T H E R M A L A N A L Y S I S

THERMAL Heat Flow Meter

HFM 200
CONDUCTIVITY HFM 300
HFM 600
ANALYZER
Since 1957 LINSEIS Corporation has been deliv-
ering outstanding service, know how and lead-
ing innovative products in the field of thermal
analysis and thermo physical properties.

Customer satisfaction, innovation, flexibility

and high quality are what LINSEIS represents.
Thanks to these fundamentals our company
enjoys an exceptional reputation among the
leading scientific and industrial organizations.
LINSEIS has been offering highly innovative
benchmark products for many years.

The LINSEIS business unit of thermal analysis

is involved in the complete range of thermo
Claus Linseis
analytical equipment for R&D as well as qual- Managing Director
ity control. We support applications in sectors
such as polymers, chemical industry, inorganic
building materials and environmental analytics.
In addition, thermo physical properties of solids,
liquids and melts can be analyzed.
LINSEIS provides technological leadership. We
develop and manufacture thermo analytic and
thermo physical testing equipment to the high-
est standards and precision. Due to our innova-
tive drive and precision, we are a leading manu-
facturer of thermal Analysis equipment.
The development of thermo analytical testing
machines requires significant research and a
high degree of precision. LINSEIS Corp. invests
in this research to the benefit of our customers.

2
German engineering Innovation

The strive for the best due diligence and ac- We want to deliver the latest and best tech-
countability is part of our DNA. Our history is af- nology for our customers. LINSEIS continues
fected by German engineering and strict quality to innovate and enhance our existing thermal
control. analyzers. Our goal is constantly develop new
technologies to enable continued discovery in
Science.

3
INTRODUCTION
An insulating material is a material with low HFM where a square specimen (200x200mm,
thermal conductivity, which in the construction 300x300mm or 600x600mm) is located bet-
industry, equipment manufacturing, or the pro- ween a hot and a cold plate (temperature gra-
duction of refrigerators, freezers, etc. is used for dient). The heat transfer coeffcient can be cal-
thermal insulation. culated from the measured heat flow through
The physical properties to determine the effec- the sample divided by the cross-section area
tiveness of insulation material are the thermal and the applied temperature difference. For a
conductivity, the heat transfer coefficient. homogeneous material the thermal conducti-
The performance of an insolation material com- vity lambda is given by the quotient of DELTA
ponent is given by its heat transfer coefficent divided by the sample thickness.
DELTA. This value can be determined with a

LINSEIS offers a complete range

of thermal conductivity analy-
-125 – 1600°C
zers, ranging from Laser Flash
and Xenon Flash Thermal con-
Diamond
1000 stant Analyzers (small samples,
liquids, powders, pasts, multila-
Aluminium, Graphite yer samples, broad measuring
Silicon range and temperature) to Heat
100 Flow Meters (Building and Insu-
Thermal Conductivity [W/(m·K)]

Iron, Steel lation material) and a Transient

Hot Bridge Analyzer (Solids, Li-
Flash

Alumina, Carbon Bricks

-50 – 200°C quids, Powders, Pasts and Gas-
ses).
10.0 Silicon nitride
Furthermore Dilatometers (DIL
Alumina Silicates L76 and L75) for length and
density change and Differential
Porous Ceramics, Refractories Scanning Calorimeters DSC for
1.0
THB

determination of Specific Heat

Concrete, Glass, Fire clay
Cp are available.
-40 – 150°C Water

Wood, Polymers, Coal

0.1
Heat Flow Meter

Building boards, Oils

Fiber boards, Fiber Insulations

0.01 Air, Polystyrene, PUR Foams

Vacuum Isolation

0.001
Methods

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THE INSTRUMENTS
This Heat Flow Meter provides a rapid and easy Sample Thickness
to use instrument to determine the thermal The instrument has two built in linear potenti-
conductivity properties of low thermal conduc- ometer, offering automated highest precision
tive insulation materials and other materials sample thickness determination.
with a high level of accuracy. The instrument´s Two heat flux sensors then measure the heat
design is based on ASTM C518, JIS A1412, ISO flow, which is precisely defined between the hot
8301 and DIN 12667. The principle of measure- and cold plate.
ment is to position a sample between a hot and
a cold plate, and to measure the heat flow.

Service and Maintenance

The robust system design and the unique “zero
maintenance” peltier heating and cooling cycle
ensure a minimum of upholding cost.

Test Cycles
The double heat flux sensor configuration en-
sures shortest possible measurement cycles. A
typical measurement for most samples can take
as little as 15 minutes until the temperature sta-
bilizes.

HFM 600

HFM 300 5
SYSTEM DESIGN
The LINSEIS Heat Flow Meter is a robust and potentiometers for length measurements (μm-
reliable instrument. Its unique design enables resolution) provide immediate sample thick-
highly accurate measurements within minutes. ness data.
The intelligent peltier heating and cooling tech-
nology for the model 200, 300 and 600 allows Instrument Features
highest precision temperature control, and in • Highest precision and accuracy
addition reduces maintenance and downtimes • Very robust design
significantly. The system provides an excellent • Very easy handling
long term stability enabling precise long term • Fast sampling (approx. 15min for QC)
aging studies. Fast measurement cycles as litt- • Automated operation
le as 15 minutes can be achieved, resulting • Measurement range extension to 2.5 W/mK
in a high sampling rate. To enable these fast • Up to 99 measurement points
and precise sampling intervals the instrument • No PC required
uses a dual sensor arrangement. Integrated

Water cooling
Peltier modules
Direction of heat flow

Hot plate
thickness determination
Potetiometer setup for

Heat flux transducer

Test sample

Heat flux transducer

Cold plate

Peltier modules
Water cooling

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SOFTWARE
The instrument can be operated through the • Report printing, layout can be customized
touch screen front panel. Optional software, • Multi language software versions
free of charge, is available. This powerfull soft- • Instrument monitoring (plate temperature,
ware package enables convenient temperature thermal conductivity results and output signal
programming, data storage and instrument monitoring)
control. • Software help functions
• Optional user login and data monitoring
Key features:
• Easy measurement parameter input
• Measurement data storage and export

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SPECIFICATIONS
HFM 200 HFM 300 HFM 600

Temperature range 0 to 90°C 0 to 90°C -20 to 70°C

(plates) -20 up to 90°C -20 up to 90°C
-40 up to 90°C -35 up to 90°C

Cooling system External chiller or ac- External chiller or ac- External chiller or ac-
tive refrigerating chiller tive refrigerating chiller tive refrigerating chiller
Temperature control Peltier Peltier Peltier
(plate)
Measurement data 99 99 99
points
Sample size 205 x 205 x 105 mm3 305 x 305 x 105 mm3 600 x 600 x 200 mm3

Thermal resistance 0.2 to 8.0 m2 K/W 0.2 to 8.0 m2 K/W 0.2 to 8.0 m2 K/W
measuring range with Extension* with Extension* with Extension*
0.036 to 8.0 m2 K/W 0.036 to 8.0 m2 K/W 0.036 to 8.0 m2 K/W

Thermal conductivity 0.001 to 0.5 W/m∙K 0.001 to 0.5 W/m∙K 0.001 to 0.5 W/m∙K
measuring range with Extension* with Extension* with Extension*
0.001 to 2.5 W/m∙K 0.001 to 2.5 W/m∙K 0.001 to 2.5 W/m∙K

Reproducibility 0.25% 0.25% 0.25%

Accuracy +/- 1 to 3% +/- 1 to 3% +/- 1 to 3%

Variable contact 0 - 25 kPa 0 - 25 kPa 0 - 25 kPa

pressure*
*optional

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APPLICATIONS
Elastomer Foam
The present measurement
0.043 clearly demonstrates the out-
Measurement 1 standing reproducibility of the
Measurement 2
LINSEIS HFM series. A repro-
0.042 Measurement 3
Measurement 4 ducibility of 0.25% was achie-
ved. The graph display four
0.041 measurements of an Elastomer
Thermal Conductivity [W/(m·K)]

Foam in the temperature ran-

ge 15 to 40°C. The sample was
0.040 removed and placed into the
instrument again after each
0.039 measurement.

0.038

0.037

0.036
10 15 20 25 30 35 40 45
Temperature [°C]

IRMM-440certified reference material

Repeatability:
0.035 15 Measurement of the IRMM-
Test at 15°C (Average: 0.03102 + -0.00012 W/m·K)
Average 440certified reference ma-
Test at 30°C (Average: 0.03274 + -0.00015 W/m·K) terial (Resin bonded glass
Average
0.034 fibreboard) with a thermal
conductivity of 0.03274
+-0.00015 at 30°C and 0.03102
Thermal Conductivity [W/(m·K)]

0.033 + -0.00012 W/m·K at 15°C.

0.032

0.031

0.030

0.029
0 2 4 6 8 10 12 14 16
Number of measurement

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Glass wool specimen
Precision:
0.036 The graph shows two measure-
Measurement 1 [W/m·K] ments of the same glass wool
Measurement 2 [W/m·K]
0.035 Literature Values specimen at several tempera-
tures. The black line shows the
0.034 thermal conductivity according
the manufactorer information.
Thermal Conductivity [W/(m·K)]

0.033

0.032

0.031

0.030

0.029

0.028

0.027
-20 -10 0 10 20 30 40 50 60
Temperature [°C]

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 LINSEIS GmbH Germany LINSEIS Inc. USA
Vielitzerstr. 43 109 North Gold Drive
95100 Selb Robbinsville, NJ 08691
Tel.: (+49) 9287 880 0 Tel.: (+1) 609 223 2070
E-mail: info@linseis.de E-mail: info@linseis.de

LINSEIS China LINSEIS France

Kaige Scientific Park 2653 Hunan Road 2A Chemin des Eglantines
201315 Shanghai 69580 Sathonay Village
Tel.: (+86) 21 5055 0642 Tel.: (+33) 6.24.72.33.31
Tel.: (+86) 10 6223 7812 E-mail: contact@ribori-instrumentation.com
E-mail: info@linseis.de

LINSEIS Poland
ul. Dabrowskiego 1
05-800 Pruszków
Tel.: (+48) 692 773 795
E-mail: info@linseis.de

www.linseis.com

Products: DIL, TG, STA, DSC, HDSC, DTA, TMA, MS/FTIR, In-Situ EGA, Laser Flash, Seebeck Effect, Thin Film Analyzer, Hall-Effect
Services: Service Lab, Calibration Service
05/19