T.Y. B.tech Chemical Technology
T.Y. B.tech Chemical Technology
T.Y. B.tech Chemical Technology
f 2013-14
Semester – V
Note : Tutorials and Practical shall be conducted in batches with batch strength not exceeding 18 students.
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Semester – VI
Note: Tutorials and Practical shall be conducted in batches with batch strength not exceeding 18 students.
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Unit II 08Hours
Steam and Boilers : Steam generation and its application in chemical process plants,
distribution and utilization, design of efficient steam heating systems, steam economy,
condensate utilization, steam traps, their characteristics, selection and application, waste
heat utilization. Classification of Boilers: Fire tube and water tube boilers Tube shape and
position, firing, Head Sources, Fuel, Fluid, circulation, furnace position, furnace type,
General Shape, Boiler mountings and accessories, Boiler draught.
Unit VI 06Hours
Inert gases: Introduction, properties of inert gases and their use, sources and
methods of generation, comparison of nitro generation routes, general arrangement for inert
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
REFERENCES:
1. Jack Broughton, Process utility systems, Institution of Chemical Engineers U.K.
2. Reid, Prausnitz poling, The properties of gases and liquids, IV edition, McGraw-Hill
International edition.
3. S.C.Arora & S.Domkumdwar, A course in refrigeration and air conditioning, Dhanpat
Rai and Co.(P) Ltd.
4. R.L.Ballaney, Thermal Engineering, Khanna Publication
5. Gupta and Prakash, Engineering Thermodynamics, Nemchand and Brothers, Roorkee
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Unit I 10Hours
Fuels, fuel gases and Industrial gases : Introduction to Chemical Manufacturing
and Processing sector. Study of the role of Chemical Engineers and Technologists in the
development of the nation. Study of the manufacture: water gas, producer gas, natural gas,
LPG, hydrogen, oxygen, nitrogen, carbon dioxide and acetylene. Concept, types and
applications of fuel cells
Unit II 06Hours
Ceramic industries: Basic raw materials, Chemical Conversions, White wares,
Structural clay products, Manufacture of refractory, Glass raw materials, Manufacture, types
and applications of glass.
Unit III 07Hours
Salt and sodium compounds, Chlor-alkali and electrolytic industries:
Manufacture of sodium chloride, sodium sulphate and byproducts. Manufacture of Soda ash,
caustic soda, chlorine, bleaching powder, sodium bicarbonate, aluminum, Sodium, chlorates
and per chlorates.
Unit IV 06Hours
Hydrochloric acid and Sulfur industries: Manufacture of hydrochloric acid,
aluminum sulphate and alums. Manufacture of sulfur and sulfuric acid.
Unit V 06Hours
Phosphate industries and Potassium industries: Study of elemental
phosphorous, raw materials and processes for phosphoric acid manufacture, Manufacture of
ammonium phosphate, baking powder. Manufacture of potassium, potassium chloride,
potassium sulphate and potassium nitrate.
Unit VI 06Hours
Nitrogen industries: Manufacture of synthetic ammonia, nitric acid, ammonium
nitrate, urea.
(Note: Subject to be taught with reference to Chemical Engineering principles involved in
each of the topic.)
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
TEXT BOOKS:
1. George T. Austin, “Shreve's Chemical Process Industries”, 5th edition. , McGraw Hill
Book Company, 1985.
REFERENCES:
1. S.D. Shukla, G.N. Pandey, “A Text book of Chemical Technology”, 3rd Edition
2. C.E. Dryden, “Outlines of Chemical Technology”, Affiliated East-West Press, 1973.
3. D.Venkteshwaralu, “Chemical Technology”, I & III manuals of Chemical Technology,
Chemical Engineering. Ed. Dev. III Madras, 1977.
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Unit I 11Hours
Economic problem and National income: Law of demand, equilibrium between
demand and supply, concepts of costs, cost curves and revenue curves of a firm, equilibrium
of a firm under perfect competition, break-even analysis, and break-even point.
Concept of national income, estimation of national income, difficulties in measurement of
national income, uses of national income figures.
Unit II 04Hours
Inflation: Meaning, types of inflation, causes, effects, control of inflation, value of
money, index numbers, construction, utility, limitations, business cycles, phases of business
cycles.
Unit III 05Hours
Industrialization: Need, capital requirement block and working, raising finance,
cottage and small scale industries, role in the Indian economy, problems of small scale
industries, remedies.
Unit IV 07Hours
Principles of management: Definition, nature, levels of management, functions of
management.
i. Planning: Nature, importance, types of plans, planning process, decision making.
ii. Organization: Principles of organization, organizational structure.
iii. Directing: Theories of motivation, communication, process and barriers, leadership
styles.
iv. Controlling: Control techniques.
Unit V 05Hours
Production management: Selection of site, plant layout, its type, functions of
P.P.C. Materials management, purchase, inventory control, production and quality control.
Unit VI 08Hours
Finance management and Marketing management: Scope and importance, capital
structure planning, working capital management, sources of funds, financial industries of
India. Marketing concepts, physical distribution, advertising and sales promotion, marketing
research, sales management.
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Shivaji University Syllabus w.e.f 2013-14
REFERENCES:
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
with stepwise columns, design concepts, determination of height and diameter of packed
absorption column. Study of cooling towers.
REFERENCE BOOKS:
1) R.E.Treybal , Mass transfer operation ,McGraw Hill Publication
2) Coulson & Richardson, Chemical Engineering (Vol. I and II), Pergamon Press
3) W.L.McCabe & J.C.Smith, .Unit Operation in Chemical Engineering. McGraw Hill
Publication
4) Christie J.Geankoplis ,Transport Processes & Unit Operations ,Prentice Hall inc
5) P. Chattopadhayay, Unit operation in Chemical Engineering. (Vol. I and II), Khanna
Publications Delhi
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Shivaji University Syllabus w.e.f 2013-14
Unit I 07Hours
Measuring Instruments: Theories, practice and applications of measurements of
temperature, mass and levels. Measurement of pressure, vacuum, humidity and pH in
process industry.
Unit II 05Hours
Flow measuring instruments: Flow measuring devices for incompressible and
compressible fluids. Electro-hydraulic valves, hydraulic servomotors, electro-pneumatic
valves. Pneumatic actuators.
UnitVI 07Hours
Frequency response analysis of linear processes: Bode’s diagram, Nyquist plots.
Design of feedback control system using frequency response technique: Bode’s stability
criteria, gain and phase margin. Ziegler- Nichols tuning technique. Nyquist stability criteria,
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Shivaji University Syllabus w.e.f 2013-14
Control Systems with Multiple Loops, Feed forward control, Cascade control, Ratio control,
selective control, split range control, Adaptive and Inferential control. Multi Variable
Control
REFERENCES:
1) Eckman, Industrial Instrumentation; Wiley Eastern
2) Erwing, Instrumental Methods of Chemical Analysis; McGraw Hill.
3) W.Bottom, Instrumentation & Process Measurements; Orient Longman.
4) George Stephanopoulos, Chemical Process Control, Prentice Hall of India.
5) D.R. Coughnour, Process System Analysis and Control, McGraw-Hill.
6) R.P.Vyas, Process Control & Instrumentation, 2nd edition, Central Techno publication,
Nagpur
7) K. Krishnaswamy, Process Control, New age International.
8) Peter Harriott, “Process Control”, Tata McGraw Hill, New Delhi, 1977.
9) Coulson and Richardson, “Chemical Engineering” Volume – III, Second
Edition, Pergmon Press, (UK), 1985.
10) Stephanopoulos G., “Chemical process control and introduction to theory and practice”
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Shivaji University Syllabus w.e.f 2013-14
Unit I 03Hours
Measurement systems and measuring instruments: Measurements, Types and
sources of errors, voltmeter, Ammeter, Wattmeter, Multimeter, CRO basic principle, CRT,
Horizontal and vertical deflection systems. Signal generators, Function generators
Unit II 03Hours
Study of power supply and voltage regulators: Half and Full wave rectifiers,
Bridge Rectifier, Fixed voltage regulators 78XX, 79XX series, Variable regulator LM317,
SMPS Basics.
Unit III 03Hours
Analog and digital electronics: Analog signals, Digital signals, Analog to Digital
conversion techniques, Digital to analog conversion techniques, ADC and DAC chips, Pulse
counters.
Unit IV 02Hours
Transducers and measurements: Transducers and their selection, Different types
of transducers, strain gauges,RTD,Thermister,Thermocouple,PT100 ,Bellows, bourdon
tubes, LVDT, humidity transducers, flow rate, liquid level measurements, pH value
measurement.
Unit V 02Hours
Indicating and recording devices: LED, LCD, Nixie, Plasma display, recorders
i.e. strips charts and X-Y recorder, seven segments displays with drivers.
Unit VI 02Hours
Microcontrollers: Basics of microcontrollers, Microcontroller based pH
measurement system, Data acquisition system, Temperature indicator, Process controllers.
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Shivaji University Syllabus w.e.f 2013-14
TEXT BOOKS:
1. Allen Mottershed, Electronic devices and circuits, PHI
2. H .S. Kalsi , Electronic Instrumentation’, 2nd edition, Tata McGraw Hill Publication
3. A. D. Helfrick, W. D. Cooper, Modern Electronic Instrumentation and Measurement
Techniques, Pearson Education
REFERENCE BOOK:
1. A.K.Sawhney ‘A Course in Electrical & Electronics Measurement & Instrumentation.’ –
11th Edition, 1996 --Dhanpat Rai & son
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
1) Diffusion in Still Air: To estimate mass transfer coefficient for given system at room
temperature.
2) Liquid-Liquid Diffusion: To determine diffusion coefficient for given system as function
of concentration.
3) Solid-Liquid Diffusion: To determine mass transfer coefficient for dissolution of benzoic
acid without chemical reaction.
4) Simple Distillation: To verify Rayleigh’s equation for simple distillation
5) Ternary Diagram: To construct ternary diagram for acetic acid –water – benzene
6) Liquid-Liquid Extraction: To study and determine the efficiency of cross current liquid-
liquid extraction.
7) Wetted Wall Column: To determine mass transfer coefficient for air – water system.
8) Absorption in Packed Column: To find mass transfer coefficient of given system.
9) Cooling Tower: To determine volumetric mass transfer coefficient for air – water system.
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
Practical Work will consist of minimum eight experiments from list given below.
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Shivaji University
Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
1) Study of Electronic Components and characteristics.
2) Study of CRO for waveform measurements.
3) Study of electronics measuring instruments.
4) Study of temperature transducers.
5) Study of HWR with and without filter.
6) Study of FWR with and without filter.
7) Study of bridge rectifier with and without filter.
8) Study of ADC 0809 IC.
9) Study of pressure measurement.
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Shivaji University Syllabus w.e.f 2013-14
CH317 SEMINAR
The students shall deliver minimum three seminars (each of 15 to 20 minutes) and submit
the seminar reports on different technical subjects during the semester. The assessment of
the term-work shall be based on the: -
1. Attendance to the seminar
2. Performance of the seminar delivery
3. Seminar reports and
4. Asking and answering questions during the seminars.
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Shivaji University Syllabus w.e.f 2013-14
Evaluation Scheme: The course auditor will evaluate the students for their performance in
the course and the students will be given the grade by the teacher.The grade will be based on
total marks obtained out of 50.
Unit I 05Hours
Communication in a Business Organization: Internal (Upward, Downward,
Horizontal, Grapevine, Problems, Solutions) External Communication, Strategies for
conducting successful business meetings, documentation (notice, agenda minutes) of
meetings. Introduction to modern communication techniques (for e.g. e-mail, internet, video
conferencing etc), Legal & ethical issues in communication (intellectual property rights,
patents)
Unit II 05Hours
Advanced Technical Writing: a. Report – Writing and presentation: Definition and
importance of reports. Qualities of Reports, language and style in reports, type of reports,
formats (letter, memo, and project- reports), and methods of compiling data using computer-
aids
b. Technical Paper Writing
c. Writing Proposals
Unit III 05Hours
Interpersonal Skills: Introduction to emotional intelligence, Motivation,
Negotiation and conflict-resolution Assertiveness, Leadership, Term-building, Decision-
making, And Time-management.
Unit IV 05Hours
Interview Techniques: Preparing for job interviews, verbal and non-verbal
communication during interview. Observation sessions and role-play techniques may be
used to demonstrate interview strategies.
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Shivaji University Syllabus w.e.f 2013-14
Unit V 05Hours
Group Discussion: Dynamics of Group Behavior, Techniques for effective
participation.
ASSIGNMENTS:
a) Written
Assignments on Communication topics (minimum 2)
Assignments on Report writing (minimum 3)
Assignments on Interpersonal Skills (minimum 3)
b) One class test
c) Oral: Practical sessions on Group-discussion / Interview Skills / Project Presentation /
Power point Presentation.
Break up of Marks
a) Assignments Written: 20 marks b) Test: 10 marks c) Performance in GD and PI: 20 marks
Total 50 marks
Books Recommended:
A. For classroom teaching
1. Fred Luthans, ‘Organizational Behavior’ McGraw Hill International Edition
2. Lesiker and Petit ‘Report writing For Business’ McGraw Hill International Edition
3. Huckin and Olsen ‘Technical Writing and Professional Communication’ McGraw Hill
International Edition
4. Wallace and Masters ‘Personal Development for life and Work’, Thomson Learning
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
4. Vikas Gupta: Comdex Computer Course Kit, IDG Books Pvt, Ltd.
5. Heller & Handle: The Essential Manager’s Manual – Dorleen Kindercey
6. The Sunday Times ‘Creating Success Series’
1. Develop your Assertiveness.
2. Make every Minute Count.
3. Successful Presentation Skills.
4. How to motivate people.
5. Team building.
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Note: There will be an industrial tour for 3days. The students will prepare a brief report of
the industry visits during the tour.
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Shivaji University Syllabus w.e.f 2013-14
Unit I 05Hours
Introduction to the Subject: Chemical Kinetics and thermodynamics of reaction;
Classification of reactions - Homogeneous and Heterogeneous reactions. Rate of reaction,
broad definition for homogeneous and heterogeneous reactions.
Unit II 07Hours
Kinetics of homogeneous reactions: Irreversible and reversible reactions,
Equilibrium; Order and molecularity of reaction. Elementary and non elementary reactions;
Stoichiometry, fractional conversion. Rate of reaction based on all components of the
reaction and their interrelation. Law of mass action, Rate Constant-Based on thermodynamic
activity, partial pressure, mole fraction and concentration of the reaction components and
their interrelation, Temperature dependency of rate Constant -Arrhenius law, Transition
state theory and collision theory.
Unit IV 08Hours
Ideal flow reactors: Concept of ideality. Types of flow reactors and their
differences, Space-time and Space velocity. Design equation for plug flow reactor and
CSTR; Design equations for first and second order reversible and irreversible constant
volume and variable volume reactor, Graphical interpretation of these equations; Mean
holding time; Development of rate expression for mean holding time for a plug flow reactor.
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Shivaji University Syllabus w.e.f 2013-14
Unit V 07Hours
Single and multiple reactor system: Size comparison of single reactors;
Optimum size determination; Staging of reactors, Reactors in series and parallel;
Performance of infinite number of back mix reactors in series, Back mix and plug flow
reactors of different sizes in series and their optimum way of staging; Recycle reactors,
Optimum recycle ratio for auto-catalytic (recycle) reactors.
Unit VI 07Hours
Design for multiple reactions: Yield and selectivity, Parallel reactions
Requirements for high yield, best operating condition for mixed and plug flow reactors,
Series reactions Maximization of desired product rate in a plug flow reactor and back mixed
reactor.
REFERENCES:
1. Octave Levenspeil, “Chemical Reaction Engineering”, 2nd Edition, John Wiley, London.
2. S. M. Walas, “Reaction Kinetics for Chemical Engineers”, McGraw Hill, New York
3. J. M. Smith, “Chemical Engineering Kinetics”, McGraw Hill, New York.
4. J. Rajaram and J. C. Kuriacose, “Kinetics and Mechanics of Chemical Transformation”,
McMillan India Ltd., 1993.
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Shivaji University Syllabus w.e.f 2013-14
Unit I 06Hours
Food Industries: Types of food processing, preservation method, Food Products.
Sugar and Starch Industries: sugar and starches. Fermentation Industries: Absolute alcohol,
Beer, Wines and liquors, vinegar, citric acid, galactic acid.
Unit II 06Hours
Oil, Fat and Waxes: Manufacture of Vegetable oils, animal Fats and oils, Waxes,
Soaps and detergents,
Unit IV 06Hours
Pulp and paper industries: Manufacturing of pulp, manufacturing of paper, and
structural boards.
Unit V 07Hours
Explosives, Plastic industries: Types of Explosives, Explosive characteristics,
Industrial explosives, propellants, rockets, Missiles, pyrotechnics, matches, toxic chemical
weapons. Raw Materials, general polymerization processes, manufacturing processes,
Compounding and Moulding operation.
Unit VI 08Hours
Petroleum and Petrochemicals, Dyes and their intermediates: Petroleum
production and Refining, Manufacturing of Methanol, Formaldehyde, Ethylene and
Acetylene, Ethylene dioxide, Isopropanol, Acetone, Isopropyl, Benzene, Butadiene, Phenol
styrene. Classification and manufacturing of dyes and their intermediates.
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Shivaji University Syllabus w.e.f 2013-14
REFERENCES:
th
1) George T. Austin, “Shreve’s Chemical Process Industries”, 5 Edition, McGraw Hill
Book Company.
2) C.E. Dryden, Outline of Chemical Technology, Affiliated East WestPress.1973.
rd
3) S.D.Shukla, G.N.Pandey, A text book of Chemical technology, 3 Edition.
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Shivaji University Syllabus w.e.f 2013-14
Unit I 06Hours
Introduction: Types of Pollution. Introduction to Pollution control aspects.
Environmental Legislation: Water (Prevention and Control of Pollution) Act, 197, Air
(Prevention and control of Pollution) Act, 1981. Industrial Waste Water Analysis. Industrial
Gaseous Effluent Analysis. General Instrument for Gaseous Pollutants.
Unit II 05Hours
Removal of BOD: Introduction to removal of BOD Biological oxidation Units:
Activated Sludge Process; Trickling /Biological Filters; Waste Stabilization Ponds.
Anaerobic Treatment. Numerical Examples based on removal of BOD. Removal of
Chromium.
Unit III 07Hours
Removal of Heavy Metals: Introduction to removal of Chromium. Control
Methods, Reduction precipitation, Ion Exchange, Reverse Osmosis, Lime coagulation and
adsorption. Introduction of removal of mercury, Measurement of Mercury, Ventron mercury
removal process. Removal of ammonia/urea: Introduction to removal of ammonia/urea,
Methods for removal of nitrogen, Physico-chemical processes, Biological methods.
Unit IV 05Hours
Treatment of Phenolic Effluents: Introduction to Treatments of Phenolic Effluents,
Sources of phenols. Treatments/Removal Methods: Steam Gas Stripping. Adsorption/Ion
Exchange; Extraction of phenols using Phenosolvants Biological Methods of Treatment.
Removal of particulate matter: Introduction to removal of particulate matter, Gravity settling
chamber, solid traps, cyclone separators, fibre filters, fabric filters, liquid scrubbers and
ESP. Numerical Examples based on settling chamber, cyclone separators, fiber filter, liquids
scrubber and ESP.
Shivaji University
Shivaji University Syllabus w.e.f 2013-14
REFERENCES:
1. S. P. Mahajan, “Pollution Control in Process Industries”, Tata McGraw hill, 1985.
2. Metcalf and Eddy, “Waste Water Engineering Treatment”, Tata McGraw Hill, 1979.
3. Warren Riesman and Mark J. Hammer, “Water supply and Pollution control”, Harper &
Row, New York, 1985.
4. M.V. Rao and A. K. Datta : “Waste Water Treatment”.
5. U. N. Mahida, “Water Pollution and disposal of Waste Water on land”.
6. Soli Arceivala, “Waste Water Treatment for Pollution Control”.
7. Lund H. F,”Industrial Pollution Control”, Hand Book, McGraw Hill, 1971.
8. H. C. Perkins, “Air Pollution”, McGraw Hill 1974.
9. L. D. Benfield and C. W. Randall, “Biological Process Design for Waste Water
Treatment”, Prentice Hall, 1980.
10. C. P. Gaudy Jr. and H. C. Lim “Bio-logical Waste Water Treatment”, 1980.
11. M. J. Hammer, “Water & waste water Technology”, Wiley, 1975.
12. Artur L. Kohi and Fred C. Reisenfled, “Gas Purification”, Gulf Publishing Co.1979.
13. Arcadio P. Sincero, Gregoria A. Sincero, “Environmental engineering” (Design
approach), Prentice Hall of India Pvt. Ltd, New Delhi, 1999
14. C. S. Rao “Environmental pollution control engineering” Wiley Eastern Ltd, 1994.
15. David H. F. Liu, Bela Liptak, “Environmental engineers’ handbook”, Lewis
Publishers, 2nd edition, New Jersey, 1996
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Shivaji University Syllabus w.e.f 2013-14
Unit I 07Hours
Drying: Principles of drying, phase equilibrium, cross circulation drying, through
circulation drying, drying of suspended particles, rate of drying curve, dryers for solids and
pastes, dryers for solutions and slurries i.e. various types of dryers
Unit II 08Hours
Humidification: Terms, definitions, wet bulb temp., dry bulb temp. And measurement
of humidity, adiabatic saturation temp., study of temp humidity chart, Enthalpy-humidity
charts, Determination of humidity, and concept of dehumidification. Equipments for
humidification operations.
Unit IV 07Hours
Adsorption: Adsorption equilibria, types of adsorption, properties of adsorbents,
single and multi-stage adsorption, adsorption isotherms, principles of adsorption, break
through curves, Adsorption of liquids, Basic equations, and Adsorber design. Adsorption
equipments. Ion Exchange: Principles of ion exchange, Techniques and applications, Ion
exchange equilibria, Rate of ion exchange.
Unit V 07Hours
Evaporation: Principles of evaporation, applications of evaporation, liquid
characteristics and types of evaporator, single effect evaporator calculation, pattern of liquor
flow in multiple effect evaporators.
Unit VI 07Hours
Membrane Separation Operations: Introduction to membrane separation process,
Different Types of membrane separation process, (Ultra filtration, Reverse Osmosis,
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Shivaji University Syllabus w.e.f 2013-14
.REFERENCES:
1) Coulson and Richardson, Chemical Engineering (Vol. II), Pergamon Press
2) RE. Tryebal, Mass Transfer Operation, McGraw hill.
3) Christie J. Geankoplis, Transport Processes and Unit Operations, Prentice Hall Inc
4) P. Chattopadhyay, Unit operations in Chemical Engineering. Vol. I and II, Khanna
Publication, New Delhi
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Shivaji University Syllabus w.e.f 2013-14
Unit I 08Hours
Design Considerations and Keys: Design codes, Maximum working pressure,
Design pressure, Design Temperature, Design stress, Factors of safety, Selection of factor of
safety, Design wall thickness, Corrosion ratio, Poisson ratio, Criteria of failure, Elastic
stability. Materials of construction: Mechanical properties, Materials, Corrosion, Protective
coating, Corrosion prevention, Choice of materials, Introduction, Types of keys, Strength of
sunk key, Effect of key ways, Design of keys, Design of Heads: Introduction, Analysis and
design of conical head, Flat cover head, Standard dished heads. Gaskets and Flanges:
Introduction, Types of Gaskets and Flanges. Pipe joints: Standard pipe flanges for steam,
Hydraulic pipe joints for high pressure, Design of circular flange pipe joints. Welded Joints,
Riveted joints
Unit II 04Hours
Storage vessels: Introduction, Design fixed conical roof cylindrical tank, Storage of
gases in Spherical vessels Supports for vessels: Introduction, Bracket or Lug supports, Leg
Supports, Skirt Supports
Unit IV 06Hours
Process Design of Heat Exchanger: Introduction, Types of Heat Exchanger,
Process Design of Shell and Tube Heat Exchanger. Process Design of Evaporator:
Introduction, Types of Evaporators, Methods of Feeding of Evaporators, Design of
Evaporator.
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Shivaji University Syllabus w.e.f 2013-14
Unit V 06Hours
Process Design of Reaction Vessels: Introduction, Materials of Construction,
Agitation, Classification of Reaction Vessels, Heating Systems, Design of Reaction Vessels.
Crystallizer Design: Introduction, Types of Crystallizers, Design of crystallizers. Process
Design of Rotary Dryer: Introduction, Types Dryers, Design of Rotary Dryer.
Unit VI 10Hours
Design of Tall Vessels and Design for Distillation Column and Agitator :
Introduction, the Axial Stresses Due to Dead Loads, the Axial Stresses Due to Pressure,
Longitudinal Bending Stresses due to Dynamic Loads, Design Of Distillation (Tall)
Column (Tower). Design of Sieve Tray for Distillation Column, Design of Thick Walled
High Pressure Vessel, Design of Bubble Cap Tray For Distillation Operation, Agitators :
Introduction, Types Of Agitators, Baffling, Power Requirements, Design Of Turbine
Agitator.
REFERENCES:
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
1. Determine activation energy of acid catalyzed hydrolysis of methyl acetate.
2. To study effect of concentration of reactant and temperature on the rate of reaction.
3. Determination of specific reaction rate of acid catalyzed hydrolysis of ethyl acetate
4. Determination of specific reaction rate of acid catalyzed hydrolysis of ethyl acetate
by sodium hydroxide at 298 K
5. To study the reaction between potassium persulphate and iodide
6. Kinetics of hydrolysis of methyl acetate by strong acid.
7. To study acid- catalyzed iodination of acetone.
8. To study saponification of ethyl acetate.
9. Study of Isothermal continuous stirred tank reactor
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
1) Natural Drying (Batch): To obtain drying curve for batch drying operation.
2)Fluidized Bed Dryer: To determine the rate of drying and to obtain mass transfer
coefficient for the given material.
3) Study of industrial driers
4) Study of industrial humidification systems
4) Study of Crystallization Equipments
5) Adsorption: To study adsorption of acidic acid on activated charcoal
6) Study of Ion Exchange adsorption
7) Study of Evaporation systems.
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Shivaji University Syllabus w.e.f 2013-14
LABORATORY PRACTICALS:
1) Standard equipment symbols , Standard instrumentation symbols
2) Pipe fittings , flanges and gaskets, Heads and closures
3) Keys and couplings , Riveted joints , Welded joints
4) Pressure relief devices
5) Supports for vessels-Bracket Support ,Leg Support, Skirt Support.
6) Design and drawing of packed absorption tower
7) Design of heat exchangers.
8) Design of tall vertical vessels, Design of reaction vessel.
9) Design of evaporator.
10) Design of agitation system.
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Shivaji University Syllabus w.e.f 2013-14
The purpose of this particular exercise is to promote self-study, critical thinking and
independent research ability. Students have to initiate their own small conceptual or
practical based projects individually or as a team of no more than 2 members. While making
this exercise it is expected that the knowledge acquired by them through Research
Methodology subject is applied by them
Carrying out mini project work will certainly help the students to satisfactorily
complete their major project in the final year.
The students will deliver a seminar and will make the demonstration of their work.
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Shivaji University Syllabus w.e.f 2013-14
The students will prepare a brief report of the industry visits during the tour. There
will be an Internal vice voce based on their visits during the tour.
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Shivaji University
Shivaji University Syllabus w.e.f 2013-14
Evaluation Scheme: The course auditor will evaluate the students for their performance in
the course and the students will be given the grade by the teacher. The grade will be based
on total marks obtained out of 50.
interaction, response surface and contour plots, General arrangement for a two‐factor
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Shivaji University Syllabus w.e.f 2013-14
REFERENCES:
1. Montgomery, Douglas C. (2007), 5/e, Design and Analysis of Experiments, (Wiley India)
2. Montgomery, Douglas C. & Runger, George C. (2007), 3/e, Applied Statistics &
Probability for Engineers (Wiley India)
3. Kothari, C.R., Research Methodology –Methods and techniques, New Age
Publications, New Delhi, 2009.
4. Krishnaswamy, K.N., Sivakumar, Appa Iyer and Mathiranjan M. (2006), Management
Research Methodology; Integration of Principles, Methods and Techniques ( Pearson
Education, New Delhi)
5. Panneerselvam, R., Research Methodology, Prentice-Hall of India, New Delhi, 2004.
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Note: All the students will have to undergo 21 days ‘in plant training’ after VI semester.
They will prepare a report of the same. Their performance will be assessed in the VII
semester by conducting a vice voce based on their training.
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Shivaji University
Shivaji University Syllabus w.e.f 2013-14
The Equivalence for the subjects of Chemical Technology at T.Y B Tech Semester V
and VI pre-revised course under the faculty of Engineering and Technology is as follows.
The examination pattern is changed from percent marks into credit system and the contents
in all the subjects have been unitized into 6 units (chapters)
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Shivaji University
Shivaji University Syllabus w.e.f 2013-14
1. Chemical Reaction Engineering Reaction Engineering-I The subject was vast and
needs to be split up into Part I
and II. Also its title is changed
and it is converted to credits
2. Chemical Technology-II Organic Chemical Syllabus is the same only title
Technologies is changed. It is converted to
credits
3. Industrial Pollution Control No change in the subject
content (only practical work is
Industrial Pollution Control omitted on account of
repetition). It is converted to
credits
4. Mass Transfer-II Mass Transfer-II No change in the subject
content. It is converted to
credits
5. Process Equipment Design and No change in the subject
Process Equipment Design
Drawing content. It is converted to
and Drawing
credits
6. Presentation and Communication ---------------------------- Shifted to V semester.
Techniques
The examination pattern is changed from percent marks into credit system and the contents
in all the subjects have been unitized into 6 units (chapters)
The students from the pre-revised syllabus need not complete the course work of newly
added subjects i.e. Research Methodology, Mini Project.
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Shivaji University