Quality Assurance of Pressure-Sensitive Tapes: Standard Practice For
Quality Assurance of Pressure-Sensitive Tapes: Standard Practice For
Quality Assurance of Pressure-Sensitive Tapes: Standard Practice For
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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TABLE 1 Sampling Plans for Inspection by VariablesA (Variability Unknown—Single Specification Limit)
Acceptable Quality Levels (Normal Inspection) Acceptable Quality Levels (Reduced Inspection)
Lot Size (100-m2[yd2] Sample .65 1.00 1.50 2.50 4.00 6.50 10.00 Sample 1.00 1.50 2.50 4.00 6.50 10.00
Units) Size Size
k k k k k k k k k k k k k
1 to 300 3 l ↓ ↓ 0.587 0.502 0.401 0.296 3 l 0.587 0.502 0.401 0.296 0.178
301 to 500 4 l 0.651 0.598 0.525 0.450 0.364 0.276 3 l 0.587 0.502 0.401 0.296 0.178
↓ l
501 to 800 5 0.663 0.614 0.565 0.498 0.431 0.352 0.272 3 l 0.587 0.502 0.401 0.296 0.178
801 to 1 300 7 0.613 0.569 0.525 0.465 0.405 0.336 0.266 3 ↓ 0.587 0.502 0.401 0.296 0.178
1 301 to 3 200 10 0.755 0.703 0.650 0.579 0.507 0.424 0.341 4 0.598 0.525 0.450 0.364 0.276 0.176
3 201 to 8 000 15 0.792 0.738 0.684 0.610 0.536 0.452 0.368 5 0.565 0.498 0.431 0.352 0.272 0.184
8 001 to 22 000 25 0.815 0.779 0.723 0.647 0.571 0.484 0.398 7 0.525 0.465 0.405 0.336 0.266 0.189
3.2.5 defective unit—a unit of product that contains one or number of defective units 3 100
Percent defective 5 number of units inspected (2)
more defects.
3.2.6 end item—the actual product or commodity being sold 3.2.15 quality characteristic—for inspection, that charac-
under the material specification. It is in its most complete form teristic of a unit of product that is actually measured to
and may be either packed for shipping or at a production stage determine conformance with a given requirement.
just preceding packing. It may or may not be the same as the 3.2.16 specification limit(s)—the requirement that a quality
unit of product defined in 3.2.17. characteristic should meet. This requirement may be expressed
3.2.7 end-item examination—the inspection of the roll of as an upper specification limit, or a lower specification limit;
tape for those characteristics which are either easily discernible called herein a single specification limit.
by visual inspection or can be simply measured by a hand rule 3.2.17 unit of product—the entity of product inspected in
(such as width). All characteristics of this type are considered order to determine its measurable quality characteristic. For
as attributes. this practice the unit of product will usually be a roll of tape.
3.2.8 end-item testing—the inspection of the unit of product The unit of product may or may not be the same as the unit of
that involves measurement of physical properties on a continu- purchase, supply production, or shipment. It is also called
ous scale. All characteristics of this type are considered as sample unit in this practice.
variables.
3.2.9 inspection—the process of measuring, examining, 4. Significance and Use
testing, gaging, or otherwise comparing the unit of product 4.1 The quality of a tape product is determined by the
with the applicable requirements (see ANSI/ASQC A2). quality systems of the tape producer, including all processes
3.2.10 inspection by attributes—inspection whereby either involved in the engineering and production of the product. It is
the unit of product is classified simply as defective or non- recommended that appropriate sections of ANSI/ASQC Q94 be
defective or the number of defects in the unit of product is included in a producer’s quality systems. This practice does not
counted, with respect to a given requirement or set of require- intend to standardize these systems. A producer’s reputation, a
ments (see ANSI/ASQC A2). producer’s certification of conformance, or evidence of a
3.2.11 inspection by variables—inspection wherein a speci- producer’s quality systems are often sufficient to ensure a
fied quality characteristic on a unit of product is measured on purchaser or user of a consistent quality. Acceptance sampling
a continuous scale, such as pounds, inches, feet per second, is useful when an objective basis of contract or specification
etc., and a measurement is recorded (see ANSI/ASQC A2). conformance is desired.
3.2.12 inspection lot—a collection of units of product from 4.2 The intention of this practice is to provide a reasonably
which a sample is drawn and inspected to determine compli- simple document which can be used by both the buyer and
ance with the acceptability criteria. seller of pressure-sensitive tape to determine if the product
3.2.13 material specification—that document covering a offered for sale meets some predetermined specification for the
product or set of products and specifying the parameters that product. This practice offers the procedures for determining the
define the product(s) (see ANSI/ASQC A3). size of the sample to be inspected and the criteria for
3.2.14 percent defective—the number of defective units of determining whether the lot (amount of material offered for
product contained therein, divided by the total number of sale) should be accepted or rejected. This practice draws from
product, the quotient multiplied by one hundred (a unit being and is based on both ANSI/ASQC Z1.4 and ANSI/ASQC Z1.9.
considered defective if it contains one or more defects). 4.3 Two forms of sampling plans are included: sampling by
Expressed as an equation: attributes and sampling by variables. Sampling by attributes is
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used for end-item examination and both are used where 5.3 End-Item Examination:
appropriate for end-item testing. Sampling by attributes has the 5.3.1 Sampling:
advantage of simplicity while sampling by variables has the 5.3.1.1 Lot Size, for the purpose of determining the sample
advantage of costing less for the equivalent assurance of the size, shall be expressed in units of rolls for examination under
correctness of decisions. 5.3.2.1-5.3.2.3 inclusive, and shall consist of all the tape
4.3.1 Sampling plans for inspection by attributes (see Table material presented for examination at one time. The material
2), should be used for end-item examination (see 5.3). shall be of the same type, class, and color, manufactured by the
4.3.2 Sampling plans for inspection by variables (see Table same process, from the same components, at one plant by one
1 and 5.4), should be used for end-item testing except as manufacturer under the same conditions.
indicated in 5.4.1.2(a). 5.3.1.2 Sample Size—The number of units of product (rolls
4.4 Use of this practice assumes that a specification defining of tape) to be examined shall be found in Table 2 under sample
one or more quality characteristics exists. It is suggested that size. Use the sampling plans for normal inspection unless
buyer and seller agree on acceptable quality levels (AQL) from tightened or reduced inspection has been specifically agreed
within the choices shown in the tables of this practice. upon.
4.5 When conditions warrant switching from normal to 5.3.1.3 The following table illustrates the AQLs that have
tightened or reduced inspection, the appropriate sampling plans commonly been used with the examinations found in 5.3.2.
are available in Table 1 and Table 2. The decision to switch The graduation follows traditional levels of importance for the
should be agreed upon between the buyer and the seller. When attributes collected together in the tables given in 5.3.2.1,
lots are rejected under normal inspection it is usual to go to 5.3.2.2, and 5.3.2.3. Table 2 illustrates only these AQLs.
tightened inspection. No change in AQL is made, but the Examination Paragraph AQL, %
assurance of making the correct decision is improved usually 5.3.2.1 2.5
by the sampling plan calling for a larger sample size. Reduced 5.3.2.2 4.0
5.3.2.3 10.0
inspection is a switch from normal inspection made when some
number of lots, usually 10, passes in consecutive order. 5.3.2 Examination—Examine in accordance with the de-
Switching should move from reduced to normal and from fects listed in 5.3.2.1, 5.3.2.2 and 5.3.2.3 and AQLs set forth in
normal to tightened or from tightened to normal without the table in 5.3.1.3 when sampled from the shipment. No more
skipping an intermediate step. than two rolls, randomly selected, shall be drawn from any one
shipping container from each lot of material for each type and
5. Procedure color of tape offered for inspection for visual and dimensional
5.1 Where it can be demonstrated that a supplier’s quality characteristics.
control system provides a similar degree of assurance as that
NOTE 2—The same rolls of tape shall be used for examination under
obtained through the use of this practice, the supplier may use 5.3.2.1-5.3.2.3 inclusive, and these examinations should be made concur-
that system in place of the system described herein. In case of rently.
conflict, the system described in this practice shall be used.
5.2 Where applicable, inspection (examination or testing) at 5.3.2.1 Major Defects—The sample unit for this examina-
some prior stage of manufacture, for example in-process or raw tion shall be one roll.
material, can be used instead of inspection of the end item. An Examine Major Defect
Form Not type, class, or grade specified.
example of this might be the use of the tensile strength test Adhesive side not wound on inside of roll, unless other-
performed at the raw material testing stage rather than on the wise specified.
end item. Backing Not colored or transparent, as specified.
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Tape does not consist of the specified backing (if one is 5.4.1.1 Lot Size—The lot size for the purpose of determin-
specified). ing the number of units of product to be sampled for testing,
Unwinding of rolls When unwound, tape sticks together to the extent that
unrolling causes tearing or injury to the surface of the shall be expressed in terms of 100-m2[100-yd2] units and shall
backing; adhesive separates from the backing; adhesive consist of all tape of the same type, class, and color manufac-
material removes color coating or printing from back of tured by the same process, from the same components at one
adjacent layer.
Liner Missing, when specified. time, at one plant, by one manufacturer, under the same
Breaking; delaminates. conditions within a biweekly period; maximum size shall be
Width of tape Varies from specified width more than allowable specified
tolerance.
ten thousand 100-m2[100-yd2] units. Table 3 is for use in
Length of tape Varies from specified length more than allowable speci- converting number of rolls to number of 100-m2[100-yd2]
fied tolerance. (Length to be determined in relaxed state.) units. The unit of product shall be the amount of tape required
Cores Inside diameter less than 76.2 mm [3 in.] or more than
79.4 mm [31⁄16 in.] or not other specified dimension. to perform all of the tests required one time. This may be one
Core crushed, broken, mutilated, or collapsed. or more rolls depending on whether the material specification
5.3.2.2 Intermediate Defects—The sample unit for this ex- required whole rolls for aging or more than one width of tape
amination shall be one roll. to perform certain required tests.
Examine Intermediate Defect 5.4.1.2 Sample Size—The number of units of product to be
Workmanship Adhesive coat not evenly and smoothly applied over the tested shall be found in Table 1 under sample size, entering the
entire area of the backing, as specified; any bare spots, table with the lot size. Use the sampling plans for normal
lumps, or foreign particles.
Holes, tears, cuts, cracks, or sharp creases; edges not inspection unless tightened or reduced inspection has been
clean cut, nicked, gouged, broken, uneven, sticky, or not specifically agreed upon. (See Table 3 to convert number of
straight.
Tapes not securely laminated; layer separated; presence
rolls to lot size in 100-m2[100-yd2] units.) In the event the
of blisters (reinforced tapes only). inspection lot does not contain rolls of tape of the width
Telescoping of roll. required for test samples, the manufacturer shall supply tape of
Unwinding of rolls Roll not continuous more than allowable number of
splices per roll; splices separate on unwinding.
the required widths to be used as test samples. This additional
Core Identification markings omitted, incorrect, incomplete, tape shall be taken from the same manufacturing lot(s) as the
illegible, or not as specified. tape undergoing inspection. When the requirement for a
5.3.2.3 Minor Defects—The sample unit for this examina- physical property test is a word description (not a numerical
tion shall be one roll. minimum or maximum) the sampling plans for inspection by
Examine Minor Defect attributes (Table 2) shall be used. In this case, enter Table 2
Tape on rolls Rolls not evenly and uniformly wound; not wound on ei- with the lot size expressed in 100-m2[100-yd2] units as found
ther paper fiber or plastic core; core not same width as in 5.4.1.1 instead of the lot expressed in number of rolls. See
tape.
Unwinding of rolls Does not unwind evenly and uniformly without raveling the following example:
(where applicable). (a) Example—Physical property test with objective require-
Tape wound unevenly causing wrinkles or creases within
the roll. ments stated and no numerical limits: The requirement for
Minor Defect weathering is that the tape shall exhibit no curling at the edges,
Splices not evenly and neatly made (not trimmed, loose
ends, edges ragged).
blistering or separation from the panel. An AQL of 4.0 % is
Note—A mill splice in cloth backing shall not be specified in the material specification. Paragraph 5.4.1.2 re-
considered a splice when properly coated. quires that these requirements be considered as attributes and
Splice adheres to adjacent layers of tape.
that the sampling plans of Table 2, normal inspection, should
5.4 End-Item Testing: be used. The paragraph states to convert the lot size (10 000
5.4.1 Sampling: rolls, 66 m [72 yd] in length by 48 mm [2 in. ] in width) to
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100-m2[100-yd2] units (400) and enter Table 2 with this 6.2 End-Item Testing—The degree of conformance of a
number instead of the number of rolls in the lot. This results in quality characteristic with respect to a single specification limit
a sampling plan calling for a sample size of 13. Note that with should be judged by the quantity (U − X̄)/ R̄ or ( X̄ − L)/ R̄.
a lot size of four hundred 100-m2[100-yd2] units, Table 2 6.2.1 The following quantity shall be computed: (U − X̄)/ R̄
shows a downward arrow at the intersection of the column or ( X̄ − L)/ R̄, depending on whether the specification limit is
headed by AQL of 4.0 and the row for lot size 151 to 500. This an upper or a lower limit,
arrow means that the sampling plan in the row below is to be
used including the sample size shown in that row. After where:
weathering, it is found that the test for one of the 13 rolls U = upper specification limit,
exhibits lifting (curling) at the edges. This is a failure for that L = lower specification limit,
X̄ = sample mean, and
roll. None of the other rolls shows this failure nor do any of the
R̄ = average range of the sample.
rolls exhibit blistering or separation from the panel. The
In this practice, R̄ is the average of several subgroup ranges.
acceptability criterion is to compare the number of defective
The subgroups are formed as follows: First, notice in Table 1
rolls (one) with the acceptance and rejection numbers for the
that there are three sample sizes (10, 15, and 25) which are
sampling plan. This sampling plan shows an acceptance
divisible by 5, and for which the quotient is a whole number
number (Ac) of 1 and a rejection number (Re) of 2. Since the
greater than 1. These are the only sample sizes which can be
number of defective samples (1) is less than the rejection
broken into subgroups. For these sample sizes the subgroups
number (2) we accept the lot, at least with respect to the quality
are formed by segregating the data into groups of 5 data points.
characteristic of weathering.
Use the first five to be obtained as the first subgroup. The order
5.4.2 Testing—The end item should be tested in accordance in which the data were achieved must be retained. The next 5
with the requirements of the material specification. Only one data points become the second subgroup and so on until there
test specimen should be selected from each unit of product for are 2, 3, or 5 subgroups for the sample sizes of 10, 15, and 25
each test except where the test method specifically requires respectively. The range of a subgroup is the difference between
more than one specimen. In the latter case, the value used to the largest and the smallest measurement in a subgroup.
represent any single unit of product for that quality character- 6.2.2 In 6.2.5, Example 1, the data are shown in two rows.
istic should be the one specified to be reported in the test The first five data points are in the first row beneath the
method. discussion paragraph and form the first subgroup whose range
(R1) is 34 − 24 = 10. The second subgroup is the next 5 data
6. Determination of Acceptability points which are on the second row (R2 = 7). In Line 4 of the
6.1 End-Item Examination—The following example ex- calculation, R̄ is computed. The general form for the calcula-
plains how to use the results of each examination paragraph tion of R̄ is to divide the sum of the individual subgroup ranges
with the acceptability criterion to determine the acceptability of by the number of subgroups. In this case R̄ = (10 + 7)/2.
the lot: 6.2.3 In 6.2.6, Example 2, the sample size is 4, so only 4
6.1.1 A lot containing 57 000 rolls is examined for major measurements will be used in the calculations. In this case
defects in accordance with 5.3.2.1. The sample size is 32 rolls there can be only one subgroup. A similar situation occurs
(see Table 2, normal inspection). The examination disclosed when the sample size is 3, 5, or 7 since not more than one
that 3 of the 32 rolls are found to have at least one of the major complete subgroup can be formed containing 5 measurements
defects listed in 5.3.2.1. The balance of 29 rolls show none of in any of these cases. In these cases, the average range ( R̄) is
the listed defects. The sampling plan (Table 2) for this lot size the same as the range of the group (R). Thus, on Line 4 of the
at an AQL of 2.5 shows an acceptance number (Ac) of 2 and calculation in Example 2, R̄ is shown as having the same value
a rejection number (Re) of 3. The acceptability criterion is to as the single group range (R).
compare the number of defective rolls (3) with these numbers. 6.2.4 Compare the quantity (U − X)/ R̄ or ( X̄ − L)/ R̄
If the number of defective rolls is less than or equal to the with the acceptability constant k found in Table 1. If (U − X̄)/
acceptance number, accept the lot (at least with respect to this R̄ or ( X̄ − L)/ R̄ is equal to or greater than k, the lot meets the
examination paragraph). If the number of defective rolls is acceptability criterion. If (U − X̄)/ R̄ or ( X̄ − L)/ R̄ is less than
equal to or greater than the rejection number, reject the lot. In k or negative, then the lot does not meet the acceptability
this example, reject the lot. No further examination would be criterion. Repeat this comparison for each quality characteris-
necessary. If 2 or fewer defective rolls had been found, the lot tic.
would be accepted with respect to 5.3.2.1. Then, examine the 6.2.5 Example 1—Lower specification limit L is given.
32 rolls according to 5.3.2.2 and follow the same procedure as Compute the quantity ( X̄ − L)/ R̄ and compare it with k.
for 5.3.2.1, except use the number of defective rolls found 6.2.5.1 A lot of 75 000 rolls 66 m by 24 mm [72 yd by 1 in.
during the previous examinations and the acceptance and ] wide (equals fifteen hundred 100-m2[100-yd2] units) from
rejection number appropriate to the sampling plan with an AQL Table 1 is tested for peel adhesion for which the minimum
of 4.0. If the lot fails to meet the acceptability criterion, reject requirement is 27 N/100 [25 oz/in.] of width. The sample size
it. If it meets, proceed to 5.3.2.3 and repeat the process as (Table 1) is 10, so 10 rolls of tape will represent the sample.
before with the number of defective rolls found during such The material specification cites an AQL of 4.0.
examination and acceptance and rejection numbers appropriate 6.2.5.2 The values obtained from the 10 rolls arranged into
to an AQL of 10.0. two subgroups in the order of performing the test with the
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range for each subgroup R1 and R2 are: has a maximum requirement of 70 N/100 [4.0 lb/in.] of width.
27 31 34 24 29 (R1 = 34 − 24 = 10) The material specification cites an AQL of 2.5. The test results
28 32 31 34 35 (R2 = 35 − 28 = 7) were: 3.9, 4.0, 3.9, 3.3 ( R̄ = R therefore 4.0 − 3.3 = 0.7 = R̄)
6.2.5.3 Determine compliance with the acceptability crite- (see 6.2.3).
rion as follows: 6.2.6.2 Determine compliance with the acceptability crite-
Line Information Needed Value Obtained Explanation rion as follows:
1 Sample size: n 10 ... Line Information Needed Value Obtained Explanation
2 Sum of measurements: (X 305 ... 1 Sample size: n 4 ...
3 Sample mean X̄: (X/n 30.5 ... 2 Sum of measurements: (X 15.1 ...
4 Average range R̄: (R/number 8.5 (10 + 7)/2 3 Sample mean X̄: (X/n 3.77 15.1/4
of subgroups 4 Average range R̄:( R/number 0.7 One subgroup so R̄ =
5 Specification limit (lower): L 25 ... of subgroups R
6 The quantity: (X̄ − L)/R̄ 0.65 (30.5 − 25)/8.5 5 Specification limit (Upper): U 4.0 ...
7 Acceptability constant: k 0.507 see Table 1 (normal 6 The quantity: (U − X̄)/R̄ 0.33 (4.0–3.77)/0.7
inspection) 7 Acceptability constant: k 0.525 see Table 1 (normal
8 Acceptability criterion: 0.65 > 0.507 see 6.2.4 inspection)
compare (X̄ − L)/R̄ with k 8 Acceptability criterion: 0.33 < 0.525 see 6.2.4
Compare (U − X̄)/R̄ with k
The lot does meet the acceptability criterion for the adhesion
tests, since ( X̄ − L)/ R̄ is greater than k. The lot does not meet the acceptability criterion, since (U −
6.2.6 Example 2—Upper specifications limit U is given. X̄)/ R̄ is less than k. This lot should be rejected on the basis of
Compute the quantity (U − X̄)/ R̄ and compare it with k. this failure.
6.2.6.1 A lot size of 20 000 rolls 66 m by 24 mm [72 yd by
1 in. ] wide (equals four hundred 100-m2[100-yd2] units from 7. Keywords
Table 3) gives a sample size of 4 (Table 1). The test for unwind 7.1 pressure-sensitive tape; quality assurance; sampling
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