Location via proxy:   [ UP ]  
[Report a bug]   [Manage cookies]                
Scribd Logo
Upload

Welcome to Scribd!

  • Peroxide Test: Mquant

    Uploaded by

    rosalia destika
    56 views1 page
    media

    Original Title

    Peroxide-110011/

    Copyright

    © © All Rights Reserved

    Available Formats

    PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    media

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    56 views1 page

    Peroxide Test: Mquant

    Uploaded by

    rosalia destika
    media

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    Download as pdf or txt
    of 1

    7.7590.0007-xxxxxxxxx msp.

    November 2018

    1.10011.0001 6. Preparation
    • Samples containing more than 25 mg/l H2O2
    1.10011.0002 must be diluted with distilled water or perox-
    ide-free ether.
    • The pH of the aqueous sample must be
    MQuant®
    O22-
    within the range 2 - 12.

    Peroxide Test If necessary, buffer the sample with sodium


    acetate or, respectively, adjust the pH with
    hydrochloric acid.

    1. Method 7. Procedure
    Peroxidase transfers peroxide oxygen to an Protect the reaction zones from light (also
    organic redox indicator. This produces a blue during the reaction time)!
    oxidation product. The peroxide concentration is
    measured semiquantitatively by visual com- Determination in aqueous solutions:
    parison of the reaction zone of the test strip
    with the fields of a color scale. Immerse the reaction zone of the test strip in the
    pretreated sample (15 - 30 °C) for 1 sec.
    2. Measuring range and number Allow excess liquid to run off via the long edge of
    the strip onto an absorbent paper towel and after
    of determinations 15 sec determine with which color field on the
    label the color of the reaction zone coincides most
    Measuring range / color- Number of exactly.
    scale graduation determinations Read off the corresponding result in mg/l H2O2.

    25
    Notes on the measurement:
    (Cat. No. 1.10011.0002)
    0.5 - 2 - 5 - 10 - 25 • Every blue colouration within 3 min can be
    or
    mg/l H2O2 interpreted as a positive result.
    100
    (Cat. No. 1.10011.0001) • If the color of the reaction zone is equal to or
    more intense than the darkest color on the
    scale or if another color emerges, repeat the
    3. Applications measurement using fresh samples diluted
    This test measures inorganic peroxides in aque- with distilled water or, respectively, peroxide-
    ous solutions and organic solvents. Polymeric free ether until a value of less than 25 mg/l
    peroxides are not at all or only incompletely H2O2 is obtained.
    measured.
    Sample material: Determination in organic solvents (readily
    Simple ethers volatile ethers):
    UHT milk
    Pickling and copper-stripping baths Immerse the reaction zone of the test strip in the
    Bleaching and oxidizing agents (paper and tex- pretreated sample (15 - 30 °C) for 1 sec.
    tile industries) After the solvent has evaporated (gently fan the
    Disinfectant and rinsing solutions (e. g. food strip back and forth for 3 - 30 sec), humidify the
    technology, laundries) reaction zone for 1 sec with 1 drop of distilled
    water and allow excess liquid to run off via the
    Swimming-pool water long edge of the strip onto an absorbent paper
    towel.
    4. Influence of foreign substances After 15 sec assess the color of the reaction
    This was checked individually in solutions with zone.
    12.5 and 0 mg/l H2O2. The determination is not
    yet interfered with up to the concentrations of Note on the measurement:
    foreign substances given in the table. Cumulative It is recommended to treat the measure-
    effects were not checked; such effects can, ment results obtained in organic solvents
    however, not be excluded. only as guideline values, since the color in
    appearance and intensity may vary depend-
    Concentrations of foreign substances in mg/l
    ing on the solvent medium. In this connec-
    CrO42- 10 IO4- 40 tion every blue coloration of the reaction
    [Fe(CN)6]4- 10 MnO4- 2 zone indicates that peroxide is present.
    [Fe(CN)6]3- 10 S2O82- 20
    Hg 250
    +
    VO3 5
    -
    8. Method control
    To check test strips and handling:
    Make up 5.0 ml of Perhydrol® (H2O2 30 %
    5. Reagents and auxiliaries ^ 333 000 mg/l H O ) to 500 ml with distilled
    = 2 2

    The test strips are stable up to the date


    water and mix. Take 1.5 ml of this solution,
    stated on the pack when stored closed at
    make up to 500 ml with distilled water, and
    +2 to +8 °C.
    mix. Subsequently analyze immediately
    (solution is not stable) as described in
    Failure to adhere to the storage tempera-
    section 7. The content of H2O2 determined
    ture of +2 to +8°C will lower the shelf life
    should be 10 mg/l.
    Additional notes see under
    of the test strips and the accuracy of the
    www.qa-test-kits.com.
    measuring values.
    Package contents: 9. Note
    Tube containing 25 test strips
    (Cat. No. 1.10011.0002) Reclose the tube containing the test strips
    or immediately after use.
    containing 100 test strips
    (Cat. No. 1.10011.0001)
    Other reagents:
    MQuant® Universal indicator strips pH 0 - 14,
    Cat. No. 109535
    Sodium acetate anhydrous GR for analysis,
    Cat. No. 106268
    Hydrochloric acid 1 mol/l Titripur®,
    Cat. No. 109057
    Diethyl ether for analysis EMSURE®, Merck KGaA, 64271 Darmstadt, Germany,
    Cat. No. 100921 Tel. +49(0)6151 72-2440
    www.analytical-test-kits.com
    Hydrogen peroxide 30 % H2O2 (Perhydrol®)
    GR for analysis, Cat. No. 107209 EMD Millipore Corporation, 400 Summit Drive
    Burlington MA 01803, USA, Tel. +1-978-715-4321

    You might also like