Distilled Water

Background and the purpose of the study: This study reports the laboratory optimization for the preparation of salbutamol sulphate-ethylcellulose microparticles by a non-solvent addition coacervation technique through adjustment of the ratio of salbutamol sulphate to ethylcellulose. The variation of drug release between the microparticles and tabletted microparticles was also investigated. Methods: In vitro release profiles of developed microparticles and tabletted microparticles were studied using USP XXIV dissolution apparatus I and II, respectively, in 450 ml double distilled water at 50 rpm maintained at 37°C. Results: White microparticles with no definite shape having good entrapment efficiency (96.68 to 97.83%) and production yield (97.48 ± 1.21 to 98.35 ± 1.08%) were obtained. In this investigation, initial burst effect was observed in the drug release behavior. The rate of drug release from microparticles decreased as the concentration of polyisobutylene was increased from 6...

Potential of plants to remove radionuclides/toxic elements from soils and solutions can be successfully applied for removal of important radionuclides such as strontium-90 (90Sr) and cesium-137 (137Cs). When uptake of 137Cs and 90Sr by Calotropis gigantea plants incubated in distilled water spiked with the radionuclides either alone or in combination was studied, it was found to have a high efficiency for the removal of 90Sr, with 90% being removed from solutions (5 × 103 kBq l−1) within 24 h of incubation. However, in case of 137Cs, about 44% could be removed from solutions (5 × 103 kBq l−1) at the end of 168 h of incubation. Accumulation of 90Sr and 137Cs was higher in roots compared to shoots. The plants could remediate both 90Sr and 137Cs when they were added together to the solution. When two months old plants were incubated in low level nuclear waste, 99% of activity disappeared at the end of 15 days. The present study suggests that C. gigantea could be used as a potential candidate plant for phytoremediation of 90Sr and 137Cs.

Isolated Chinese hamster metaphase chromosomes were resuspended in 4 M ammonium acetate and spread on a surface of distilled water or 0.15 to 0.5 M ammonium acetate. The DNA was released in the form of a regular series of rosettes connected by interrossette DNA. The mean length of the rosette DNA was 14 μm, similar to the mean length of 10 μm for chromomere DNA of Drosophila polytene chromosomes. The mean interrosette DNA was 4.2 μm. SDS gel electrophoresis of the chromosomal nonhistone proteins showed them to be very similar to nuclear nonhistone proteins except for the presence of more actin and tubulin. Nuclear matrix proteins were present in the chromosomes and may play a role in forming the rosettes. Evidence that the rosette pattern is artifactual versus the possibility that it represents a real organizational substructure of the chromosomes is reviewed.

Effect of the aqueous chemistry on the mechanical strength of chalk has extensively been studied during the last decade. At high temperatures (~130°C), chalk exposed to seawater is significantly weaker compared to chalk exposed to distilled water when considering the hydrostatic yield strength and the following creep phase. The explanation of these experimental results must be of a chemical nature, as the density and viscosity of the aqueous phase vary little among these different brines. We present the results from simplified aqueous chemistry using MgCl2 brines, and compare these results with seawater. Previous studies show that different ions, e.g. Ca2+, Mg2+, \({{\rm SO}{_{4}}^{2-}}\) in the injected brine, as well as the chalk mineralogy have an impact on the stability of the rock. We performed mechanical tests on chalk cores from Liège and Stevns Klint; it was found that these two outcrop chalks exhibit an unexpected difference in their mechanical responses when comparing cores flooded with NaCl and MgCl2 at 130°C. The results of this study show that the effects of magnesium seem to be governed not only by the differences in mineralogy, but also a time dependency on chalk deformation is additionally observed. Independent of the chalk type tested, the chemical analyses performed show that when MgCl2 is flooded through the core, a significant loss of magnesium and a considerable additional amount of calcium are detected in the effluent. The experimental observations fit very well with the time-dependent chemical changes gained from the mathematical model of this study that accounts for transport effects (convection and molecular diffusion) as well as chemical processes such as precipitation/dissolution. Based on the calculations and chemical analyses, we argue that the loss of magnesium and the production of calcium cannot solely be a consequence of a substitution process. The calculations rather indicate that magnesium is precipitated forming new mineral phases and in this process not only calcite, but also silicates are dissolved. The amount of dissolved calcium and silicon from the rock matrix is significant and could thus cause an additional deformation to take place. Both the retention of magnesium in the chalk core and the formation of newly precipitated magnesium-bearing carbonates and/or magnesium-bearing clay-like minerals after flooding with MgCl2 brine were demonstrated using scanning electron microscopic methods. In addition, precipitation of anhydrite as a result of flooding with seawater-like brine was proven. The water-induced strain not only depends on the ion composition of the injected brine; moreover, the presence of non-carbonate minerals will most likely also have a significant influence on the mechanical behaviour of chalk.

Based on its use in traditional African medicine, the antidiarrhoeal activity of the aqueous leaf extract of Byrsocarpus coccineus, Connaraceae, was evaluated on normal and castor oil-induced intestinal transit, castor oil-induced diarrhoea, enteropooling and gastric emptying. The extract (50, 100, 200 and 400mg/kg, p.o.) produced a significant (P<0.05) dose dependent decrease in propulsion in the castor oil-induced intestinal transit in

The aim of this study was to evaluate the influence of caries-detecting dyes on the microleakage of adhesive materials. Sixty cubic class V cavities were prepared on buccal and lingual surfaces of 30 human third molars. Coronal margins were located in enamel and gingival margins in cementum. The teeth were randomly divided into six groups of ten restorations each. Cavities were restored with an adhesive system (Single Bond, 3M ESPE, St. Paul, Minn., USA), a compomer (F2000, 3M ESPE), or a composite resin (Z100, 3M ESPE) according to the manufacturer's directions. Acid red dye (Seek, Ultradent, South Jordan, Ut., USA) and basic fuchsin dye (Vide Cárie, Inodon, Porto Alegre, Brazil) were tested. Control groups were prepared without the use of dyes. After 7 days of storage in distilled water, the restorations were polished and the teeth were subjected to thermal cycling followed by immersion in 2% methylene blue. The teeth were sectioned, and microleakage scores were evaluated under magnification (40×). Data were submitted to statistical analysis using the nonparametric Kruskal-Wallis test. A statistically significant difference (PF2000) but not in enamel. Control and experimental groups using dyes showed similar results. It was concluded that dyes for caries detection did not increase microleakage of the adhesive materials tested.

The conventional agriculture leads to some important pollution of ground water (particularly, by nitrates). The solution is the coating of fertilizers by degradable polymers. In this work, we have studied the water vapour and liquid diffusion through polymer films detached from their support. Therefore, we may classify polymers as a function of their properties like water vapour and liquid barrier. We may choose the best polymer(s) for coating.coated fertilizers by chosen polymer(s) with mechanical techniques such as fluidised bed and pan coating. Moreover, the electron microscopy used to see the quality of the wall has showed the presence of pores due to the rapid evaporation of solvent. A drying in air current and an annealing could be done to avoid this problem.followed the ions release of fertilizers immersed in distilled water by conductimetry. The more interesting result was obtained with fertilizers coated by polylactic acid. In effect, the total release reached three weeks.

Indigenous proteases in the skin of unicorn leatherjacket (Alutherus monoceros) were characterised using autolytic study. Maximised autolysis was found at pH 7 and 50 °C. Autolysis was markedly inhibited by 0.04 mM soybean trypsin inhibitor (SBTI), suggesting that heat activated serine protease was predominant in the skin. The impact of indigenous proteases on the properties of gelatin extracted from unicorn leatherjacket skin was investigated. Gelatin was extracted from unicorn leatherjacket skin using distilled water at 50 °C for 12 h in the presence and absence of 0.04 mM SBTI. In the presence of SBTI, the degradation was markedly inhibited, but a lower gelatin extraction yield was obtained (P < 0.05). Extracted gelatins contained α1 and α2 chains as the predominant components with some degradation peptides. FTIR spectra indicated a greater loss of molecular order of the triple helix and a higher degradation was found in gelatin extracted in the absence of 0.04 mM SBTI. The net charge of gelatin samples extracted with and without 0.04 mM SBTI became zero at pHs of 8.45 and 7.31, respectively, as determined by ζ-potential titration. Higher gel strength (320.68 ± 3.02 g) was obtained in gelatin extracted with SBTI, compared with that of gelatin extracted without SBTI (288.63 ± 1.44 g). High emulsifying activity index but lower emulsifying stability index was observed in the former. Therefore, heat-activated serine protease was involved in the degradation of gelatin molecules, thereby affecting the yield, proteinaceous components and properties of gelatin from unicorn leatherjacket skin.► Indigenous proteases hydrolysed gelatin from skin of unicorn leatherjacket during extraction. ► Soybean trypsin inhibitor (SBTI) could prevent the degradation of gelatin during extraction. ► Gelatin extracted in the presence of SBTI had the improved functional properties.

The effects of reconstitution of sorghums on dry matter, energy, pro tein and amino acid digestibilities, and the nature of protein binding by sorghum tan nins during digestion were investigated. Grains from a high and a low tannin sorghum were reconstituted by adding ...

The present work highlights the importance of using the Fresnel lens technique to enhance the productivity of a conventional solar still (CSS). In this regard, the effect of using Fresnel lenses to improve the productivity of a CSS is investigated experimentally under the climate conditions of Basra city (30.5258°N latitude and 47.7738°E longitude), Iraq. The Fresnel lenses integrated conventional single-slop-basin type solar still (CSS FL) adjustable to be rotated manually at different angles was examined, compared to the CSS which showed a remarkable enhancement of producing output. The study concerned the variation of daily solar radiation and temperature effect on the distillate output and the efficiency of both the conventional and modified solar stills at 1 and 2 cm saline water depths during July and September of the year 2019. The experimental results showed better performance during July where it has been found that the productivity of the CSS FL improved over the CSS by about 68.6% at 1 cm depth and about 59.3% at 2 cm depth. Moreover, the average daily thermal efficiency of the CSS and the CSS FL at 1 cm depth was 21% and 36%, respectively. Several conclusions and recommendations are presented for future work.

An experimental investigation has been carried out to determine the local forced convective boiling heat transfer coefficient in small tube bundles consisting of horizontal tubes in a vertical column arranged in a large channel under low cross-flow velocities in saturated distilled water at atmospheric pressure. The effects of the impressed heat flux, cross-flow velocity and tube geometry on the heat transfer characteristics have been investigated. While no significant effect of the bundle geometry was observed on the heat transfer coefficient of the bottom tube compared to that of the single tube, vapour bubbles rising from the lower tubes and agitating the liquid around the upper tubes were found to yield higher values for heat transfer coefficients on the upper tubes. A Chen-type relation has been used to correlate the data on local forced convective heat transfer coefficients of upper tubes with reasonably accuracy.

The production of extracellular amylase by Bacillus spp was optimized in a submerged fermentation. The production of the enzyme was maximum at 10 h after inoculation. The effect of incubation period, pH of the medium and incubation temperature was optimized. The maximum production of enzyme were obtained at 35°C and pH 7. Amylases are enzymes that break down starch or Microorganism: Bacillus spp was isolated from glycogen. The amylases can be derived from several environment and maintained on nutrient agar slants and sources such as plants, animals and microbes. The sub cultured for every 10 days. major advantage of using microorganisms for production of amylases is in economical bulk Inoculum and Fermentation Medium: The inoculum production capacity and microbes are also easy to was prepared by the addition of sterile distilled water in manipulate to obtain enzymes of desired characteristics to the freshly grown nutrient agar slants, from this (1). The microbial amylases meet indus...

The ability of a restorative material to withstand fracture is of crucial importance especially in stress-bearing area. Therefore, the study aims to analyse the fracture toughness of a large number of dental restorative materials categories. The fracture toughness (K(IC)) of 69 restorative materials belonging to ten materials categories-micro-hybrid, nanofilled, microfilled, packable, ormocer-based, and flowable resin-based composites (RBC), compomers and flowable compomers, as well as glass ionomer cements (GIC) and resin-modified GIC was measured by means of the single-edge notched-beam method after storing the samples (n = 8) for 24 h in distilled water. Data were analyzed with the one-way analysis of variance (ANOVA) followed by the Tukey&amp;amp;amp;#39;s test and partial eta-squared statistics (p &amp;amp;amp;lt; 0.05). Large variations between the tested materials within a material category were found. The lowest fracture toughness was reached in the GIC group, followed by the microfilled RBCs, resin-modified GIC, and flowable compomers, which do not differ significantly among each other as a material group. The ormocer-based, packable, and micro-hybrid RBCs performed statistically similar, reaching the highest fracture toughness values. Between the two categories of flowables-composites and compomers-no differences were measured. The correlation between K(IC) and filler volume (0.34) and respective filler weight (0.40) was low. K(IC) increased with the volume fraction of fillers until a critical value of 57%, following with a plateau, with constant values until ca. 65% volume fraction. Above this value, K(IC) decreased slightly. Due to the very large variability of the fracture toughness within a material type, the selection of a suitable restorative material should have not been done with respect to a specific material category, especially in stress-bearing areas, but by considering the individual measured material properties.