPLEX INTEGRATION 12

Line integral - Cauchy’s integral theorem – Cauchy’s integral formula – Taylor’s and
Laurent’s series – Singularities – Residues – Residue theorem – Application of residue
theorem for evaluation of real integrals – Use of circular contour and semicircular contour
with no pole on real axis.
UNIT V LAPLACE TRANSFORMS 12

Existence conditions – Transforms of elementary functions – Transform of unit step function
and unit impulse function – Basic properties – Shifting theorems -Transforms of derivatives
and integrals – Initial and final value theorems – Inverse transforms – Convolution theorem –
– Transform of periodic functions – Application to solution of linear ordinary differential
equations with constant coefficients.
TOTAL : 60 PERIODS
COURSE OUTCOMES
Upon successful completion of the course, students should be able to:
 Evaluate real and complex integrals using the Cauchy integral formula and the
residue theorem
 Appreciate how complex methods can be used to prove some important theoretical
results.
21
 Evaluate line, surface and volume integrals in simple coordinate systems
 Calculate grad, div and curl in Cartesian and other simple coordinate systems, and
establish identities connecting these quantities
 Use Gauss, Stokes and Greens theorems to simplify calculations of integrals and
prove simple results.
TEXT BOOKS
1. Erwin Kreyszig, "Advanced Engineering Mathematics", John Wiley and Sons, 9th Edition,
New Delhi, 2014.
2. Grewal B.S., “Higher Engineering Mathematics”, Khanna Publishers, New Delhi, 43rd
Edition, 2014.
REFERENCE BOOKS
1. Ramana, B.V. “Higher Engineering Mathematics”, Tata McGraw Hill, New Delhi, 2010.
2. Glyn James, “Advanced Modern Engineering Mathematics”, Pearson Education, New
Delhi, 2007.
3. Jain R.K. and Iyengar S.R.K., “Advanced Engineering Mathematics”, Narosa
Publications, New Delhi, 3rd Edition, 2007.
4. Bali N., Goyal M. and Watkins C., “Advanced Engineering Mathematics”, Firewall Media
(An imprint of Lakshmi Publications Pvt., Ltd.,), New Delhi, 7th Edition, 2009.
5. Peter V. O’Neil , “Advanced Engineering Mathematics”, Cengage Learning India Pvt.,
Ltd, New Delhi, 2007.
PH7257 PHYSICS OF MATERIALS L T P C

3 0 0 3
OBJECTIVE:
 To introduce the physics of various materials relevant to different branches of technology
UNIT I PREPARATION OF MATERIALS 9

Phases - phase rule – binary systems – tie line rule – lever rule – phase diagram – invariant
reactions - nucleation – homogeneous and heterogeneous nucleation – free energy of formation
of a critical nucleus – Thin films – preparation: PVD, CVD method – Nanomaterials
Preparation: wet chemical, solvothermal, sol-gel method.
UNIT II ELECTRICAL AND SUPERCONDUCTING MATERIALS 9

Classical free electron theory - expression for electrical conductivity – thermal conductivity, -
Wiedemann-Franz law - Quantum free electron theory – applications of Schrodinger wave
equation: particle in a finite potential well – particle in a three-dimensional box- degenerate
states – Fermi-Dirac statistics – density of energy states – electron in periodic potential –
electron effective mass – concept of hole. Superconducting phenomena, properties of
superconductors – Meissner effect and isotope effect. Type I and Type II superconductors,
High Tc superconductors – Magnetic levitation and SQUIDS.
UNIT III SEMICONDUCTING MATERIALS 9

Elemental Semiconductors - Compound semiconductors - Origin of band gap in solids
(qualitative) - carrier concentration in metals - carrier concentration in an intrinsic
semiconductor (derivation) – Fermi level – variation of Fermi level with temperature – electrical
conductivity – band gap determination – carrier concentration in n-type and p-type
semiconductors (derivation) – variation of Fermi level with temperature and impurity
concentration – Hall effect – determination of Hall coefficient – LED - Solar cells.
22
UNIT IV DIELECTRIC AND MAGNETIC MATERIALS 9
Dielectric, Paraelectric and ferroelectric materials - Electronic, Ionic, Orientational and space
charge polarization – Internal field and deduction of Clausius Mosotti equation – dielectric loss –
different types of dielectric breakdown – classification of insulating materials and their
applications - Ferroelectric materials - Introduction to magnetic materials - Domain theory of
ferromagnetism, Hysteresis, Soft and Hard magnetic materials – Anti-ferromagnetic materials –
Ferrites, Giant Magneto Resistance materials.
UNIT V NEW MATERIALS AND APPLICATIONS 9

Ceramics – types and applications – Composites: classification, role of matrix and reinforcement
– processing of fibre reinforced plastics and fibre reinforced metals – Metallic glasses – Shape
memory alloys – Copper, Nickel and Titanium based alloys – grapheme and its properties –
Relaxor ferroelectrics - Bio materials – hydroxyapatite – PMMA – Silicone - Sensors: Chemical
Sensors - Bio-sensors – Polymer semiconductors – Photoconducting polymers.
TOTAL: 45 PERIODS
OUTCOME:
 On completion of the course the students are expected to have a through knowledge on the
various materials and their physical properties.
REFERENCES:
1. Callister W. D. and Rethwisch, D. G., “Materials Science and Engineering”, 9th Edition,
Wiley (2014).
2. Raghavan V., “Materials Science and Engineering”, Prentice Hall of India (2004).
3. Askeland D.R. and Wright, W.J., “Essentials of Materials Science and Engineering”, 3rd
Edition, Cengage Learning (2014).
4. Pillai, S.O., “Solid State Physics”, New Age International, 7th Edition (2015).
5. Viswanathan, B., “Nanomaterials”, Narosa Book Distributors Pvt Ltd. (2011).
CY7255 CHEMISTRY FOR TECHNOLOGISTS L T P C

3 0 0 3
OBJECTIVE
 The students should be conversant with
• boiler feed water requirements, water treatment techniques,
• Applications of oil and its properties, principles of different chemical analysis.
• Different kinds of preparations of important chemicals.
OUTCOME
• Will be familiar with boiler feed water requirements, water treatment techniques.
• Will know the oil and its properties, principles of different chemical analysis.
• Will know the preparations of important chemicals.
UNIT I WATER TECHNOLOGY 9

Water quality parameters- hardness -definition - units of hardness - determination of hardness
(EDTA method).Alkalinity - definition - determination of alkalinity.TDS, BOD, COD and iron and
their significance. Softening – zeolite and demineralization processes. Boiler troubles (scale,
sludge, boiler corrosion, caustic embrittlement and carry over) and remedies – removal of oils
and silica, internal conditioning.Desalination by electro-dialysis and reverse osmosis.
23
UNIT II OILS, FATS, SOAPS & LUBRICANTS 9
Chemical constitution, chemical analysis of oils and fats – free acid, saponification and iodine
values, definitions, determinations and significance.Soaps and detergents - cleaning action of
soap. Lubricants - definition, characteristics, types and properties – viscosity, viscosity index,
carbon residue, oxidation stability, flash and fire points, cloud and pour points, aniline point.
Solid lubricants – graphite and molybdenum disulphide.
UNIT III CHEMICAL ANALYSIS – AN ANALYTICAL INSIGHT 9

Gravimetric analysis – principles – method – applications.redox titrations – principle – method –
applications. Thin layer chromatography – principles – techniques – applications. Principles
underlying the estimations of nitrogen in nitrogeneous fertilizers, phenol and aniline.
UNIT IV DYE CHEMISTRY 9

Witt’s theory and modern theory of colors – synthesis of methyl red, methyl orange, congo red,
malachite green, p-rosaniline, phenolphthalein, fluorescence, eosin dyes.
UNIT V CHEMICALS AND AUXILIARIES 9

Preparations of bleaching powder, sodium hypochlorite, hydrogen peroxide, chlorine dioxide –
estimation of available chlorine in hypochlorite – determination of strength of hydrogen peroxide.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Jain & Jain, "Engineering Chemistry", 16th Edition, 2014,DhanpatRai Publishing Company,
New Delhi.
2. Sharma B.K, "Industrial Chemistry", 16th Edition, 2014, GOEL Publishing House, Meerut.
REFERENCE BOOKS
1. Dara SS, Umare SS, "A Textbook of Engineering Chemistry", S. Chand & Company Ltd.,
New Delhi, 2010.
2. Puri BR, Sharma LR, Pathania S, "Principles of Physical Chemistry", 42nd Edition, 2008,
Vishal Publishing Co., Jalandhar.
3. Morrison RT, Boyd RN, Bhattacharjee SK, “Organic Chemistry”, 7th Edition, Pearson India,
2011.
GE7152 ENGINEERING GRAPHICS L T P C

3 2 0 4
OBJECTIVES
• To develop in students, graphic skills for communication of concepts, ideas and design of
engineering products and expose them to existing national standards related to technical
drawings.
CONCEPTS AND CONVENTIONS (NOT FOR EXAMINATION) 1

Importance of graphics in engineering applications – Use of drafting instruments – BIS
conventions and specifications – Size, layout and folding of drawing sheets – Lettering and
dimensioning.
UNIT I PLANE CURVES ANDFREE HANDSKETCHING 14

Basic Geometrical constructions, Curves used in engineering practices-Conics –
Construction of ellipse, parabola and hyperbola by eccentricity method – Construction of
cycloid – construction of involutes of square and circle – Drawing of tangents and normal to
the above curves. Visualization concepts and Free Hand sketching: Visualization principles –
Representation of Three Dimensional objects – Layout of views- Free hand sketching of
multiple views from pictorial views of objects
24
14
UNIT II PROJECTION OF POINTS, LINES AND PLANE SURFACES
Orthographic projection- principles-Principal planes-First angle projection-Projection of points.
Projection of straight lines (only First angle projections) inclined to both the principal planes-
Determination of true lengths and true inclinations by rotating line method and trapezoidal
method and traces Projection of planes (polygonal and circular surfaces) inclined to both the
principal planes by rotating object method.
UNIT III PROJECTION OF SOLIDS 14

Projection of simple solids like prisms, pyramids, cylinder, cone and truncated solids when
the axis is inclined to both the principal planes by rotating object method and auxiliary plane
method.
UNIT IV PROJECTION OF SECTIONED SOLIDS AND DEVELOPMENT OF 14

SURFACES
Sectioning of solids in simple vertical position when the cutting plane is inclined to the one of
the principal planes and perpendicular to the other – obtaining true shape of section.
Development of lateral surfaces of simple and sectioned solids – Prisms, pyramids cylinders
and cones. Development of lateral surfaces of solids with cut-outs and holes.
15
UNIT V ISOMETRIC AND PERSPECTIVE PROJECTIONS
Principles of isometric projection – isometric scale –Isometric projections of simple solids and
truncated solids - Prisms, pyramids, cylinders, cones- combination of two solid objects in
simple vertical positions and miscellaneous problems.
Perspective projection of simple solids-Prisms, pyramids and cylinders by visual ray method
and vanishing point method.
COMPUTER AIDED DRAFTING (DEMONSTRATION ONLY) 3

Introduction to drafting packages and demonstration of their use.
L=45+T=30, TOTAL: 75 PERIODS
OUTCOMES:
On Completion of the course the student will be able to
 Perform free hand sketching of basic geometrical shapes and multiple views of
objects.
 Draw orthographic projections of lines, Planes and Solids
 Obtain development of surfaces.
 Prepare isometric and perspective views of simple solids.
TEXT BOOK:
1. N.D.Bhatt and V.M.Panchal, “Engineering Drawing”, Charotar Publishing House, 50th
Edition, 2010.
REFERENCES:
1. K.R.Gopalakrishna., “Engineering Drawing” (Vol I&II combined) SubhasStores,
Bangalore, 2007
2. Luzzader, Warren.J., and Duff,John M.,,’’ Fundamentals of Engineering Drawingwith an
introduction to Interactive Computer Graphics for Design and Production”,Eastern
Economy Edition, Prentice Hall of India Pvt Ltd, New Delhi, 2005
3. M.B.Shah and B.C.Rana, “Engineering Drawing”, Pearson, 2nd Edition, 2009
4. K.Venugopal and V.Prabhu Raja, “Engineering Graphics”, New Age International
(P)Limited ,2008.
5. K. V.Natarajan, “A text book of Engineering Graphics”, 28th Edition, Dhanalakshmi
Publishers, Chennai, 2015.
25
6. BasantAgarwal and Agarwal C.M., “Engineering Drawing”, Tata McGraw Hill Publishing
Company Limited, New Delhi, 2008.
7. N.S Parthasarathy and Vela Murali, “ Engineering Drawing”, Oxford University Press,
2015
Publication of Bureau of Indian Standards:

1. IS 10711 – 2001: Technical products Documentation – Size and lay out ofdrawing
sheets
2. IS 9609 (Parts 0 & 1) – 2001: Technical products Documentation – Lettering.
3. IS 10714 (Part 20) – 2001 & SP 46 – 2003: Lines for technical drawings.
4. IS 11669 – 1986 & SP 46 – 2003: Dimensioning of Technical Drawings.
5. IS 15021 (Parts 1 to 4) – 2001: Technical drawings – Projection Methods.
Special points applicable to University Examinations on Engineering Graphics:

1. There will be five questions, each of either or type covering all units of the syllabus.
2. All questions will carry equal marks of 20 each making a total of 100.
3. The answer paper shall consist of drawing sheets of A3 size only. The students will be
permitted to use appropriate scale to fit solution within A3 size.
4. The examination will be conducted in appropriate sessions on the same day.
CY7256 ORGANIC CHEMISTRY LTPC

3003
AIM
To study the type of components in which organic reactions take place and also to know the
preparation of the essential organic compounds.
OBJECTIVES
At the end of the course students will be in a position to have knowledge on various reaction
mechanism, preparation of organic compounds and their properties. This will be a precursor for
the study on Chemical Reaction Engineering.
UNIT I CARBOHYDRATES 9
Introduction – various definitions and classifications of carbohydrates – Preparation, Physical &
Chemical propertie, Structure and Uses of Monosaccharides (Glucose & Fructose)
Interconversions – Aldo pentose to aldo hexose–Aldo hexose to aldo pentose- aldose to
isomeric Ketose – Ketose to isomeric Aldose – Aldose to epimer
UNIT II HETEROCYCLIC COMPOUNDS 9

Preparation, Physical & Chemical properties and Uses of Pyrrole, Furan, Furfural, Tetrahydro
Furan, Thiophene, Indole, Pyridine, Quinoline and Isoquinoline.
UNIT III PREPARATION OF SYNTHETIC INTERMEDIATES 9

Preparations of Benzil from benzyl aldehydes - Furyl from furfural, Vanniline from catechol,
Gramine from indole, N-actetyl-5- bromo indoline from indole, Salol from phenol, Alanine from
propionic acid, Heteroauxin from indole - Uses, Preparation of Chlorampenicol - Uses
UNIT IV SYNTHETIC ORGANIC CHEMISTRY 9

Preparation and Synthetic utilities of Grignard reagent, Ethyl aceto acetate and Malonic ester.
UNIT V PHARMACEUTICAL CHEMISTRY 9

Synthesis of Malonyl urea, Phenacetin, Isoniazid, Para amino benzoic acid (PABA), Tryptophan
Isopentaquine, chloroquine, Sulphaniliamide and Sulphapyridine.
26
TOTAL : 45 PERIODS
TEXT BOOKS
1. R.T. Morrison and R.N. Boyd “Organic Chemistry” VI Edition Prentice Hall Inc (1996) USA.
2. K.S. Tiwari, N.K. Vishnoi and S.N. Malhotra “A text book of Organic Chemistry” Second
Edition, Vikas Publishing House Pvt. Ltd. (1998) New Delhi.
REFERENCE BOOKS
1. Chemistry in Engineering and Technology, Vol.2, TMH Publishing Co Ltd., New Delhi,
1994.
2. I L Finar “Organic Chemistry” ELBS (1994).
CH7261 CHEMICAL ANALYSIS LABORATORY L T P C

0 0 4 2
(Minimum of 8 experiments to be conducted)
OBJECTIVE
 To make the student acquire practical skills in the wet chemical and
instrumentalmethods for quantitative estimation of nitrite in water, cement, oil, coal and
Phenol.
LIST OF EXPERIMENTS
1. Determination of Redwood / Saybolt numbers, kinematic viscosity and viscosity index of
Lubricating oils
2. Determination of flash point, fire point, cloud and pour point of oils
3. Determination of acid value and iodine value of oils
4. Determination of COD of water samples
5. Cement Analysis
a. Estimation of silica content
b. Estimation of mixed oxide content
c. Estimation of calcium oxide content
d. Estimation of calcium oxide by rapid method
6. Coal Analysis
a. Estimation of sulphur present in coal
b. Ultimate analysis of coal
c. Proximate analysis of coal
7. Soap Analysis
a. Estimation of total fatty acid
b. Estimation of percentage alkali content
8. Flue gas analysis by Orsat’s apparatus
9. Estimation of phenol.
10. Determination of calorific value using bomb calorimeter
11. Determination of nitrite in water.
TOTAL: 60 PERIODS
OUTCOME
• Familiarization with equipment like viscometers, flash and fire point apparatus etc
• Familiarization of methods for determining COD
• Familiarization of a few simple synthetic techniques for soap
27
REFERENCE BOOKS
1. Environmental pollution analysis, S.M.Khopkar, New age international. 2011
2. Manual of environmental analysis, N.C Aery, Ane books. 2010
3. Text book of quantitative chemical analysis, J.Mendham, Pearson education 2008
GE7162 ENGINEERING PRACTICES LABORATORY L T P C

(Common to all Branches of B.E. / B.Tech. Programmes) 0 0 4 2
COURSE OBJECTIVES
• To provide exposure to the students with hands-on experience on various Basic Engineering
Practices in Civil, Mechanical, Electrical and Electronics Engineering.
GROUP – A (CIVIL & ELECTRICAL)

1. CIVIL ENGINEERING PRACTICES 15
PLUMBING
• Basic pipe connections involving the fittings like valves, taps, coupling, unions, reducers,
elbows and other components used in household fittings. Preparation of plumbing line
sketches.
• Laying pipe connection to the suction side of a pump.
• Laying pipe connection to the delivery side of a pump.
• Practice in connecting pipes of different materials: Metal, plastic and flexible pipes used in
householdappliances.
WOOD WORK
• Sawing, planing and making joints like T-Joint, Mortise and Tenon joint and Dovetail joint.
STUDY
• Study of joints in door panels and wooden furniture
• Study of common industrial trusses using models.
2. ELECTRICAL ENGINEERING PRACTICES 15

• Basic household wiring using Switches, Fuse, Indicator and Lamp etc.,
• Stair case light wiring
• Tube – light wiring
• Preparation of wiring diagrams for a given situation.
• Study of Iron-Box, Fan Regulator andEmergency Lamp
GROUP – B (MECHANICAL AND ELECTRONICS)
3. MECHANICAL ENGINEERING PRACTICES 15

WELDING
• Arc welding of Butt Joints, Lap Joints, and Tee Joints
• Gas welding Practice.
• Basic Machining - Simple turning, drilling and tapping operations..
• Study and assembling of the following:
a. Centrifugal pump
b. Mixie
c. Air Conditioner.
DEMONSTRATION ON FOUNDRY OPERATIONS.
4. ELECTRONIC ENGINEERING PRACTICES 15

• Soldering simple electronic circuits and checking continuity.
• Assembling electronic components on a small PCB and Testing.
• Study of Telephone, FM radio andLow Voltage Power supplies.
28
TOTAL : 60 PERIODS
COURSE OUTCOMES
 Ability to fabricate carpentry components and to lay pipe connections including plumbing
works.
 Ability to use welding equipments to join the structures
 Ability to do wiring for electrical connections and to fabricate electronics circuits.
MA7357 PROBABILITY AND STATISTICS L T PC

4 0 0 4
OBJECTIVES:
 To make the students acquire a sound knowledge in statistical techniques that model
engineering problems.
 The Students will have a fundamental knowledge of the concepts of probability.
UNIT I RANDOM VARIABLES 12

Discrete and continuous random variables – Moments – Moment generating functions –
Binomial, Poisson, Geometric, Uniform, Exponential, Gamma, Weibull and Normal distributions
- Functions of a random variable.
UNIT II TWO-DIMENSIONAL RANDOM VARIABLES 12

Joint distributions – Marginal and conditional distributions – Covariance – Correlation and Linear
regression – Transformation of random variables – Central limit theorem (for independent and
identically distributed random variables).
UNIT III TESTS OF SIGNIFICANCE 12

Sampling distributions - Tests for single mean, proportion, Difference of means (large and small
samples) – Tests for single variance and equality of variances – χ2- test for goodness of fit –
Independence of attributes – Non-parametric tests: Test for Randomness and Rank - sum test
(Wilcoxon test).
UNIT IV DESIGN OF EXPERIMENTS 12

Completely randomized design – Randomized block design – Latin square design - 22 -
factorial design - Taguchi’s robust parameter design.
UNIT V STATISTICAL QUALITY CONTROL 12

Control charts for measurements ( X and R charts) – Control charts for attributes (p, c and np
charts) – Tolerance limits - Acceptance sampling.
TOTAL : 60 PERIODS
OUTCOMES:
 Students will be able characterize probability models using probability mass (density)
functions & cumulative distribution functions.
 The students can independently participate in the processes of analysis, planning,
formulating strategies of development, decision-making, governing and management, and
independent making of tactical and strategic decisions related to the statistics.
29
TEXT BOOKS:
1. Milton, J. S. and Arnold, J.C., “Introduction to Probability and Statistics”, Tata McGraw Hill,
New Delhi, 4th Edition, 3rd Reprint, 2008.
2. Johnson, R.A. and Gupta, C.B., “Miller and Freund’s Probability and Statistics for
Engineers”, Pearson Education, Asia, 8th Edition, 2011.
REFERENCES:
1. Devore, J.L., “Probability and Statistics for Engineering and the Sciences”, Thomson
Brooks/Cole, International Student Edition, New Delhi, 7th Edition, 2008.
2. Walpole, R.E., Myers, R.H., Myers, S.L. and Ye, K., “Probability and Statistics for Engineers
and Scientists”, Pearson Education, Asia, 8th Edition, 2007.
3. Ross, S.M., “Introduction to Probability and Statistics for Engineers and Scientists”, Elsevier,
New Delhi, 3rd Edition, 2004.
4. Spiegel, M.R., Schiller, J. and Srinivasan, R.A., “Schaum’s Outline of Theory and Problems
of Probability and Statistics”, Tata McGraw Hill, New Delhi, 2004.
AS7302 PETROLEUM CHEMISTRY LTPC

3 003
AIM
To take an overview of downstream petroleum industry.
OBJECTIVES
To get acquainted with the various standards for the analysis s of petroleum products
UNIT I 9
Composition of Petroleum – separation by molecular weight, type; Composition maps;
Petroleum analysis and evaluation – ASTM evaluation, spectroscopic methods
UNIT II 9
Metals and heteroatom’s in heavy crude oil – heteroatom’s concentrations, structure of
heteroatom functions; Asphaltenes and structure of petroleum
UNIT III 9
Thermal chemistry of petroleum constituents – visbreaking, coking, hydro treating, hydro
cracking
UNIT IV 9
Heavy oil up gradation processes- carbon rejection, hydrogen addition; Hydro cracking
reactions, catalysts, process configurations
UNIT V 9
Instability of petroleum products – distillate and residual products; Incompatibility in refining
Operations
TOTAL : 45 PERIODS
TEXT BOOK
1. Speight, J.G., Petroleum chemistry and refining Taylor and Francis, London, 2015
REFERENCE
1. Speight, J.G., The chemistry and technology of petroleum, Marcel Dekker, New York, 2014
30
AS7301 FLUIDS AND SOLID OPERATIONS LTPC
4 004
AIM
To understand the principles and applications of fluid mechanics and mechanical operations.
OBJECTIVES
To impart to the student knowledge on fluid properties, fluid static and dynamic characteristics
flow metering and transport, particle mechanics, techniques of solid – fluid separation
UNIT I PROPERTIES OF FLUID 9

Newtonian fluids Classification of fluid motion Fluid statics – equilibrium of fluid element –
pressure variation in a static fluid – Differential analysis of fluid motion – continuity, Euler’s and
Bernoulli equation
UNIT II FLOW THROUGH PIPES & BOUNDARY LAYER CONCEPTS 9

Reynolds number regimes, Flow through pipes – pressure drop under laminar and turbulent flow
conditions; boundary layer concepts; different types of flowmeters; Valves, pumps, compressors
– characteristics and sizing; Agitation and Mixing;
UNIT III SIZE ANALYSIS 9

General characteristics of solids, techniques of size analysis; Laws of size reduction,
equipments for size reduction
UNIT IV FLOW THROUGH FLUIDIZED BEDS 9

Flow over a sphere – friction and pressure drag - flow through fixed and fluidized beds. Filtration
– batch and continuous, filtration equipments - selection, operation
UNIT V CLASSIFIERS 9
Screening, gravity separation - sedimentation, thickening, elutriation, classifiers - Centrifugal
separation - continuous centrifuges, cyclones and hydro cyclones, electrostatic and magnetic
separators
TEXT BOOKS
1. Noel de Nevers, "Fluid Mechanics for Chemical Engineers ", Second Edition, McGraw-Hill,
(1991).
2. Badger W.L. and Banchero J.T., "Introduction to Chemical Engineering", Tata McGraw Hill,
1997.
REFERENCES
1. Munson, B. R., Young, D.F., Okiishi, T.H. “Fundamentals of Fluid Mechanics”, 5th Edition“,
John Wiley, 2006
2. McCabe W.L, Smith, J C and Harriot. P “Unit operations in Chemical Engineering”, McGraw
Hill, V Edition, 2001
3. Coulson, J.M. and Richardson, J.F., "Chemical Engineering" Vol. I, 4th Edn., Asian Books
Pvt. Ltd., India, 1998.
31
GE7153 ENGINEERING MECHANICS L T P C
4 0 0 4
OBJECTIVE :
The objective of this course is to inculcate in the student the ability to analyze any problem in
a simple and logical manner and to predict the physical phenomena and thus lay the
foundation for engineering applications.
UNIT I STATICS OF PARTICLES 12

Fundamental Concepts and Principles, Systems of Units, Method of Problem Solutions,
Statics of Particles -Forces in a Plane, Resultant of Forces, Resolution of a Force into
Components, Rectangular Components of a Force, Unit Vectors.
Equilibrium of a Particle- Newton’s First Law of Motion, Space and Free-Body Diagrams,
Forces in Space, Equilibrium of a Particle in Space.
UNIT II EQUILIBRIUM OF RIGID BODIES 12

Principle of Transmissibility, Equivalent Forces, Vector Product of Two Vectors, Moment of a
Force about a Point ,Varignon’s Theorem, Rectangular Components of the Moment of a
Force, Scalar Product of Two Vectors, Mixed Triple Product of Three Vectors, Moment of a
Force about an Axis, Couple - Moment of a Couple, Equivalent Couples, Addition of Couples,
Resolution of a Given Force into a Force -Couple system, Further Reduction of a System of
Forces, Equilibrium in Two and Three Dimensions - Reactions at Supports and Connections.
UNIT III DISTRIBUTED FORCES 16

Centroids of lines and areas – symmetrical and unsymmetrical shapes, Determination of
Centroids by Integration , Theorems of Pappus-Guldinus, Distributed Loads on Beams,
Center of Gravity of a Three-Dimensional Body, Centroid of a Volume, Composite Bodies ,
Determination of Centroids of Volumes by Integration.
Moments of Inertia of Areas and Mass - Determination of the Moment of Inertia of an Area by
Integration , Polar Moment of Inertia , Radius of Gyration of an Area , Parallel-Axis Theorem ,
Moments of Inertia of Composite Areas, Moments of Inertia of a Mass - Moments of Inertia
of Thin Plates , Determination of the Moment of Inertia of a Three-Dimensional Body by
Integration.
UNIT IV FRICTION 8
The Laws of Dry Friction. Coefficients of Friction, Angles of Friction, Wedges, Wheel Friction.
Rolling Resistance , Ladder friction.
UNIT V DYNAMICS OF PARTICLES 12

Kinematics - Rectilinear Motion and Curvilinear Motion of Particles.
Kinetics- Newton’s Second Law of Motion -Equations of Motions , Dynamic Equilibrium,
Energy and Momentum Methods - Work of a Force , Kinetic Energy of a Particle, Principle of
Work and Energy, Principle of Impulse and Momentum, Impact, Method of Virtual Work -
Work of a Force, Potential Energy, Potential Energy and Equilibrium.
L – 45 + T – 15 TOTAL: 60 PERIODS
OUTCOMES:
 Upon completion of this course, students will be able to construct meaningful
mathematical models of physical problems and solve them.
TEXT BOOK
1. Beer,F.P and Johnson Jr. E.R, “Vector Mechanics for Engineers”, McGraw-Hill Education
(India) Pvt. Ltd. 10th Edition, 2013.
32
REFERENCES
1. Hibbeller, R.C., Engineering Mechanics: Statics, and Engineering Mechanics:
Dynamics, 13th edition, Prentice Hall, 2013.
2. J.L. Meriam & L.G. Karige, Engineering Mechanics: Statics (Volume I) and Engineering
Mechanics: Dynamics, 7th edition, Wiley student edition, 2013.
3. P. Boresi & J. Schmidt, Engineering Mechanics: Statics and Dynamics, 1/e, Cengage
learning, 2008.
4. Irving H. Shames, G. Krishna Mohana Rao, Engineering Mechanics - Statics and
Dynamics, Fourth Edition – PHI / Pearson Education Asia Pvt. Ltd., 2006.
5. Vela Murali, “Engineering Mechanics”, Oxford University Press (2010)
AS7303 SPECTROSCOPIC TECHNIQUES FOR PETROLEUM ENGINEERS LTPC

3003
AIM
To know the principle and importance of various analytical instruments used for the
characterization of various materials.
OBJECTIVES
To have thorough understanding of theory, instrumentation and applications of analytical
equipments used in industries for testing quality of raw materials, intermediates and finished
products.
To know the importance of analytical instrumentation during the purification, compounding and
formulating the finished product.
OUTCOME
To get knowledge in different analytical techniques and apply them to analyze the chemical and
petroleum products explored.
UNIT I INTRODUCTION TO SPECTROSCOPIC METHODS OF ANALYSIS 9

Electromagnetic radiation - Various ranges, Dual properties, Various energy levels, Interaction
of photons with matter, absorbance & transmittance and their relationship, Permitted energy
levels for the electrons of an atom and simple molecules, Jablonski diagrams, Various electronic
transitions in organic and inorganic compounds effected by UV and Visible radiations, Various
energy level diagrams of saturated, unsaturated and carbonyl compounds, excitation by UV and
Visible radiations, Choice of solvents, cut off wavelengths for solvents, Effects of auxochromes
and effects of conjugation on the absorption maxima, Different shifts of absorption peaks
(Bathochromic, hypsochromic, hypochromic, hyperchromic),
UNIT II UV AND VISIBLE SPECTROSCOPY 9

Qualitative Spectroscopy- Lamda max and epsilon max rules, , Woodward -Fieser rules for the
calculation of absorption maxima (Lamda max) for dienes and carbonyl compounds, Fieser and
kuhn rules - Instrumentation for UV and Visible spectrophotometer (source, optical parts and
detectors)-Applications of UV and Visible spectroscopy.
UNIT III QUANTITATIVE SPECTROSCOPY 9

Beer-Lambert's law, Limitations, Deviations (Real, Chemical, Instrumental), Estimation of
inorganic ions such as Fe, Ni and estimation of Nitrite using Beer-Lambert's Law.
Multicomponent analysis (no overlap, single way overlap and two way overlap), Photometric
titration (Experimental set-up and various types of titrations and their corresponding curves).
33
UNIT IV IR SPECTROSCOPY 9
Theory of IR spectroscopy, various stretching and vibration modes for diatomic and triatomic
molecules (both linear and nonlinear), various ranges of IR (Near, Mid, Finger print and Far) and
their usefulness, Instrumentation (Only the sources and detectors used in different regions),
sample preparation techniques. Qualitative analysis of alkanes, alkenes and carbonyl
compounds.
UNIT V ATOMIC SPECTROSCOPY 9

Atomic absorption spectrophotometry: Principle, Instrumentation (Types of burners, Types of
fuels, Hollow cathode lamp, Chopper only) and Applications, Various interferences observed in
AAS (Chemical, radiation and excitation)
Flame photometry: Principle, Instrumentation, quantitative analysis (Standard addition
method and internal standard method) and applications
Differences between AAS and FES.
TOTAL : 45 PERIODS
REFERENCES
1. Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Instrumental Analysis, CENGAGE
Learning, India, 7th Edition, 2007.
2. Willard H.H, Merritt L.L, Dean J.A and Settle F.A, Instrumental method of analysis, 7th
edition,Wadsworth Publishing Company, 1988.
3. Sharma, B.K., Instrumental Methods of Analysis, Goel publishing House, 24th Edition.
4. William Kemp, Organic Spectroscopy, 3rd Edition, Palgrave publishers, 2007.
5. Gurdeep R. Chatwal, Sharma K. Anand, Instrumental methods of Chemical Analysis,
Himalaya Publishers, New Delhi, 2014
6. John R Dyer, Applications of Absorption Spectroscopy of Organic Compounds, Prentice-hall
of India Pvt. Ltd., 2012
7. Robert M.Silverstein, Francis X.Webstrer, David Kiemle, David L.Bryce, Spectrometric
Identification of Organic Compounds, Wiley, 8th Edition
EE7254 PRINCIPLES OF ELECTRICAL AND ELECTRONICS ENGINEERING LTPC

3003
OBJECTIVES:
To impart knowledge on
• Electric circuit laws, single and three phase circuits and wiring
• Working principles of Electrical Machines
• Various electronic devices and measuring instruments
UNIT I ELECTRICAL CIRCUITS 9

Basic principles involved in power generation, transmission and distribution, Ohms Law
,Kirchoff’s Law , steady state solution of DC circuits , Thevinin’s Theorem, Norton’s Theorem,
Superposition Theorem.
UNIT II AC CIRCUITS 9
Introduction to AC circuits – waveforms and RMS value – power and power factor, single phase
and three-phase balanced circuits, housing wiring, industrial wiring, materials of wiring.
UNIT III ELECTRICAL MACHINES 9

Principles of operation and characteristics of DC machines. Transformers (single and three
phase) ,Synchronous machines , three phase and single phase induction motors.
34
UNIT IV ELECTRONIC DEVICES & CIRCUITS 9
Types of Materials –Silicon & Germanium- N type and P type materials – PN Junction –Forward
and Reverse Bias –Semiconductor Diodes –Bipolar Junction Transistor – Characteristics –
transistor as an Amplifier –Introduction to operational Amplifier –Inverting Amplifier –Non
Inverting Amplifier –DAC – ADC .
UNIT V MEASUREMENTS & INSTRUMENTATION 9

Introduction to transducers: pressure, temperature, position, electrical measurements
,Classification of instruments – moving coil and moving iron Ammeter and Voltmeter –
multimeters – dynamometer type Wattmeter – three-phase power measurements – energy
meter – megger – instrument transformers (CT and PT )
TOTAL : 45 PERIODS
OUTCOMES:
Ability to
 Understand electric circuits and working principles of electrical machines
 Understand the concepts of various electronic devices
 Choose appropriate instruments for electrical measurement for a specific application
REFERENCES
1. Del Toro, “Electrical Engineering Fundamentals”, Pearson Education, New Delhi, 2007
2. John Bird, “Electrical Circuit Theory and Technology”, Elsevier, First Indian Edition, 2006
3. Allan S Moris, “Measurement and Instrumentation Principles”, Elseveir, First Indian Edition,
2006
4. Rajendra Prasad, “Fundamentals of Electrical Engineering”, Prentice Hall of India, 2006
5. Thereja .B.L., “Fundamentals of Electrical Engineering and Electronics”, S. Chand & Co.
Ltd., 2008
6. V.K Mehta and Rohit Mehta, “Principle of Electrical Engineering”, S. Chand & Company,
2008
EE7312 ELECTRICAL ENGINEERING LABORATORY LTPC

FOR TECHNOLOGISTS 0042
OBJECTIVES
To provide the practical knowledge and control methods of electrical machines
OUTCOMES
To impart practical knowledge on
I. Characteristics of different machines
II. Method of speed control of machines
III. Measurement of various electrical parameters.
1. Study of Starters
2. Power Measurements in Three-Phase Circuits
3. Speed Control of DC Motor
4. Load Test on DC Shunt Motor
5. OCC & Load Test on DC Shunt Generator
6. Load Test on DC series motor.
7. OC and SC Test on Single- Phase Transformer
8. Load Test on Single-Phase Transformer
9. Load Test on Single-Phase Induction Motor
10. Load Test on Three-Phase Induction Motor
11. Load Characteristics of Alternator.
TOTAL : 60 PERIODS
35
AS7313 FLUID MECHANICS AND MECHANICAL OPERATIONS LABORATORY LT P C
0042
OBJECTIVES
• To learn experimentally to calibrate flow meters, find pressure loss for fluid flows and
determine pump characteristics.
• Students develop a sound working knowledge on different types of crushing equipments and
separation characteristics of different mechanical operation separators.
OUTCOME:
Use variable area flow meters and variable head flow meters
Analyze the flow of fluids through closed conduits, open channels and flow past immersed
bodies Select pumps for the transportation of fluids based on process conditions/requirements
and fluid properties.
Determine work index, average particle size through experiments by crushers, ball mill and
conducting sieve analysis.
Design size separation equipments such as cyclone separator, sedimentation, Filters etc.
LIST OF EXPERIMENTS - Phase - I

1. Calibration of constant and variable head meters
2. Open drum orifice and draining time
3. Flow through straight pipe
4. Flow through annular pipe
5. Flow through helical coil and spiral coil
6. Characteristic curves of pumps
7. Pressure drop studies in packed column
EQUIPMENT REQUIRED
1. Venturi meter
2. Orifice meter
3. Rotameter
4. Weir
5. Open drum with orifice
6. Pipes and fittings
7. Helical and spiral coils
8. Centrifugal pump
9. Packed column
10. Fluidized bed
LIST OF EXPERIMENTS - Phase- II

1. Sieve analysis
2. Batch filtration studies using a Leaf filter
3. Batch filtration studies using a Plate and Frame Filter press
4. Characteristics of batch Sedimentation
5. Reduction ratio in Jaw Crusher
6. Reduction ratio in Ball mill
7. Separation characteristics of Cyclone separator
8. Reduction ratio of Roll Crusher
EQUIPMENT REQUIRED
1. Sieve shaker
2. Leaf filter
3. Plate and Frame Filter Press
4. Sedimentation Jar
36
5. Jaw Crusher
6. Ball Mill
7. Cyclone Separator
8. Roll Crusher
9. Elutriator
10. Drop Weight Crusher
11. Sieves.
TOTAL : 60 PERIODS
AS7401 CHEMICAL ENGINEERING THERMODYNAMICS LTPC

4004
AIM
To study the basic concepts involved in Thermodynamics and their application
OBJECTIVE
Students will learn heat and work effects associated with process, PVT behavior of fluids, laws of
thermodynamics and their application, Phase and Reaction equilibrium.
OUTCOME
Evaluate the thermodynamic properties of fluids.
Analyze the feasibility of systems/devices.
Calculate chemical reaction rate and equilibrium composition.
UNIT I ZEROTH AND FIRST LAW OF THERMODYNAMICS 12

Definitions and Concepts, Scope of Thermodynamics, Zeroth law; Temperature scales; Equations
of state for ideal and real gases; First law and internal energy; First law for the non flow and flow
systems; Enthalpy and heat capacity; Limitations of first law.
UNIT II SECOND LAW OF THERMODYNAMICS 12

Statements of the second law of thermodynamics; Carnot cycle and Carnot theorems;
Thermodynamic temperature scale; Entropy and its calculation; Clausius Inequality; Applications of
the second law.
UNIT III THERMODYNAMIC FORMULATIONS 12

Measurable quantities; Basic energy relations, Maxwell relations, Thermodynamic formulations to
calculate enthalpy, internal energy and entropy as a function of pressure and temperature;
Formulations involving Cp and Cv; Complex thermodynamic formulations, Thermodynamic
properties of an ideal gas, entropy change in reversible and irreversible process.
UNIT IV THERMODYNAMIC PROPERTIES OF REAL GASES 12

PVT behavior of fluids; Mathematical representation for PVT behavior; Generalized compressibility
factor correlation; Generalized equation of state; Partial molar properties; Chemical potential,
fugacity and fugacity coefficient for pure species and species in solution; Residual properties;
Properties of solutions; ideal solutions; Excess properties; Gibbs free energy models; Henry’s law.
UNIT V PHASE EQUILIBRIA AND CHEMICAL EQUILIBRIA 12

Criteria for equilibrium between phases in multi component non- reacting systems; Applications of
phase rule; Qualitative behavior of Vapor- liquid equilibrium in binary and multicomponent system;
Chemical Reaction Equilibria – Reaction coordinate; Criteria for chemical equilibria; Equilibrium
constant; Equilibrium compositions of homogeneous gas and liquid phase reactions.
TOTAL: 60 PERIODS
37
TEXT BOOK
1. Smith, J.M., Van Ness, H.C., “Introduction to Chemical Engineering Thermodynamics ",
Kogakushai 1976.
REFERENCES
1. Hougen, O.A., Watson, K.M., and Ragatz, R.A., " Chemical Process Principles " Part II 2nd
edition, John Wiley Newyork 1970.
2. Dodge, B.F., " Chemical Engineering Thermodynamics ", McGraw-Hill, Newyork 1960.
3. Sandler, S.I., " Chemical and Engineering Thermodynamics 4th edition. ", John Wiley, 2007.
4. Kyle, B.G., " Chemical and Process Thermodynamics 3rd edition. ", Prentice Hall of India
Pvt.Ltd., 2003.
AS7403 RESERVOIR ENGINEERING LTPC

3 003
AIM
To understand a reservoir and know its properties.
OBJECITVES
To learn about basic rock and fluid properties relevant to petroleum reservoir.
To understand the causes of variation in the behavior of rocks and fluids.
To understand the drive mechanism of a reservoir
UNIT I RESERVOIR FLUID BEHAVIOR AND PROPERTIES 9

Classification of Reservoir and Reservoir Fluids. Properties of Natural Gases. Direct Calculation
of Compressibility Factors. Methods of Calculating Viscosity of Natural Gases, Properties of
Crude Oil Systems. Methods of Calculating Viscosity of the Dead Oil. Properties of Reservoir
Water.
UNIT II ANALYSIS OF RESERVOIR FLUID AND ROCK PROPERTIES 9

Composition of Reservoir Fluid, Separation Test, Laboratory Analysis of Gas Condensate
System, Porosity and Capillary Pressure. Rock Compressibility, Reservoir Heterogeneity.
Dynamic Pseudo-Relative Permeabilities, Two Phase and Three Phase Relative Permeability.
UNIT III FUNDAMENTALS OF RESERVOIR FLUID FLOW 9

Reservoir Geometry, Fluid Flow Equations, Steady State and Unsteady State Flow, Constant
Terminal Pressure Solution. Horizontal and Vertical Oil Well and Gas Well Performance.
UNIT IV RECOVERY MECHANISM AND MATERIAL BALANCE 9

Primary Recovery Mechanism, Material Balance Equation, Performance prediction Methods and
Relating Reservoir Performance to Time. Volumetric Method and the Material Balance
Equations as a Straight Line in Gas Reservoir.
UNIT V WATER FLOODING AND VAPOR LIQUID PHASE EQUILIBRIUM 9

Factors to consider in Water Flooding, Optimum Time to Water Flooding, Selection of Flooding
Patterns, Overall Recovery Efficiency, Displacement Efficiency, Vertical Sweep Efficiency.
Equilibrium Ratio, Flash Calculations, Equilibrium Ratios for Real Solution. Application of the
Equilibrium Ratio in Reservoir Engineering.
TOTAL : 45 PERIODS
38
REFERENCES
1. Ahmed, T, “Reservoir Engineering Handbook”, 3rd Edition, Elsevier, 2010.
2. Slip Slider, H.C. “Worldwide Practical Petroleum Reservoir Engineering Method”, PennWell
Publishing Company, 1983.
3. Gian.Luigichierici, “Principles of Petroleum Reservoir Engineering”, Elsevier, 2011.
AS7402 INDUSTRIAL STOICHIOMETRY LTPC

3003
OBJECTIVES
To acquire a concept of degree of freedom and its application to solution of mass and energy
balance equations for single and network of units and introduce to process simulators
OUTCOME
Understand the fundamentals of units and stoichiometric equations. Write material balance for
different chemical process. Understand the fundamentals of ideal gas behavior and phase
equilbria. Write energy balance for different chemical process.
UNIT I 9
Units, dimensions and conversion; Chemical & Petrochemical Process variables and properties;
Stoichiometric Equations, Degrees of freedom
UNIT II 9
Introduction to material balances. Material balance problems for single units; Stoichiometry and
Petrochemical & Chemical reaction equations; material balance for processes involving reaction
bypass, purging, recycle operations.
UNIT III 9
Ideal gases, Real gases, Single component two phase systems, Multiple component phase
systems, Phase rule, Phase equilbria, Combustion processes.
UNIT IV 9
Energy balances, Conservation of Energy processes without reaction, Heat capacity, Energy
balances with chemical reaction, Efficiency applications.
UNIT V 9
Application of energy balances. Unsteady state material and energy balances. Solving material
and energy balances using process simulators.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Himmelblau, D.M., “Basic Principles and Calculations in Chemical Engineering”, EEE Sixth
Edition, Prentice Hall Inc., 2003
2. Felder, R. M. and Rousseau, R. W., “Elementary Principles of Chemical Processes”, 3rd
Edn., John Wiley & Sons, New York, 2000.
3. Bhatt, B.L., Vora, S.M., “Stoichiometry “, 4th Edition,Tata McGraw-Hill (2004)
REFERENCES
1. Hougen O A, Watson K M and Ragatz R A, “Chemical process principles” Part I, CBS
publishers (1973).
39
ME7251 BASIC MECHANICAL ENGINEERING LTPC
3003
OBJECTIVE
To impart knowledge on thermodynamics and thermal engineering power generating units such
as engines and theory of machines
OUTCOME
• Students should learn thermodynamics and thermal engineering to understand the
principles behind the operation of thermal equipments like IC engines and turbines etc.,
Students should be able to appreciate the theory behind operation of machinery and be
able to design simple mechanisms
UNIT I LAWS OF THERMODYNAMICS 10

Basic concepts and hints; Zeroth law; First Law of Thermodynamics - Statement and
application; Steady flow energy equation-problems- Second law of Thermodynamics – Kelvin
- Plank statement and Clausius statement- problems; Limitations; Heat Engine, Refrigerator and
Heat Pump, Available energy, Third law of Thermodynamics - Statement.
UNIT II HEATING AND EXPANSION OF GASES 6

Expressions for work done, Internal energy and heat transfer for Constant Pressure, Constant
Volume, Isothermal, Adiabatic and Polytropic processes-Derivations and problems; Free
expansion and Throttling process.
UNIT III AIR STANDARD CYCLES 6

Carnot cycle; Stirlings cycle; Joule cycle; Otto cycle; Diesel cycle; Dual combustion Cycle-
Derivations and problems.
UNIT IV I.C. ENGINES, STEAM AND ITS PROPERTIES AND STEAM

TURBINES 12
Engine nomenclature and classification; SI Engine; CI Engine; Four Stroke cycle, Two stroke
cycle; Performance of I.C.Engine; Brake thermal efficiency; Indicated Thermal Efficiency,
Specific fuel consumption.
Steam - Properties of steam; Dryness fraction; latent heat; Total heat of wet steam; Dry steam;
Superheated steam. Use of steam tables; volume of wet steam, volume of superheated steam;
External work of evaporation; Internal energy; Entropy of vapour, Expansion of vapour, Rankine
cycle.
Steam turbines – Impulse and Reaction types - Principles of operation.
UNIT V SIMPLE MECHANISM, FLY WHEEL, DRIVES AND BALANCING 11

Definition of Kinematic Links, Pairs and Kinematic Chains; Flywheel-Turning moment Diagram;
Fluctuation of Energy. Belt and rope drives; Velocity ratio; slip; Creep; Ratio of tensions; Length
of belt; Power Transmitted; gear trains-types. Balancing of rotating masses in same plane;
Balancing of masses rotating in different planes.
TOTAL : 45 PERIODS
TEXT BOOKS
1. Nag, P.K., “ Engineering Thermodynamics “, II Edition, Tata McGraw Hill Publishing Co.,
Ltd., 1995
2. Rajput, R .K, “Thermal Engineering”, Laxmi publications (P) Ltd, 2001.
3. Khurmi R.S., and Gupta J.K, “Theory of Machines”, Eurasia Publishing House (P) Ltd.,
2004.
40
REFERENCES
1. Smith, “ Chemical Thermodynamics “, Reinhold Publishing Co., 1977.
2. Bhaskaran, K.A., and Venkatesh, A., “ Engineering Thermodynamics “,Tata McGraw Hill,
1973.
3. Pandya A. and Shah, “ Theory of Machines “, Charatakar Publishers, 1975.
4. Khurmi R.S., and Gupta J.K, “Thermal Engineering”, S.Chand & Company (P) Ltd.,2001.
5. Kothandaraman and Dhomkundwar,”: A course in Thermal Engineering (SI Units)”, Dhanpat
Rai and Sons, Delhi (2001)
ME7262 MECHANICAL ENGINEERING LABORATORY LTPC

0042
OBJECTIVE
To impart practical knowledge in operating IC engines and conduct experiments. To understand

test procedures in testing material for engineering applications
OUTCOME
• Students will be able to understand Power-generating units such as engines and operate
IC engines and conduct tests. They will be able to appreciate the theory behind the
functioning of engines. Material properties, their behavior under different kinds of loading
and testing can be visualized.
LIST OF EXPERIMENTS
1. Port timing diagram

2. Valve timing diagram
3. Study of 2,4 stroke I C Engines
4. Load test on 4-stroke petrol engine
5. Performance test on 4-stroke single cylinder diesel engine
6. Performance test on 4-stroke twin cylinder diesel engine
7. Heat balance test on diesel engines
8. Tension test
9. Compression test
10. Deflection test
11. Hardness test (Rockwell and Brinell)
12. Spring test
13. Torsion test
14. Impact test
TOTAL : 60 PERIODS
* Minimum 10 experiments shall be offered.
41
AS7412 ORGANIC CHEMISTRY LABORATORY FOR
PETROCHEMICAL ENGINEERS LT P C
0042
OBJECTIVES
 To learn basic principles involved in analysis and synthesis of different organic derivatives.
OUTCOME:
Conduct simple experiments to identify the functional groups
Prepare derivatives for aldehydes, ketones, sugars, amine and phenol
To separate organic mixtures
To carry out recrystallization
LIST OF EXPERIMENTS
1. Identification and characterization of various functional groups by their characteristic

reactions: a) alcohol, b) aldehyde, c) ketone, d) carboxylic acid, e) phenol f) primary,
secondary and tertiary amines
2. preparation of solid derivatives : a) 2,4 tri nitro phenyl hydrazone for aldehydes and
ketones, b) Osazone for sugras, c) acetyl and benzoyl derivatives for amine and phenol
d) diazotization of aromatic amine
3. Preparation of Methyl red and Fluorescein
4. Separation of organic mixtures: a) aldehyde and acid, b) amine and phenol
5. Recrytallization of benzoic acid and acetanilide
6. Preparation of simple pharmaceuticals a) acetanilide, b) methyl salicylate, c) aspirin
7. Detection of peroxide in ether and its removal
TOTAL : 60 PERIODS
REFERENCE
1. Practical organic chemistry, S.P. Bhutani, Ane books. 2009
2. Practical chemistry, V K Ahluwalia, University press. 2011
3. Text book of practical organic chemistry. Brain S Furniss, Pearson education 2011
4. Practical Organic Chemistry by Dey and Raman
5. Laboratory Manual of Organic Synthesis by M.N.Khramkina MIR publishers Moscow,
First published in 1980, revised editions once in every five year. Last revised edition
2010.
6. Practical Chemistry by Balwant Rai Satija, Allied Publishers Pvt Ltd 1988.
AS7503 PETROLEUM REFINING - I LTPC

3 003
AIM
To know the knowledge of petroleum refining process.
OBJECTIVES
To understand the nature of hydrocarbon reservoirs.
To be familiar with pressure transient analysis.
42
UNIT I 9
Exploration and Refining of Crude Oil: Introduction, Indian and world reserve of crude oil and its
processing capacity, Market demand & supply of petroleum Fractions. Exploration, Drilling and
Production of crude oil; engineering data of crude and fractions. Characterization factor, Key
Fraction Number and correlation index methods for evaluation of crude & fractions. TBP, ASTM,
EFV, and their inter-convertibility, yield Curve etc.
UNIT II 9
Desalting of crude, pipe still furnaces, preflashing operation, Atmospheric and vacuum distillation
units, different types of Reflux arrangements, Calculation of tray requirement for ADU column.
Test methods and specifications: Distillation, Aniline point, Reid vapour pressure, Smoke point,
flash point fire point, Carbon residue, viscosity and viscosity index, refractive index, Copper &
silver strip corrosion, Octane No, Cetane No, Sulphur content, Calorific value, Total acid number,
oxidation stability, cloud point, pour point etc.
UNIT III 9
Thermal conversion Processes: Thermal cracking processes – mechanism, applications e.g.
visbreaking, thermal cracking, coking operations, Catalytic Conversion Processes : Catalytic
cracking processes, Different FCC operating modes, Catalytic reforming operations, Hydro
cracking, Simple process calculations.
UNIT IV 9
Thermal Polymerization, Isomerization processes, Alkylation, Catalytic Polymerization for
gasoline stock preparation.
UNIT V 9
Finishing & Treatment processes: Different Hydro treatment (e.g. Hydro desulfurization)
processes, Merox process, Doctor’s sweetening, Smoke point improvement, etc. Simple process
calculations Alternative fuels, Production and Specifications: Synthetic gasoline, Bio Diesel,
Ethanol, Automotive LPG
TOTAL : 45 PERIODS
TEXT BOOKS
1. Petroleum Refinery Engineering – W.L. Nelson, Mc Graw Hill, 2007.
2. Modern Petroleum Refining Processes – B.K. Rao. Oxford & IBM., 2007.
REFERENCES
1. Petroleum Refining Technology – Dr. Ram Prasad, Khanna Publishers.
2. Advanced Petroleum Refining: Dr. G. N. Sarkar, Khanna Publishers.
AS7502 NATURAL GAS ENGINEERING LTPC

3 003
AIM
The main of learning this subject is that student will be able to understand the basics of Natural
Gas engineering techniques.
OBJECTIVES
The objective of studying this subject is that student will be understanding the basic concept
and applications of Natural Gas Engineering.
43
UNIT I 9
Natural gas technology and earth science: Branches of petroleum Industry. Sources of
Information for natural gas engineering and its applications. Geology and earth sciences: Earth
sciences-Historical geology, Sedimentation process, Petroleum reservoirs, Origin of petroleum.
Earth temperatures & pressure, Earth temperatures, Earth pressure. Petroleum: Natural gas, LP
gas, Condensate, & Crude oil.
UNIT II 9
Properties of Natural Gases: typical compositions. Equations of state: general cubic equations,
specific high accuracy equations. Use of equation of state to find residual energy properties, gas
measurement gas hydrates, condensate stabilization, acid gas treating, gas dehydrations,
compressors, process control deliverability test, gathering and transmission, and natural gas
liquefaction.
UNIT III 9
Gas Compression: Positive displacement and centrifugal compressors; fans. Calculation of poser
requirements. Compressible Flow in Pipes, Fundamental equations of flow: continuity,
momentum, elegy equations.
UNIT IV 9
Isothermal flow in pipes: the Weymouth equation. Static and flowing bottom-hole pressures in
wells. Fundamentals of Gas flow in porous media: Steady state flow equations. Definition of
pseudo-pressure function. Gas flow in cylindrical reservoirs: general equation for radial flow of
gases in symmetrical homogeneous reservoirs.
UNIT V 9
Non-dimensional forms of the equation; derivation of coefficients relation dimensionless to real
variables. Infinite reservoir solution: Pseudo-steady-state solution. Gas Well Deliverability Tests:
Flow-after-flow tests: prediction of IPR curve and AOF for the well. Isochronal tests. Draw down
tests: need for data at two flow rates.
TOTAL : 45 PERIODS
TEXT BOOK
1. Katz D.L.et al., Natural Gas Engineering (Production & storage), McGraw-Hill, Singapore.
REFERENCE :
1. Standard Handbook of Petroleum and Natural Gas Engineering. 2nd Edition. William C
Lyons, Gary C Plisga. Gulf Professional Publishing.
AS7501 HEAT AND MASS TRANSFER FOR PETROCHEMICAL ENGINEERS LTPC

4004
AIM
To learn heat transfer by different modes of heat transfer and to develop skills of the students
in the area of Mass Transfer operation
OBJECTIVES
Students gain knowledge in various heat transfer and mass transfer operations in process
engineering and also to design heat transfer and mass transfer equipments
44
UNIT I 12
Importance of heat transfer in Chemical Engineering operations - Modes of heat transfer -
Fourier’s law of heat conduction - one dimensional steady state heat conduction equation for flat
plate, hollow cylinder, - Heat conduction through a series of resistances - Thermal conductivity
measurement; effect of temperature on thermal conductivity; Radiation heat transfer - Black
body radiation, Emissivity, Stefan - Boltzman law, Plank’s law, radiation between surfaces.
UNIT II 12
Concepts of heat transfer by convection - Natural and forced convection, analogies between
transfer of momentum and heat - Reynold’s analogy, Prandtl and Coulburn analogy.
Dimensional analysis in heat transfer, heat transfer coefficient for flow through a pipe, flow past
flat plate, flow through packed beds. Heat transfer to boiling liquids - mechanism of boiling,
nucleate boiling and film boiling.
UNIT III 12
Theory of evaporation - single effect and multiple effect evaporation - Design calculation for
single and multiple effect evaporation. Log mean temperature difference - Single pass and
multipass heat exchangers; plate heat exchangers; use of correction factor charts; heat
exchangers effectiveness; number of transfer unit - Chart for different configurations - Fouling
factors
UNIT IV 12
Introduction to mass transfer operations; Molecular diffusion in gases, liquids and solids;
diffusivity measurement and prediction; multi-component diffusion. theories of mass transfer, ,
relationship between individual and overall mass transfer coefficients. Stage-wise and
differential contractors. Gas Absorption and Stripping – Equilibrium; material balance; limiting
gas-liquid ratio; tray tower absorber - calculation of number of theoretical stages,
UNIT V 12
Principle of distillation - flash distillation, differential distillation, steam distillation, multistage
continuous rectification, Number of ideal stages by Mc.Cabe - Thiele method and Ponchan -
Savarit method, Introduction to multi-component distillation, azeotropic and extractive
distillation. Liquid - liquid extraction - solvent characteristics-equilibrium stage wise contact
calculations for batch and continuous extractors
TOTAL : 60 PERIODS
TEXT BOOKS
1. Holman, J. P., ‘Heat Transfer ’, 8th Edn., McGraw Hill, 1997.
2. Ozisik, M. N., Heat Transfer: A Basic Approach, McGraw-Hill, 1984
3. Kern, D.Q., “Process Heat Transfer “, McGraw-Hill, 1999.
4. Seader, J.D. and E.J. Henley, “Separation Process Principles”, 2nd Ed., John Wiley,2006.
REFERENCES
1. McCabe, W.L., Smith, J.C., and Harriot, P., “Unit Operations in Chemical Engineering”, 6th
Edn., McGraw-Hill, 2001.
2. Coulson, J.M. and Richardson, J.F., “Chemical Engineering “ Vol. I, 4th Edn., Asian
Books Pvt. Ltd., India, 1998.
45
GE7351 ENGINEERING ETHICS AND HUMAN VALUES LTPC
300 3
OBJECTIVES
• To emphasise into awareness on Engineering Ethics and Human Values.
• To understand social responsibility of an engineer.
• To appreciate ethical dilemma while discharging duties in professional life.
UNIT I HUMAN VALUES 3
Morals, Values and Ethics – Integrity – Work Ethic – Honesty – Courage –Empathy – Self-
Confidence – Discrimination- Character.
UNIT II ENGINEERING ETHICS 9

Senses of 'Engineering Ethics' - variety of moral issued - types of inquiry - moral dilemmas -
moral autonomy - Kohlberg's theory - Gilligan's theory - consensus and controversy – Models of
Professional Roles - theories about right action - Self-interest –Professional Ideals and Virtues
- uses of ethical theories. Valuing Time – Co-operation – Commitment –
UNIT III ENGINEERING AS SOCIAL EXPERIMENTATION 9

Engineering as experimentation - engineers as responsible experimenters - codes of ethics –
Importance of Industrial Standards - a balanced outlook on law – anticorruption- occupational
crime -the challenger case study.
UNIT IV ENGINEER’S RIGHTS AND RESPONSIBILITIESON SAFETY 12

Collegiality and loyalty – Respect for authority – Collective Bargaining – Confidentiality- Conflict
of interest – Occupational Crime – Professional Rights – IPR- Safety and risk - assessment of
safety and risk - risk benefit analysis and reducing risk - the Three Mile Island, Bhopal Gas plant
and chernobyl as case studies.
UNIT V GLOBAL ISSUES 12

Multinational corporations - Environmental ethics - computer ethics - weapons development -
engineers as managers-consulting engineers-engineers as expert witnesses and advisors -
moral leadership-Sample code of conduct.
TOTAL : 45 PERIODS
OUTCOMES
 Students will have the ability to perform with professionalism , understand their rights , legal
,ethical issues and their responsibilities as it pertains to engineering profession with
engaging in life-long learning with knowledge of contemporary issues.
TEXT BOOKS
1. Mike Martin and Roland Schinzinger, “Ethics in Engineering”, McGraw-Hill, New York
2005.
2. Charles E Harris, Michael S. Protchard and Michael J Rabins, “Engineering Ethics –
Concepts and Cases”, Wadsworth Thompson Leatning, United States, 2000 (Indian
3. Govindarajan M, Natarajan S, Senthil Kumar V. S, “Engineering Ethics”, Prentice Hall of
India, New Delhi, 2004.
REFERENCES
1. Charles D. Fleddermann, “Engineering Ethics”, Pearson Education / Prentice Hall, New
Jersey, 2004
2. Charles E Harris, Michael S. Protchard and Michael J Rabins, “Engineering Ethics –
Concepts and Cases”, Wadsworth Thompson Leatning, United States, 2000
3. John R Boatright, “Ethics and the Conduct of Business”, Pearson Education, New Delhi,
2003.
4. Edmund G Seebauer and Robert L Barry, “Fundamentals of Ethics for Scientists and
Engineers”, Oxford Press , 2000
5. R.Subramanian , “Professional Ethics “,Oxford University Press ,Reprint ,2015.
46
CH7561 HEAT TRANSFER LABORATORY LTPC
0042
OBJECTIVES
Students develop a sound working knowledge on different types of heat transfer
equipments
LIST OF EXPERIMENTS*
1. Performance studies on Cooling Tower
2. Batch drying kinetics using Tray Dryer
3. Heat transfer in Open Pan Evaporator
4. Boiling Heat Transfer
5. Heat Transfer through Packed Bed
6. Heat Transfer in a Double Pipe Heat Exchanger
7. Heat Transfer in a Bare and Finned Tube Heat Exchanger
8. Heat Transfer in a Condenser
9. Heat Transfer in Helical Coils
10. Heat Transfer in Agitated Vessels
EQUIPMENT REQUIRED
1. Cooling Tower
2. Tray Dryer
3. Open Pan Evaporator
4. Boiler
5. Packed Bed
6. Double Pipe Heat Exchanger
7. Bare and Finned Tube Heat Exchanger
8. Condenser
9. Helical Coil
10. Agitated Vessel
*Minimum 10 experiments shall be offered
TOTAL : 60 PERIODS
OUTCOMES
Determine Heat transfer co-efficient and evaluate performance of different types of
equipments including cooling towers, tray dryers, pan evaporator, packed bed, heat
exchangers, condensers, helical coils and agitated vessels
AS7511 PETROLEUM TESTING LABORATORY LTPC

0042
AIM:
To introduce various methods of analysis by using instruments and analytical equipment to
determine various physical properties of petroleum and petroleum products
OBJECTIVES:
On completion of the course, the students should be conversant with the theoretical
principles and experimental procedures for quantitative estimation.
47
LIST OF EXPERIMENT
1. Determination of flash point.
2. Carbon residue determination of petroleum products.
3. Distillation of crude oil
4. Determination of viscosity capillary viscometer.
5. Density of crude oil by hydrometer.
6. Pour point of crude oil and petroleum products.
7. Determination of calorific value of fuels.
8. Determination of refractive index of the petroleum products.
9. Determination of salacity of oil field waters
10. Characterization of formation waters
11. Water content in crude oil
12. Moisture content in crude oil and products
13. BS&W in crude oil
TOTAL : 60 PERIODS
LIST OF EQUIPMENT
1. Flash point apparatus.
2. Centrifuge
3. Dean and Stark Apparatus
4. API standard distillation apparatus
5. Capillary Viscometer
6. Gas Chromatograph
7. Bomb calorimeter
8. Refractometer
9. Junker gas calorimeter
10. Glass wares, balance, hot plate and heating mantle
11. Pour Point Apparatus
12. Karl Fisher Apparatus
AS7603 PETROLEUM REFINING – II LTPC

4 004
AIM
To know the processes involved in refining of petroleum products
OBJECTIVES
Know surface facility equipment and facilities for production and separation of hydrocarbons.
Knowledge of different types of bottom hole production tools and their utility.
Understanding of multiphase flows and their equations for production operations.
UNIT I CRACKING 9
Need and significance, types and functions of Secondary Processing. Cracking, Thermal
Cracking and Visbreaking. Different Feed Stocks, Products Yields, Qualities and Recent
Development. Catalytic Cracking, Commercial Catalyst, Feedstock and Catalytic Cracking
Conditions, Types and Processes- Fixed Bed Cracker, Fluid Catalytic Cracking (FCC), Flexi
Cracking.
UNIT II CATALYTIC REFORMING 9

Theory, Reaction Conditions and Catalyst for Catalytic Reforming, Plat forming, Houdri Forming,
Rhein Forming, Power Forming, Selecto Forming. Ultra Forming and Rex Forming. Naphtha
Cracking, Feedstock Selection and Effect of Steam.
48
UNIT III ALKYLATION AND ISOMERIZATION 9
Feed Stocks and Reactions for Alkylation Process- Cascade Sulphuric Acid Alkylation,
Hydrofluoric Acid Alkylation. Isomerization Process- Isomerization with Platinum Catalyst and
Aluminum Chloride Process.
UNIT IV COKING 9
Methods of Petroleum Coke Production – Koppers, Thermal Cracking, Delayed Coking, Fluid
Coking and Contact Coking. Hydro Cracking- principles, reactions in Hydro Cracking, Catalyst,
Hydro Cracking Reaction Conditions, Iso Max Processes and Hydro Desulphurization
Processes.
UNIT V ASPHALT TECHNOLOGY 9

Source of Asphalt (Bitumen), Chemical Structure of Asphalt, Action of Heat on Asphalt, Types of
Asphalts. Air Blowing of Bitumen and Up gradation of Heavy Crudes. Specialty Products:
Industrial Grease- Manufacture of Calcium Grease, Liquid Paraffin and Petroleum Jelly’s.
TOTAL : 60 PERIODS
TEXT BOOKS
1. Jones, D.S.J. and Pujadó, P.R., Handbook of petroleum processing, Springer, The
Netherlands, 2006
2. Nelson, W. L “Petroleum Refinery Engineering”, McGraw Hill Publishing Company Limited,
1985.
3. Watkins, R. N “Petroleum Refinery Distillations”, 2nd Edition, Gulf Publishing Company,
Texas, 1981.
REFERENCES
1. Parkash, S., Refining processes handbook, Gulf Professional Publishing, 2003
2. Hobson, G. D “Modern Petroleum Refining Technology”, 4th Edition, Institute of
Petroleum,U. K. 1973.
AS7602 PETROCHEMICALS LTPC

4 004
AIM
To know about various processes involved in petroleum products.
OBJECTIVES
To develop understanding of the principles, techniques, standard tools of process optimization.
To formulate multi objective optimization problem with and without constraints based on process
requirements.
UNIT I 12
Overview of petrochemical industrial Growth in India, Economics, Feedstock Selection for
Petrochemicals
UNIT II 12
Steam reforming, Hydrogen, Synthesis gas, cracking of gaseous and liquid for stocks, Olefins,
Diolifins, Acetylene and Aromatics and their separation.
UNIT III 12
Alkylation, Oxidation, Dehydrogenation, Nitration, Chlorination, Sulphonation and Isomerization
UNIT IV 12
Chemicals from synthesis gas, Olefins, Diolefins, Acetylene and Aromatics
49
UNIT V 12
Modes and techniques, Production of Polyethylene, PVC, Polypropylene, SAN, ABS, SBR,
Polyacrylonitrile, Polycarbonates, Polyurethane, Nylon, PET
TOTAL : 60 PERIODS
REFERENCES
1. Brownstein A.M. Trends in Petrochemical Technology, Petroleum Publishing Company,
1976.
2. Sitting M., Aromatics Hydrocarbons, Manufacture and Technology, Noyes Data Corporation,
1976.
3. Stevens P.M. Polymer Chemistry, Addison Wesley Publishing Company, 1975.
4. Hatch F. and Sami Mater, “From Hydrocarbon to Petrochemicals”, Gulf Publishing
Company, Texas 1998.
5. Petrochemical Hand book Hydrocarbon Processing 1989.
AS7601 CATALYTIC REACTION ENGINEERING LT PC

40 04
AIM
To impart knowledge to design different types of chemical reactors
OBJECTIVES
To gain knowledge on different types of chemical reactors, the design of chemical reactors
under isothermal and non-isothermal conditions
UNIT I CHEMICAL KINETICS AND IDEAL REACTORS 12

Rate equation, elementary, non-elementary reactions, theories of reaction rate and Prediction;
Design equation for constant and variable volume batch reactors, Design of continuous
reactors - stirred tank and tubular flow reactor
UNIT II DESIGN FOR MULTIPLE REACTIONS 12

Design of reactors for multiple reactions - consecutive, parallel and mixed reactions - factors
affecting choice, optimum yield and conversion, selectivity, reactivity and yield. Recyle reactor,
size comparison of reactors
UNIT III TEMPERATURE AND PRESSURE EFFECTS 12

Non-isothermal homogeneous reactor systems, adiabatic reactors, rates of heat exchanges for
different reactors, design for constant rate input and constant heat transfer coefficient, operation
of batch and continuous reactors, optimum temperature progression.
UNIT IV BASICS OF NON-IDEAL FLOW 12

The residence time distribution as a factor of performance; residence time functions and
relationship between them in reactor; basic models for non-ideal flow; conversion in non-ideal
reactors
UNIT V HETEROGENEOUS NON CATALYTIC REACTIONS 12

Fluid solid non catalytic reactions . rate controlling steps; time for complete conversion for single
and mixed sizes, fluidized and static reactors. Kinetics of fluid –fluid reactions, Absorption
combined with chemical reactions; mass transfer coefficients and kinetic constants; application
of film, penetration and surface renewal theories; Hatta number and enhancement factor for first
order reaction, tower reactor design.
50
TOTAL : 60 PERIODS
TEXT BOOKS
1. Levenspiel O, “Chemical Reaction Engineering”, Wiley Eastern Ltd., II Edition, 2000.
2. Smith, J.M, “Chemical Engineering Kinetics”, McGraw Hill, III Edition, 1981.
3. Fogler.H.S., “Elements of Chemical Reaction Engineering”, Prentice Hall of India Ltd., IVth
Edition, 2005.
REFERENCE
1. Froment. G.F. & K.B.Bischoff, “Chemical Reactor Analysis and Design”, II Edition, Wiley
New York, 1990.
HS7551 EMPLOYABILITY SKILLS L T P C

3 0 0 3
COURSE DESCRIPTION
This course aims to help the students acquire the employability skills necessary for the
workplace situations. It also attempts to meet the expectations of the employers by giving
special attention to language skills, presentation skills, group discussion skills and soft skills.
This will be achieved through expert guidance and teaching activities focusing on employability
skills.
COURSE OBJECTIVES
• To enhance the employability skills of students with a special focus on presentation
skills, group discussion skills and interview skills
• To help them improve their reading skills, writing skills, and soft skills necessary for the
workplace situations
• To make them employable graduates
CONTENTS
UNIT I READING AND WRITING SKILLS 9

Reading: skimming & scanning strategies – note making skills – interpreting visual material
(charts & tables) – critical reading – fast reading necessary for reading letters & files - preparing
job applications - writing covering letter and résumé - applying for jobs online - email etiquette –
writing official letters (placing an order, letters to consumers, etc. ) writing reports – collecting,
analyzing and interpreting data
UNIT II SOFT SKILLS 9

Hard skills & soft skills – soft skills: self-management skills & people skills - training in soft skills
- persuasive skills – sociability skills –interpersonal skills – team building skills – leadership skills
– problem solving skills – adaptability - stress management – motivation techniques – life skills -
UNIT III PRESENTATION SKILLS 9

Preparing slides with animation related to the topic – organizing the material - Introducing
oneself to the audience – introducing the topic – answering questions – individual presentation
practice–– presenting the visuals effectively – 5 minute presentation
UNIT IV GROUP DISCUSSION SKILLS 9

Participating in group discussions – understanding group dynamics - brainstorming the topic -–
questioning and clarifying –GD strategies (expressing opinions, accepting or refusing others
opinions, turn taking) – activities to improve GD skills – viewing recorded GD - mock GD
51
UNIT V INTERVIEW SKILLS 9
Interview etiquette – dress code – body language – mock interview -–attending job interviews –
answering questions confidently – technical interview – telephone/Skype interview - practice in
different types of questions – one to one interview &panel interview – FAQs related to job
interview- Emotional and cultural intelligence.
LEARNING OUTCOMES
 Students will be able to make presentations and participate in group discussions with
high level of self-confidence.
 Students will be able to perform well in the interviews
 They will have adequate reading and writing skills needed for workplace situations
TOTAL : 45 PERIODS
REFERENCES:
1. Corneilssen, Joep. How to Prepare for Group Discussion and Interview. New Delhi:
Tata-McGraw-Hill, 2009.
2. Dabreo, Desmond A. Group Discussion and Team Building. Mumbai: Better Yourself
Books, 2004.
3. Ramesh, Gopalswamy, and Mahadevan Ramesh. The ACE of Soft Skills. New Delhi:
Pearson, 2010.
4. Gulati, Sarvesh. Corporate Soft Skills. New Delhi: Rupa and Co. 2006.
5. Van Emden, Joan, and Lucinda Becker. Presentation Skills for Students. New York:
Palgrave Macmillan, 2004.
EXTENSIVE READING
1. Covey, Stephen R. The 7 Habits of Highly Effective People. New York: Free Press,
2013.
2. Bagchi, Subroto. The Professional. New Delhi: Penguin Books India, 2009.
WEB RESOURCES
1. www.humanresources.about.com
2. www.careerride.com
3. https://bemycareercoach.com/softskills
AS7612 MASS TRANSFER LABORATORY FOR PETROCHEMICAL ENGINEERS LTPC

0042
AIM
To impart knowledge on mass transfer by practice
OBJECTIVES
Students develop a sound working knowledge on different types of mass transfer equipments.
OUTCOME
Acquiring knowledge in separation of petroleum products using various distillation techniques
LIST OF EXPERIMENTS
1. Separation of binary mixture using simple distillation
2. Separation of binary mixture using Steam distillation
3. Separation of binary mixture using Packed column distillation
4. Measurement of diffusivity
5. Liquid-liquid extraction
52
6. Drying characteristics of Vacuum Dryer
7. Drying characteristics of Tray dryer
8. Drying characteristics of Rotary dryer
9. Estimation of mass/heat transfer coefficient for cooling tower.
10. Demonstration Gas – liq Absorption
EQUIPMENTS REQUIRED
1. Simple distillation setup
2. Steam distillation setup
3. Packed column Liquid-liquid extractor
4. Liquid – Liquid Extractor
5. Vacuum Dryer
6. Tray dryer
7. Rotary dryer
8. Rotating Disc Contactor
9. Cooling Tower
10. Absorption Column
Minimum 10 experiments shall be offered.

TOTAL : 60 PERIODS
AS7611 COMPUTATIONAL PROGRAMMING IN CHEMICAL ENGINEERING

LABORATORY FOR PETROCHEMICAL ENGINEERS LT P C
0042
OBJECTIVES
Students will solve chemical engineering problems from core courses using C and MATLAB
programming and also using computational tools like Excel and Aspen.
OUTCOME:
Able to solve chemical engineering problems using C and MATLAB programming and Microsoft
Excel software.
Analyse and estimate the physical properties of data bank and non data bank components;
calculate bubble and dew points and generate T-xy and P-xy diagram by simulating flash drum
using ASPEN PLUS Process Simulator.
Programming in C
C programs will be written to solve problems from core courses of chemical and petrochemical
engineering.
Microsoft Excel Software

The computational, plotting and programming abilities in Excel will be used to solve different
chemical engineering problems.
Programming in MATLAB
Chemical engineering problems will be solved using the powerful computational and graphical
capability of MATLAB.
ASPEN Software
Individual process equipments and flowsheets will be simulated using Aspen Plus and property
analysis and estimation will be done using Aspen Properties.
53
Evaluation
This lab course will have two or three online assessment tests and an online end semester
examination in the Process Simulation Laboratory and assignments in all the above four units.
TOTAL : 60 PERIODS
CH7651 PROCESS INSTRUMENTATION DYNAMICS AND CONTROL LT P C

3003
OBJECTIVES
To introduce dynamic response of open and closed loop systems, control loop components and
stability of control systems along with instrumentation.
UNIT I INSTRUMENTATION 9
Principles of measurements and classification of process instruments, measurement of
temperature, pressure, fluid flow, liquid weight and weight flow rate, viscosity, pH, concentration,
electrical and thermal conductivity, humidity of gases.
UNIT II OPEN LOOP SYSTEMS 9

Laplace transformation, application to solve ODEs. Open-loop systems, first order systems and
their transient response for standard input functions, first order systems in series, linearization
and its application in process control, second order systems and their dynamics; transportation
lag.
UNIT III CLOSED LOOP SYSTEMS 9

Closed loop control systems, development of block diagram for feed-back control systems,
servo and regulatory problems, transfer function for controllers and final control element,
principles of pneumatic and electronic controllers, transient response of closed-loop control
systems and their stability.
UNIT IV FREQUENCY RESPONSE 9

Introduction to frequency response of closed-loop systems, control system design by frequency
response techniques, Bode diagram, stability criterion, tuning of controller settings
UNIT V ADVANCED CONTROL SYSTEMS 9

Introduction to advanced control systems, cascade control, feed forward control, Smith predictor
controller, control of distillation towers and heat exchangers, introduction to computer control of
chemical processes.
TOTAL : 45 PERIODS
OUTCOME:
Understand the prerequisites of control strategies and design different process control systems
Evaluate the suitable controllers for different chemical process.
Analyse and tune the control systems unto stability
Understand the mechanism of advance control systems
TEXT BOOKS
1. Stephanopoulos, G., “Chemical Process Control“, Prentice Hall of India, 2003.
2. Coughnowr, D., “ Process Systems Analysis and Control “, 3rd Edn., McGraw Hill, New
York, 2008.
54
REFERENCES
1. Marlin, T. E., “Process Control “, 2nd Edn, McGraw Hill, New York, 2000.
2. Smith, C. A. and Corripio, A. B., “Principles and Practice of Automatic Process Control”,
2nd Edn., John Wiley, New York, 1997.
AS7701 PETROLEUM EQUIPMENT DESIGN LTPC

3003
AIM
To give practice to students to design in detail different process equipments used in petroleum
industry.
OBJECTIVE
Students learn to do in detail process and mechanical design and engineering drawing of
different equipments generally used in petroleum industry
UNIT I HEAT TRANSFER OPERATIONS 9

Fired heaters, Heat Exchangers, Condensers, Evaporators, Reboilers,
UNIT II DESIGN OF PHASE SEPARATION EQUIPMENT 9

Design of physical separation equipments such as cyclones, centrifuges, thickeners,filtration
equipment
UNIT III MASS TRANSFER OPERATIONS 9

Absorption column, Distillation Column, Extraction Column ,Cooling tower, Dryer, Crystallizer
UNIT IV REACTORS AND STORAGE VESSELS 9

Packed bed Reactors, FCC units, Pressure Vessel, Storage Vessel
UNIT V MATERIALS OF CONSTRUCTION AND PLANT LAYOUT 9

Design of Plant Layout, Pipe Lines and Pipe Layouts, Design Schematics and Presentation,
Materials of Construction and Selection of process
TOTAL : 45 PERIODS
REFERENCES
1. Baranan, C.R., “Rules of Thumb for Chemical Engineers”, 3rd Edition, Gulf Professional
Publishing Co, Texas, 2002.
2. R. K. Sinnott, “Coulson & Richardson’s Chemical Engineering Design ”, Vol. 6, IV Edition
Butterworth Heinermann, Oxford, 2005.
3. Dawande, S. D., “Process Design of Equiments”, IV Edition, Central Techno Publications,
Nagpure, 2005.
4. Green D. W., “Perry’s Chemical Engineer’s Handbook”, VIII Edition McGraw Hill, 2007.
55
GE7251 ENVIRONMENTAL SCIENCE AND ENGINEERING LTPC
3 003
OBJECTIVES:
To the study of nature and the facts about environment.
 To find and implement scientific, technological, economic and political solutions to
environmental problems.
 To study the interrelationship between living organism and environment.
 To appreciate the importance of environment by assessing its impact on the human
world; envision the surrounding environment, its functions and its value.
 To study the dynamic processes and understand the features of the earth’s interior and
surface.
 To study the integrated themes and biodiversity, natural resources, pollution control and
waste management.
UNIT I ENVIRONMENT, ECOSYSTEMS AND BIODIVERSITY 14

Definition, scope and importance of environment – need for public awareness - concept of an
ecosystem – structure and function of an ecosystem – producers, consumers and decomposers
– energy flow in the ecosystem – ecological succession – food chains, food webs and ecological
pyramids – Introduction, types, characteristic features, structure and function of the (a) forest
ecosystem (b) grassland ecosystem (c) desert ecosystem (d) aquatic ecosystems (ponds, streams,
lakes, rivers, oceans, estuaries) – Introduction to biodiversity definition: genetic, species and
ecosystem diversity – biogeographical classification of India – value of biodiversity: consumptive
use, productive use, social, ethical, aesthetic and option values – Biodiversity at global, national and
local levels – India as a mega-diversity nation – hot-spots of biodiversity – threats to biodiversity:
habitat loss, poaching of wildlife, man-wildlife conflicts – endangered and endemic species of India
– conservation of biodiversity: In-situ and ex-situ conservation of biodiversity.
Field study of common plants, insects, birds
Field study of simple ecosystems – pond, river, hill slopes, etc.
UNIT II ENVIRONMENTAL POLLUTION 8

Definition – causes, effects and control measures of: (a) Air pollution (b) Water pollution
(c)Soil pollution (d) Marine pollution (e) Noise pollution (f) Thermal pollution (g) Nuclear
hazards– soil waste management: causes, effects and control measures of municipal solid
wastes – role of an individual in prevention of pollution – pollution case studies – disaster
management: floods, earthquake, cyclone and landslides.
Field study of local polluted site – Urban / Rural / Industrial / Agricultural.
UNIT III NATURAL RESOURCES 10

Forest resources: Use and over-exploitation, deforestation, case studies- timber extraction,
mining, dams and their effects on forests and tribal people – Water resources: Use and over-
utilization of surface and ground water, floods, drought, conflicts over water, dams-benefits
and problems – Mineral resources: Use and exploitation, environmental effects of extracting
and using mineral resources, case studies – Food resources: World food problems, changes
caused by agriculture and overgrazing, effects of modern agriculture, fertilizer-pesticide
problems, water logging, salinity, case studies – Energy resources: Growing energy needs,
renewable and non renewable energy sources, use of alternate energy sources. case studies
– Land resources: Land as a resource, land degradation, man induced landslides, soil erosion
and desertification – role of an individual in conservation of natural resources – Equitable use
of resources for sustainable lifestyles.
Field study of local area to document environmental assets – river / forest / grassland / hill /
mountain.
UNIT IV SOCIAL ISSUES AND THE ENVIRONMENT 7

From unsustainable to sustainable development – urban problems related to energy –
56
water conservation, rain water harvesting, watershed management – resettlement and
rehabilitation of people; its problems and concerns, case studies – role of non-governmental
organization- environmental ethics: Issues and possible solutions – climate change, global
warming, acid rain, ozone layer depletion, nuclear accidents and holocaust, case studies. –
wasteland reclamation – consumerism and waste products – environment production act– Air
(Prevention and Control of Pollution) act – Water (Prevention and control of Pollution) act –
Wildlife protection act – Forest conservation act – enforcement machinery involved in
environmental legislation- central and state pollution control boards- Public awareness.
UNIT V HUMAN POPULATION AND THE ENVIRONMENT 6

Population growth, variation among nations – population explosion – family welfare programme –
environment and human health – human rights – value education – HIV / AIDS – women and
child welfare – role of information technology in environment and human health – Case studies.
TOTAL: 45 PERIODS
OUTCOMES:
Environmental Pollution or problems cannot be solved by mere laws. Public participation is an
important aspect which serves the environmental Protection. One will obtain knowledge on the
following after completing the course.
 Public awareness of environment at infant stage.
 Ignorance and incomplete knowledge has lead to misconceptions.
 Development and improvement in standard of living has lead to serious environmental
disasters.
TEXT BOOKS:
1. Gilbert M.Masters, ‘Introduction to Environmental Engineering and Science’, 2nd edition,
Pearson Education 2004.
2. Benny Joseph, ‘Environmental Science and Engineering’, Tata McGraw-Hill, New Delhi,
2006.
REFERENCES:
1. R.K. Trivedi, ‘Handbook of Environmental Laws, Rules, Guidelines, Compliances
and Standards’, Vol. I and II, Enviro Media.
2 . Cunningham, W.P. Cooper, T.H. Gorhani, ‘Environmental Encyclopedia’,Jaico Publ.,
House, Mumbai, 2001.
3. Dharmendra S. Sengar, ‘Environmental law’, Prentice hall of India PVT LTD,New Delhi,
2007.
4. Rajagopalan, R, ‘Environmental Studies-From Crisis to Cure’, Oxford University Press
2005.
AS7711 PROCESS CONTROL LABORATORY FOR PETROCHEMICAL ENGINEERS

LTPC
0042
OBJECTIVES
Students will gain the hands on training about the control systems
OUTCOME:
Understand the prerequisites of control strategies and design different process control systems
Evaluate the suitable controllers for different chemical & Petrochemical process.
Analyse and tune the control systems unto stability
57
LIST OF EXPERIMENTS
1. Open loop study on a level system
2. Open loop study on a flow system
3. Open loop study on a thermal system
4. Closed loop study on a level system
5. Closed loop study on a flow system
6. Closed loop study on a thermal system
7. Response of first order system
8. Response of second order system
9. Response of Non-Interacting level System
10. Response of Interacting level System
11. Tuning of a level system
12. Tuning of a flow system
13. Tuning of a thermal system
14. Flow co-efficient of control valves
15. Characteristics of different types of control valves
*Minimum 10 experiments shall be offered.

TOTAL : 60 PERIODS
CH7661 CHEMICAL REACTION ENGINEERING LABORATORY LTPC

0042
OBJECTIVES
Students develop a sound working knowledge on different types of reactors.
LIST OF EXPERIMENTS*
1. Kinetic studies in a Batch reactor
2. Kinetic studies in a Plug flow reactor
3. Kinetic studies in a CSTR
4. Kinetic studies in a Packed bed reactor
5. Kinetic studies in a PFR followed by a CSTR
6. RTD studies in a PFR
7. RTD studies in a Packed bed reactor
8. RTD studies in a CSTR
9. Studies on micellar catalysis
10. Study of temperature dependence of rate constant using CSTR.
11. Kinetic studies in Sono chemical reactor
12. Batch reactive distillation
13. Kinetics of photochemical reaction
14. Demonstration of heterogeneous catalytic reaction
15. Demonstration of gas-liquid reaction
EQUIPMENT REQUIRED
1. BATCH REACTOR
2. Plug flow reactor
3. CSTR
4. Sono-chemical reactor
5. Photochemical reactor
6. Packed bed reactor
*Minimum 10 experiments shall be offered.
TOTAL : 60 PERIODS
58
OUTCOMES
Understand rate equation for different types of reactors.
Design experiments in kinetics to determine conversion and effect of temperature on
rate constant.
Assess the performance of Plug flow Mixed flow and Packed bed by studying the
residence time distribution.
MA 7354 NUMERICAL METHODS LTPC

4004
OBJECTIVES:
 To provide the mathematical foundations of numerical techniques for solving linear
system, eigenvalue problems, interpolation, numerical differentiation and integration and
the errors associated with them;
 To demonstrate the utility of numerical techniques of ordinary and partial differential
equations in solving engineering problems where analytical solutions are not readily
available.
UNIT I SOLUTION OF EQUATIONS AND EIGENVALUE PROBLEMS 12

Solution of algebraic and transcendental equations - Fixed point iteration method – Newton-
Raphson method- Solution of linear system of equations - Gauss elimination method – Pivoting
- Gauss-Jordan methods – Iterative methods of Gauss-Jacobi and Gauss-Seidel - Matrix
Inversion by Gauss-Jordan method - Eigenvalues of a matrix by Power method and by Jacobi’s
method.
UNIT II INTERPOLATION AND APPROXIMATION 12

Interpolation with unequal intervals - Lagrange interpolation – Newton’s divided difference
interpolation – Cubic Splines - Interpolation with equal intervals - Newton’s forward and
backward difference formulae – Least square method - Linear curve fitting.
UNIT III NUMERICAL DIFFERENTATION AND INTEGRATION 12

Approximation of derivatives using interpolation polynomials - Numerical integration using
Trapezoidal, Simpson’s 1/3 and Simpson’s 3/8 rules – Romberg’s method - Two point and three
point Gaussian quadrature formulae – Evaluation of double integrals by Trapezoidal and
Simpson’s rules.
UNIT IV INITIAL VALUE PROBLEMS FOR ORDINARY DIFFERENTIAL

EQUATIONS 12
Single step-methods - Taylor’s series method - Euler’s method - Modified Euler’s method -
Fourth order Runge-Kutta method for solving first and second order equations - Multi-step
methods - Milne’s and Adams-Bashforth predictor-corrector methods for solving first order
equations.
UNIT V BOUNDARY VALUE PROBLEMS IN ORDINARY AND PARTIAL

DIFFERENTIAL EQUATIONS 12
Finite difference methods for solving two-point linear boundary value problems - Finite
difference techniques for the solution of two dimensional Laplace’s and Poisson’s equations on
rectangular domain – One dimensional heat-flow equation by explicit and implicit (Crank-
Nicholson) methods - One dimensional wave equation by explicit method.
TOTAL: 60 PERIODS
59
OUTCOMES:
 Demonstrate understanding of common numerical methods and how they are used to
obtain approximate solutions.
 Apply numerical methods to obtain approximate solutions to mathematical problems.
 Derive numerical methods for various mathematical operations and tasks, such as
interpolation, differentiation, integration, the solution of linear and nonlinear equations,
and the solution of differential equations.
 Analyse and evaluate the accuracy of common numerical methods.
TEXT BOOKS:
1. Grewal, B.S. and Grewal,J.S., “Numerical methods in Engineering and Science”, Khanna
Publishers, New Delhi, 9th Edition, 2007.
2. Sankara Rao . K, " Numerical Methods for Scientists and Engineers" PHI
3. Learning Pvt Ltd. New Delhi, 2007.
REFERENCES:
1. Brian Bradie, “A Friendly Introduction to Numerical Analysis”, Pearson Education Asia, New
Delhi, 1st Edition, 2007.
2. Gerald, C.F. and Wheatley, P.O., “Applied Numerical Analysis”, Pearson Education Asia,
New Delhi, 6th Edition, 2006.
3. Laurene V. Fausett, “Applied Numerical Analysis using MATLAB”, Pearson Education, New
Delhi, 1st print, 2nd Edition, 2009.
4. S. R. K. Iyengar, R. K. Jain, Mahinder Kumar Jain, "Numerical Methods for Scientific and
Engineering Computation", 6th Edition, New Age International Publishers, New Delhi, 2012.
AS7017 REFINERY PROCESS DESIGN LTPC

3003
AIM
To get acquainted with process design of distillation columns involving multicomponent and
complex mixtures. To learn methodologies practiced in rating and designing heat transfer
equipment used in refining and process industry.
OBJECTIVE
Students learn process design aspects related to distillation column, Fired Heaters, pumps and
compressors
UNIT I MULTICOMPONENT DISTILLATION 9

Dew point and bubble point for multi component mixtures. Design of multi component distillation
column, Number of variables, Selection of key components, Selection of column pressure, Feed
condition, Plate-to-plate calculations, Empirical short cut methods, Introduction to rigorous
solution procedures.
UNIT II PETROLEUM REFINERY DISTILLATION 9

TBP, EFV, ASTM distillation curves and their relevance, Material balance and flash zone
calculations for petroleum refinery distillation columns, Pump around and pump back
calculations, Overall energy requirements, Estimation of number of equilibrium stages, Design
using Packie charts and Watkins method, Introduction to rigorous solution procedure based on
pseudo components.
60
UNIT III COLUMN DESIGN 9
Process design of distillation towers. Flooding charts. Trays and packings. Vacuum
devices.Pressure drops. Height,diameter,supports.Piping requirements. Aspects of mechanical
design. A typical P&ID for a distillation column. .
UNIT IV FIRED HEATERS 9

Heat load calculations for furnace heaters used in crude refining, Basic constructional features,
Different furnace types, Review of factors to be considered in the design of fired heaters,
Introduction to manual cal'culations methods.
UNIT V PUMPS AND COMPRESSORS 9

Types of pumps and compressors. Selection criteria. Power rating calculations based on
process duty.Use of operating curves of centrifugal pump. NPSHR and NPSHA. Pump
Cavitation. Surge problem in compressors.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Van Winkle M., “Distillation”, McGraw Hill, 1967.
2. Watkins, “Petroleum Refinery Distillation”, McGraw Hill, 1993
3. Sinnott R. K., “Coulson and Richardson’s Chemical engineering”, Vol. 6, III Edition, Butter
Worth-Heinemann, 1999.
4. Kern D. Q., “Process Heat Transfer”, McGraw Hill, 1965.
5. Cao Eduardo,”Heat Transfer in Process Engineering”, McGraw Hill,2010
AS7029 ENGINEERING ECONOMICS LTPC

3 003
AIM
To emphasize the importance of time value of money in petroleum projects.
OBJECTIVES
To understand the economic and decision analysis parameters in Petroleum Engineering and
Petroleum Business.
To understand the background of functioning of petroleum industry as an economic entity.
The themes of economics – scarcity and efficiency – three fundamental economic problems –
society’s capability – Production possibility fronties (PPF) – Productive efficiency Vs. economic
efficiency – economic growth & stability – Micro economies and Macro economies – the role of
markets and government – Positive Vs. negative externalities.
UNIT II CONSUMER AND PRODUCER BEHAVIOUR 9

Market – Demand and Supply – Determinants – Market equilibrium – elasticity of demand and
supply – consumer behavior – consumer equilibrium – Approaches to consumer behavior –
Production – Short-run and long-run Production Function – Returns to scale – economies Vs.
diseconomies of scale – Analysis of cost – Short-run and long-run cost function – Relation
between Production and cost function.
UNIT III PRODUCT AND FACTOR MARKET 9

Product market – perfect and imperfect market – different market structures – Firm’s equilibrium
and supply – Market efficiency – Economic costs of imperfect competition – factor market –
Land, Labor and capital – Demand and supply – determination of factor price – Interaction of
product and factor market – General equilibrium and efficiency of competitive markets.
61
UNIT IV PERFORMANCE OF AN ECONOMY – MACRO ECONOMICS 9
Macro-economic aggregates – circular flow of macroeconomic activity – National income
determination – Aggregate demand and supply – Macroeconomic equilibrium – Components of
aggregate demand and national income – multiplier effect – Demand side management – Fiscal
policy in theory.
UNIT V AGGREGATE SUPPLY AND THE ROLE OF MONEY 9

Short-run and Long-run supply curve – Unemployment and its impact – Okun’s law – Inflation
and the impact – reasons for inflation – Demand Vs. Supply factors –Inflation Vs.
Unemployment tradeoff – Phillips curve –short- run and long-run –Supply side Policy and
management- Money market- Demand and supply of money – money-market equilibrium and
national income – the role of monetary policy.
TOTAL: 45 PERIODS.
OUTCOME
Understanding of petroleum fiscal system within the context of India.
TEXT BOOKS
1. Paul A. Samuelson and William D. Nordhaus, ‘’Economics’’ 19th edition, Tata McGraw Hill,
2010.
REFERENCES
1. William Boyes and Michael Melvin, ‘’Textbook of Economics’’, 9th edition. Cengage
Learning 2009
2. N. Gregory Mankiw, ‘’Principles of Economics’’, edition, 6th edition. South-Western, 2011
3. Richard Lipsey and Alee Charystal, ‘’Economics’’, 12thedition, Oxford University Press,
New Delhi, 2011.
4. Karl E. Case and Ray C. fair, ‘’Principles of Economics’’, 10th edition, Pearson Education
Asia, New Delhi, 2012.
MA7072 STATISTICS AND LINEAR PROGRAMMING LTPC

4 004
OBJECTIVE:
This course aims at providing the required skill to apply the statistical and Linear Programming
tools for engineering problems.
UNIT I TESTING OF HYPOTHESIS 12

Sampling distributions - Tests for single mean , proportion and difference of means (Large and
small samples) – Tests for single variance and equality of variances – Chi-Square test for
goodness of fit – Independence of attributes.
UNIT II DESIGN OF EXPERIMENTS 12

Completely randomized design – Randomized block design – Latin square design - 22 factorial
design.
UNIT III STATISTICAL QUALITY CONTROL 12

Control charts for measurements ( and R charts) – Control charts for attributes (p, c and np
charts) – Tolerance limits - Acceptance sampling.
UNIT IV LINEAR PROGRAMMING 12

Formulation of LPP – Graphical methods for two variables – Simplex method - Big M method –
Transportation Problem - Basic feasible solution – North west corner rule – Vogel’s
62
approximation method (Unit penalty method) – Matrix minima method (Least cost method) –
Optimal solution – Non degeneracy and degeneracy problem –
Assignment problem – Hungarian method – Balanced and unbalanced.
UNIT V ADVANCED LINEAR PROGRAMMING 12

Dual simplex method – Formation and using simplex method – Integer programming – Cutting
plane algorithm.
TOTAL : 60 PERIODS
OUTCOMES:
 The students will have a fundamental knowledge of the concepts of statistical inference.
 Have the knowledge of applying Linear programming tools in management problems.
TEXT BOOKS:
1. Johnson, R.A. and Gupta, C.B., “Miller and Freund’s Probability and Statistics for
Engineers”, 7th Edition, Pearson Education, Asia, 2007.
2. Taha, H.A., “Operations Research”, 8th Edition, Pearson Education, Asia, 2007.
REFERENCES:
1. Walpole, R.E., Myers, R.H., Myers, S.L. and Ye, K.,“ Probability and Statistics for Engineers
and Scientists”, 8th Edition, Pearson Education, Asia, 2007.
2. Devore, J.L., “Probability and Statistics for Engineering and the Sciences”, 7th Edition,
Thomson Brooks/Cole, International Student Edition, 2008.
3. Winston, W.L., “Operations Research – Applications and Algorithms”, 4th Edition, Thomson,
1st Indian Reprint, 2007.
AS7028 DRILLING OPERATIONS LT PC

30 0 3
AIM
Students will understand the Drilling Process and Drilling Equipments.
OBJECTIVES
Students will understand the concepts and techniques used in well drilling. They will learn the
design requirements of well planning and construction.
UNIT I 9
Drilling operations – Location to Rig. Release Well Bore Diagram, Crews – Operator – Drilling,
contractor – Third Party Services – Rig Types – Land Types – Marine types
UNIT II 9
Components- Overall Drilling Rig, Drilling Sub systems – Power – Hoisting Line – speeds and
Loads Power – Loading Components – Drill Pipe, Heavy Weight Drill Pipe (HWDP), Drill String
Loads Uniaxial.
UNIT III 9
Directional Drilling, Well Planning, Two Dimensional, Horizontal, Tools, Techniques, MWD,
surveying – Radius of Curvature, Long’s Method – Errors, Muds, Mud Use, Property
measurements, Types, - Pneumatic (Air, Gas, Mist, Foam), Water based, Oil based, solids
Control, Definitions, Equipment, Problems, Contaminations Effect.
UNIT IV 9
Hydraulics, Classifications of Fluids, Rheological Models – Rotary Drilling Hydraulics – Jet
Hydraulic Optimizing and Maximizing – Circulations Rate Selection – Drill Bit – Jet Sizing –
63
Equivalent Circulations Density, Hole Cleaning. Theory – Vertical and Deviated Holes, Annular
Velocities – Carrying Capacity – Pills and Slugs.
UNIT V 9
Origin of Overpressure, Kick Signs, shut –in Procedures, Kill sheets, Kill Procedures, Driller’s
Methods – Engineer’s Method (Wait and Weight)
TOTAL : 45 PERIODS
TEXT BOOKS
1. Rabia.H. ‘Oil Well Drilling Engineering, Principles And Practices’ Graham And Trotman Ltd.
1985.
2. Standard Handbook of Petroluem and Natural Gas Engineering, 2nd Edition, William C
Lyons, Gary C Pilisga, Gulf Professional Publishing
AS7023 WELL COMPLETION TECHNIQUES L T P C

3 0 0 3
AIM
To provide insights into the Well Operation during the hydrocarbon Explorations.
OBJECTIVES
Student will be able to understand the basics and operations of Well Completion techniques.
UNIT I 9
Well design: Prediction of formation pore pressure and stress gradients. Determination of
safety mud weight bounds for different in-situ stress conditions. Design and planning well
trajectory. Surveying tools and methods.
UNIT II 9
Design of drill string including bottom hole (BHA) assembly. Drilling methods and equipment for
directional, horizontal and multilateral wells. Selection of casing shoes, material properties and
design of casing program.
UNIT III 9
Well Completion and Stimulations: Well completion design, types of completion, completion
selection and design criteria. Interval selection and productivity considerations: effects of
producing mechanisms. Inflow performance and multiple tubing performance analyses using
commercial software.
UNIT IV 9
Well stimulation and workover planning. Tubing-packer movement and forces. Tubing design:
graphical tubing design and simplified tensional strength design. Selection of down hole
equipment, tubing accessories and wellhead equipment.
UNIT V 9
Basics of perforation, selection of equipment and procedure for perforation oil and gas wells.
Technology of sand control: gravel packing. Fundamentals of well stimulation technologies:
acidization and hydraulic fracturing.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Wellsite Geological Techniques for Petroleum exploration by Sahay .B. et al
2. Petroleum Exploration Hand Book by Moody, G.B.
REFERENCE
1. Standard Hand Book of Petroleum & Natural Gas Engineering” – 2nd Edition 2005-William
C.Lyons & GaryJ.Plisga-Gulf professional publishing comp (Elsevier).
64
AS7012 PLANT SAFETY AND RISK ANALYSIS LTPC
3 003
AIM
To get awareness on the importance of plant safety and risk analysis
OBJECTIVES
Students learn about implementation of safety procedures, risk analysis and assessment,
hazard identification.
UNIT I NEED FOR SAFETY IN INDUSTRIES 9

Importance & objectives of safety- Safety Programmes – components and realization; Potential
hazards – extreme operating conditions, toxic chemicals; safe handling
UNIT II PLANT SAFETY AND SAFETY REGULATION 9

Implementation of safety procedures – periodic inspection and replacement; Accidents -
identification and prevention; Criteria for setting & layout of chemical plant, Factories Act and
Safety Regulations.
UNIT III PLANT HAZARDS & RISK ANALYSIS 9

Fire hazards- Chemical hazards, Toxic hazards, Explosion hazards, Electrical hazards,
Mechanical hazards, Radiation hazards, Noise hazards-Over all risk analysis--emergency
planning-on site & off site emergency planning, risk management ISO 14000, EMS models case
studies. Quantitative risk assessment - rapid and comprehensive risk analysis; Risk due to
Radiation, explosion due to over pressure, jet fire-fire ball.
UNIT IV SAFETY AUDIT 9

Objective of safety audit- Hazard identification safety audits, checklist, what if analysis,
vulnerability models event tree analysis fault tree analysis, Hazan past accident analysis
Fixborough-Mexico-Madras-Vizag Bopal analysis
UNIT V RISK ANALYSIS TECHNIQUES 9

Hazard & Operability (HAZOP) studies- Hazard Analysis (HAZAN)-Fault Tree Analysis
Consequence Analysis.
TOTAL : 45 PERIODS
TEXT BOOKS
1. Chemical Process Safety: Fundamentals with Applications, Daniel A. Crowl, J.F. Louvar,
Prantice Hall, NJ, 1990.
2. Fawatt, H.H. and Wood, W.S., “Safety and Accident Prevention in Chemical Operation“,
Wiley Interscience, 1965.
3. Marcel, V.C., Major Chemical Hazard- Ellis Harwood Ltd., Chi Chester, UK, 1987. 4. Hyatt,
N., Guidelines for process hazards analysis, hazards identification & risk analysis, Dyadem
Press, 2004
REFERENCES
1. Handley, W., “Industrial Safety Hand Book “, 2nd Edn., McGraw-Hill Book Company, 1969.
2. Heinrich, H.W. Dan Peterson, P.E. and Rood, N., “ Industrial Accident Prevention“, McGraw-
Hill Book Co., 1980.
3. Taylor, J.R., Risk analysis for process plant, pipelines and transport, Chapman and Hall,
London, 1994
65
AS7030 ENHANCED OIL RECOVERY LTPC
3003
AIM
To understand the nature of reservoirs and strategy for increasing reservoir efficiency.
OBJECTIVES
To be able to design an oil recovery technique. To be able to predict the future performance of a
reservoir.
UNIT I FUNDAMENTALS OF ENHANCED OIL RECOVERY 9
Pore Geometry, Microscopic Aspects of Displacement. Residual Oil Magnitude and
Mobilization. Buoyancy Forces and Prevention of Trapping, Wettability, Residual Oil and Oil
Recovery. Macroscopic Aspect of Displacement.
UNIT II WATER FLOODING 9

Properties, sampling and analysis of Oil Field Water; Injection waters; Water flooding – Sweep
Efficiency, Predictive Techniques, Improved Water Flood Processes, Performance of some
Important Water Floods.
UNIT III ENHANCED OIL RECOVERY OPERATIONS-1 9

Flooding – miscible, CO2, polymer, alkaline, surfactants, steam;
UNIT IV ENHANCED OIL RECOVERY OPERATIONS-2 9

Gas injection, in-situ combustion technology, microbial method
UNIT V PROBLEMS IN ENHANCED OIL RECOVERY 9

Precipitation and Deposition of Asphaltenes and Paraffins, Scaling Problems, Formation of
Damage Due to Migration of Fines, Environmental factors.
TOTAL : 45 PERIODS
REFERENCES
1. Donaldson, E.C. and G. V. Chilingarian, T. F. Yen, “Enhanced oil Recovery – I & II”,
2. Fundamentals and Analysis, Elsevier Science Publishers, New York, 1985.
3. Lake, L.W., “Enhanced oil recovery”, Prentice Hall, 1989.
4. Schumacher, M.M., “Enhanced oil recovery: Secondary and tertiary methods”, Noyes Data
Corp., 1978.
5. Van Pollen, H.K. “Fundamentals of enhanced oil recovery”, Penn Well Books, 1980.
AS7011 PETROLEUM PRODUCTION ENGINEERING LTPC

3 003
AIM
To develop a logical built up of the various facets of the oil and gas production technology.
OBJECTIVES
An ability to understand and apply operational and maintenance of has lift wells along with
surface facilities
An ability to understand and apply other methods of artificial lift systems with awareness of their
advantages and disadvantages
66
OUTCOME
An ability to understand and apply need of stimulation techniques and their types for
enhancement in production
UNIT I 9
Petroleum production system, properties of oil and natural gas, reservoir deliverability
UNIT II 9
Wellbore performance, choke performance, well deliverability, forecast of well production,
production decline analysis
UNIT III 9
Equipment design and selection – well tubing, separation and transportation systems
UNIT IV 9
Artificial lift methods - sucker rod pumping, gas lift, artificial lift methods
UNIT V 9
Production enhancement – well problem identification, matrix acidizing, hydraulic fracturing,
production optimization
TOTAL : 45 PERIODS
REFERENCE
1. Guo, B, Lyons, W.C. and Ghalambor, A., Petroleum production engineering: a computer
assisted approach, Gulf Professional Publishing, Burlington,
AS7019 SCIENCE AND HEALTH IN RESONANCE LTPC

3003
AIM
To sensitize and create an awakening among the course participants on adhering to principles
of healthy living and instilling the style modifications.
OBJECTIVE
To cause behavioral changes in the learning clientele and creating the necessary psycho
sociological ramiflications, motivating the participants to adopt a healthy life style.
UNIT I IMPORTANCE OF MICRONUTRIENTS AND ADHERING TO LOW GLYCEMIC

INDEX FOODS 9
Millets and fibre rich foods –Their high nutritive value –Dangers of consumption of refined foods
–Iron protein combination –Micronutrients –Their importance in upkeep of good health –
Overcoming their deficiency –Foods rich in micronutrients – Glycemic index –Its importance –
Comparative glycemic index of various foods.
UNIT II IMMUNIZATION SCHEDULING – NEED FOR ADHERENCE 9

Protein calorie malnutrition –Importance of intake of folic acid supplements to prevent genital
abnormalities –Necessity to avoid early marriage –Need for various immunizations their dosage
schedules-Need to immunize adolescent and girl children to prevent cervical cancer.
UNIT III LIFE SAVING CHILD SURVIVAL STRATEGIES 9

Drastically cutting down mortality and morbidity –Causative factors of dehydration –Warning
symptoms –Need to administer life saving Oral Rehydration Salt solution (ORS) –Methodology
of preparing ORS solution –Importance of zinc as an additive.
67
UNIT IV STRATEGIES FOR INCREASING HDL AND LOWERING LDL CHOLESTEROL
9
Healthy fats –Need to avoid saturated and trans fats –Optimum value of HDL and LDL
cholesterols –Need to lower triglycerides –Ways of reducing bad LDL cholesterol –Role of
Thyroid Simulating Hormone (TSH) –Importance of mental health –Positive and optimistic
outlook on life –Pronic breathing as a stress relief mechanism.
UNIT V ORGANIC FARMING – BIOPESTICIDES PRODUCTION – WEALTH FROM

WASTE 9
Eco friendly organic vegetables and fruits –Biopesticides –Neem based –Use of BIOBLOOM in
conversion of waste into Bio manure –Healthy equilibrium between work and rest –Maintaining
good postures to avoid back and neck pain syndrome – Principles of ERGONOMICS –Gender
sensitization –Respecting each others domain and contribution.
TOTAL : 45 PERIODS
REFERENCE
1. Kedar N.Prasad, Micronutrients in Health and Disease, CRC Press, 1st Edition, 2010
AS7021 TECHNICAL ANALYSIS – AN ANALYTICAL INSIGHT LTPC

3003
AIM
The elective will enable the students to have a good grasp over the principles and
generalizations of Technical analysis.
OBJECTIVE
The study of the elective will enhance the cognitive domain of the Learners and motivate them
to extrapolate the principles of analysis to their analytical skills and to make an indelible
evergreen impression in their minds about the logical, sequential, stepwise approach to
analysis.
UNIT I TYPES OF ANALYSIS – UNDERLYING PRINCIPLES 9

Purity of simple sugars – Glycemic Index and its importance – Principles underlying Bertrand’s
estimation of percentage purity of glucose – Estimation of percentage purity of aniline –
Underlying principles
UNIT II COAL AND FERTILZER ANALYSIS – BASIC PRINCIPLES 9

Correlation between thermal energy and fixed carbon – Estimation of Sulphur in coal – Fluidized
bed technology to reduce sulphur – Estimation of Nitrogen in soil and nitrogenous fertilizers –
Analysis of coal for grading
UNIT III CLASSIFICATION OF CEMENT – OPTIMUM PARAMETER FOR QUALITY

9
Types of analysis of cement – Standard and Rapid method – Underlying theory behind
percentage estimation of SiO2, Mixed oxides and Calcium oxides – Optimum Quality parameter
and ratios for good quality cement – Gel formation – Use of additives
UNIT IV ANALYSIS OF OILS – PURITY CRITERIA – OILS AND GOOD HEALTH 9

Principles underlying estimation of acid, saponification and iodine value of an oil – Importance of
increase in HDL and lowering LDL cholesterol – Optimum values for HDL and LDL cholesterol –
Lowering of triglycerides – Various approaches
68
UNIT V DRINKING WATER STANDARDS – STRATEGIES FOR STERILIZATIONS 9
Estimation of chloride, sulphate, Total dissolved solids and dissolved oxygen in a given sample
of water – Principles underlying the above fundamentals and generalizations underlying
determination of chemical oxygen demand – Reduction of BOD – Various strategies, Principles
underlying water purification – WHO standards of drinking water.
TOTAL : 45 PERIODS
REFERENCES
1. Commercial methods of Analysis by Foster Dee Snell and Frank M Biffen – Chemical
Publishing Company, Revised edition, 1988
2. Technical Analysis lab manuals – Volume-I and II by Dr K Srinivasan and Dr P
Gnanasundaram, Anna University, Chennai. Revised edition 2013.
AS7032 MULTICOMPONENT DISTILLATION LTPC

3003
AIM
To understand the concepts of Multicomponent distillation systems.
OBJECTIVE
Students able to design multicomponent distillation unit. They learn about various types of MCD
column.
UNIT I THERMODYNAMIC PRINCIPLES 9

Fundamental Thermodynamic principles involved in the calculation of vapor – liquid equilibria
and enthalpies of multi component mixtures – Use of multiple equation of state for the
calculation of K values – Estimation of the fugacity coefficients for the vapor phase of polar gas
mixtures – calculation of liquid – phase activity coefficients.
UNIT II THERMODYNAMIC PROPERTY EVALUATION 9

Fundamental principles involved in the separation of multi component mixtures – Determination
of bubble-point and Dew Point Temperatures for multi component mixtures – equilibrium flash
distillation calculations for multi component mixtures – separation of multi component mixtures
at total reflux.
UNIT III MINIMUM REFLUX RATIO FOR MCD SYSTEM 9

General considerations in the design of columns – Column sequencing – Heuristics for column
sequencing – Key components – Distributed components – Non-Distributed components –
Adjacent keys. Definition of minimum reflux ratio – calculation of Rm for multi component
distillation – Underwood method – Colburn method.
UNIT IV VARIOUS METHODS OF MCD COLUMN DESIGN 9

Theta method of convergence – Kb method and the constant composition method – Application
of the Theta method to complex columns and to system of columns – Lewis Matheson method –
Stage and reflux requirements – Short cut methods and Simplified graphical procedures.
UNIT V VARIOUS TYPES OF MCD COLUMNS 9

Design of sieve, bubble cap, valve trays and structured packing columns for multi component
distillation – computation of plate efficiencies.
TOTAL : 45 PERIODS
69
TEXT BOOKS
1. Holland, C.D., “Fundamentals of Multi Component Distillation”, McGraw Hill Book Company,
I Edition, 1997
2. Van Winkle, “Distillation Operations”, McGraw Hill Publications, 1987.
CH7071 ENERGY TECHNOLOGY LTPC

3 003
OBJECTIVES
Students will gain knowledge about different energy sources
UNIT I ENERGY 9
Introduction to energy – Global energy scene – Indian energy scene - Units of energy,
conversion factors, general classification of energy, energy crisis, energy alternatives
UNIT II CONVENTIONAL ENERGY 9

Conventional energy resources, Thermal, hydel and nuclear reactors, thermal, hydel and
nuclear power plants, efficiency, merits and demerits of the above power plants, combustion
processes, fluidized bed combustion.
UNIT III NON-CONVENTIONAL ENERGY 9

Solar energy, solar thermal systems, flat plate collectors, focusing collectors, solar water
heating, solar cooling, solar distillation, solar refrigeration, solar dryers, solar pond, solar thermal
power generation, solar energy application in India, energy plantations. Wind energy, types of
windmills, types of wind rotors, Darrieus rotor and Gravian rotor, wind electric power generation,
wind power in India, economics of wind farm, ocean wave energy conversion, ocean thermal
energy conversion, tidal energy conversion, geothermal energy.
UNIT IV BIOMASS ENERGY 9

Biomass origin - Resources – Biomass estimation. Thermochemical conversion – Biological
conversion, Chemical conversion – Hydrolysis & hydrogenation, solvolysis, biocrude, biodiesel
power generation gasifier, biogas, integrated gasification.
UNIT V ENERGY CONSERVATION 9

Energy conservation - Act; Energy management importance, duties and responsibilities; Energy
audit – Types methodology, reports, instruments. Benchmalcing and energy performance,
material and energy balance, thermal energy management.
TOTAL : 45 PERIODS
OUTCOMES
Understand conventional Energy sources, Non- conventional Energy sources, biomass
sources and develop design parameters for equipment to be used in Chemical process
industries. Understand energy conservation in process industries
TEXTBOOKS
1. Rao, S. and Parulekar, B.B., Energy Technology, Khanna Publishers, 2005.
2. Rai, G.D., Non-conventional Energy Sources, Khanna Publishers, New Delhi, 1984.
3. Nagpal, G.R., Power Plant Engineering, Khanna Publishers, 2008.
4. Energy Management, Paul W.O’Callaghan McGraw – Hill, 1993
REFERENCES
1. Nejat Vezirog, Alternate Energy Sources, IT, McGraw Hill, New York.
2. El. Wakil, Power Plant Technology, Tata McGraw Hill, New York, 2002.
70
3. Sukhatme. S.P., Solar Enery - Thermal Collection and Storage, Tata McGraw hill, New
Delhi, 1981.
4. Handbook of Energy Audit by 7th edition Albert Thumann, P.E., C.E.M & William J Younger
C.E.M, Faiment Press 2008
AS7024 ADVANCED SEPARATION TECHNIQUES LTPC

3 003
AIM
To identify the multiple factors influencing the choice of separation techniques.
OBJECTIVES
To be able to qualitatively and quantitatively address the fundamental aspects of specialty
separation processes.
UNIT I GENERAL REVIEW 9

Mechanisms: Separation factors and its dependence on process variables, classification and
characterization, thermodynamic analysis and energy utilization, kinetics and mass transport.
Theory and Equipment used in cross flow Filtration, cross flow Electro Filtration.
UNIT II MEMBRANE SEPARATIONS 9

Types and choice of membranes, their merits, commercial, pilot plant polarization of membrane
processes and laboratory membrane permeators, dialysis, reverse osmosis, ultra filtration,
Concentration and economics of membrane operations, Design controlling factors.
UNIT III SEPARATION BY SORPTION TECHNIQUES 9

Types and choice of adsorbents, chromatographic techniques, Types, Retention theory
mechanism, Design controlling factors ion exchange chromatography equipment and
commercial processes, recent advances and economics.
UNIT IV IONIC SEPARATIONS 9

Controlling factors, applications, Theory mechanism and - equipments for electrophoresis,
dielectrophoresis and electro dialysis - commercial applications - Design considerations.
UNIT V THERMAL SEPARATION 9

Thermal diffusion: Basic rate law, phenomenological theories of thermal diffusion for gas and
liquid mixtures, Equipments design and applications. Zone melting: Equilibrium diagrams,
Controlling factors, Apparatus and applications.
TOTAL : 45 PERIODS
TEXT BOOKS:
1. H.M. Schoen, "New Chemical Engineering Separation Techniques”, Wiley Interscience, New
York, 1972.
2. C.J. King, "Separation Processes", Tata McGraw Hill, New Delhi, 1982.
3. B. Sivasankar, “Bioseparations – Principles and Techniques”, Prentice Hall of India Pvt. Ltd,
New Delhi, 2005.
4. “Membrane Separation processes”, Kaushik Nath, PHI ,2008.
REFERENCES
1. Roussel, R. W., “Handbook of Separation Process Technology”, John Wiley, New York,
1987.
2. Nakagawal, O. V., “Membrane Science and Technology”’ Marcel Dekkar, 1992.
3. R.E. Lacey and S. Loeb, “Industrial Processing with Membranes,” Wiley–Inter sciences,
New York, 1972
71
AS7014 PROCESS OPTIMIZATION LT PC
30 0 3
AIM
To acquaint the student with the concepts and techniques of single and multivariable
optimization techniques using numerical search and analytical methods
OBJECTIVE
The student will enable to optimize the problems related to design, planning and operations
involved in a chemical industry
UNIT I OPTIMISATION 9
Introduction; formulation of objective functions; fitting models to data; classification of functions;
necessary and sufficient conditions for optimum; unimodal, multimodal functions; analytical
methods lagrange multiplier methods.
UNIT II NUMERICAL METHODS 9

Unimodel functions; newton's quasi newton, secant methods; region elimination methods,
polynomial approximation; quadratic and cubic interpolation techniques for optimum. Multimodal
functions; direct methods; random, grid. Hooke’s nelder and mead methods; Powell’s technique;
indirect methods; gradient and conjugate gradient methods; secant methods.
UNIT III LINEAR AND NON-LINEAR PROGRAMMING APPLICATIONS 9

Review on basic concepts of LP formulations; Simplex methods; Integer, quadratic, geometric
and dynamic programming. Heat transfer and energy conservation; separation processes; fluid
flow systems; reactor design and operation; large scale systems.
UNIT IV MULTIVARIABLE OPTIMIZATION WITHOUT AND WITH CONSTRAINTS 9

Necessary and sufficient conditions for optimum; direct search methods; indirect search
methods.
UNIT V APPLICATIONS OF OPTIMIZATION 9

Formulation of objective functions; fitting models to data; applications in fluid mechanics,
heat transfer, mass transfer, reaction engineering, equipment design, resource allocation
and inventory control.
TOTAL : 45 PERIODS
TEXT BOOKS.
1. Edgar, T.F., Himmelblau, D.M., “Optimisation of Chemical Processes”, McGraw-Hill II
Edition 2001.
2. Reklaitis, G.V., Ravindran, A., Ragsdell, K.M. “Engineering Optimisation”, John Wiley, II
Edition 2006
REFERENCES
1. Biles, W.E., Swain, J.J.; “Optimisation and Industrial Experimentation”, Inter Science, New
York, 1980.
2. Seinfeld, J.H.; Lapidus, L; “Process Modelling, Estimation and Identification”, Prentice Hall,
Englewood Cliffs, New Jersey, 1974.
3. Beveridge, C.S.; Schechter, R.S.; “Optimisation: Theory and Practice”, McGraw-Hill Book
Co., New York, 1970
72
AS7025 CHEMICAL PROCESS MODELLING AND SIMULATION LTPC
3003
OBJECTIVES
Students will develop suitable chemical process model to get process output
Introduction to modeling and simulation, classification of mathematical models, conservation
equations and auxiliary relations.
UNIT II STEADY STATE LUMPED SYSTEMS 9

Degree of freedom analysis, single and network of process units, systems yielding linear and
non-linear algebraic equations, flow sheeting – sequential modular and equation oriented
approach, tearing, partitioning and precedence ordering, solution of linear and non-linear
algebraic equations.
UNIT III UNSTEADY STATE LUMPED SYSTEMS 9

Analysis of liquid level tank, gravity flow tank, jacketed stirred tank heater, reactors, flash and
distillation column, solution of ODE initial value problems, matrix differential equations,
simulation of closed loop systems.
UNIT IV STEADY STATE DISTRIBUTED SYSTEM 9

Analysis of compressible flow, heat exchanger, packed columns, plug flow reactor, solution of
ODE boundary value problems.
UNIT V UNSTEADY STATE DISTRIBUTED SYSTEM &

OTHER MODELLING APPROACHES 9
Analysis laminar flow in pipe, sedimentation, boundary layer flow, conduction, heat exchanger,
heat transfer in packed bed, diffusion, packed bed adsorption, plug flow reactor, hierarchy in
model development, classification and solution of partial differential equations. Empirical
modeling, parameter estimation, population balance and stochastic modeling.
TOTAL : 45 PERIODS
OUTCOME:
Understand the fundamentals of modelling and their applications to transport/energy equations,
chemical and phase equilibria kinetics etc.,
Create the mathematical models for different unit operations equipments such as stirred tank
heaters, Heat exchangers, Evaporators, Reactors, distillation columns etc.,.
Analyze the principles of steady state/unsteady state lumped systems and steady state/
unsteady state distributed systems and can select proper equation of state for estimating
component properties and process flow sheeting.
TEXT BOOKS
1. Ramirez, W.; “Computational Methods in Process Simulation “, 2nd Edn., Butterworths
Publishers, New York, 2000.
2. Luyben, W.L., “Process Modelling Simulation and Control”, 2nd Edn, McGraw-Hill Book Co.,
1990
REFERENCES
1. Felder, R. M. and Rousseau, R. W., “Elementary Principles of Chemical Processes “, John
Wiley, 2000.
2. Franks, R. G. E., “Mathematical Modelling in Chemical Engineering “, John Wiley, 1967
73
AS7015 PROCESS PLANT UTILITIES FOR PETROCHEMICAL ENGINEERS LTPC
3003
AIM
To understand the fundamentals and principles of main utilities required for process plants are
water, steam, air & refrigerants.
OBJECTIVES
• State the principles involved during water treatment, generation of steam and its uses,
refrigeration cycles.
• Describe the different equipment’s used to run the process plant with different utilities
UNIT I WATER 9
Hard and Soft water, Requisites of Industrial Water and its uses. Methods of water Treatment
such as Chemical Softening and Demineralization, Resins used for Water Softening and
Reverse Osmosis. Effects of impure Boiler Feed Water.
UNIT II STEAM 9
Properties of Steam, problems based on Steam, Types of Steam Generator such as Solid Fuel
Fired Boiler, Waste Gas Fired Boiler and Fluidized Bed Boiler. Scaling and Trouble Shooting.
Steam Traps and Accessories.
UNIT III REFRIGERATION 9

Refrigeration Cycles, Methods of Refrigeration used in Industry and Different Types of
Refrigerants such as Monochlorodifluro Methane, Chlorofluro Carbons and Brines. Refrigerating
Effects and Liquefaction Processes.
UNIT IV COMPRESSORS AND COOLING TOWERS 9

Classification of Compressor, Reciprocating Compressor, Single Stage and Two Stage
Compressor, Velocity Diagram for Centrifugal Compressor, Slip Factor, Impeller Blade Shape.
Properties of Air –Water Vapors and use of Humidity Chart. Equipment’s used for
Humidification, Dehumidification and Cooling Towers.
UNIT V FUEL AND WASTE DISPOSAL 9

Types of Fuel used in Chemical Process Industries for Power Generation such as Natural Gas,
Liquid Petroleum Fuels, Coal and Coke. Internal Combustion Engine, Petrol and Diesel Engine.
Waste Disposal.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Perry R. H. Green D. W. “Perry's chemical Engineer's Handbook”, McGraw Hill, New York,
2008.
REFERENCES
1. W.Eckenfelder.Jr. “Industrial Water Pollution Control” 3rd edition, McGraw-Hill: New York,
1999.
2. P. L. Ballaney, “Thermal Engineering”,24th edition, Khanna Publisher New Delhi, 2011.
3. P. N. Ananthanarayan, “Basic Refrigeration & Air conditioning”, 4th edition, Tata McGraw
Hill, New Delhi, 2013.
74
AS7020 SUPPLY CHAIN MANAGEMENT FOR PETROCHEMICAL ENGINEERS
LTPC
3003
OBJECTIVES
Students will gain knowledge about practices followed in supply chain management
OUTCOMES
Understand the logistics Smanagement and supply chain network design Apply latest
technology used in supply chain management.
Definition of Logistics and SCM: Evolution, Scope, Importance& Decision Phases – Drivers
of SC Performance and Obstacles
UNIT II LOGISTICS MANAGEMENT 10

Factors – Modes of Transportation - Design options for Transportation Networks-Routing
and Scheduling – Inbound and outbound logistics- Reverse Logistics – 3PL- Integrated
Logistics Concepts- Integrated Logistics Model – Activities - Measuring logistics cost and
performance – Warehouse Management - Case Analysis
UNIT III SUPPLY CHAIN NETWORK DESIGN 10

Distribution in Supply Chain – Factors in Distribution network design –Design options-
Network Design in Supply Chain – Framework for network Decisions - Managing cycle
inventory and safety.
UNIT IV SOURCING, AND PRICING IN SUPPLY CHAIN 9

Supplier selection and Contracts - Design collaboration - Procurement process. Revenue
management in supply chain
UNIT V COORDINATION AND TECHNOLOGY IN SUPPLY CHAIN 10

Supply chain coordination - Bullwhip effect – Effect of lack of co-ordination and obstacles
– IT and SCM - supply chain IT frame work. E Business & SCM. Metrics for SC
performance – Case Analysis
TOTAL : 45 PERIODS
REFERENCES
1. Supply Chain Management, Strategy, Planning, and operation – Sunil Chopra and
Peter Meindl- PHI, Second edition, 2007
2. Logistics, David J.Bloomberg, Stephen Lemay and Joe B.Hanna, PHI 2002
3. Logistics and Supply Chain Management –Strategies for Reducing Cost and Improving
Service. Martin Christopher, Pearson Education Asia, Second Edition
4. Modeling the supply chain, Jeremy F.Shapiro, Thomson Duxbury, 2002
5. Handbook of Supply chain management, James B.Ayers, St.Lucle Press, 2000
ME7074 DESIGN OF HEAT EXCHANGERS LT P C

3003
AIM
To learn heat flow in condensers, cooling towers.
OBJECTIVES
To learn the thermal and stress analysis on various parts of the heat exchangers.
To analyze the sizing and rating of the heat exchangers for various applications.
75
Types of heat exchangers, shell and tube heat exchangers – regenerators and recuperators
- Temperature distribution and its implications - Parts description, Classification as per Tubular
Exchanger Manufacturers Association (TEMA)
UNIT II PROCESS DESIGN OF HEAT EXCHANGERS 9

Heat transfer correlations, Overall heat transfer coefficient, analysis of heat exchangers – LMTD
and effectiveness method. Sizing of finned tube heat exchangers, U tube heat exchangers,
Design of shell and tube heat exchangers, fouling factors, pressure drop calculations.
UNIT III STRESS ANALYSIS 9

Stress in tubes – header sheets and pressure vessels – thermal stresses, shear stresses -
types of failures, buckling of tubes, flow induced vibration.
UNIT IV COMPACT AND PLATE HEAT EXCHANGER 9

Types- Merits and Demerits- Design of compact heat exchangers, plate heat exchangers,
performance influencing parameters, limitations.
UNIT V CONDENSERS AND COOLING TOWERS 9

Design of surface and evaporative condensers – cooling tower – performance characteristics.
TOTAL : 45 PERIODS
OUTCOME
To study heat exchange in different systems.
TEXT BOOKS
1. SadikKakac and Hongtan Liu, Heat Exchangers Selection, Rating and Thermal Design,
CRC Press, 2002.
2. Shah,R. K., Dušan P. Sekulić, Fundamentals of heat exchanger design, John Wiley &
Sons,2003.
REFERENCES
1. Robert W. Serth, Process heat transfer principles and applications, Academic press,
Elesevier, 2007.
2. Sarit Kumar Das, Process heat transfer, Alpha Science International, 2005
3. John E. Hessel greaves,Compact heat exchangers: selection, design, and operation,
Elsevier science Ltd, 2001.
4. T. Kuppan, Heat exchanger design hand book, New York : Marcel Dekker, 2000.
5. Eric M. Smith, Advances in thermal design of heat exchangers: a numerical approach:
direct-sizing, step-wise rating, and transients, John Wiley & Sons, 1999.
6. Arthur. P Frass, Heat Exchanger Design, John Wiley & Sons, 1989
76
AS7016 PRODUCT DESIGN AND DEVELOPMENT FOR
PETROCHEMICAL ENGINEERS LTPC
3 003
AIM
To understand the fundamental concepts of equipment and product design.
OBJECTIVE
To teach the students basic concepts of Product Design and Process Development. Expose the
students to the importance, various stages, concepts, management and prototyping of Product
Design and Process Development.
Strategic importance of Product development - integration of customer, designer, material
supplier and process planner, Competitor and customer - behavior analysis. Understanding
customer-promoting customer understanding-involve customer in development and managing
requirements - Organization process management and improvement.
UNIT II CONCEPT GENERATION, SELECTION AND TESTING 9

Plan and establish product specifications. Task - Structured approaches - clarification - search
externally and internally-Explore systematically - reflect on the solutions and processes -
concept selection - methodology - benefits. Implications - Product change - variety – component
standardization - product performance – manufacturability.
UNIT III PRODUCT ARCHITECTURE 9

Product development management - establishing the architecture - creation - clustering -
geometric layout development - Fundamental and incidental interactions - related system level
design issues - secondary systems -architecture of the chunks - creating detailed interface
specifications-Portfolio Architecture.
UNIT IV INDUSTRIAL DESIGN 9

Integrate process design - Managing costs - Robust design - Integrating CAE, CAD, CAM tools
– Simulating product performance and manufacturing processes electronically – Need for
industrial design-impact – design process - investigation of customer needs - conceptualization -
refinement - management of the industrial design process.
UNIT V DESIGN FOR MANUFACTURING AND PRODUCT DEVELOPMENT 9

Definition - Estimation of Manufacturing cost-reducing the component costs and assembly costs
– Minimize system complexity - Prototype basics - Principles of prototyping – Planning for
prototypes - Economic Analysis.
TOTAL : 45 PERIODS
OUTCOME
An ability to understand the concepts of manufacturing and product development.
TEXT BOOK
1. Ulrich K.T. and Eppinger S.D., “Product Design and Development” McGraw – Hill
International Editions,1999.
REFERENCES
1. Belz A., 36-Hour Course: “Product Development” McGraw-Hill, 2010.
2. Rosenthal S., “Effective Product Design and Development”, Business One Orwin,
Homewood, 1992, ISBN 1-55623-603-4.
3. Pugh S., “Total Design – Integrated Methods for successful Product Engineering”, Addison
Wesley Publishing, 1991, ISBN 0-202-41639-5.
77
AS7026 COMPUTATIONAL FLUID DYNAMICS FOR
PETROCHEMICAL ENGINEERS LT PC
3 00 3
AIM
The course gives an introduction into modeling using Computational Fluid Dynamics (CFD),
which has become a indispensible tool for many engineers.
OBJECTIVE
Be able to demonstrate competence in setting up computational fluid dynamics models for some
industrially important applications. This technical competence in building and conducting CFD
simulations is a skill which enhances employability.
UNIT I CONSERVATION LAWS AND TURBULENCE MODELS 9

Governing equations of fluid flow and heat transfer –mass conservation, momentum and energy
equation, differential and integral forms, conservation and non-conservation form.
Characteristics of turbulent flows, time averaged Navier Strokes equations, turbulence models-
one and two equation, Reynolds stress, LES and DNS
UNIT II FINITE DIFFERNCE APPROXIMATION 9

Mathematical behaviour of PDE, finite difference operators, basic aspects of discretization by
FDM, explicit and implicit methods, error and stability analysis
UNIT III FINITE VOLUME METHOD 9

Diffusion problems – explicit and implicit time integration; Convection-diffusion problems –
properties of discretisation schemes, central, upwind, hybrid, QUICK schemes; Solution of
discretised equations.
UNIT IV FLOW FIELD COMPUTATION 9

Pressure velocity coupling, staggered grid, SIMPLE algorithm, PISO algorithm for steady and
unsteady flows
UNIT V FINITE VOLUME METHOD FOR UNSTEADY FLOWS AND

IMPLEMENTATION OF BOUNDARY CONDITIONS 9
One-dimensional unsteady heat conduction, Discretisation of transient convection-diffusion
equation, Solution procedures for unsteady flow calculations, Implementation of Inlet, outlet and
wall boundary conditions, constant pressure boundary condition. .
TOTAL : 45 PERIODS
TEXT BOOKS
1. Anderson, J. D., “Computational Fluid Dynamics: The Basics with Applications”, McGraw-
Hill, 1995.
2. Fletcher, C. A. J., “Computational Techniques for Fluid Dynamics, Vol. 1: Fundamental and
General Techniques, 2nd Edition., 2013
3. Versteeg, H.K. and Malalasekera, W., “An Introduction to Computational Fluid Dynamics:
The Finite Volume Method”, Pearson Education Ltd., 2007.
4. Chung T.J Computational Fluid Dynamics Cambridge University Press 2003.
5. Muralidhar, K., and Sundararajan, T., “Computational Fluid Flow and Heat Transfer”,
NarosaPublishing House, New Delhi, 2001.
REFERENCE
1. Vivek V. Ranade, Computational flow modeling for chemical reactor engineering Academic
Press, San Diego, 2002.
78
GE7071 DISASTER MANAGEMENT LTPC
3003
OBJECTIVES:
 To provide students an exposure to disasters, their significance and types.
 To ensure that students begin to understand the relationship between vulnerability,
disasters, disaster prevention and risk reduction
 To gain a preliminary understanding of approaches of Disaster Risk Reduction (DRR)
 To enhance awareness of institutional processes in the country and
 To develop rudimentary ability to respond to their surroundings with potential
disaster response in areas where they live, with due sensitivity
UNIT I INTRODUCTION TO DISASTERS 9
Definition: Disaster, Hazard, Vulnerability, Resilience, Risks – Disasters: Types of disasters –
Earthquake, Landslide, Flood, Drought, Fire etc - Classification, Causes, Impacts including
social, economic, political, environmental, health, psychosocial, etc.- Differential impacts- in
terms of caste, class, gender, age, location, disability - Global trends in disasters: urban
disasters, pandemics, complex emergencies, Climate change- Dos and Don’ts during various
types of Disasters.
UNIT II APPROACHES TO DISASTER RISK REDUCTION (DRR) 9

Disaster cycle - Phases, Culture of safety, prevention, mitigation and preparedness community
based DRR, Structural- nonstructural measures, Roles and responsibilities of- community,
Panchayati Raj Institutions/Urban Local Bodies (PRIs/ULBs), States, Centre, and other stake-
holders- Institutional Processess and Framework at State and Central Level- State Disaster
Management Authority(SDMA) – Early Warning System – Advisories from Appropriate
Agencies.
UNIT III INTER-RELATIONSHIP BETWEEN DISASTERS AND DEVELOPMENT 9

Factors affecting Vulnerabilities, differential impacts, impact of Development projects such as
dams, embankments, changes in Land-use etc.- Climate Change Adaptation- IPCC Scenario
and Scenarios in the context of India - Relevance of indigenous knowledge, appropriate
technology and local resources.
UNIT IV DISASTER RISK MANAGEMENT IN INDIA 9

Hazard and Vulnerability profile of India, Components of Disaster Relief: Water, Food,
Sanitation, Shelter, Health, Waste Management, Institutional arrangements (Mitigation,
Response and Preparedness, Disaster Management Act and Policy - Other related policies,
plans, programmes and legislation – Role of GIS and Information Technology Components in
Preparedness, Risk Assessment, Response and Recovery Phases of Disaster – Disaster
Damage Assessment.
UNIT V DISASTER MANAGEMENT: APPLICATIONS AND CASE STUDIES AND

FIELD WORKS 9
Landslide Hazard Zonation: Case Studies, Earthquake Vulnerability Assessment of Buildings
and Infrastructure: Case Studies, Drought Assessment: Case Studies, Coastal Flooding: Storm
Surge Assessment, Floods: Fluvial and Pluvial Flooding: Case Studies; Forest Fire: Case
Studies, Man Made disasters: Case Studies, Space Based Inputs for Disaster Mitigation and
Management and field works related to disaster management.
TOTAL: 45 PERIODS
79
OUTCOMES:
The students will be able to
 Differentiate the types of disasters, causes and their impact on environment and society
 Assess vulnerability and various methods of risk reduction measures as well as
mitigation.
 Draw the hazard and vulnerability profile of India, Scenarious in the Indian context,
 Disaster damage assessment and management.
TEXTBOOKS:
1. Singhal J.P. “Disaster Management”, Laxmi Publications, 2010. ISBN-10: 9380386427
ISBN-13: 978-9380386423
2. Tushar Bhattacharya, “Disaster Science and Management”, McGraw Hill India Education
Pvt. Ltd., 2012. ISBN-10: 1259007367, ISBN-13: 978-1259007361]
3. Gupta Anil K, Sreeja S. Nair. Environmental Knowledge for Disaster Risk Management,
NIDM, New Delhi, 2011
4. Kapur Anu Vulnerable India: A Geographical Study of Disasters, IIAS and Sage Publishers,
New Delhi, 2010.
REFERENCES
1. Govt. of India: Disaster Management Act , Government of India, New Delhi, 2005
2. Government of India, National Disaster Management Policy,2009.
GE7074 HUMAN RIGHTS LTPC

3003
OBJECTIVES :
 To sensitize the Engineering students to various aspects of Human Rights.
UNIT I 9
Human Rights – Meaning, origin and Development. Notion and classification of Rights –
Natural, Moral and Legal Rights. Civil and Political Rights, Economic, Social and Cultural
Rights; collective / Solidarity Rights.
UNIT II 9
Evolution of the concept of Human Rights Magana carta – Geneva convention of 1864.
Universal Declaration of Human Rights, 1948. Theories of Human Rights.
UNIT III 9
Theories and perspectives of UN Laws – UN Agencies to monitor and compliance.
UNIT IV 9
Human Rights in India – Constitutional Provisions / Guarantees.
UNIT V 9
Human Rights of Disadvantaged People – Women, Children, Displaced persons and
Disabled persons, including Aged and HIV Infected People. Implementation of Human
Rights – National and State Human Rights Commission – Judiciary – Role of NGO’s,
Media, Educational Institutions, Social Movements.
TOTAL : 45 PERIODS
80
OUTCOME :
 Engineering students will acquire the basic knowledge of human rights.
REFERENCES:
1. Kapoor S.K., “Human Rights under International law and Indian Laws”, Central Law Agency,
Allahabad, 2014.
2. Chandra U., “Human Rights”, Allahabad Law Agency, Allahabad, 2014.
3. Upendra Baxi, The Future of Human Rights, Oxford University Press, New Delhi.
CY7352 PHYSICAL CHEMISTRY LTPC

3003
AIM
 To make the students understand the principle and application of various physical
chemistry concepts
OBJECTIVE
 To acquire knowledge in the fields of electrochemistry, corrosion, phase equilibria,
colloids, colligative properties towards different applications
UNIT I ELECTROCHEMISTRY 9
Electrical Resistance - Specific Resistance - Electrical conductance - Specific Conductance -
Equivalent Conductance - Cell Constant - Determination of Cell Constant - Variation of
conductance with dilution - Kohlrausch's law - Single electrode potential - Galvanic cell - Cu - Zn
cell - EMF and its measurement - Reference electrode - Standard hydrogen Electrode - Calornel
electrode - Nerst equation - Electrochemical series - Applications of EMF Measurements.
UNIT II CORROSION & ITS CONTROL 9

Introduction - Dry or Wet corrosion Types - Wet or Electrochemical Corrosion - Mechanism -
Galvonic corrosion - Concentration Cell Corrosion - Soil Corrosion - Pitting Corrosion -
intergranular corrosion - pipeline corrosion - Water line Corrosion - Factors influencing
Corrosion and Corrosion Control.
UNIT III PHASE EQUILLIBRIA 9

Phase - Components - Degrees of freedom - The Gibbs Phase rule - Derivation of the Phase
rule - One Component system - The water System - The Sulphur System - Two Component
system - Simple Eutectic System - Thermal analysis - cooling curves - Lead-Silver System -
Desilverisation of Lead - Congruent and Incongruent Melting points.
UNIT IV COLLOIDS 9
Introduction to colloids - Classification of Colloids - Preparation of lyophobic colloidal solutions -
Purification of Colloidal Solutions - Properties of Colloids - Origin of charge on colloidal particles
- Determination of Size of colloidal particles - Donnan Membrane equilibrium - Emulsions - Gels
- Application of Colloids in Catalysis and drug delivery systems.
UNIT V THE DISTRIBUTION LAW & COLLIGATIVE PROPERTIES 9

Distribution Co-efficient - Distribution Law - Conditions for the validity of the Distribution law - I2-
CCl4-H2O System - Nature of interaction of the solute with one of the solvents - Dissociation -
Association - applications of Distribution law - Process of Extraction - Colligative properties -
Vapour Pressure Lowering - Osmosis and Osmotic Pressure - The boiling Point elevation - The
freezing point depression.
TOTAL : 45 PERIODS
81
TEXT BOOKS
1. Kund and Jain, Physical Chemistry, S. Chand and Company, New Delhi (1996).
2. Puri B. H. sharma L.R. and M.S. Prathma, " Principles of Physical Chemistry", S. Chand and
Company, New Delhi (2005)
3. B.S.Bahl, Arun Bahl and G.D. Tuli, "Essentials of Physical Chemistry", S.Chand and
Company, New Delhi (2005)
REERENCES
1. Gordon M. Barrow, Physical Chemistry, Sixth Edition, Tata McGraw Hill (1998).
2. Peters Atkins & Julio de Paula, Atkins' Physical Chemistry, 8th Edition, Oxford university
press. (2006).
AS7018 SAFETY AND ENVIRONMENTAL HEALTH L T P C

3 0 0 3
AIM : To know how to monitor the safety performance in industry
OBJECTIVE
To ensure that potential hazards are identified and mitigation measures are in place to
prevent accidents.
UNIT I CONCEPTS 9
Evolution of modern safety concept- Safety policy - Safety Organization - line and staff
functions for safety- Safety Committee- budgeting for safety.
UNIT II TECHNIQUES 9
Incident Recall Technique (IRT), disaster control, Job Safety Analysis (JSA), safety survey,
safety inspection, safety sampling, Safety Audit.
UNIT III ACCIDENT INVESTIGATION AND REPORTING 9

Concept of an accident, reportable and non reportable accidents, unsafe act and condition –
principles of accident prevention, Supervisory role- Role of safety committee – Accident
causation models - Cost of accident. Overall accident investigation process - Response to
accidents, India reporting requirement, Planning document, Planning matrix, Investigators
Kit, functions of investigator, four types of evidences, Records of accidents, accident reports-
Class exercise with case study.
UNIT IV SAFETY PERFORMANCE MONITORING 9

permanent total disabilities, permanent partial disabilities, temporary total disabilities -
Calculation of accident indices, frequency rate, severity rate, frequency severity incidence,
incident rate, accident rate, safety “t” score, safety activity rate – problems.
UNIT V SAFETY EDUCATION AND TRAINING 9

Importance of training-identification of training needs-training methods – programme,
seminars, conferences, competitions – method of promoting safe practice - motivation –
communication - role of government agencies and private consulting agencies in safety
training – creating awareness, awards, celebrations, safety posters, safety displays, safety
pledge, safety incentive scheme, safety campaign – Domestic Safety and Training.
TOTAL : 45 PERIODS
82
REFERENCES
1. Accident Prevention Manual for Industrial Operations”, N.S.C.Chicago, 1982
2. Heinrich H.W. “Industrial Accident Prevention” McGraw-Hill Company, New York, 1980.
3. Krishnan N.V. “Safety Management in Industry” Jaico Publishing House, Bombay, 1997.
4. John Ridley, “Safety at Work”, Butterworth & Co., London, 1983.
5. Blake R.B., “Industrial Safety” Prentice Hall, Inc., New Jersey, 1973.
AS7033 PETROLEUM GEOLOGY L T P C

3 0 0 3
AIM
To have a basic understanding of a broad array of tools used in the search for and production of
hydrocarbon reserves. To learn the principles of mapping a subsurface reservoir and estimating
the volumetrics.
OBJECTIVES
Students able to understand how geologists conduct the search for petroleum resources
through the value chain or the life cycle of a petroleum resource.
UNIT I 9
Introduction to earth science - Origin of earth. Nature and properties of minerals and rocks.
Sedimentation and sedimentary environment. Stratigraphy and geological time scale.
Introduction of plate tectonics.
UNIT II 9
Sedimentalogy of Petroleum bearing sequences - Sedimentary basins. Generation and
Migration of Petroleum. Physical and Chemical properties of Petroleum.
UNIT III 9
Subsurface Environment – Formation fluids – Composition, temperature, pressure and
dynamics. Traps and Seals. The Reservoir. Generation and Migration and Distribution.
UNIT IV 9
Exploration Methods - Well drilling. Formation Evaluation. Geophysical. Borehole Seismic and
4D Seismic. Subsurface geology.
UNIT V 9
Non conventional petroleum resources and reserve estimation.– Plastic and solid hydrocarbons.
Tar sands. Oil and gas shales. Coal bed methane. Assessment of reserves.
TOTAL : 45 PERIODS
TEXT BOOKS
1. Cox, P.A., “The Elements on Earth”, Oxford University Press, Oxford 1995
2. Wilson, M., Igneous Petrogenesis”, Unwin Hyman, London 1989.
REFERENCES
1. Boggs, S., “Principles of Sedimentology and Stratigraphy”, second edition, Merrill Publishing
Co., Toronto, 1995.
2. Krumblein, W.C. and Sloss, L.L., “Stratigraphy and Sedimentation”, second edition W.H.
Freeman and Co., 1963.
83
AS7013 PROCESS ENGINEERING LTPC
3003
OBJECTIVE:
 To impart knowledge on the fundamentals of Process Engineering activities in designing
the oil and gas facilities.
OUTCOME:
 To get familiarized on the roles and responsibilities of a Process Design Engineer.
 Understand the Engineering Drawings used in Design.
 To know the basics of performing various Hydraulic Calculations and sizing of
Equipments.
 Aware of various Design Codes & Standards used in Project.
UNIT I INTRODUCTION TO OIL AND GAS FACILITIES 9

Introduction to Oil and Gas Industry-Process description- Piping elements- Instruments: field
instruments, control valves- Process equipments- Role of Process Engineer.
UNIT II INTRODUCTION TO PROJECT ENGINEERING 9

Elements in Project Execution, Different Phases of a Project-(Basic Engineering package-BEP,
Front End Engineering Design-FEED, Proposal Engineering, EPC-EPCM Contract, LSTK),
Elements of Engineering, Process Engineering Deliverables.
Introduction to Piping design engineering, Instrument Design Engineering.
UNIT III PROCESS SIMULATION AND DESIGN 9

Introduction and purpose- Softwares used for Simulation, Simulation inputs- Steady state
simulation- Typical operation in simulation schemes- Heat and material balance generation,
Dynamic Simulation Study and its uses. Introduction to Relief and Blow down Studies, Pipeline
Flow assurance Study-Steady State and Transient, Softwares used in Flow assurance Studies,
Introduction to AIV/FIV studies, CFD analysis
UNIT IV ENGINEERING DIAGRAMS 9

Block flow diagram-Process/Utility flow diagram-Symbols for P&ID development: piping
elements, control system-Operation & control philosophy-Cause and Effect chart- typical PID
development for Glycol Dehydration unit, Process Safety Flow diagrams, SAFE Chart.
Introduction to Plot plan, General arrangement drawings.
UNIT V FACILITIES ENGINEERING 9

Process Design Basis and Design Criteria, Overview of various process equipments and its
design principles: Separators, Pumps, Compressors, Heat exchangers, Absorber column,
Heaters, Air coolers, Storage Tanks, Line hydraulics(Gas, Liquid and Multiphase lines)- Pump
hydraulics-Control valve hydraulics, Softwares used in Equipment design (Column, Heat
Exchanger etc). Introduction to various Codes and Standards followed in a PROJECT
(API,TEMA,ISA etc)
TOTAL : 45 PERIODS
REFERENCES
1. Perry's Chemical Engineers' Handbook, Robert H. Perry, October 2007.
2. GPSA Engineering Data Book, Gas Processors Suppliers Association, 13th Edition 2012.
3. American Petroleum Institute (API) Standards.
4. ISA Standards
5. TEMA standards, Tubular Exchanger Manufacturers Association, Inc.
84
AS7027 CRUDE OIL TRANSPORTATION LTPC
3 00 3
AIM To understand the crude oil transportation and to learn the concepts of storage.
OBJECTIVES
Students would be able to design various terminal design. They will be familiarize with the
storage systems.
Crude oil Trade, Selection of Port Location, Ship Building/Shipyards.
UNIT II NATURAL GAS REGASIFICATION TECHNOLOGY 9

Commercial Sourcing of Natural Gas, Different Kinds of Regasification Techniques,
Regasification Process & Cold Utilization, Synchronization of Degasified gas and Pipelines,
Current Status in India
UNIT III CRUDE OIL TRANSPORTATION 9

Transportation techniques of crude oil, Pipeline specification, Corrosion Prevention techniques,
Pressure drop, Pumps and Booster station, Wax deposition and prevention, Chemical treatment
UNIT IV DESIGN 9
Basic Engineering Aspects of Terminal Design, Design of Liquefaction Train, Ship
Building/Shipyards, Storage Facilities
UNIT V CHARACTERISTICS OF STORAGE VESSELS 9

Supply & Demand, Variation Gas Field & Aquifers, Technical Qualities and Storage, Properties
of Storage Reservoir, Rocks & Fluids. Flow through Storage Reservoir; Inventory Concept,
Pressure- Content Hysteresis, Inventory Verification, Gas Flow Performance, Gas Deliverability.
Design & Development of Underground Storage Fields: Operation of Storage Fields. Threshold
Pressure. Water Influx/Efflux Quantities. Aquifer Equilibrium Pressure. Error and Uncertainty.
Gas Storage in Salt Cavity & Caverns: Thermodynamics, Temperature and Pressure Effect.
Recent Developments Advanced Storage Techniques, Case Histories.
TOTAL : 45 PERIODS
TEXT BOOKS
1. Oilfield Processing: Crude Oil (Oilfield Processing of Petroleum R. Solvay, Pennwell Books
1995.
2. Advances in Environmental Control Technology: Storage Tank Paul Cheremisinoff Gulf
Professional Publishing; 1ST edition (May 9, 1996)
AS7031 EQUILIBRIUM STAGED OPERATIONS LTPC

3003
AIM
To impart knowledge on the design of different staged operations using the concept of
equilibrium
OBJECTIVES
The students will learn in detail the unifying theory and design of different staged operations like
absorption, distillation, extraction and adsorption.
85
UNIT I ABSORPTION 9
Gas Absorption and Stripping – Equilibrium; material balance; limiting gas-liquid ratio; tray
tower absorber - calculation of number of theoretical stages, tray efficiency, tower diameter;
packed tower absorber – rate based approach; determination of height of packing using HTU
and NTU calculations.
UNIT II DISTILLATION 9
Principle of distillation - flash distillation, differential distillation, steam distillation, multistage
continuous rectification, Number of ideal stages by Mc.Cabe - Thiele method and Ponchan -
Savarit method, Total reflux, minimum reflux ratio, optimum reflux ratio. Desing of azeotropic
and extractive distillation columns.
UNIT III MULTICOMPONENT DISTILLATION 9

Fundamental principles involved in the separation of multi component mixtures –equilibrium
flash distillation calculations for multi component mixtures – separation of multi component
mixtures at total reflux. Calculation of minimum reflux ratio. Determination of number of trays
UNIT IV LIQUID-LIQUID EXTRACTION 9

Liquid - liquid extraction - solvent characteristics-equilibrium stage wise contact calculations for
batch and continuous extractors- differential contact equipment-spray, packed and mechanically
agitated contactors and their design calculations-packed bed extraction with reflux. Pulsed
extractors, centrifugal extractors-Supercritical extraction
UNIT V ADSORPTION & MEMBRANE SEPARATION PROCESS 9

Adsorption - Types of adsorption, nature of adsorbents, adsorption equilibria, effect of pressure
and temperature on adsorption isotherms, Adsorption operations - stage wise operations,
steady state moving bed and unsteady state fixed bed adsorbers, break through curves. Solid
and liquid membranes; concept of osmosis; reverse osmosis; electro dialysis; ultrafiltration
TOTAL : 45 PERIODS
TEXT BOOKS
1. Wankat, P., "Equilibrium Stage Separations", Prentice Hall, 1993.
2. Treybal, R.E., "Mass Transfer Operations ", 3rd Edn., McGraw-Hill, 1981.
3. Seader, J.D. and E.J. Henley, “Separation Process Principles”, 2nd Ed., John Wiley, 2006.
REFERENCES
1. W.L McCabe J.C.Smith, and Harriot. P., "Unit Operations of Chemical Engineering ", Sixth
edition McGraw-Hill. International Edition, 2001
2. C.Judson King “Separation Processes ", Tata McGraw-Hill 1974.
3. R.F.Strigle (jr), Packed Tower Design and Application, 2nd Edn Gulf Publishing company
U.S.A.1994
AS7022 TRANSPORT PHENOMENA FOR PETROCHEMICAL ENGINEERS LTPC

3003
AIM
To give an overview of mass, momentum and energy transport, present the fundamental
equations and illustrate how to use them to solve problems.
OBJECTIVE
To describe mass, momentum and energy transport at molecular, microscopic and macroscopic
level, to determine velocity, temperature and concentration profiles.
86
OUTCOME
Understand the similarity between heat, mass and momentum transport and their analogy.
Develop the ability to formulate and solve mathematical models for physical situations.
Understand the science of turbulence, its prediction through various models and their utility.
Mathematical formulation of heat transfer problem and its numerical solution.
UNIT I MOMENTUM TRANSPORT 9

Viscosity, temperature effect on viscosity of gases and liquids, Newton’s law, mechanism of
momentum transport, shell balance method, pressure and velocity distributions in falling film,
circular tube, annulus, slit.
UNIT II ENERGY TRANSPORT 9

Thermal conductivity, temperature and pressure effect on thermal conductivity of gases and
liquids, Fourier’s law, mechanism of energy transport, shell energy balance, temperature
distribution in solids and laminar flow, with electrical, nuclear, viscous, chemical heat source,
heat conduction through composite walls, cylinders, spheres, fins, slits.
UNIT III TEMPERATURE DISTRIBUTION 9

Energy equations, special forms, use of equations of change, dimensional analysis of equations
of change, time-smoothed equations of change, empirical expressions, temperature distribution
for turbulent flow in tubes, jets.
UNIT IV CONCENTRATION DISTRIBUTION 9

Diffusivity, temperature and pressure effect, Fick’s law, mechanism of mass transport, theory of
diffusion in gases and liquids, shell mass balances, concentration distribution in solids and in
laminar flow: stagnant gas film, heterogeneous and homogeneous chemical reaction systems,
falling film, porous catalyst. The equation of continuity, summary of equations of change and
fluxes, use of equations of change, dimensional analysis, time smoothed equations of change,
empirical expressions for turbulent mass flux.
UNIT V ANALOGIES BETWEEN TRANSPORT PROCESSES 9

Turbulence, Reynolds equation for incompressible turbulent flow, Reynolds stresses Prandtl’s
mixing length theory, Eddy viscosity, the statistical theory of turbulence, Correlation coefficients,
intensity and scale of turbulence. Turbulence measurement, Hot – wire anemometer.
Turbulence flow in a closed conduit, Prandtl’s Power law of Velocity distribution in smooth and
rough pipes. Analogy between Momentum, Heat and Mass transfer. The Reynolds’ Analogy for
turbulent flow over a flat plate, The Prandtl’s Analogy, The Von karmon Analogy, Coulburn
analogy
TOTAL : 45 PERIODS
TEXT BOOKS
1. Bird R.B., Stewart W.E. and Lightfoot E.N., Transport Phenomena, 2nd Edition, Wiley, New
York, 2006,
2. Brodkey, R. S., and Hershey, H. C., “ Transport Phenomena - A unified approach”,
McGraw-Hill, 1988.
REFERENCES
1. Welty, J. R., Wilson, R. W., and Wicks, C. W., “Fundamentals of Momentum Heat and Mass
Transfer ”, 5thedition John Wiley, New York, 2007.
2. Slattery, J. S., “Advanced Transport Phenomena”, 2nd Edition, Cambridge University Press,
London, 1999
3. Knudson J.G. and Katz D.L., “Fluid Dynamics and Heat Transfer ”, 2nd Edition, McGraw Hill,
New York, 2000
87

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ANNA UNIVERSITY, CHENNAI

PROGRAMME EDUCATIONAL OBJECTIVES (PEOs) :

I. To inculcate in students, a professional and ethical attitude, effective communication

PROGRAMME OUTCOMES (POs):

I. Graduates will be able to demonstrate their knowledge professionally and shoulder

CURRICULA AND SYLLABI I - VIII SEMESTERS

S.No COURSE COURSE TITLE CATE CONTACT

S.No COURSE COURSE TITLE CATE CONTACT

S.No COURSE COURSE TITLE CATE CONTACT

S.No COURSE COURSE TITLE CATE CONTACT

S.No COURSE COURSE TITLE CATE CONTACT

*Course from the curriculum of other UG Programmes

S.No COURSE COURSE TITLE CATE CONTACT

*Course from the curriculum of other UG Programmes

S.No COURSE COURSE TITLE CATE CONTACT

7. AS7711 Process Control

S.No COURSE COURSE TITLE CATE CONTACT

TOTAL NO. OF CREDITS : 180

PROFESSIONAL ELECTIVES (PE)

S.No COURSE COURSE TITLE CATEG CONTACT L T P C

S.No COURSE COURSE TITLE CATEGORY CONTACT L T P C

BASIC SCIENCES (BS)

S.No COURSE COURSE TITLE CATE CONTACT L T P C

ENGINEERING SCIENCES (ES)

S.NO COURSE COURSE TITLE CATE CONTACT L T P C

PROFESSIONAL CORE (PC)

S.No COURSE COURSE TITLE CATEG CONTACT L T P C

EMPLOYABILITY ENHANCEMENT COURSES (EEC)

S.No COURSE COURSE TITLE CATEGORY CONTACT L T P C

Credits per Semester

UNIT I GREETING AND INTRODUCING ONESELF 12

UNIT II GIVING INSTRUCTIONS AND DIRECTIONS 12

UNIT III READING AND UNDERSTANDING VISUAL MATERIAL 12

UNIT IV CRITICAL READING AND WRITING 12

UNIT V LETTER WRITING AND SENDING E-MAILS 12

UNIT I DIFFERENTIAL CALCULUS 12

UNIT II FUNCTIONS OF SEVERAL VARIABLES 12

UNIT III INTEGRAL CALCULUS 12

UNIT IV MULTIPLE INTEGRALS 12

UNIT V DIFFERENTIAL EQUATIONS 12

UNIT I PROPERTIES OF MATTER 9

UNIT II ACOUSTICS AND ULTRASONICS 9

UNIT III THERMAL AND MODERN PHYSICS 9

UNIT IV APPLIED OPTICS 9

UNIT V CRYSTAL PHYSICS 9

CY7151 ENGINEERING CHEMISTRY L T P C

UNIT I POLYMER CHEMISTRY 9

UNIT II SURFACE CHEMISTRYAND CATALYSIS 9

UNIT III PHOTOCHEMISTRY AND SPECTROSCOPY 9

UNIT IV CHEMICAL THERMODYNAMICS 9

GE7151 COMPUTING TECHNIQUES L T P C

UNIT II C PROGRAMMING BASICS 9

UNIT V FUNCTIONS AND USER DEFINED DATA TYPES 9

BS7161 BASIC SCIENCES LABORATORY LTPC

PHYSICS LABORATORY: (Any Seven Experiments)

To introduce different experiments to test basic understanding of physics concepts applied in

10. Ultrasonic interferometer – determination of the velocity of sound and compressibility of

(Minimum of 8 experiments to be conducted)