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4.5 Optek Brochure

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Product Information

Control 4000
Photometric Analyzers

inline control

Control 8000
Universal Analyzers

english
deutsch
espaol
portuguese

franais
italiano

www.optek.com

For over 30 years, optek has focused


on measuring process liquids through
their interaction with light in facilities all
over the world. Although global, optek
remains a family owned company with
a team of more than 100 qualied,
customer-driven professionals.
Our condence is born from experience. With the expertise of more than
30,000 installations worldwide, our value to the customer resides in providing
a superior product that pays back. High
quality materials withstand the toughest process conditions including aggressive media, high temperature, and

high pressure applications. Cleanability


is ensured using high quality wetted
materials, superior design, as well as
sapphire optical windows.
As a global partner to various industries, optek offers the most advanced
technologies including superior signal
amplication, inline calibration support,
PROFIBUS PA, FOUNDATION FieldbusTM
and multilingual user interfaces for
easy onsite operations.
Our support ensures long term satisfaction with programs such as SpeedParts and SwapRepair to provide our

customers sustainable operations and


minimized downtime at the lowest cost
of ownership.
Conformity to international (ISO 9001),
industry-specic (FM/ATEX approval) or
company standards is easily achieved
with optek. Wherever process composition is controlled, the name optek has
become synonymous with world-class
products and support.

Optimize your process


with optek inline control.

Content
C4000 / C8000 converters

03

C4000 photometric converter (congurations)

04

C8000 universal converter (congurations)

06

C4000 / C8000 accessories

08

C4000 / C8000 technical data

09

Optical sensors overview

10

Optical sensors principles

11

Turbidity sensors AF16-N / TF16-N

12

Color sensors AF16-F / AF26

14

UV sensors AF45 / AF46

16

Probe sensors AS16 / AS56

18

Probe sensors ASD12-N / ASD19-N / ASD25-N

20

Conductivity sensor ACF60

22

pH electrode adapter PF12

23

Single Use Cell (S.U.C.)

24

Sensor body (armature)

26

System calibration

27

optek worldwide contact

28

See our TOP 5 brochures for applications in your industry.

www.optek.com

C4000/C8000 - Converters I 03

Control 4000 and Control 8000


are powerful, microprocessorbased converters.
The advanced modular design enables
precision process monitoring and control with multiple sensors.
The menu-based software is easy to
use and congure, and available in German, English, French, Dutch, Spanish,
Russian and Portuguese. The software
includes adjustable signal damping,
16 linearization tables and advanced
calculation capabilities. Multiple
outputs transmit the measurements in
real-time for precise process control.
An integrated data logger captures vital
process information for quality assurance and plant control records.
This data is easily transferred to a PC
via an RS232 port.

C4000 - Photometric Converter


The Control 4000 photometric converter is designed for optek ultraviolet
(UV), visible (VIS), near-infrared (NIR)
absorption based and scattered light
based sensors.
The graphic display can show absorbance, transmittance and concentration in real-time and in any unit of
measure such as CU, OD, %-Tr., ppm
(DE), EBC, FTU, g/l and many others.

These measurements may also be


displayed as text, bar graphs or trend
values. A factory zero is implemented
as an additional feature for scattered
light sensors. A secondary user zero
for additional offset is included, as
well as a slope and shift adjustment.
This manual adjustment can be used
to compensate for long-term process
related disturbances.

Sensors
Optical sensors (optek)

C4000 C8000
1-4

1-2

pH-Probes

Conductivity sensors (optek)

Communications

C4000 C8000

mA-outputs (0/4 - 20 mA)

2/4

mA-inputs (4 - 20 mA)

0/2

Relay-outputs
Failsafe-relay (active)
Remote-IN: Zero
Remote-IN: Range

C8000 - Universal Converter

Remote-IN: Hold

The Control 8000 universal converter


operates optek photometric sensors
along with 2 pH-probes and 2 conductivity sensors (optek patented ACF
series) simultaneously.

Profibus PA

All measurements (2 x optical, 2 x pH,


2 x conductivity and 2 x temperature)
are transmitted with the standard 8
mA-outputs and may also be displayed
as text and bar graphs.
The combination of C8000 and ACF60
conductivity sensors allows a wide dynamic range from 0 10 S/cm up to
0 850 mS/cm with the same sensor.

FOUNDATION FieldbusTM

Explosion-Proof

C4000 C8000

Ex-proof ATEX

Ex-proof FM

04 I C4000 - Photometric Converter

www.optek.com

The Control 4000 is available


in various congurations to
meet the exact needs of your
process.
Multiple photometric sensors
Multiple parameter sets
Multiple linearization tables
Data logger
Factory zero for scattered light
sensors
Remote control
Ex proof versions FM and ATEX

Sensor
1

4101
4121
4151
4161

4201
4221
4251
4261

4202
4222
4252
4262

4322
4352
4362

AF16 (AS16)

AF16 (AS16)

AF16 (AS16)

AF16 (AS16)

AF26 or AF45 or TF16

AF26

AF26

AF26 or AF45 or TF16

AF45

AF45

AF45 or TF16

AF46

TF16

TF16
ASD12, 19 or 25

TF16

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

ASD12, 19 or 25

4422
4452
4462

*C4422 can handle up to 4 sensors AS56

Display Modes

Remote Control

1 - 4 simultaneously displayed
values (congurable)
Numeric with bar graph and alarm
setting
Trendline

Parameter set (e. g. range)


Zero
Hold

Software Tools
8 parameter sets (incl. range, alarm, display, etc.)
16 linearization tables (max. 11 points)
8 offset and slope sets
Auto zero (local or remotely activated)
Factory zero (scattered light sensors only)
Password protection (3 levels and none)
Memory (non-volatile) retains all congurations and logged data

C4000 - Photometric Converter I 05

C4000 Conguration
Profibus PA
FOUNDATION FieldbusTM

www.optek.com

4101 4201 4202 4121


4151
4161

Detector inputs (optek)

Power supply 115/230 or 24 V

4221

Relay-outputs

4452
4462

Remote-IN: (Zero, Range, Hold) 3

4352
4362

4252
4262

4422

4251
4261

4322

Failsafe-relay (active)

4222

Lamp outputs (optek)

mA-outputs (0/4 - 20 mA)

mA-inputs (4 -20 mA)

pH-probe

(with C8000 only)

Conductivity (optek ACF)

(with C8000 only)

Ex-proof (optional)

PROFIBUS PA

FOUNDATION FieldbusTM

Fullls application prole for process automation


(version 3.01)
Cyclic:
- 4 measuring outputs, each with 4x limit and status
- Status of all 4 relays
- 2 measuring inputs
Acyclic:
- Zero, Hold, Product change, Monitors, Error codes
GSD, EDD le and DTM for FDT interface provided
Interface to probus DP segment using a segment
coupler

Fullls FOUNDATIONTM Fieldbus H1 (IEC 61158-2)


Registered function blocks: 1xRB, 8xAI(s), 4xDI(s), 2xAO(s)
H1 Prole class: 31P, 32L
H1 Device class: basic, link master
4 Measuring outputs with status
(C8000 8 measuring outputs with status)
4 Relays with status (C8000 1 Relay with status)
2 Measuring inputs (only C4000)
With optek specic resource block parameter:
Zero, Hold, Product change
Device description (DD) and capabilities les provided

www.optek.com

06 I C8000 - Universal Converter

C8000 Sensor Combination


1 AF, AS or TF Sensor or 2 ASD Sensors
1
AF16 VIS-NIR Absorption
AS16

VIS-NIR Absorption

AF26

Dual Channel Color

AF45

UV-Absorption

AF46

Dual Channel UV

TF16

11 Scattered Light

ASD12 NIR Absorption

ASD19 NIR Absorption

ASD25 NIR Absorption

4 Electrochemical Sensors
pH-probe

Conductivity optek ACF (6-pol)

The Control 8000 is available


in various congurations to
meet the exact needs of your
process.
1 or 2 photometric sensors
2 conductivity sensors
2 pH sensors
Multiple parameter sets
Multiple linearization tables
Data logger
Factory zero for scattered light
sensors
Remote control

Software Tools

Remote Control

8 parameter sets
(incl. range, display etc.)
16 linearization tables
(max. 11 points)
8 offset and slope sets
Auto zero
(local or remotely activated)
Factory zero
(scattered light sensors only)
Password protection
(3 levels and none)
Memory (non-volatile) retains all
congurations and logged data

Parameter set
Zero

Display Modes
2 - 8 simultaneously displayed
values (congurable)
Numeric with bar graph

C8000 - Universal Converter I 07

www.optek.com

1
2

8 Measurements
5 Sensors
3 Armatures
1 Converter

C8000 - Configuration

The C8000 provides optical density or forward scatter


turbidity measurements in the ultraviolet (UV), visible
(VIS), and near infrared (NIR) ranges. In addition to
optical sensors, the C8000 monitors up to two pH
sensors and two conductivity sensors with integrated
temperature measurements. One converter assures
easy operation with an intuitive user interface in a
compact package.

Detector inputs (optek)

Power supply 115/230 or 24 V

Remote-IN: (Zero, Range)

Relay-outputs
Failsafe-relay (active)

Lamp output (optek)

mA-outputs (0/4 - 20 mA)

mA-inputs (4 -20 mA)

1 Converter

Pre- and post-column chromatography monitoring


During purication, accurate, reliable
and repeatable measurements are
necessary to ensure accurate pooling
to maximize yields and protein/DNA
fraction purity.

pH-probe

Volume: < 22 ml
Height: 96 mm (3.78 in.)

UV

Cond.

pH

C8486

5 Sensors
AF46
Dual Channel
UV Absorption

8
3

(with C4000 only)

8 Measurements
UV Absorption
at 280 nm
UV Absorption
at 300 nm

Conductivity
ACF60
0 - 10 S/cm
(patented 6 electrode to 0 - 850 mS/cm
probe based on
Temperature
4 pole technique)
-10 C - 135 C (14 - 275 F)
Volume: < 44 ml
PF12
pH
Height: 96 mm (3.78 in.) (various pH
0 - 14 pH
electrodes)
Conductivity
ACF60
0 - 10 S/cm
Line size: 0.50 in.
(patented 6 electrode to 0 - 850 mS/cm
Clamp TC L14 AM7
probe based on
Temperature
PN: 0120-3508-33
4 pole technique)
-10 C - 135 C (14 - 275 F)
Volume: < 44 ml
PF12
pH
Height: 96 mm (3.78 in.) (various pH
0 - 14 pH
electrodes)
Line size: 0.50 in.
Clamp TC L14 AM7
PN: 0120-3508-33

C8480

pH

3 Armatures
Line size: 0.50 in.
Clamp TC L14 AM7
PN: 0120-3507-33
OPL: 5 mm

C8480

(with C4000 only)

FOUNDATION FieldbusTM

Ex-proof (optional)

Application (example):

(with C4000 only)

Profibus PA

Conductivity (optek ACF)

Cond.

www.optek.com

08 I C4000/C8000 - Accessories
The PC-Transfer software allows communication between converter and PC via a
RS-232 port. Documentation and set-up
including identical set-up of multiple converters are made simple.
Converter to PC:

Parameter set
Trend data online
Data logger

PC to converter:

Parameter set
Software update
Mathematics module
(C4000 only)

The advanced version features an additional mathematics module for complex


measuring tasks and parameter creation
on the PC.

C
B

A
A

S19-42

Wall mount housing (IP65)


Material: stainless steel 1.4301 / SS304
A: 301 mm (11.9 in.)
B: 340 mm (13.4 in.)
C: 237 mm ( 9.4 in.)

B19-42
B19-4

Wall m
mount housing (IP66)
Materia
Material: plastic (ABS)
A: 287 mm (11.3 in.)
B: 353 mm (13.9 in.)
C: 147 mm ( 5.8 in.)
D: 237 mm ( 9.4 in.)

B
C

T19-42

Table top housing


Material: aluminum
A: 150 mm ( 5.9 in.)
B: 260 mm (10.2 in.)
C: 320 mm (12.6 in.)

Front-Kit

Front panel mounting (IP65 - front only)


(not shown)

ATEX E
EX d

Flamepro housing EX d (IP65)


Flameproof
Cl
ication: II 2 (2) G Ex de [ia] II B T5
Classi
Approval: KEMA 08 ATEX 0123
Material: cast aluminum
A: 320 mm (12.6 in.)
B: 450 mm (17.7 in.)
C: 355 mm (14.0 in.)
D: 500 mm (19.7 in.)

C4000/C8000 - Technical Data I 09


C4000

Housing

19"- version for mounting in control cabinets 3 U / 42 HP


- dimensions: W 213.0 mm (8.39 in.) H 128.4 mm (5.06 in.) D 230.0 mm (9.05 in.)
- material:
stainless steel / polyester / silicone / glass / diverse plastics
- protection: front IP40 / rear IP20 (mains supply secured against accidental touching)

Display

LCD graphic display black on white (240 x 128 pixel), LED background illuminated

Operation

18-button keyboard

System clock

accuracy approx. 1 minute/month (battery life approx. 15 years)

LED

1 LED (green): power on


1 LED (red-flashing): system failure
3 LEDs (yellow): alarm I, II, III

1 LED (green): power on


1 LED (red-flashing): system failure

Data logger

4 parallel measuring values


(ring buffer with approx. 25,000 data points x 4)
(interval: 1/second - 1/hour)

8 parallel measuring values


(ring buffer with approx. 12,500 data points x 8)
(interval: 1/second - 1/hour)

Sensor-inputs

1 - 4 for optek photometric sensors


n/a
n/a

4 for optek photometric sensors


2 for optek conductivity sensors
2 for pH-probes (temperature compensated)

Sensor-inputs (explosion proof)

optional: 1 - 4 for optek photometric sensors (intrinsic safe)

n/a

mA-inputs

optional:
2 x 4 - 20 mA (functionally galvanically isolated)
- accuracy: < 0.5 %
- resolution: < 0.05 %
- load:
< 200 Ohm

n/a

Remote-inputs

optional:
7 x 24 V (19 ... 29 V DC), typically 6.0 mA
for remote range setting, remote zero, remote hold

standard:
4 x 24 V (19 - 29 V DC), typically 6.0 mA
for remote range setting, remote zero

optional: Profibus PA profile, version 3.01, amendment 2

n/a

Profibus PA interface

C8000

FOUNDATION Fieldbus interface optional: FOUNDATION FieldbusTM H1 (IEC 61158-2)


TM

Sensor lamp-outputs

1 or 2 lamp supply for optek photometric sensors


4.5 ... 8.5 V DC

1 lamp supply for optek photometric sensors


4.5 ... 7.8 V DC

mA-outputs

2 or 4 x 0/4 - 20 mA (NAMUR)
(functionally galvanically isolated)
- accuracy: < 0.5 %
- resolution: < 0.05 %
- load:
< 600 Ohm

8 x 0/4 - 20 mA (NAMUR)
(functionally galvanically isolated)
- accuracy: < 0.5 %
- resolution: < 0.05 %
- load:
< 600 Ohm

Relay-outputs

3 independent software-configurable relay contacts


0 - 50 V AC, 0 - 75 V DC, 0 - 2 A
- for alarm or status feedback
- initiation delay configurable: 0 - 999 sec.

n/a

Failsafe-output

1 SPDT contact to alarm in case of lamp or system failure (active)


0 - 50 V AC, 0 - 75 V DC, 0 - 2 A

Serial communication

RS232 bi-directional interface on front panel (with software package optek PC-transfer)
- upload / download of configuration, download of data logger content

Cable lengths (sensor)

2, 3, 5, 10, 15, 20, 30 ... 100 m


(7, 10, 16, 33, 49, 66, 98 ... 328 ft)
cable length > 100 m on request up to 1,000 m (3,280 ft)
sensors AS56 / AS16: max: 50 m
sensors ASD: 2, 3 ,5 or 10 m (7, 10, 16 or 33 ft.)

Power supply

115 / 230 V AC, selectable (93.5 - 132 / 187 - 264 V AC, 47 - 64 Hz) or
24 V AC / DC (AC: 20.4 - 26.4 V AC, 47 - 64 Hz; DC: 20.4 - 28.8 V DC)
- power consumption: < 50 VA

Ambient conditions

temperature during operation (no direct sunlight):


- converter:
- with optional stainless steel housing S19-42 (IP65):
- with optional plastic housing B19-42 (IP66):
- with optional EX d housing (IP65):
temperature during transport (no direct sunlight) :

Software languages

English, German, French, Spanish, Dutch, Portuguese, Russian

Data given are subject to changes without prior notice.

2, 3, 5, 10, 15, 20, 30 m


(7, 10, 16, 33, 49, 66, 98 ft)
sensors ASD: 2, 3, 5 or 10 m (7, 10, 16 or 33 ft.)

-10 - 55 C (14 - 131 F)


-20 - 45 C ( -4 - 113 F)
-10 - 40 C (14 - 104 F) (C4000 only)
-20 - 40 C ( -4 - 104 F) (C4000 only)
-20 - 70 C ( -4 - 158 F)

www.optek.com

Technical Data

10 I Optical Sensors Overview

www.optek.com

Sensor Specifications
Basic Measuring Principle:

ASD

AS16

AS56

AF16

AF26

AF45

AF46

TF16

Absorption of light - 1-channel


Absorption of light - 2-channel

Scattering of light - 11

NIR (730 - 970 nm) - Turbidity

AS16-N

AS56-N

AF16-N

VIS (385 - 1000 nm) - Color

AF16-F

VIS (430 - 620 nm) - Color

AS16-F

AS56-F

AF16-F

UV (254 - 313 nm)

OPL (optical path length) mm

(*)

1 - 40

5 / 10

Window gaskets (various)

n/a

n/a

n/a

Basic Measuring Ranges:


CU / AU / OD / %-Tr.
ppm / FTU / EBC

Wavelengths Used:
NIR (840 - 910 nm)

Windows and OPL:


Window material: Pyrex

Window material: Sapphire


1 - 1000

1 - 1000

1 - 160

1 - 160

40

Process Adaption:
Armature in pipe
Insertion through port

Process Ratings:
Max. pressure up to bar (psi)

(*)

20 (290)

10 (145)

100 (1450) depending on materials and design (higher on request)

Max. temperature up to C (F) - continuously

(*)

100 (212)

90 (194)

120 (248)

120 (248)

70 (158)

70 (158)

120 (248)

HT (high temperature) up to C (F) - continuously

240 (464)

240 (464)

120 (248)

120 (248)

240 (464)

VB (calibration adapter)

EX-proof ATEX

EX-proof FM

Options:

* See individual sensor data for details


Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user. Data given are subject to changes without prior notice.

ASD (e.g. ASD12)

AS (e.g. AS16)

AF, TF (e.g. TF16)

Optical Sensors - Principles I 11


1

Probe ASD12 / ASD19 / ASD25

Lamp

Detector

Detector

Lamp

Probe AS16 / AS56

www.optek.com

NIR-Absorption,
single channel concentration measurement

VIS- and NIR-Absorption,


single channel concentration and
color measurement

Sensor AF16

VIS- and NIR-Absorption,


single channel concentration
and color measurement

Abs.
Abs.

Abs.

Sensor AF46

UV-Absorption,
dual channel concentration measurement
with compensation of lamp intensity

Abs.

Sensor AF45

UV-Absorption,
single channel concentration measurement
with compensation of lamp intensity

Detector(s)

Sensor AF26

VIS-Absorption,
dual channel color measurement
with turbidity compensation

Lamp

Abs.
Abs.

Sensor TF16

11 scattered light and NIR-Absorption


dual channel turbidity measurement

11
Abs.
11

12 I Turbidity Sensors AF16-N/TF16-N


3

Model AF16-N Single Channel Absorption (NIR)

2 1 2

5
4
5
7

2 1 2

2 Windows
4 Measurement detector
6 Lamp module

Models AF16-N and TF16-N are high


precision turbidity sensors for use in
various industries. The sensors are designed for inline operation and provide
accurate concentration measurements
with remarkable repeatability, linearity
and resolution.
Modular construction of the sensors
offers maximum exibility in adapting
to various process needs. Options
include electro-polished sensor bodies,
hazardous location (explosion-proof)
capability, chemical resistant materials
(sapphire windows, titanium, Hastelloy,
etc.) and high temperature or high
pressure versions.

AF16-N
(NIR-Absorption / Turbidity)
A special tungsten lamp produces
a constant light beam that passes
through the process medium. The attenuation of the light intensity, caused
by absorption and/or scattering by
dissolved and undissolved substances,
is detected by a sealed silicon photodiode.
The AF16-N uses light from 730 - 970 nm
(NIR) to measure solids concentration
independent from color or color changes. Depending on the optical path
length, measuring ranges from high
percentage (OPL = 1 mm) to 0 - 100 ppm
(OPL = 160 mm) are possible.

7
1
3
5
7

Model TF16-N Dual Channel Scattered Light (11)


Sensor body
Focusing optics
Eight 11 detectors
Lamp module

Detectors

www.optek.com

1 Sensor body
3 Filter
5 Optics module

2 Windows
4 Detector 0 (Abs.)
6 Optics module

TF16-N
(Scattered Light / Turbidity)
Light scattered from particles (trace
suspended solids, undissolved liquids
or gas bubbles) in the medium is
detected by eight hermetically sealed
silicon photodiodes at an angle of 11.
At the same time, the unscattered light
is detected by a reference photodiode
(comparable to an AF16-N). The sensor
can be calibrated in ppm (DE), EBC or
FTU and measures extremely low particle sizes and concentrations. Additionally, high particle concentrations can
be monitored independent of color at
the direct light detector.

OPL
Special optical windows are made from
a single crystal sapphire, providing
superior resistance to all abrasive and
corrosive media. With the appropriate
choice of sensor bodies and windows
in various lengths, the optimal OPL

(optical path length = distance between the windows) can be achieved to


meet the measurement requirements,
e. g. low/high measuring ranges at
highest resolution.

NIST-traceable
NIST-traceable calibration accessories
(AF16-N only) provide absolute measurement condence (for details refer to
page 27).

Typical Applications:
Separator control, pulp
concentration (AF16-N)
Filter control, oil in water (TF16-N)

See our TOP 5 brochures for


applications in your industry.

optek TF16-EX-HT-N
Scattered Light Dual Channel Turbidity
Turbidi Sensor

Turbidity Sensors AF16-N/TF16-N I 13


Technical Data

AF16-N (Turbidity)

TF16-N (Turbidity)

Measurement principle
Measurement wavelength
Detector(s)

Measuring range NIR-Absorption

1- Channel absorption of light and


2- Channel scattering of light (11)

730 nm - 970 nm

730 nm - 970 nm

1 silicon photodiode (hermetically sealed)

1 silicon photodiode (hermetically sealed) (Abs.)


8 silicon photodiodes (hermetically sealed) (11)
any measuring range between
0 - 0.05 to 5 CU
0 - 50 to 8,000 ppm (DE)
0 - 20 to 3,200 FTU
0 - 5 to 800 EBC

any measuring range between


0 - 0.05 to 6 CU
0 - 50 to 40,000 ppm (DE)
0 - 20 to 16,000 FTU
0 - 5 to 4,000 EBC

any measuring range between


0 - 0.5 to 500 ppm (DE)
0 - 0.2 to 200 FTU
0 - 0.05 to 50 EBC
(higher [i.e. 100 EBC] with reduced resolution, accuracy)

Measuring range Scattered Light (11) n/a

Optical path length


Calibration

1 - 1000 mm

40 mm standard
(10 - 60 mm with reduced accuracy)

Abs.: CU (concentration units)


application specic calibration

Abs.: CU (concentration units)


application specic calibration
basic calibration 11: in ppm (DE) / FTU / EBC

Light source

special incandescent tungsten lamp 5.0 V DC, 970 mA


typical life span: 3 to 5 years (25,000 to 40,000 hours)

Resolution

< 0.05 % of respective measuring range

Repeatability

< 0.5 % of respective measuring range (scattered light < 0.3 %)

Linearity

< 1 % of respective measuring range (specic to application)

Protection

all optical parts have an IP rating of IP65 or higher

Material

Stainless steel 1.4435 (SS 316L), 1.4539, 1.4571 (SS 316Ti), 1.4462,
Titanium 3.7035 (Grade 2), Hastelloy 2.4602 (C22), Plastic TFM4215, PVC, ... others on request

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

Sensor Body

Process connection
Process pressure

Flanges (ASME, DIN, JIS), Clamps (TC, ISO, DIN), Female Threads (NPT, DIN),
Sanitary Threads (DIN 11851), Tube Ends (DIN, ISO, OD), Varivent, ... others on request
10 mbar to 100 bar (0.15 psi to 1450 psi) - higher on request
depending on process connection, materials and design

Windows

1-Pyrex, 2-Sapphire, 3-Sapphire Biotech

Window gaskets

Silicone (FDA), Viton (FDA), EPDM (FDA / USP Class VI), Kalrez 4079, ... others on request

Process temperature

permanent: 0 - 120 C ( 32 - 248 F) / peak 15 min/day: 0 - 150 C ( 32 - 302 F)

Process temperature OPTION HT

permanent: -30 - 240 C (-22 - 464 F) / peak 15 min/day: -30 - 260 C (-22 - 500 F)

Process temperature OPTION EX

permanent: -30 - 120 C (-22 - 248 F) / peak 15 min/day: -30 - 150 C (-22 - 302 F)

Process temperature OPTION EX-HT

permanent: -30 - 240 C (-22 - 464 F) / peak 15 min/day: -30 - 260 C (-22 - 500 F)

Ambient temperature

operation: 0 - 40 C ( 32 - 104 F)
operation: -30 - 40 C (-22 - 104 F) with options HT / EX / EX-HT
transport: -20 - 70 C ( -4 - 158 F)

Ex-proof

none

Ex-proof OPTION EX (EN-D)

Sensor assembly in ex-proof version acc. ATEX (EN-D) - Approval: DMT ATEX E 176

Ex-proof OPTION EX (FM-D)

Sensor assembly in ex-proof version acc. FM (FM-D) - Approval: FMG J. I. 3013884

Calibration adapter

none

n/a

Calibration adapter OPTION VB


- recommended -

Filter adapter FH03 (detector side)


for calibration lter used for sensor verication

n/a

Temperature Ratings

Explosion Proof

Calibration

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

www.optek.com

Measurement
1- Channel absorption of light

14 I Color Sensors AF16-F/AF26


3

Model AF16-F Single Channel Absorption (VIS)

www.optek.com

1 Sensor body
3 Filter
5 Optics module
6

2 1 2

3
9

4
1
3
5
7
9

2 Windows
4 Measurement detector
6 Lamp module

Model AF26 Dual Channel Absorption (VIS-NIR)


Sensor body
Beam splitter
Measurement detector A
Measurement detector B
Lamp module

2
4
6
8

Windows
Filter A
Filter B
Optics module

2 1 2

Models AF16-F and AF26 are high


precision color sensors used to measure color or color changes in various
industries. The sensors are designed
for inline operation and provide accurate concentration measurements with
remarkable repeatability, linearity and
resolution.
Modular construction of the sensors
offers maximum exibility in adapting
to various process needs. Options
include electro-polished sensor bodies,
hazardous location (explosion-proof)
capability, chemical resistant materials
(sapphire windows, titanium, Hastelloy,
etc.) and high temperature or high
pressure versions.

VIS-Absorption (Color)
A special tungsten lamp produces
a constant light beam that passes
through the process medium. The attenuation of the light intensity, caused
by absorption and/or scattering by dissolved and undissolved substances, is
detected by sealed silicon photodiodes.

monitored using color measurements.


For instance, increasing iron or nickel
contents result in a yellow liquid.

OPL
Special optical windows are made from
a single crystal sapphire, providing
superior resistance to all abrasive and
corrosive media. With the appropriate
choice of sensor bodies and windows
in various lengths, the optimal OPL (optical path length = distance between
the windows) can be achieved to meet
the measurement requirements, e. g.
low/high measuring ranges at highest
resolution.

Dual Wavelengths
Selected combinations of optical lters
make it possible to focus on specic
wavelengths ensuring suitable adaption to the application. While the AF16-F
uses one wavelength, an AF26 is
equipped with an internal beam splitter
making it possible to measure two
wavelengths simultaneously.
Connected to optek Control 4000 or
Control 8000 converters, the second

wavelength can be used to compensate for (varying) background turbidity


and any lamp intensity variation to
assure the highest level of precision
and long-term performance. Combined
with a long optical path length, even
the smallest color changes can be
measured.

NIST-traceable
NIST-traceable calibration accessories
provide absolute measurement condence (for details refer to page 27).

Typical Applications:
Monitoring of various color scales
0-10 to 0-500 APHA Hazen,
30 to -16 Saybolt,
0-1 to 0-8 ASTM etc.
Measuring various concentrations
0-100mg/l chlorine,
0-5mg/l iron in hydrochloric acid,
0-100% chlorine gas,
0-10 ppm to 0-15g/l chlorine dioxide

See our TOP 5 brochures for


applications in your industry.

At a specic wavelength in the visible


range (385 - 670 nm) there is a loss
of light as a result of an increase in
color depth. optek sensors measure
in various color scales such as Hazen,
APHA, ASTM, EBC, Gardner, Saybolt,
and many more. Also, many dissolved
substances in liquids can be precisely
optek AF26 Dual Channel Absorption Sensor

Color Sensors AF16-F/AF26 I 15


Technical Data

AF16-F (Color)

AF26 (Color)

Measurement principle

1- Channel absorption of light

2- Channel absorption of light

385, 400, 430, 470, 525, 620, 670, 750, 1000 nm,
others on request

385/430, 385/550, 400/550, 400/620,420/700,


430/525, 430/620, 430/700, 460/620,470/620,
470/700, 525/620, 525/700, 525/750,550/800,
620/800, 670/550,670/750, 1000/800 nm,
others on request

Measurement wavelength(s)

Detector(s)
Measuring range
Optical path length
Calibration
Light source
Resolution
Repeatability
Linearity
Protection

1 silicon photodiode (hermetically sealed)

2 silicon photodiodes (hermetically sealed)

any measuring range between


0 - 0.05 to 2.8 CU (dependent on used lter)
contact product specialist for
application specic ranges
1 - 1000 mm

any measuring range between


0 - 0.05 to 3 CU (dependent on used lter)
contact product specialist for
application specic ranges

CU (concentration units)
application specic calibration
special incandescent tungsten lamp 5.0 V DC, 970 mA
typical life span: 3 to 5 years (25,000 to 40,000 hours)
< 0.05 % of respective measuring range
< 0.5 % of respective measuring range
< 1 % of respective measuring range (specic to application)
all optical parts have an IP rating of IP65 or higher

Sensor Body
Material

Stainless steel 1.4435 (SS 316L), 1.4539, 1.4571 (SS 316Ti), 1.4462,
Titanium 3.7035 (Grade 2), Hastelloy 2.4602 (C22), Plastic TFM4215, PVC, ... others on request

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

Process connection
Process pressure

Flanges (ASME, DIN, JIS), Clamps (TC, ISO, DIN), Female Threads (NPT, DIN),
Sanitary Threads (DIN 11851), Tube Ends (DIN, ISO, OD), Varivent, ... others on request
10 mbar to 100 bar (0.15 psi to 1450 psi) - higher on request
depending on process connection, materials and design

Windows

1-Pyrex, 2-Sapphire, 3-Sapphire Biotech

Window gaskets

Silicone (FDA), Viton (FDA), EPDM (FDA / USP Class VI), Kalrez 4079, ... others on request

Process temperature

permanent:

Process temperature OPTION HT

permanent: -30 - 240 C (-22 - 464 F) / peak 15 min/day: -30 - 260 C (-22 - 500 F)

Process temperature OPTION EX

permanent: -30 - 120 C (-22 - 248 F) / peak 15 min/day: -30 - 150 C (-22 - 302 F)

Process temperature OPTION EX-HT

permanent: -30 - 240 C (-22 - 464 F) / peak 15 min/day: -30 - 260 C (-22 - 500 F)

Ambient temperature

operation:
0 - 40 C ( 32 - 104 F)
operation: -30 - 40 C (-22 - 104 F) with options HT / EX / EX-HT
transport: -20 - 70 C ( -4 - 158 F)

Ex-proof

none

Ex-proof OPTION EX (EN-D)

Sensor assembly in ex-proof version acc. ATEX (EN-D) - Approval: DMT ATEX E 176

Ex-proof OPTION EX (FM-D)

Sensor assembly in ex-proof version acc. FM (FM-D) - Approval: FMG J. I. 3013884

Calibration adapter

none

Calibration adapter OPTION VB


- recommended -

Filter adapter FH03 (detector side)


for calibration lter used for sensor verication

Temperature Ratings
0 - 120 C ( 32 - 248 F) / peak 15 min/day: 0 - 150 C ( 32 - 302 F)

Explosion Proof

Calibration

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

www.optek.com

Measurement

16 I UV Sensors AF45/AF46
5

www.optek.com

1 Sensor body
3 Filter
5 Reference detector

2 1 2

9
6
4

10

Model AF45 Single Channel Absorption (UV)

1
3
5
7
9

2 Windows
4 Measurement detector
6 Lamp module (mercury)

Model AF46 Dual Channel Absorption (UV)


Sensor body
Beam splitter
Measurement detector A
Measurement detector B
Reference detector B

2
4
6
8
10

Windows
Filter A
Filter B
Reference detector A
Lamp module (mercury)

2 1 2

Models AF45 and AF46 are high precision UV absorption sensors for use
in the biotech and chemical industries. The sensors are designed for
inline operation and provide accurate
concentration measurements with
remarkable repeatability, linearity and
resolution.
Modular construction of the sensors
offers maximum exibility in adapting
to various process needs. Options
include electro-polished sensor bodies,
hazardous location (explosion-proof)
capability, chemical resistant materials
(sapphire windows, titanium, Hastelloy,
etc.) and high temperature or high
pressure versions.

UV-Absorption
A special mercury lamp produces
a constant light beam that passes
through the process medium. The attenuation of the light intensity, caused
by absorption and/or scattering by dissolved and undissolved substances, is
detected by sealed silicon photodiodes.
The light intensity of the lamp itself
is measured by sealed silicon photodiodes using the same lter as the
measurement wavelength. The sealed
silicon photodiodes also compensate
for any variances in lamp intensity,
assuring the highest level of precision
and long-term performance. Specic
lamp design and capability of optek

converters operating with lowest photocurrents provide a prolonged life span


at the lowest cost of ownership.

OPL
Special optical windows are made from
a single crystal sapphire, providing
superior resistance to all abrasive and
corrosive media. With the appropriate
choice of sensor bodies and windows
in various lengths, the optimal OPL (optical path length = distance between
the windows) can be achieved to meet
the measurement requirements, e. g.
low/high measuring ranges at highest
resolution.

Dual Wavelengths
Selected combinations of optical lters
make it possible to focus on specic
wavelengths. Different peak wavelengths are available with a variety of
bandwidth options ensuring suitable
adaption to the application.

optek AF46-VB
Dual Channel UV Absorption Sensor
with Calibration Option

While the AF45 uses one wavelength,


an AF46 is equipped with an internal
beam splitter making it possible to
measure two wavelengths simultaneously. Connected to an optek Control
4000 or Control 8000 converter, a
wide dynamic range is possible to
measure at high and low values with
one sensor in one setup. This ensures
minimal hold-up volume and installation cost.

NIST-traceable
NIST-traceable calibration accessories
provide absolute measurement condence (for details refer to page 27).

Typical Applications:
Monitoring of chromatographic
columns (i.e. protein concentration)
Measuring concentrations of
aromatics

See our TOP 5 brochures for


applications in your industry.

UV Sensors AF45/AF46 I 17
Technical Data

AF45 (UV)

AF46 (UV)

Measurement principle

1- Channel absorption of light

2- Channel absorption of light

254-13, 280-09, 280-13, 290-13,


300-13, 313-13 nm, ... others on request

254-13 / 280-13,
280-09 / 300-05,
280-09 / 313-13,
280-13 / 313-13,
others on request

Measuring detector(s)

1 silicon photodiode (hermetically sealed)

2 silicon photodiodes (hermetically sealed)

Reference detector(s)

1 silicon photodiode (hermetically sealed)

2 silicon photodiodes (hermetically sealed)

Measuring range

any measuring range between


0 - 0.05 to 3 CU (dependent on used lter / OPL)
(contact product specialist for
application specic ranges)

any measuring range between


0 - 0.05 to 2 CU (dependent on used lter / OPL)
(contact product specialist for
application specic ranges)

Optical path length

1 - 160 mm

Calibration

CU (concentration units)
application specic calibration

Light source

low pressure mercury lamp


typical life span: 1 to 2 years (8,000 to 16,000 hours)

Resolution

< 0.05 % of respective measuring range

Repeatability

< 0.5 % of respective measuring range

Linearity

< 1 % of respective measuring range (specic to application)

Protection

all optical parts have an IP rating of IP65 or higher

Material

Stainless steel 1.4435 (SS 316L), 1.4539, 1.4571 (SS 316Ti), 1.4462,
Titanium 3.7035 (Grade 2), Hastelloy 2.4602 (C22), Plastic TFM4215, PVC, ... others on request

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

Measurement wavelength(s)

254-13 / 313-13,
280-09 / 300-13,
280-13 / 300-13,
290-13 / 313-13 nm, ...

Sensor Body

Process connection
Process pressure

Flanges (ASME, DIN, JIS), Clamps (TC, ISO, DIN), Female Threads (NPT, DIN),
Sanitary Threads (DIN 11851), Tube Ends (DIN, ISO, OD), Varivent, ... others on request
10 mbar to 100 bar (0.15 psi to 1450 psi) - higher on request
depending on process connection, materials and design

Windows

2-Sapphire, 3-Sapphire Biotech (do not use Pyrex)

Window gaskets

Viton (FDA), EPDM (FDA / USP Class VI), Kalrez 4079, ... others on request (do not use Silicone)

Process temperature

permanent:

Process temperature OPTION HT

permanent: -30 - 120 C (-22 - 248 F) / peak 15 min/day: -30 - 150 C (-22 - 302 F)

Process temperature OPTION EX

permanent: -30 - 70 C (-22 - 158 F) / peak 15 min/day: -30 - 135 C (-22 - 275 F)

Process temperature OPTION EX-HT

permanent: -30 - 120 C (-22 - 248 F) / peak 15 min/day: -30 - 150 C (-22 - 302 F)

Ambient temperature

operation:
0 - 40 C ( 32 - 104 F)
operation: -30 - 40 C (-22 - 104 F) with options HT / EX / EX-HT
transport: -20 - 70 C ( -4 - 158 F)

Temperature Ratings
0 - 70 C ( 32 - 158 F) / peak 15 min/day:

0 - 135 C ( 32 - 275 F)

Explosion Proof
Ex-proof

none

Ex-proof OPTION EX (EN-D)

Sensor assembly in ex-proof version acc. ATEX (EN-D) - Approval: DMT ATEX E 176

Ex-proof OPTION EX (FM-D)

Sensor assembly in ex-proof version acc. FM (FM-D) - Approval: FMG J. I. 3013884

Calibration adapter VB

Filter adapter FH03 (detector side) for calibration lter used for sensor verication

Calibration

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

www.optek.com

Measurement

www.optek.com

18 I Probe Sensors AS16/AS56

Model AS16 (AS56) Single Channel Absorption

1 OPL
3 Lamp module
5 Detector module
5

No window gaskets used

Models AS16 and AS56 are high


precision sensors measuring turbidity
(AS16-N and AS56-N) or color (AS16-F
and AS56-F) for use in various industries. The sensors are designed for
inline operation and provide accurate
concentration measurements with
remarkable repeatability, linearity and
resolution.

AS16
The AS16 series offers the high-end
range of optek probe sensors. A wide
selection of different optical path
lengths and insertion depths combined
with optional calibration lters and
electro-polished stainless steel meet
all requirements of the biotechnology
industry.

AS56
The AS56, based on the same design
as the AS16 with seal-less window construction, is typically used in food and
beverage applications. Limited variations allow cost effective measurement
(i.e. phase separation).

NIR-Absorption (Turbidity)
VIS-Absorption (Color)
A special tungsten lamp produces
a constant light beam that passes
through the process medium. The attenuation of the light intensity, caused
by absorption and/or scattering by
dissolved and undissolved substances,
is detected by a sealed silicon photodi-

2 Windows
4 Optics modules (incl. lter)

ode. The AS16-N and AS56-N uses light


from 730 - 970 nm to measure solids
concentration independent from color
or color changes (e.g. yeast concentration in beer during tank draining).
The AS16-F and AS56-F uses a specic
wavelength in the visible spectrum to
measure color in liquids with little or
no turbidity (i.e. beer in water during
phase change).

OPL
Special optical windows are made from
a single crystal sapphire, providing
superior resistance to all abrasive
and corrosive media. opteks superior
manufacturing techniques allow mounting the windows without gaskets or
glue for lifetime without maintenance.
The appropriate choice of the optimal
OPL (optical path length = distance
between the windows) supports all
measurement requirements,
e. g. low/high measuring ranges at
highest resolution.

NIST-traceable
NIST-traceable calibration accessories
(AS16 only) provide absolute measurement condence (for details refer to
page 27).

Typical Applications:
Cell density in fermentation (AS16-N)
Milk/water phase separation (AS56-N)
Beverage blending (AS16-F)
Beer/water phase separation (AS56-F)

See our TOP 5 brochures for


applications in your industry.

optek AS16-N Single Channel Absorption Probe

optek AS16-VB-N
Single Channel Absorption Probe with Calibration Option

Probe Sensors AS16/AS56 I 19


Technical Data

AS16

AS56

Measurement principle

1- Channel absorption of light

Detector

1 silicon photodiode (hermetically sealed)

Measurement wavelength

AS16-N: 730 - 970 nm


AS16-F: 430, 550 or 620 nm

AS56-N: 730 - 970 nm


AS56-F: 430 nm

AS16-N:
any measuring range between 0 - 0.05 to 6 CU
AS16-F:
any measuring range between 0 - 0.05 to 2 CU
(depending on wavelength)
1, 5, 10, 20 or 40 mm

AS56-N:
any measuring range between 0 - 0.05 to 4 CU
AS56-F:
any measuring range between 0 - 0.05 to 1.5 CU

Measuring range

Optical path length

5 or 10 mm

Calibration

CU (concentration units)
application specic calibration

Light source

special incandescent tungsten lamp 5.0 V DC, 970 mA


typical life span: 3 to 5 years (25,000 to 40,000 hours)

special incandescent tungsten lamp 5.0 V DC, 450 mA


typical life span: 3 to 5 years (25,000 to 40,000 hours)

Resolution

< 0.05 % of respective measuring range

< 0.5 % of respective measuring range

Repeatability

< 0.5 % of respective measuring range

< 1.0 % of respective measuring range

Linearity

< 1 % of respective measuring range


(specic to application)

< 2 % of respective measuring range


(specic to application)

Protection

all optical parts have an IP rating of IP65 or higher

Process Adaption
Material

Port connection
Port gasket
Insertion depth

wetted parts:
stainless steel 1.4435 (SS 316 L) dF < 1 %, BN2
surface: electro-polished Ra < 0.4 m
housing: stainless steel 1.4571 (SS 316 Ti)
thread G1-1/4 in., ISO 228/1
for port AS25 (similar Ingold-port)
diameter: 25 mm ( D= 25 H7)
O-ring groove for 30 mm and for 60 mm port length

wetted parts:
stainless steel 1.4435 (SS 316 L)
surface: electro-polished Ra < 0.8 m
housing: stainless steel 1.4571 (SS 316 Ti)

O-ring 18.64 x 3.53 mm EPDM (FDA / USP Class VI)


35 mm (1.38 in.) + OPL
at a port length of 60 mm (2.36 in.)
n/a

35 mm (1.38 in.) + OPL


at a port length of 60 mm (2.36 in.)
135 mm (5.31 in.) + OPL
at a port length of 60 mm (2.36 in.)

Process pressure

10 mbar to 20 bar (0.15 psi to 290 psi)

Windows

sapphire (seal-less)

Window gaskets

n/a

Installation accessories

weld-in ports, Varivent adapter (50.00), clamp adapter (1.5 and 2.0 in.)
optek T-pieces DIN 11850 (DN50 - DN100), optek T-pieces OD (BS4821-1) (2.0 - 4.0 in.)

10 mbar to 10 bar (0.15 psi to 145 psi)

Temperature Ratings
Process temperature

permanent:
peak 60 min/day:

Ambient temperature

operation:
transport:

0 - 100 C (32 - 212 F)


0 - 150 C (32 - 302 F)

permanent:
0 - 90 C (32 - 194 F)
peak 60 min/day: 0 - 100 C (32 - 212 F)

0 - 40 C (32 - 104 F)
-20 - 70 C ( -4 - 158 F)

Calibration
Calibration adapter

none

n/a

Calibration adapter OPTION VB

Filter adapter FH03


for calibration lter used for sensor verication

n/a

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

Installation accessories:

Tri-Clamp

Varivent

Weld-in port 15

Weld-in port 0

T-piece

www.optek.com

Measurement

www.optek.com

20 I Probe Sensors ASD12-N/ASD19-N/ASD25-N

Model ASD

1 OPL
3 Detector
5 LED light source
5

No window gaskets used

The ASD12-N, ASD19-N and ASD25N absorption sensors are designed


for use in pilot and production scale
fermenters or bioreactors to precisely
measure the growth of microbial or cell
cultures as a function of NIR absorption.

NIR-Absorption
A precisely dened and constant LED
light beam penetrates the process
medium. ASD12-N, ASD19-N and
ASD25-N use light from 840 nm to
910 nm (NIR). The attenuation of the
light intensity, caused by absorption by
dissolved substances and undissolved
material is detected by a hermetically
sealed photodiode.

ASD12-N
The ASD12-N probe is specically engineered for use in laboratory fermenters. The seal-less sapphire window
design eliminates crevices and gaps to
assure the highest level of sterility.
All wetted parts are electro-polished
steel. The ASD12-N is autoclavable and
mounts conveniently through any headplate with a PG13.5 threaded port.
The ASD12-N is available in three different insertion depths with either
5 or 10 mm OPLs (optical path length =
distance between the windows).
Shorter optical path lengths are typically used for dense cell cultures such
as bacterial and yeast cultures. Longer
OPLs are used for less dense cell

2 Sapphire windows
4 Daylight lter

cultures e.g. mammalian cells and dissolution / precipitation / crystallization


reactions.

ASD19-N
The ASD19-N, based on the same design as the ASD12-N with seal-less
window construction, is typically used
in larger fermenters or bioreactors.
Connection is through a standard
19 mm port (M26 x 1) in the fermenter
or bioreactor headplate. The ASD19-N
is available in three different insertion
depths and with OPLs of 1 mm, 5 mm,
10 mm or 20 mm.

Typical Applications:
Cell growth in mammalian cell cultures and bacterial fermentation
Algae concentration monitoring
Biomass concentrations
Crystallization process monitoring

See our TOP 5 brochures for


applications in your industry.

ASD25-N / ASD25-BT-N
Models ASD25-N and ASD25-BT-N
are designed for use in pilot or production scale fermenters or bioreactors.
These extremely durable probes are
designed for sanitary bioprocess environments and can be used in CIP/ SIP
processes.
The ASD25-N is conveniently mounted
through a standard 25 mm Ingold
type port and the ASD25-BT-N through
a standard 25 mm safety port.

optek ASD12-N
Single Channel Absorption Probes

Sapphire windows (seal-less)

Probe Sensors ASD12-N/ASD19-N/ASD25-N I 21


Technical Data

ASD12-N

ASD19-N

ASD25-N

ASD25-BT-N

1-Channel absorption of light

Detector

1-Silicon photodiode (hermetically sealed)

Measurement wavelength 840 nm - 910 nm


Measuring range
Optical path length

any measuring range between: 0 - 0,05 to 4 CU


5 or 10 mm others on

1, 5, 10 or 20 mm

request

Calibration

CU (concentration units) application specific calibration

Light source

Hybrid LED (hermetically sealed), 5.4 V DC, 100 mA, typical life span: approx 10 years
IP68

Protection

IP65

Process Adaption
Material

Port connection

Port gasket

Insertion depth

Process pressure

wetted parts:
stainless steel 1.4435 (SS 316L) dF < 1%, BN2
surface: electro-polished Ra < 0.4 m
housing: stainless steel 1.4571 (SS 316 Ti)
Fermenter head plates
diameter: 12 mm
thread: PG 13.5

Fermenter head plates


diameter: 19 mm
thread: M26 X 1

OSP25-GS60 (similar Ingold-port)


nominal length: 60 and 30 mm
diameter: 25 mm
thread: G1-1/4 in. ISO 228/1

O-ring 11.00 x 3.00 mm


EPDM (FDA / USP Class VI)

O-ring 15.60 x 1.78 mm


EPDM (FDA / USP Class VI)

O-ring 18.64 x 3.53 mm EPDM (FDA / USP ClassVI),


others on request

110 mm + OPL
215 mm + OPL
315 mm + OPL
others on request
pressure-free
(+/- 0.5 bar) (+/- 7.25 psi)

35 mm + OPL
140 mm + OPL
with port length 60 mm
210 mm + OPL
310 mm + OPL
others on request
10 mbar to 10 bar (0.15 psi to 145 psi)

35 mm + OPL
with port length 52 mm

weld-in ports

Windows

Sapphire (seal-less)
special adapters on request

Installation accessories

Adapter PG 13.5 Variable


depth
Adapter M 26 x 1 - PG 13.5

permanent:
5 - 50 C (41 - 122 F)

permanent:
5 - 65 C (41 - 149 F)
peak (60 min./day): 5 - 135 C (41 - 275 F)
thermal shutdown at approximately 75 C (167 F)

weld-in ports,
Varivent adapter (50.00),
clamp adapter,
optek T-pieces DIN 11850, optek
T-pieces OD (BS4821-1)

Temperature Ratings
Process temperature

Ambient temperature

operation: 0 - 40 C (32 - 104 F)


transport: -20 - 70 C (-4 158 F)

Sterilization conditions

Sterilization must be performed outside the process and


the ASD must be disconnected from the power source
(autoclaving possible without cable)
max. pressure: 4 bar (58 psi)
max. temperature: 135 C (275 F) (max. 60 min./day)

Autoclaving not possible

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

optek ASD19-N
Single Channel Absorption Probe
optek ASD25-N
Single Channel Absorption Probe

OSP25-GS52 (similar safety- port)


nominal length: 52 and 30 mm
diameter: 25 mm
thread: G1-1/4 in. ISO 228/1

www.optek.com

Measurement
Measurement principle

22 I Conductivity Sensor ACF60

Patented six-electrode design

www.optek.com

reduces sensitivity to fouling and polarization


Wide measuring range:
0 - 10 S/cm up to 0 - 850 mS/cm
Integrated Pt1000 temperature sensor
No O-rings or epoxy - suitable for CIP/SIP

Six-Electrodes
The ACF60 conductivity sensor features
a superior six-electrode, four-pole design. The patented arrangement of the
four current electrodes around the two
potential electrodes results in a reliable
and precise measurement. This unique
design also provides greatly reduced sensitivity to sensor fouling and
polarization. The combination of optek
C8000 universal converter and ACF60
conductivity sensors allow a wide dynamic range from 0 10 S/cm up to
0 850 mS/cm with the same sensor.

Temperature Measurement
The integrated Pt1000 platinum RTD
in the tip of the ACF60 sensor provides
fast-response temperature measurement for compensation, which can be
displayed and transmitted from the
C8000 converter.

Sanitary Design
Designed for ultra-sterility, the six electrodes are sealed in the FDA (USP class
VI) compliant PEEK sensor tip without
the use of O-rings or epoxy. Mounted in
an optek inline sensor body, the design
ensures smooth and unrestricted ow
of all process uids with minimized
hold-up and hydrostatic shear. The
ACF60 sensor is suitable for CIP/SIP
applications.

Typical Applications:
Chromatography process monitoring
Monitoring of CIP processes
Measuring ultrapure water
ACF60
Conductivity Sensor

Technical Data ACF60


Material

probe body: PEEK (FDA, USP class VI)

Electrodes

stainless steel 1.4435 (SS 316L), dF < 1%, BN2

Port-gaskets

O-ring: EPDM (FDA / USP Class VI), ... others on request

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

Process pressure

20 bar (290 psi) - 50 C (122 F)


10 bar (145 psi) - 100 C (212 F)
4 bar ( 58 psi) - 135 C (275 F)
Process temperature permanent:
-10 - 90 C (14 - 194 F)
peak 30 min/day: -10 - 135 C (14 - 275 F)
Ambient temperature operation: -10 C - 40 C (14 F - 104 F)
transport: -20 C - 70 C ( -4 F - 158 F)
Temperature sensor

integrated Pt1000 RTD (IEC Class A)


accuracy: 0.25 C at 25 C (77 F)

Protection

all parts have an IP rating of IP65 or higher

Measuring range

any measuring range between 0 - 10 S/cm to 850 mS/cm

Accuracy

Repeatability

0 - 10 S/cm

calibrated:
1 % of measuring value 0.2 S/cm
uncalibrated: 3 % of measuring value 0.2 S/cm

0.5 %

0 - 250 mS/cm

calibrated:
1 % of measuring value 0.2 S/cm
uncalibrated: 3 % of measuring value 0.2 S/cm

0.5 %

250 - 500 mS/cm

calibrated: 2 % of measuring value 0.2 S/cm


uncalibrated: 6 % of measuring value 0.2 S/cm

1%

500 - 850 mS/cm

calibrated: 5 % of measuring value 0.2 S/cm


uncalibrated: 12 % of measuring value 0.2 S/cm

3%

Pressure and temperature ratings specied herein may be subject to limitations - see instruction manual.
The appropriate choice of material for all wetted parts is the sole responsibility of the user.
Data given are subject to changes without prior notice.

pH Electrode Adapter PF12 I 23

12-degree electrode orientation provides

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improved performance

pH electrode solution ground allows


inline diagnostics

Designed to enhance ow and minimize hold-up volume


Suitable for most 12 x 120 mm pH-electrodes

12 Degree

Sanitary Design

The optek PF12 pH electrode adapter


is designed to mount pH electrodes at
the optimal angle of 12 degrees. This
allows the sensor to use electrolytelled glass electrodes and improves
the functionality and life span of the pH
electrodes. The PF12 electrode adapter
is compatible with a broad variety of pH
electrodes.

Mounted in an optek inline sensor


body, the design of the PF12 ensures
smooth and unrestricted ow of all
process uids. The PF12 meets sterility
requirements and is compatible with
CIP/SIP while minimizing hold-up volume and hydrostatic shear.

PF12
pH Electrode Holder

Solution Ground
The PF12 is equipped with a solution
ground (earth) connection mounted to
the sensor body. This allows the use of
pH electrodes that incorporate differential pH input techniques. Additionally,
the solution earth connection provides
a highly stable measurement while enabling sensor diagnostics including low
glass impedance, out-of sample, and
broken electrode/cable warnings.

PF12
ACF60

Technical Data PF12

pH and conductivity measurement


combined for low hold-up volume
Line Size

Volume

Volume

cond. only

pH + cond.

Material

Stainless steel 1.4435 (SS 316L), dF < 1 %, BN2

Surface

electro polished (Ra < 0.4 m)

0.25 in.

< 22 ml

< 41 ml

Solution ground

female SA483 for solution ground plug

0.50 in.

< 26 ml

< 44 ml

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

0.75 in.

< 34 ml

< 52 ml

Electrode types

suitable for wide variety of electrodes with dimensions


12 x 120 mm, PG 13.5 thread

1.00 in.

< 48 ml

< 65 ml

Process temperature

-10 C - 135 C (14 F - 275 F)

Process pressure

6 bar (87 psi)

Pressure and temperature ratings specied herein may be subject to limitations see instruction manual. The appropriate choice of material for all wetted parts is the sole
responsibility of the user. Data given are subject to changes without prior notice.

24 I Single Use Cell (S.U.C.)


Same performance as conventional systems

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Compatible with various optek sensors


Reduced risk of contamination
Four measurements in one Single Use Cell
Minimized hold-up volume
USP Class VI and FDA approval

The Single Use Cell (S.U.C.) is designed


to optimize separation, purication,
concentration and formulation processes in disposable chromatography and
ultraltration systems.
Cross-contamination between products
and batches will no longer be an issue
as gamma irradiated Single Use Cells
decrease the risk of contamination
to virtually zero.

S.U.C. Design
The S.U.C. is available in four different
designs. Two versions are primarily for
pre-column chromotography measurements (SUC 01/03) and two versions
for post-column measurements (SUC
05/07) with optical windows for
optek UV sensors.
Each S.U.C. is clearly labeled with data
specic to that particular cell. This data
includes the sensorr constant of the
conductivity sensor, as well as the UV
OPL (optical path length)
ngth) adaptation
data (for SUC 05/07).
7).

S.U.C. Holder

S.U.C. (Single Use Cells)

Integral parts of the S.U.C. system


include the holder and locking
mechanism guaranteeing proper installation. To enable easy and fast installation into the process instrumentation,
the S.U.C. holder comes equipped with
the conductivity sensor ACF60-SU-35.

The versatile design of the optek


S.U.C. has been developed to meet
the specic demands of biopharmaceutical manufacturing (see tables on
page 25 for details).
With low hold-up volumes and easy
installation they are fully compatible
with the optek range of UV, NIR and
color absorption sensors.

S.U.C. pH Adapter
SUC 03 and SUC 07 are equipped with
the pH adapter, which is compatible
with a broad variety of standard pH
electrodes (12 mm x 120 mm).
When no pH adapter is required (for
SUC 01 and SUC 05) a plug is used
to cover the pH input. This pH plug
has the same dimensions as the pH
electrode, keeping the hold-up
volume minimal.

The Single Use Cells are


manufactured in a clean room
facility and are gamma irradiation
ready
Simple fast exchange of the S.U.C.
eliminates the need for system
cleaning and validation
Improved productivity due to
simpler exchange procedures and
low down time between products/
batches

8 Measurements
5 Sensors
2 Single Use Cells
1 Converter

Technical Data

S.U.C. Holder Including ACF60-SU-35

Material (non wetted)

SS 316 L

Measuring range
Temperature compensation
of conductivity sensor
Protection
Cleanability

Technical Data

0 S/cm to 150 mS/cm


Accuracy: 2 % of measuring value 0.4 S/cm (dependent on ambient and process temperature being equal)
Accuracy 0.8 % of measuring value at temperature conditions (T ambient - T process) 20 C ( 68 F)
IP65
Cleaning with standard cleaning agents (alcoholic surface disinfectants, quaternary ammonium compounds) is permitted.
Caution! Ensure that windows are clean and dry and the contact unit for the electrodes is dry before starting measurement.

Single Use Cell (S.U.C.)


Windows (SUC 05, SUC 07): Quartz, UV transparent
Gasket: EPDM (FDA, USP class VI)
Conductivity electrode pins: stainless steel 1.4435 (SS 316L), dF < 1%, BN2
Sensor body: Polyphenylsulfone (PPSU)

Material (wetted)
The plastic and elastomeric wetted parts of the sensor have passed the bio-reactivity tests according to USP <87> and <88> class
VI and comply with FDA Regulations 21 CFR 177.2600. All wetted parts are of non-animal origin and any materials of animal origin
or containing animal substances are not used during manufacture. All wetted parts are of bovine-free origin and any materials of
bovine origin or containing TSE have not been used during manufacture.
Material (non wetted)

Adhesive: Epoxy LOCTITE M-31CL

Surface (wetted parts)

Ra < 0.8 m

Process connection
Line Size
OPL (SUC 05, SUC 07)

Hose barb
1/4 in., 3/8 in., 1/2 in., 5/8 in., ... others on request
1 mm, 2.5 mm, 10 mm, others on request

Shelf life

30 months after manufactoring date with adequate storage climatic conditions

Permitted gamma irradiation

typical 25 - 40 kGy (tested to 50 kGy)

Process pressure

0 - 6 bar (0 - 87 psi) May be reduced in combination with pH probe. Refer to corresponding instruction manual for specications of
pH probe.

Process temperature

2 - 50 C (35.6 - 122 F) May be reduced in combination with pH probe. Refer to corresponding instruction manual for specications of pH probe.

Ambient conditions

Temperature during operation: 2 - 30 C (35.6 - 86 F)


Relative humidity 80 % for temperature up to 31 C (87 F)

Temperature and Pressure Ratings

Data given are subject to changes without prior notice.

Available Models
S.U.C. Types Conductivity pH UV
SUC 01

SUC 03

SUC 05

SUC 07

Hold-up Volume

20 ml

20 ml

Example

(OPL 1 mm): 22 ml
(OPL 2.5 mm): 23 ml
(OPL 10 mm): 25 ml
(OPL 1 mm): 22 ml
(OPL 2.5 mm): 23 ml
(OPL 10 mm): 25 ml

Fully assembled SUC 07


for measuring conductivity, pH, UV and temperature

www.optek.com

Single Use Cell (S.U.C.) I 25

www.optek.com

26 I Sensor Body (Armature)

15

14

13

12

11

Example Exploded View - Model AF26:


1
2
3
4
5
6
7
8
9
10
11
12
13
14
15

Sensor body in. to 6 in. (DN 6 to DN 150)


O-rings (EPDM, Viton, Kalrez etc.)
Windows (Sapphire, Pyrex)
Window ring M24 (1.4571 / 316 Ti)
8 Screws (M5 x 12) with lock washer
O-ring (Viton)
Detector module AF26
O-ring (EPDM, Viton, Kalrez etc.)
SS-plug protection (1.4571 / 316 Ti)
4 Screws (M3 x 6)
Optics module AF26
O-ring 31,47 x 1,78 mm
Optical housing OP06 (1.4571 / 316 Ti)
Lamp module AF26
4 Screws (M3 x 6)

Sensor Body
For Variations and Details see Separate Sensor Body Datasheet
Material

Stainless steel 1.4435 (SS 316L), 1.4539, 1.4571 (SS 316Ti), 1.4462,
Titanium 3.7035 (Grade 2), Hastelloy 2.4602 (C22), Plastic TFM4215,
PVC, ... others on request

Line size

1/4 in. to 6 in. (DN 6 to DN 150), ... others on request

Process connection

Flanges (ASME, DIN, JIS), Clamps (TC, ISO, DIN), Female Threads (NPT,
DIN), Sanitary Threads (DIN 11851), Tube Ends (DIN, ISO, OD), Varivent,
... others on request

Process pressure
Windows
Window gaskets

10 mbar to 100 bar (0.15 psi to 1450 psi) - higher on request


depending on process connection, materials and design
1-Pyrex, 2-Sapphire, 3-Sapphire Biotech
Silicone (FDA), Viton (FDA), EPDM (FDA / USP Class VI), Kalrez 4079,
... others on request

Windows available in different lengths for OPL


(optical path length) adjustment

10

www.optek.com

System Calibration I 27

optek calibration accessories are


specically designed for nonintrusive
calibration and verication of optek
systems.

UV Sensors
Three series of solid lters are available to ensure condence in measurements. The UV-L lter series is used
to calibrate photometric accuracy and
linearity. The UV-B lter series veries
integral blocking and the UV-S lter
series tests for long-term stability of the
sensor.

VIS/NIR Sensors
A special series of solid lters is
available for each wavelength (range)
to ensure best measurement performance. The calibration lters are used
to calibrate photometric accuracy and
linearity.

NIST-Traceable
All optek lters ship with NIST-traceable
(National Institute of Standards and
Technology) certication. The optek
laboratory is equipped with a high quality, NIST-traceable spectrophotometer
to assure quality and quick turnaround
time for recertication of lters.

Concept
Advantages of optek calibration concept include:
- Only 1 lter (set) for multiple sensors
ensures identical calibration
- Only the lter needs to be sent back
for recertication, while the sensor
remains operating
Calibration Filters UV-L
Nominal absorption:
0.45, 0.9, 1.8 and 2.4 CU
Calibration Filter UV-B
Nominal absorption:
> 3 CU
Calibration Filters UV-S
Nominal absorption:
Application specic
Calibration Filters VIS-L
Nominal absorption:
0.45, 0.9 and 1.8 CU
Calibration Filters NIR-L
Nominal absorption:
0.45, 0.9 and 1.8 CU

Calibration Case
Holds up to 7 calibration lters
Calibration Cuvette
The unique calibration cuvette,
FH03, enables product calibration
without need to interfere with the
process line.
The cuvette allows users to create a
correlation of absorption signals to
the concentration of product or an
equivalent substance, creating an
easy link from lab to process.

Calibration cuvette FH03

inline control

Germany

optek-Danulat GmbH
Emscherbruchallee 2
45356 Essen / Germany
Phone: +49 201 63409 0
Fax: +49 201 63409 999
E-Mail: info@optek.de

USA

optek-Danulat Inc.
N118 W18748 Bunsen Drive
Germantown WI 53022 / USA
Phone: +1 262 437 3600
Toll free call: +1 800 371 4288
Fax: +1 262 437 3699
E-Mail: info@optek.com

Singapore

China

optek D
optek-Danulat
Shanghai Co., Ltd.
Room 718 Building 1
No.88 Keyuan Road
Pudong Zhangjiang
Shanghai, China 201203
Phone: +86 21 2898 6326
Fax: +86 21 2898 6325
E-Mail: info@optek-danulat.cn






E-Mail: info@optek-danulat.cn

optek-Danulat Pte. Ltd.


25 Intl Business Park
#02-09 German Centre
Singapore 609916
Phone: +65 6562 8292
Fax: +65 6562 8293
E-Mail: info@optek.com.sg

Please visit our website for contact details of our local distributors in other countries.

www.optek.com

1005-1001-02

Ver. 2.1 (US)

28 I Contact

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